#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/02/2230203.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230203_Fobs loop_ _publ_author_name 'Chen, Xiao-na' 'Hu, Wen-hao' 'Li, Xiao-liu' 'Xu, Hua-dong' _publ_section_title ; 3-Diazo-N-[(2S)-1-hydroxypropan-2-yl]-2-oxopropanamide ; _journal_coeditor_code ZL2366 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1192 _journal_volume 67 _journal_year 2011 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.3136 _cell_length_b 6.7551 _cell_length_c 23.3958 _exptl_crystal_F_000 360.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file zl2366Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Z in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 110.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7935.46 7509.26 297.12 o 4 0 0 24.30 32.23 0.92 o 6 0 0 67.15 78.57 2.50 o 1 1 0 4522.91 4568.99 44.90 o 2 1 0 31.38 17.01 0.33 o 3 1 0 101.10 119.13 1.12 o 4 1 0 0.89 1.69 0.31 o 5 1 0 202.84 228.91 2.56 o 6 1 0 2.27 2.56 0.78 o 0 2 0 12302.36 12543.69 157.65 o 1 2 0 13.11 13.85 0.36 o 2 2 0 68.58 74.51 0.89 o 3 2 0 35.58 31.97 0.53 o 4 2 0 115.45 127.14 1.77 o 5 2 0 30.56 28.02 0.97 o 6 2 0 8.78 5.44 0.67 o 1 3 0 916.91 977.69 9.13 o 2 3 0 58.16 65.91 0.78 o 3 3 0 1.43 1.87 0.28 o 4 3 0 26.16 24.04 0.98 o 5 3 0 124.33 124.18 2.46 o 0 4 0 3326.26 3267.74 31.63 o 1 4 0 5.56 4.89 0.27 o 2 4 0 217.48 218.92 5.02 o 3 4 0 0.67 0.29 0.21 o 4 4 0 0.36 0.25 0.29 o 5 4 0 4.73 4.28 0.58 o 1 5 0 61.41 55.73 1.00 o 2 5 0 1.61 2.09 0.31 o 3 5 0 0.04 0.83 0.31 o 4 5 0 9.36 11.05 0.75 o 0 6 0 316.70 281.28 7.93 o 1 6 0 7.83 7.96 0.60 o 2 6 0 35.39 34.03 0.87 o 3 6 0 0.30 0.01 0.31 o 4 6 0 2.44 1.06 0.48 o 1 7 0 5.29 3.60 0.90 o 2 7 0 0.15 0.38 0.42 o 3 7 0 0.04 -0.39 0.39 o 0 8 0 9.17 8.79 1.54 o 1 0 1 722.14 736.43 9.15 o 3 0 1 286.31 303.54 2.84 o 4 0 1 66.84 55.52 0.80 o 5 0 1 205.31 199.48 2.29 o 6 0 1 0.60 0.48 0.44 o 0 1 1 505.58 487.77 4.61 o 1 1 1 2368.14 2373.93 19.14 o 2 1 1 1067.40 1105.97 6.29 o 3 1 1 69.45 62.75 0.55 o 4 1 1 389.45 389.28 2.25 o 5 1 1 30.61 30.18 0.57 o 6 1 1 6.93 6.88 0.60 o 0 2 1 765.48 700.09 6.38 o 1 2 1 2566.12 2617.55 15.23 o 2 2 1 226.97 209.68 1.39 o 3 2 1 384.04 385.99 2.21 o 4 2 1 16.27 18.09 0.44 o 5 2 1 185.88 194.64 1.99 o 6 2 1 0.78 0.42 0.34 o 0 3 1 231.40 212.04 1.76 o 1 3 1 195.95 194.81 1.36 o 2 3 1 130.24 125.87 1.04 o 3 3 1 47.72 43.57 0.69 o 4 3 1 97.41 102.10 1.13 o 5 3 1 6.78 7.75 0.43 o 0 4 1 404.66 386.48 2.92 o 1 4 1 375.78 378.05 2.76 o 2 4 1 42.85 46.28 0.64 o 3 4 1 46.48 42.85 0.66 o 4 4 1 6.24 6.68 0.37 o 5 4 1 40.60 38.28 1.17 o 0 5 1 2.94 2.41 0.29 o 1 5 1 141.81 139.08 1.26 o 2 5 1 3.59 3.89 0.25 o 3 5 1 22.56 23.35 0.55 o 4 5 1 23.47 26.62 0.70 o 0 6 1 68.97 65.26 2.11 o 1 6 1 45.95 46.46 0.87 o 2 6 1 2.91 2.60 0.26 o 3 6 1 2.83 2.47 0.29 o 4 6 1 1.70 1.51 0.35 o 0 7 1 0.92 1.79 0.64 o 1 7 1 7.67 7.28 0.62 o 2 7 1 0.61 0.46 0.30 o 3 7 1 0.23 0.18 0.29 o 0 