#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:21:56 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181224 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/02/2230204.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230204_Fobs loop_ _publ_author_name 'Ye, Ting-Hong' 'Huang, Ting-Ting' 'Shi, Yao-Jie' 'Xiong, Ying' 'Yu, Luo-Ting' _publ_section_title ; N-Methyl-4-(4-pivalamidophenylsulfanyl)picolinamide hemihydrate ; _journal_coeditor_code ZQ2092 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1098 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 108.632 _cell_angle_gamma 90.000 _cell_length_a 12.7413 _cell_length_b 17.5056 _cell_length_c 17.1978 _exptl_crystal_F_000 1496.00 _reflns_d_resolution_high 0.8000 _cod_data_source_file zq2092Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 525.93 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6091.03 6463.19 23.01 o 4 0 0 3976.32 4165.04 27.21 o 6 0 0 110.86 125.93 9.76 o 8 0 0 3428.43 3295.53 46.13 o 10 0 0 164.47 95.28 23.65 o 12 0 0 1264.42 1336.40 43.80 o 14 0 0 604.15 529.56 47.96 o 3 1 0 1811.87 1823.17 11.66 o 5 1 0 16559.77 16849.77 92.84 o 7 1 0 5375.08 5685.74 87.78 o 9 1 0 158.04 151.13 8.24 o 11 1 0 134.28 144.75 17.87 o 13 1 0 113.92 88.46 24.37 o 15 1 0 41.65 37.57 27.05 o 2 2 0 3683.07 3672.89 14.12 o 4 2 0 2642.17 2810.67 16.62 o 6 2 0 3166.98 3222.40 49.46 o 8 2 0 834.45 764.31 18.09 o 10 2 0 472.39 448.51 20.59 o 12 2 0 15.12 32.40 16.90 o 14 2 0 125.86 128.59 27.30 o 1 3 0 154.55 196.12 10.03 o 3 3 0 10628.67 11050.24 41.79 o 5 3 0 2797.10 3107.40 20.99 o 7 3 0 1015.17 1047.87 18.60 o 9 3 0 232.19 227.09 15.32 o 11 3 0 509.05 495.24 21.48 o 13 3 0 4.90 25.01 23.60 o 0 4 0 276603.38 265665.16 1300.06 o 2 4 0 12.36 13.40 6.22 o 4 4 0 7850.90 7929.42 38.38 o 6 4 0 618.10 721.54 14.77 o 8 4 0 261.23 285.41 14.56 o 10 4 0 1052.73 938.85 28.00 o 12 4 0 209.43 197.68 21.84 o 14 4 0 199.81 182.76 28.88 o 1 5 0 69727.80 67055.87 980.70 o 3 5 0 7293.54 6890.96 45.62 o 5 5 0 3087.65 3042.11 39.34 o 7 5 0 3022.10 3065.68 28.44 o 9 5 0 3794.67 3974.62 37.33 o 11 5 0 0.01 3.78 14.48 o 13 5 0 287.93 281.33 36.47 o 0 6 0 1670.09 1839.62 39.30 o 2 6 0 17328.78 16866.46 115.66 o 4 6 0 2163.12 2367.85 20.97 o 6 6 0 5555.08 5590.29 62.08 o 8 6 0 457.03 406.39 15.85 o 10 6 0 223.54 255.13 16.51 o 12 6 0 149.90 163.37 25.43 o 14 6 0 581.03 630.21 57.89 o 1 7 0 84.66 93.96 15.32 o 3 7 0 5391.94 5623.84 64.17 o 5 7 0 150.81 217.56 10.55 o 7 7 0 266.90 256.69 15.35 o 9 7 0 2844.70 2805.34 34.30 o 11 7 0 83.47 111.15 20.30 o 13 7 0 115.26 120.69 40.48 o 0 8 0 6038.41 6415.00 76.07 o 2 8 0 0.05 4.54 21.27 o 4 8 0 86.34 94.90 8.69 o 6 8 0 418.78 413.71 21.02 o 8 8 0 9.22 -0.03 14.88 o 10 8 0 15.15 21.23 24.33 o 12 8 0 10.90 22.51 27.42 o 14 8 0 45.14 81.37 43.27 o 1 9 0 11615.82 11188.23 102.90 o 3 9 0 2141.45 1859.39 49.04 o 5 9 0 397.91 395.89 14.64 o 7 9 0 710.72 704.34 24.44 o 9 9 