8 1 9.85 8.25 1.07 o 0 0 2 1883.23 1899.03 30.41 o 1 0 2 839.11 845.71 7.63 o 2 0 2 192.11 136.70 1.15 o 3 0 2 46.35 45.73 0.89 o 4 0 2 103.65 107.52 1.63 o 5 0 2 245.02 252.54 2.96 o 6 0 2 3.29 4.74 0.70 o 0 1 2 1572.92 1678.53 15.05 o 1 1 2 813.01 870.80 5.14 o 2 1 2 483.74 556.33 3.00 o 3 1 2 14.93 12.96 0.23 o 4 1 2 377.61 371.88 2.36 o 5 1 2 42.96 40.26 0.70 o 6 1 2 0.54 0.86 0.40 o 0 2 2 11970.87 12416.26 110.41 o 1 2 2 334.33 317.32 2.08 o 2 2 2 1000.71 1012.24 5.84 o 3 2 2 86.53 86.37 1.29 o 4 2 2 37.95 38.15 0.80 o 5 2 2 199.36 194.67 2.00 o 6 2 2 8.79 10.15 0.58 o 0 3 2 20.10 18.92 0.39 o 1 3 2 132.99 140.56 0.96 o 2 3 2 534.15 514.91 3.68 o 3 3 2 4.23 3.96 0.24 o 4 3 2 303.67 310.88 2.76 o 5 3 2 16.71 22.26 0.65 o 0 4 2 442.17 460.44 3.42 o 1 4 2 56.71 59.29 0.56 o 2 4 2 12.97 11.41 0.35 o 3 4 2 7.83 8.88 0.34 o 4 4 2 1.28 0.78 0.25 o 5 4 2 62.70 61.69 1.06 o 0 5 2 39.53 33.80 0.67 o 1 5 2 12.78 12.55 0.35 o 2 5 2 8.58 7.20 0.31 o 3 5 2 6.45 7.07 0.34 o 4 5 2 33.06 33.70 0.72 o 0 6 2 33.43 29.27 1.20 o 1 6 2 6.80 6.53 0.46 o 2 6 2 0.77 1.08 0.22 o 3 6 2 1.77 1.31 0.24 o 4 6 2 0.56 1.04 0.33 o 0 7 2 0.09 0.22 0.50 o 1 7 2 0.75 0.14 0.31 o 2 7 2 6.62 7.14 0.48 o 3 7 2 1.02 0.85 0.32 o 0 8 2 7.29 6.40 1.38 o 1 0 3 2630.75 2572.81 23.01 o 2 0 3 235.07 209.56 1.65 o 3 0 3 14.66 20.24 0.39 o 4 0 3 36.27 47.74 0.80 o 5 0 3 183.95 198.96 2.71 o 6 0 3 1.72 1.40 0.53 o 0 1 3 577.95 558.79 5.07 o 1 1 3 122.26 93.27 0.62 o 2 1 3 101.90 88.41 0.62 o 3 1 3 68.19 72.94 0.57 o 4 1 3 332.84 331.50 2.16 o 5 1 3 71.67 68.64 1.48 o 6 1 3 5.72 7.42 0.58 o 0 2 3 161.32 160.34 1.52 o 1 2 3 593.55 608.27 3.68 o 2 2 3 147.35 185.84 1.18 o 3 2 3 436.25 454.06 2.62 o 4 2 3 54.21 48.62 0.75 o 5 2 3 23.50 22.82 0.67 o 6 2 3 3.72 1.47 0.36 o 0 3 3 1.53 0.74 0.13 o 1 3 3 364.28 367.19 2.27 o 2 3 3 73.57 81.52 0.69 o 3 3 3 145.64 150.38 1.36 o 4 3 3 167.29 170.07 1.76 o 5 3 3 50.87 52.83 1.00 o 0 4 3 24.73 23.95 0.61 o 1 4 3 36.94 38.62 0.41 o 2 4 3 15.22 12.28 0.34 o 3 4 3 33.73 32.61 0.58 o 4 4 3 12.24 11.67 0.45 o 5 4 3 15.82 18.97 0.69 o 0 5 3 28.83 29.40 0.57 o 1 5 3 6.62 6.70 0.31 o 2 5 3 6.85 7.81 0.32 o 3 5 3 11.36 11.76 0.41 o 4 5 3 21.74 24.13 0.89 o 0 6 3 6.84 5.14 0.51 o 1 6 3 25.50 26.73 0.67 o 2 6 3 0.25 -0.10 0.19 o 3 6 3 0.68 0.53 0.25 o 4 6 3 3.06 3.61 0.38 o 0 7 3 1.51 0.86 0.58 o 1 7 3 3.32 2.91 0.42 o 2 7 3 2.94 2.55 0.37 o 3 7 3 5.88 6.74 0.49 o 0 0 4 84.21 83.69 1.22 o 1 0 4 0.24 -0.11 0.07 o 2 0 4 49.57 54.28 0.58 o 3 0 4 223.92 247.10 2.02 o 4 0 4 22.07 21.33 0.51 o 5 0 4 76.06 64.18 1.62 o 6 0 4 11.28 11.33 1.09 o 0 1 4 180.42 200.14 2.10 o 1 1 4 52.53 46.20 0.37 o 2 1 4 354.61 346.12 2.00 o 3 1 4 38.23 35.70 0.42 o 4 1 4 145.88 146.40 1.19 o 5 1 4 35.28 34.87 1.20 o 6 1 4 4.76 4.06 0.48 o 0 2 4 929.95 902.84 7.05 o 1 2 4 4.60 7.76 0.15 o 2 2 4 501.51 482.08 2.73 o 3 2 4 34.21 40.07 0.44 o 4 2 4 0.70 0.49 0.17 o 5 2 4 29.62 30.14 0.80 o 6 2 4 9.23 10.05 0.54 o 0 3 4 366.66 398.84 3.12 o 1 3 4 20.72 21.51 0.27 o 2 3 4 14.61 10.37 0.22 o 3 3 4 8.26 7.45 0.29 o 4 3 4 26.40 23.09 0.55 o 5 3 4 8.31 8.60 0.46 o 0 4 4 29.17 32.69 0.60 o 1 4 4 4.67 3.46 0.19 o 2 4 4 30.77 27.68 0.51 o 3 4 4 18.22 19.86 0.46 o 4 4 4 5.31 7.22 0.38 o 5 4 4 11.21 10.61 0.55 o 0 5 4 29.97 23.51 0.52 o 1 5 4 0.00 -0.01 0.14 o 2 5 4 53.96 61.15 0.83 o 3 5 4 10.19 11.22 0.42 o 4 5 4 37.45 42.13 0.81 o 0 6 4 8.27 10.08 0.62 o 1 6 4 1.45 2.51 0.29 o 2 6 4 10.18 10.14 0.38 o 3 6 4 2.65 2.47 0.31 o 4 6 4 0.34 0.61 0.31 o 0 7 4 0.02 0.22 0.52 o 1 7 4 0.01 -0.18 0.28 o 2 7 4 2.16 1.91 0.35 o 1 0 5 7255.00 7648.86 68.01 o 2 0 5 971.04 949.87 7.01 o 3 0 5 1218.29 1282.49 9.04 o 4 0 5 1.69 1.49 0.24 o 5 0 5 15.63 13.74 0.66 o 6 0 5 4.02 4.90 0.69 o 0 1 5 247.80 227.31 3.04 o 1 1 5 931.03 937.80 4.88 o 2 1 5 103.62 112.73 0.73 o 3 1 5 195.80 238.85 1.43 o 4 1 5 73.11 73.18 0.73 o 5 1 5 59.53 58.11 0.91 o 6 1 5 4.80 5.65 0.50 o 0 2 5 0.16 0.25 0.10 o 1 2 5 54.33 60.32 0.45 o 2 2 5 393.52 482.64 2.74 o 3 2 5 71.99 79.78 0.68 o 4 2 5 0.25 0.81 0.18 o 5 2 5 61.42 73.41 1.09 o 6 2 5 6.94 5.27 0.45 o 0 3 5 28.82 26.17 0.43 o 1 3 5 98.17 109.69 0.81 o 2 3 5 20.42 21.04 0.37 o 3 3 5 111.13 119.59 1.28 o 4 3 5 8.91 9.67 0.40 o 5 3 5 39.14 38.16 1.04 o 0 4 5 0.76 0.48 0.13 o 1 4 5 140.40 130.84 1.00 o 2 4 5 68.11 64.44 0.90 o 3 4 5 63.59 65.13 0.89 o 4 4 5 4.01 5.06 0.36 o 5 4 5 3.80 3.76 0.41 o 0 5 5 3.85 4.14 0.27 o 1 5 5 14.49 13.78 0.33 o 2 5 5 10.44 12.93 0.38 o 3 5 5 16.37 17.80 0.51 o 4 5 5 4.02 4.10 0.36 o 0 6 5 0.26 -0.25 0.30 o 1 6 5 22.42 20.62 0.52 o 2 6 5 10.47 10.61 0.41 o 3 6 5 9.80 8.68 0.42 o 4 6 5 0.82 1.01 0.31 o 0 7 5 0.76 0.26 0.54 o 1 7 5 0.14 0.08 0.30 o 2 7 5 0.37 -0.11 0.31 o 0 0 6 46.55 66.69 0.98 o 1 0 6 0.72 0.38 0.14 o 2 0 6 292.21 327.18 2.62 o 3 0 6 0.09 -0.08 0.14 o 4 0 6 2.14 1.65 0.24 o 5 0 6 29.53 26.39 0.73 o 6 0 6 6.20 5.77 0.74 o 0 1 6 15.38 18.13 0.53 o 1 1 6 399.33 413.42 2.38 o 2 1 6 7.65 7.53 0.16 o 3 1 6 189.16 200.42 1.21 o 4 1 6 23.46 25.95 0.49 o 5 1 6 71.96 67.40 1.21 o 6 1 6 2.00 2.25 0.48 o 0 2 6 205.68 217.00 1.88 o 1 2 6 41.09 44.35 0.37 o 2 2 6 318.11 333.85 1.97 o 3 2 6 4.23 4.45 0.19 o 4 2 6 2.55 3.59 0.27 o 5 2 6 18.43 19.01 0.58 o 0 3 6 154.28 183.53 1.54 o 1 3 6 90.81 106.63 0.83 o 2 3 6 50.58 53.29 0.52 o 3 3 6 51.90 47.84 0.73 o 4 3 6 6.04 5.80 0.37 o 5 3 6 18.20 18.44 0.60 o 0 4 6 76.92 91.08 1.00 o 1 4 6 5.07 5.70 0.22 o 2 4 6 122.23 119.63 1.05 o 3 4 6 3.91 3.54 0.29 o 4 4 6 1.16 0.99 0.24 o 5 4 6 6.64 7.79 0.47 o 0 5 6 6.91 6.44 0.35 o 1 5 6 11.83 13.97 0.40 o 2 5 6 1.04 1.08 0.20 o 3 5 6 5.02 4.71 0.32 o 4 5 6 2.14 1.44 0.29 o 0 6 6 0.04 0.11 0.31 o 1 6 6 4.83 4.23 0.30 o 2 6 6 6.64 6.33 0.35 o 3 6 6 2.40 2.50 0.31 o 0 7 6 0.01 -0.43 0.49 o 1 7 6 0.39 0.26 0.31 o 2 7 6 0.47 -0.11 0.30 o 1 0 7 156.85 161.86 1.44 o 2 0 7 889.76 1073.14 7.54 o 3 0 7 32.37 30.62 0.64 o 4 0 7 75.26 54.82 0.82 o 5 0 7 99.20 106.27 1.54 o 6 0 7 