0 481.78 449.12 32.24 o 11 9 0 22.56 31.37 27.11 o 13 9 0 0.02 -13.48 27.72 o 0 10 0 3216.04 2739.35 60.20 o 2 10 0 8566.29 8768.12 97.61 o 4 10 0 33.84 32.38 15.62 o 6 10 0 595.65 677.78 42.36 o 8 10 0 19.18 3.81 23.84 o 10 10 0 259.20 230.15 29.14 o 12 10 0 350.29 403.34 35.81 o 1 11 0 72.38 53.49 19.63 o 3 11 0 109.00 115.29 27.49 o 5 11 0 45.45 48.43 26.76 o 7 11 0 172.30 146.58 25.73 o 9 11 0 2840.46 2763.62 58.76 o 11 11 0 16.99 23.18 26.56 o 13 11 0 5.17 22.29 29.66 o 0 12 0 176.76 193.13 33.94 o 2 12 0 411.56 456.46 35.90 o 4 12 0 194.74 227.91 30.88 o 6 12 0 133.71 143.97 32.26 o 8 12 0 56.76 50.83 24.37 o 10 12 0 0.01 -12.56 26.00 o 12 12 0 81.15 101.36 30.60 o 1 13 0 205.23 200.86 25.38 o 3 13 0 1.83 -4.88 29.04 o 5 13 0 1.69 -10.44 27.97 o 7 13 0 7.65 -2.78 23.61 o 9 13 0 2.44 10.74 25.41 o 11 13 0 2.73 0.43 27.97 o 0 14 0 1705.71 1519.64 58.82 o 2 14 0 2032.31 2045.58 46.33 o 4 14 0 1.26 -3.83 29.00 o 6 14 0 11.35 10.07 30.14 o 8 14 0 1.08 28.24 25.92 o 10 14 0 3.11 0.18 27.21 o 1 15 0 136.72 173.07 29.85 o 3 15 0 15.58 12.50 30.21 o 5 15 0 46.83 36.81 29.71 o 7 15 0 42.46 73.20 25.78 o 9 15 0 197.10 191.45 30.28 o 0 16 0 321.23 256.96 40.64 o 2 16 0 338.75 375.46 30.03 o 4 16 0 45.43 10.18 30.77 o 6 16 0 130.61 68.83 34.20 o 8 16 0 0.02 4.32 27.60 o 10 16 0 121.71 137.69 31.88 o 1 17 0 387.40 367.56 32.87 o 3 17 0 21.30 23.85 25.07 o 5 17 0 14.51 32.93 32.50 o 7 17 0 86.88 77.89 27.02 o 9 17 0 49.15 47.54 29.33 o 0 18 0 283.90 397.86 44.39 o 2 18 0 116.38 80.47 27.17 o 4 18 0 2.68 8.65 25.11 o 6 18 0 5.29 -1.23 25.28 o 8 18 0 51.17 55.51 28.64 o 1 19 0 124.81 104.69 27.73 o 3 19 0 22.99 23.37 26.29 o 5 19 0 45.07 58.17 27.76 o 7 19 0 0.66 3.77 27.20 o 0 20 0 23.41 17.36 35.62 o 2 20 0 55.37 35.91 27.13 o 4 20 0 160.70 167.18 29.99 o 6 20 0 61.12 79.86 24.14 o 1 21 0 15.92 22.56 26.91 o 3 21 0 14.57 27.67 28.60 o -15 1 1 264.40 318.65 32.16 o -13 1 1 0.26 -3.14 22.40 o -11 1 1 2.61 7.42 21.06 o -9 1 1 52.70 40.00 6.34 o -7 1 1 2787.00 2976.59 37.60 o -5 1 1 32.54 22.93 6.51 o -3 1 1 3417.98 3406.74 13.31 o 3 1 1 152.99 179.98 5.16 o 5 1 1 27206.38 29998.01 87.51 o 7 1 1 2077.41 2155.50 20.68 o 9 1 1 6133.26 6057.89 50.14 o 11 1 1 1841.72 1836.46 33.55 o 13 1 1 106.60 96.42 19.06 o -14 2 1 661.85 739.15 36.81 o -12 2 1 43.06 65.16 22.61 o -10 2 1 5919.82 6023.56 50.98 o -8 2 1 784.89 854.75 18.33 o -6 2 1 423.45 486.57 11.38 o -4 2 1 1454.34 1329.26 11.64 o -2 2 1 4111.08 4062.30 23.07 o 2 2 1 96.86 123.98 6.16 o 4 2 1 3428.88 3683.87 18.06 o 6 2 1 131.44 108.70 10.84 o 8 2 1 586.10 577.69 18.87 o 10 2 1 192.63 201.65 18.02 o 12 2 1 84.97 52.06 17.38 o 14 2 1 25.86 6.76 25.98 o -15 3 1 1181.01 1329.77 70.10 o -13 3 1 415.95 426.16 30.40 o -11 3 1 69.14 73.74 21.66 o -9 3 1 1320.50 1191.44 22.32 o -7 3 1 2111.55 2239.82 24.02 o -5 3 1 1541.86 1309.12 15.34 o -3 3 1 2771.61 2916.53 24.04 o -1 3 1 27573.45 27725.32 285.46 o 1 3 1 5272.90 4954.47 27.81 o 