3.54 4.19 0.70 o 0 1 7 99.87 83.50 1.50 o 1 1 7 33.10 31.00 0.28 o 2 1 7 35.75 38.79 0.37 o 3 1 7 91.04 113.57 0.82 o 4 1 7 11.64 11.94 0.32 o 5 1 7 11.14 11.52 0.45 o 6 1 7 46.04 50.56 1.13 o 0 2 7 0.33 0.11 0.09 o 1 2 7 757.38 778.72 5.55 o 2 2 7 486.32 501.37 3.76 o 3 2 7 37.06 35.92 0.45 o 4 2 7 62.27 57.94 0.71 o 5 2 7 25.66 25.22 0.65 o 0 3 7 187.94 183.13 1.60 o 1 3 7 104.19 109.23 0.88 o 2 3 7 25.73 24.04 0.34 o 3 3 7 2.78 3.36 0.19 o 4 3 7 5.74 5.95 0.36 o 5 3 7 3.02 3.69 0.37 o 0 4 7 2.22 2.72 0.19 o 1 4 7 29.95 28.98 0.43 o 2 4 7 59.10 64.18 0.78 o 3 4 7 0.56 0.83 0.22 o 4 4 7 18.75 17.70 0.55 o 5 4 7 10.13 11.39 0.53 o 0 5 7 2.11 2.01 0.27 o 1 5 7 9.21 9.72 0.30 o 2 5 7 0.11 0.34 0.18 o 3 5 7 6.96 7.86 0.38 o 4 5 7 3.03 4.42 0.37 o 0 6 7 0.59 0.64 0.34 o 1 6 7 8.06 6.71 0.36 o 2 6 7 3.33 2.71 0.33 o 3 6 7 0.14 0.02 0.24 o 0 7 7 0.89 -0.01 0.50 o 1 7 7 0.12 -0.43 0.29 o 2 7 7 0.70 0.78 0.33 o 0 0 8 0.56 -0.15 0.10 o 1 0 8 13.92 14.60 0.27 o 2 0 8 42.77 36.87 0.55 o 3 0 8 1.50 1.31 0.18 o 4 0 8 0.61 0.17 0.19 o 5 0 8 46.09 43.80 0.94 o 6 0 8 8.39 9.64 0.87 o 0 1 8 1799.08 1967.82 13.51 o 1 1 8 144.17 180.55 1.02 o 2 1 8 214.60 246.17 1.54 o 3 1 8 85.83 80.45 0.71 o 4 1 8 30.28 25.57 0.43 o 5 1 8 47.49 45.64 0.73 o 6 1 8 15.12 18.32 0.71 o 0 2 8 86.84 110.51 1.47 o 1 2 8 0.10 0.72 0.08 o 2 2 8 34.95 35.49 0.35 o 3 2 8 8.92 7.80 0.25 o 4 2 8 16.10 14.12 0.37 o 5 2 8 33.59 33.30 0.83 o 0 3 8 410.04 386.85 3.24 o 1 3 8 67.44 67.82 0.64 o 2 3 8 76.42 70.58 0.64 o 3 3 8 17.29 17.49 0.34 o 4 3 8 3.47 4.06 0.33 o 5 3 8 30.33 26.04 0.70 o 0 4 8 2.69 4.36 0.22 o 1 4 8 32.94 32.24 0.42 o 2 4 8 13.90 15.18 0.33 o 3 4 8 6.89 6.99 0.44 o 4 4 8 9.83 9.60 0.51 o 5 4 8 10.25 11.04 0.62 o 0 5 8 11.24 7.94 0.40 o 1 5 8 3.84 4.02 0.27 o 2 5 8 3.99 3.58 0.28 o 3 5 8 5.25 4.96 0.34 o 4 5 8 0.44 -0.12 0.27 o 0 6 8 11.62 12.97 0.87 o 1 6 8 1.10 1.80 0.29 o 2 6 8 6.64 6.94 0.42 o 3 6 8 3.53 4.88 0.37 o 0 7 8 0.52 0.77 0.59 o 1 7 8 0.21 0.27 0.31 o 2 7 8 0.61 0.65 0.34 o 1 0 9 5.67 7.41 0.20 o 2 0 9 488.44 498.00 3.92 o 3 0 9 3.77 5.54 0.26 o 4 0 9 142.52 144.64 1.56 o 5 0 9 44.77 45.15 0.97 o 0 1 9 594.60 557.90 4.01 o 1 1 9 119.31 121.27 0.89 o 2 1 9 131.34 138.60 0.93 o 3 1 9 27.72 28.18 0.39 o 4 1 9 5.73 4.81 0.24 o 5 1 9 1.91 1.32 0.24 o 0 2 9 82.15 84.38 0.81 o 1 2 9 10.72 14.66 0.20 o 2 2 9 175.04 187.71 1.67 o 3 2 9 13.67 13.58 0.33 o 4 2 9 78.34 69.45 0.85 o 5 2 9 23.31 23.36 0.64 o 0 3 9 18.58 15.46 0.39 o 1 3 9 156.96 159.23 1.34 o 2 3 9 2.49 2.73 0.16 o 3 3 9 17.50 17.39 0.42 o 4 3 9 15.14 17.22 0.54 o 5 3 9 0.75 0.80 0.30 o 0 4 9 9.47 10.11 0.29 o 1 4 9 12.67 10.66 0.25 o 2 4 9 14.43 13.93 0.32 o 3 4 9 2.76 2.85 0.27 o 4 4 9 16.03 19.09 0.66 o 5 4 9 5.70 5.17 0.44 o 0 5 9 23.35 20.46 0.60 o 1 5 9 13.67 13.86 0.37 o 2 5 9 1.11 0.74 0.21 o 3 5 9 0.68 0.25 0.23 o 4 5 9 1.67 1.76 0.33 o 0 6 9 0.45 0.71 0.34 o 1 6 9 6.22 6.72 0.44 o 2 6 9 1.50 0.98 0.28 o 3 6 9 1.32 1.27 0.29 o 0 7 9 4.36 3.95 0.76 o 1 7 9 1.70 1.00 0.40 o 2 7 9 0.20 0.21 0.35 o 0 0 10 396.78 448.30 6.12 o 1 0 10 277.28 259.74 2.02 o 2 0 10 0.72 0.74 0.14 o 3 0 10 42.28 44.58 0.71 o 4 0 10 0.28 0.53 0.22 o 5 0 10 55.61 54.58 1.15 o 0 1 10 4173.09 4444.22 33.02 o 1 1 10 190.95 167.96 1.88 o 2 1 10 298.69 291.54 2.12 o 3 1 10 26.61 26.07 0.37 o 4 1 10 54.48 47.82 0.73 o 5 1 10 0.27 0.34 0.22 o 0 2 10 407.15 397.45 2.97 o 1 2 10 225.05 220.95 1.47 o 2 2 10 8.63 10.09 0.21 o 3 2 10 10.36 9.25 0.28 o 4 2 10 7.52 7.12 0.33 o 5 2 10 49.43 49.08 1.04 o 0 3 10 521.64 497.61 6.55 o 1 3 10 24.39 26.95 0.34 o 2 3 10 18.25 17.61 0.33 o 3 3 10 25.83 26.69 0.47 o 4 3 10 48.27 46.15 0.84 o 5 3 10 2.58 3.46 0.38 o 0 4 10 10.67 8.09 0.30 o 1 4 10 23.24 21.88 0.35 o 2 4 10 4.46 4.71 0.25 o 3 4 10 9.66 8.91 0.38 o 4 4 10 7.93 7.77 0.44 o 0 5 10 146.08 127.27 1.72 o 1 5 10 3.28 3.40 0.24 o 2 5 10 15.91 16.75 0.47 o 3 5 10 7.02 8.33 0.41 o 4 5 10 1.49 1.09 0.30 o 0 6 10 1.18 0.39 0.38 o 1 6 10 4.84 3.66 0.35 o 2 6 10 0.24 0.09 0.25 o 3 6 10 0.20 0.86 0.28 o 0 7 10 7.14 4.32 0.65 o 1 7 10 1.62 2.20 0.49 o 2 7 10 0.24 0.12 0.36 o 1 0 11 15.38 18.29 0.35 o 2 0 11 155.95 153.00 1.46 o 3 0 11 11.47 13.57 0.39 o 4 0 11 111.04 95.91 1.48 o 5 0 11 18.35 16.57 0.68 o 0 1 11 86.34 90.04 0.87 o 1 1 11 11.81 16.20 0.26 o 2 1 11 314.49 307.02 1.93 o 3 1 11 1.55 0.73 0.13 o 4 1 11 94.46 89.36 0.94 o 5 1 11 11.60 10.92 0.43 o 0 2 11 105.82 76.20 7.17 o 1 2 11 5.65 4.02 0.14 o 2 2 11 64.39 64.37 0.71 o 3 2 11 7.51 7.31 0.27 o 4 2 11 48.75 49.14 0.70 o 5 2 11 14.08 12.33 0.61 o 0 3 11 69.01 68.95 1.06 o 1 3 11 80.78 81.26 0.74 o 2 3 11 57.65 54.97 0.68 o 3 3 11 8.85 6.61 0.27 o 4 3 11 16.14 18.17 0.66 o 5 3 11 10.83 9.45 0.49 o 0 4 11 28.03 28.53 0.56 o 1 4 11 26.65 29.46 0.41 o 2 4 11 10.40 10.16 0.29 o 3 4 11 12.72 10.55 0.41 o 4 4 11 13.08 12.96 0.53 o 0 5 11 19.14 21.18 0.87 o 1 5 11 10.06 9.55 0.30 o 2 5 11 7.67 6.31 0.34 o 3 5 11 0.47 0.32 0.24 o 4 5 11 4.67 4.59 0.45 o 0 6 11 14.93 14.92 0.77 o 1 6 11 2.38 2.51 0.32 o 2 6 11 0.12 0.18 0.26 o 3 6 11 1.12 1.81 0.32 o 0 7 11 0.61 -0.17 0.42 o 1 7 11 3.99 3.80 0.51 o 0 0 12 3079.08 3214.36 34.90 o 1 0 12 24.34 27.70 0.48 o 2 0 12 36.18 29.25 2.86 o 3 0 12 33.97 29.31 0.56 o 4 0 12 4.62 4.03 0.38 o 5 0 12 3.76 4.75 0.42 o 0 1 12 204.28 220.75 1.81 o 1 1 12 384.91 410.84 3.44 o 2 1 12 9.80 12.74 0.24 o 3 1 12 39.07 40.59 0.53 o 4 1 12 14.81 16.09 0.44 o 5 1 12 44.46 39.62 0.73 o 0 2 12 464.28 468.02 4.96 o 1 2 12 46.20 48.51 0.43 o 2 2 12 30.11 26.03 0.36 o 3 2 12 21.81 23.86 0.44 o 4 2 12 37.24 33.67 0.57 o 5 2 12 11.10 11.15 0.51 o 0 3 12 168.79 181.75 2.77 o 1 3 12 113.27 107.22 0.85 o 2 3 12 26.64 24.25 0.41 o 3 3 12 37.38 36.83 0.79 o 4 3 12 5.22 4.82 0.37 o 5 3 12 22.84 20.69 0.70 o 0 4 12 149.11 139.22 2.47 o 1 4 12 25.69 24.51 0.39 o 2 4 12 4.22 4.81 0.23 o 3 4 12 12.24 11.43 0.56 o 4 4 12 7.26 7.12 0.44 o 0 5 12 12.04 11.62 0.59 o 1 5 12 16.50 15.34 0.39 o 2 5 12 0.11 0.01 0.19 o 3 5 12 1.46 1.47 0.29 o 4 5 12 3.22 3.67 0.42 o 0 6 12 26.28 24.98 1.03 o 1 6 12 2.39 3.35 0.33 o 2 6 12 1.52 1.81 0.32 o 3 6 12 0.05 0.38 0.28 o 0 7 12 3.90 3.24 0.55 o 1 7 12 1.87 1.82 0.50 o 1 0 13 1.15 0.41 0.11 o 2 0 13 37.93 40.81 0.73 o 3 0 13 25.23 26.51 0.55 o 4 0 13 36.87 34.43 0.80 o 5 0 13 1.17 1.12 0.34 o 0 1 13 23.56 24.51 0.41 o 1 1 13 14.60 19.33 0.27 o 2 1 13 24.16 20.56 0.34 o 3 1 13 29.28 27.32 0.45 o 4 1 13 37.75 35.40 0.72 o 5 1 13 36.07 33.53 0.70 o 0 2 13 0.33 0.63 0.12 o 1 2 13 137.29 128.65 0.87 o 2 2 13 40.93 42.99 0.48 o 3 2 13 6.55 5.31 0.25 o 4 2 13 35.38 28.13 0.53 o 5 2 13 8.41 9.03 0.54 o 0 3 13 0.44 0.37 0.15 o 1 3 13 42.38 39.59 0.45 o 2 3 13 6.85 5.63 0.23 o 3 3 13 77.49 69.06 1.04 o 4 3 13 15.83 13.95 0.55 o 5 3 13 1.19 1.15 0.32 o 0 4 13 69.48 68.25 1.67 o 1 4 13 0.69 0.56 0.14 o 2 4 13 18.88 19.34 0.40 o 3 4 13 8.56 9.15 0.40 o 4 4 13 5.64 5.07 0.41 o 0 5 13 3.46 3.63 0.50 o 1 5 13 35.33 34.96 0.61 o 2 5 13 0.26 0.26 0.19 o 3 5 13 0.17 0.07 0.33 o 0 6 13 1.56 1.27 0.41 o 1 6 13 4.20 5.34 0.38 o 2 6 13 8.41 9.19 0.52 o 0 7 13 0.91 1.77 0.61 o 0 0 14 5.88 3.78 0.27 o 1 0 14 1.84 4.51 0.21 o 2 0 14 90.59 74.79 1.06 o 3 0 14 54.47 69.36 0.95 o 4 0 14 17.12 13.65 0.55 o 5 0 14 36.46 36.37 1.00 o 0 1 14 51.13 54.90 0.66 o 1 1 14 263.87 250.85 1.52 o 2 1 14 14.53 11.56 0.29 o 3 1 14 52.77 50.05 0.60 o 4 1 14 17.63 15.07 0.52 o 5 1 14 2.59 5.18 0.37 o 0 2 14 247.07 236.25 3.06 o 1 2 14 7.30 7.32 0.25 o 2 2 14 0.66 0.55 0.13 o 3 2 14 63.45 57.14 0.93 o 4 2 14 2.09 1.52 0.22 o 5 2 14 27.80 25.73 0.67 o 0 3 14 1.88 1.72 0.24 o 1 3 14 49.93 52.49 0.70 o 2 3 14 28.34 33.51 0.68 o 3 3 14 4.85 5.11 0.31 o 4 3 14 26.78 26.16 0.72 o 0 4 14 46.21 47.82 0.80 o 1 4 14 17.19 18.54 0.38 o 2 4 14 2.30 3.06 0.23 o 3 4 14 6.96 7.51 0.38 o 4 4 14 0.91 0.98 0.32 o 0 5 14 4.46 6.14 0.42 o 1 5 14 7.10 8.66 0.33 o 2 5 14 10.48 10.56 0.51 o 3 5 14 0.79 0.80 0.29 o 0 6 14 0.03 -0.12 0.37 o 1 6 14 1.23 1.34 0.29 o 2 6 14 9.50 11.16 0.56 o 1 0 15 547.50 520.76 3.91 o 2 0 15 12.59 11.48 0.43 o 3 0 15 157.82 146.70 1.68 o 4 0 15 0.15 -0.07 0.25 o 5 0 15 0.36 0.93 0.42 o 0 1 15 22.79 17.06 0.38 o 1 1 15 44.15 39.17 0.44 o 2 1 15 451.73 446.04 2.78 o 3 1 15 6.92 4.98 0.24 o 4 1 15 11.12 10.70 0.40 o 5 1 15 27.41 27.02 0.68 o 0 2 15 32.67 30.39 0.49 o 1 2 15 0.46 0.91 0.11 o 2 2 15 35.76 38.69 0.50 o 3 2 15 376.69 358.05 2.87 o 4 2 15 8.19 8.88 0.35 o 5 2 15 10.97 12.17 0.51 o 0 3 15 1.85 1.68 0.18 o 1 3 15 47.69 45.91 0.59 o 2 3 15 184.23 184.96 3.11 o 3 3 15 9.93 10.81 0.35 o 4 3 15 6.83 6.36 0.36 o 0 4 15 22.54 25.26 0.63 o 1 4 15 27.48 27.42 0.51 o 2 4 15 43.18 46.81 0.77 o 3 4 15 58.98 58.49 1.55 o 4 4 15 2.45 1.86 0.34 o 0 5 15 2.17 2.06 0.32 o 1 5 15 1.59 1.31 0.21 o 2 5 15 36.47 36.78 0.66 o 3 5 15 2.76 3.28 0.39 o 0 6 15 2.78 1.96 0.50 o 1 6 15 0.52 0.25 0.25 o 2 6 15 3.01 3.56 0.41 o 0 0 16 193.86 188.07 2.33 o 1 0 16 95.21 95.20 1.08 o 2 0 16 109.77 111.72 1.26 o 3 0 16 201.82 176.80 1.89 o 4 0 16 1.04 1.07 0.31 o 5 0 16 16.07 14.39 0.80 o 0 1 16 239.40 240.82 2.02 o 1 1 16 62.34 61.19 0.78 o 2 1 16 58.77 57.47 0.71 o 3 1 16 49.87 48.12 0.62 o 4 1 16 0.88 0.67 0.18 o 5 1 16 39.55 39.40 0.90 o 0 2 16 171.76 175.00 1.63 o 1 2 16 38.90 38.83 0.43 o 2 2 16 134.13 123.74 1.09 o 3 2 16 86.65 90.55 1.21 o 4 2 16 0.53 0.17 0.20 o 0 3 16 1.08 1.64 0.19 o 1 3 16 43.44 43.63 0.56 o 2 3 16 23.67 25.42 0.50 o 3 3 16 1.32 0.97 0.23 o 4 3 16 4.58 4.15 0.32 o 0 4 16 64.77 69.28 1.19 o 1 4 16 7.52 8.31 0.40 o 2 4 16 78.01 77.22 1.03 o 3 4 16 28.73 28.21 0.81 o 4 4 16 3.62 4.23 0.40 o 0 5 16 15.79 15.26 0.68 o 1 5 16 6.40 5.98 0.33 o 2 5 16 21.32 27.98 0.89 o 3 5 16 2.70 2.89 0.41 o 0 6 16 0.35 0.09 0.40 o 1 6 16 0.24 0.65 0.29 o 2 6 16 5.39 5.33 0.48 o 1 0 17 451.10 439.93 3.62 o 2 0 17 149.17 137.02 1.48 o 3 0 17 634.18 616.37 5.05 o 4 0 17 18.85 18.63 0.72 o 5 0 17 20.76 23.18 0.97 o 0 1 17 19.33 18.59 0.41 o 1 1 17 92.82 85.83 0.95 o 2 1 17 243.57 250.21 1.66 o 3 1 17 112.53 111.02 1.06 o 4 1 17 8.98 8.68 0.51 o 0 2 17 23.40 23.11 0.49 o 1 2 17 4.57 2.99 0.16 o 2 2 17 106.52 113.49 1.07 o 3 2 17 130.55 129.19 1.48 o 4 2 17 18.75 18.44 0.48 o 0 3 17 44.93 43.07 0.96 o 1 3 17 61.84 56.54 0.66 o 2 3 17 122.04 124.06 1.35 o 3 3 17 23.15 25.69 0.54 o 4 3 17 0.15 0.09 0.22 o 0 4 17 6.60 7.23 0.49 o 1 4 17 26.61 26.21 0.71 o 2 4 17 12.66 10.16 0.37 o 3 4 17 94.26 102.76 1.56 o 0 5 17 0.33 -0.08 0.28 o 1 5 17 4.84 4.81 0.32 o 2 5 17 19.33 24.14 0.78 o 3 5 17 4.87 5.79 0.46 o 0 6 17 0.33 0.48 0.44 o 1 6 17 7.04 8.06 0.48 o 0 0 18 103.48 105.71 1.57 o 1 0 18 36.47 36.34 0.66 o 2 0 18 257.03 254.81 2.37 o 3 0 18 39.06 41.19 0.78 o 4 0 18 17.65 15.78 0.64 o 0 1 18 19.52 21.33 0.49 o 1 1 18 95.86 98.46 0.81 o 2 1 18 8.39 9.32 0.27 o 3 1 18 4.31 3.66 0.24 o 4 1 18 46.62 48.66 0.87 o 0 2 18 207.69 204.01 1.94 o 1 2 18 21.76 23.07 0.43 o 2 2 18 336.04 334.54 3.98 o 3 2 18 30.50 27.32 0.53 o 4 2 18 40.03 38.70 0.83 o 0 3 18 69.76 71.78 1.04 o 1 3 18 35.03 33.99 0.52 o 2 3 18 13.38 13.14 0.40 o 3 3 18 13.16 13.45 0.41 o 4 3 18 1.05 1.05 0.25 o 0 4 18 12.25 11.99 0.59 o 1 4 18 13.79 14.66 0.41 o 2 4 18 60.61 66.26 1.11 o 3 4 18 9.17 10.77 0.44 o 0 5 18 8.54 9.48 0.60 o 1 5 18 9.36 9.55 0.40 o 2 5 18 8.51 10.12 0.48 o 0 6 18 5.33 6.10 0.57 o 1 0 19 38.56 36.80 0.70 o 2 0 19 150.27 166.57 1.75 o 3 0 19 0.06 -0.04 0.21 o 4 0 19 0.35 0.95 0.33 o 0 1 19 47.35 41.93 0.69 o 1 1 19 143.11 135.25 1.03 o 2 1 19 30.00 32.26 0.46 o 3 1 19 4.33 4.93 0.30 o 4 1 19 10.72 10.94 0.47 o 0 2 19 3.05 2.14 0.23 o 1 2 19 242.77 238.61 2.03 o 2 2 19 88.47 90.34 0.97 o 3 2 19 45.15 45.56 0.72 o 4 2 19 0.35 0.65 0.22 o 0 3 19 4.07 3.88 0.33 o 1 3 19 83.56 84.87 1.41 o 2 3 19 1.81 1.91 0.22 o 3 3 19 0.14 0.03 0.20 o 0 4 19 0.04 -0.06 0.28 o 1 4 19 33.89 32.46 0.87 o 2 4 19 24.31 28.74 0.58 o 3 4 19 7.87 8.44 0.40 o 0 5 19 0.51 0.65 0.34 o 1 5 19 8.72 8.08 0.42 o 2 5 19 0.76 1.33 0.31 o 0 0 20 63.14 62.39 1.33 o 1 0 20 20.36 18.31 0.49 o 2 0 20 166.14 166.83 1.77 o 3 0 20 3.14 3.65 0.42 o 4 0 20 15.79 17.73 0.70 o 0 1 20 33.36 27.72 0.57 o 1 1 20 29.54 30.23 0.43 o 2 1 20 2.30 2.41 0.19 o 3 1 20 0.23 0.33 0.16 o 4 1 20 4.39 4.54 0.35 o 0 2 20 12.52 9.18 0.37 o 1 2 20 28.43 26.62 1.08 o 2 2 20 10.24 12.99 0.43 o 3 2 20 8.49 8.94 0.36 o 4 2 20 0.55 1.37 0.27 o 0 3 20 99.23 72.59 10.05 o 1 3 20 16.84 18.86 0.43 o 2 3 20 26.09 26.68 0.53 o 3 3 20 0.06 0.10 0.21 o 0 4 20 2.87 4.12 0.47 o 1 4 20 7.73 8.14 0.38 o 2 4 20 20.50 24.38 0.59 o 3 4 20 4.62 5.02 0.35 o 0 5 20 8.28 10.33 0.66 o 1 5 20 3.71 5.21 0.40 o 1 0 21 1.62 0.68 0.19 o 2 0 21 22.77 21.92 0.80 o 3 0 21 1.40 1.68 0.33 o 4 0 21 17.86 17.44 0.70 o 0 1 21 11.24 9.88 0.40 o 1 1 21 52.06 51.88 0.59 o 2 1 21 8.13 8.60 0.30 o 3 1 21 33.65 32.94 0.60 o 4 1 21 6.19 6.81 0.40 o 0 2 21 0.31 0.65 0.19 o 1 2 21 18.44 18.33 0.36 o 2 2 21 7.91 9.58 0.37 o 3 2 21 6.39 7.02 0.39 o 0 3 21 0.12 0.47 0.17 o 1 3 21 2.80 3.53 0.26 o 2 3 21 3.89 3.72 0.28 o 3 3 21 4.52 5.13 0.33 o 0 4 21 0.39 0.22 0.31 o 1 4 21 2.62 3.18 0.29 o 2 4 21 3.46 4.03 0.30 o 0 5 21 2.78 4.14 0.53 o 1 5 21 10.00 10.70 0.51 o 0 0 22 82.81 79.39 2.63 o 1 0 22 9.80 7.22 0.35 o 2 0 22 55.52 53.75 0.90 o 3 0 22 0.40 0.34 0.27 o 0 1 22 13.65 10.26 0.42 o 1 1 22 1.97 1.40 0.17 o 2 1 22 0.90 0.55 0.18 o 3 1 22 16.52 18.22 0.48 o 0 2 22 0.05 -0.14 0.18 o 1 2 22 6.37 5.40 0.26 o 2 2 22 0.04 0.13 0.18 o 3 2 22 0.48 0.64 0.22 o 0 3 22 4.90 3.68 0.42 o 1 3 22 2.29 1.94 0.23 o 2 3 22 0.38 0.24 0.19 o 3 3 22 8.11 8.43 0.39 o 0 4 22 8.67 9.50 0.64 o 1 4 22 2.34 3.21 0.29 o 2 4 22 5.77 7.32 0.36 o 1 0 23 89.29 91.79 1.20 o 2 0 23 0.01 0.24 0.22 o 3 0 23 5.63 5.76 0.55 o 0 1 23 0.29 0.29 0.21 o 1 1 23 0.23 0.32 0.15 o 2 1 23 2.49 2.31 0.22 o 3 1 23 2.17 2.15 0.27 o 0 2 23 0.73 0.73 0.23 o 1 2 23 64.21 60.96 0.74 o 2 2 23 0.35 0.79 0.21 o 3 2 23 10.14 9.69 0.40 o 0 3 23 1.16 1.69 0.31 o 1 3 23 3.00 2.05 0.28 o 2 3 23 0.17 0.27 0.20 o 0 4 23 0.11 0.45 0.40 o 1 4 23 13.78 14.44 0.54 o 0 0 24 0.12 0.68 0.32 o 1 0 24 3.27 5.54 0.37 o 2 0 24 0.02 0.12 0.22 o 3 0 24 13.02 13.90 0.63 o 0 1 24 7.27 10.95 0.46 o 1 1 24 4.48 3.28 0.22 o 2 1 24 1.12 1.78 0.21 o 3 1 24 28.99 34.65 0.66 o 0 2 24 23.74 25.29 0.65 o 1 2 24 7.70 9.83 0.33 o 2 2 24 10.23 9.41 0.37 o 0 3 24 2.97 3.07 0.42 o 1 3 24 1.30 0.83 0.22 o 2 3 24 0.94 0.61 0.24 o 0 4 24 2.32 2.47 0.51 o 1 0 25 20.61 14.74 0.83 o 2 0 25 12.91 16.22 0.56 o 0 1 25 0.46 0.69 0.25 o 1 1 25 0.72 1.14 0.19 o 2 1 25 0.47 0.28 0.19 o 0 2 25 1.26 1.76 0.29 o 1 2 25 4.23 4.60 0.28 o 2 2 25 13.04 15.51 0.48 o 0 3 25 0.89 0.62 0.32 o 1 3 25 1.30 2.01 0.26 o 0 0 26 2.88 1.92 0.42 o 1 0 26 1.82 2.71 0.32 o 2 0 26 3.06 5.10 0.40 o 0 1 26 2.50 2.60 0.31 o 1 1 26 4.47 4.66 0.27 o 2 1 26 1.48 1.65 0.24 o 0 2 26 5.50 5.94 0.40 o 1 2 26 0.81 1.31 0.23 o 1 0 27 4.77 6.17 0.52 o 0 1 27 0.50 0.74 0.27 o 1 1 27 4.21 3.57 0.26 o