3 3 1 531.07 567.57 10.18 o 5 3 1 14992.29 15811.52 127.61 o 7 3 1 886.45 763.79 17.22 o 9 3 1 377.73 336.96 19.02 o 11 3 1 1513.76 1534.46 31.44 o 13 3 1 164.72 167.37 19.99 o -14 4 1 23.34 26.37 24.47 o -12 4 1 416.51 417.58 28.68 o -10 4 1 1222.14 1129.11 35.29 o -8 4 1 242.57 234.88 13.29 o -6 4 1 20.77 35.27 7.63 o -4 4 1 2063.87 2072.26 20.58 o -2 4 1 1054.16 1076.96 11.74 o 0 4 1 2848.03 3236.71 37.79 o 2 4 1 2.58 11.92 8.08 o 4 4 1 11897.71 12165.10 38.02 o 6 4 1 27.09 18.41 5.14 o 8 4 1 5244.55 5256.30 39.91 o 10 4 1 568.01 582.04 22.13 o 12 4 1 470.45 436.41 22.72 o 14 4 1 11.02 25.84 27.38 o -13 5 1 164.35 173.58 26.03 o -11 5 1 4.53 0.12 18.40 o -9 5 1 166.50 154.92 16.19 o -7 5 1 419.12 364.20 11.43 o -5 5 1 873.74 1118.08 13.99 o -3 5 1 500.74 446.80 8.77 o -1 5 1 29308.53 27164.43 374.92 o 1 5 1 18369.57 18587.54 129.30 o 3 5 1 6232.52 5574.78 26.32 o 5 5 1 7040.35 7166.51 53.74 o 7 5 1 281.41 240.75 13.27 o 9 5 1 1813.53 1734.94 27.39 o 11 5 1 85.22 86.04 16.78 o 13 5 1 43.47 45.94 17.99 o -14 6 1 251.04 283.72 46.67 o -12 6 1 107.91 94.76 20.15 o -10 6 1 806.80 813.43 27.40 o -8 6 1 1539.52 1579.39 25.56 o -6 6 1 388.74 385.94 11.89 o -4 6 1 2589.90 2813.31 63.57 o -2 6 1 13521.77 13790.00 82.58 o 0 6 1 5685.21 6217.01 45.48 o 2 6 1 4865.12 4977.74 29.83 o 4 6 1 231.28 254.96 9.74 o 6 6 1 1419.12 1425.26 20.09 o 8 6 1 584.14 613.02 17.82 o 10 6 1 16.45 26.73 13.74 o 12 6 1 5.88 8.50 17.17 o 14 6 1 0.18 35.95 42.47 o -13 7 1 221.46 265.24 32.18 o -11 7 1 709.91 683.15 26.57 o -9 7 1 2192.11 2158.02 36.20 o -7 7 1 207.40 218.57 19.09 o -5 7 1 0.24 23.94 10.55 o -3 7 1 3175.40 2864.65 53.48 o -1 7 1 6646.68 6057.68 311.77 o 1 7 1 9657.50 10236.90 36.15 o 3 7 1 146.42 120.91 7.57 o 5 7 1 526.10 528.06 23.03 o 7 7 1 0.16 0.81 6.08 o 9 7 1 962.44 914.68 21.84 o 11 7 1 143.22 139.04 16.05 o 13 7 1 2.39 17.39 39.47 o -14 8 1 559.44 648.62 61.20 o -12 8 1 672.97 639.19 38.92 o -10 8 1 980.25 941.23 39.58 o -8 8 1 111.11 92.19 24.48 o -6 8 1 1216.49 1181.62 49.86 o -4 8 1 1720.84 1854.71 26.85 o -2 8 1 1336.30 1289.15 41.67 o 0 8 1 504.87 458.42 21.13 o 2 8 1 6738.46 7556.49 61.27 o 4 8 1 6888.62 6509.48 61.74 o 6 8 1 529.80 528.01 18.82 o 8 8 1 4311.43 4330.60 43.85 o 10 8 1 203.91 222.42 18.80 o 12 8 1 705.61 661.04 38.70 o -13 9 1 47.38 75.72 29.43 o -11 9 1 17.82 9.04 25.90 o -9 9 1 938.54 951.84 38.69 o -7 9 1 207.46 181.23 27.32 o -5 9 1 180.43 210.65 14.14 o -3 9 1 237.53 198.26 28.39 o -1 9 1 10504.50 10566.44 84.25 o 1 9 1 43.98 57.91 22.48 o 3 9 1 402.17 294.86 14.30 o 5 9 1 556.66 516.82 15.62 o 7 9 1 306.12 304.84 17.02 o 9 9 1 22.97 12.40 14.64 o 11 9 1 250.25 187.02 23.64 o 13 9 1 155.65 128.89 43.61 o -12 10 1 89.80 112.85 29.94 o -10 10 1 13.82 21.37 25.00 o -8 10 1 1027.87 972.74 38.03 o -6 10 1 2518.75 2328.42 35.09 o -4 10 1 127.79 150.04 14.14 o -2 10 1 4809.73 4749.78 75.44 o 0 10 1 633.71 560.86 30.69 o 2 10 1 5373.59 5328.00 74.11 o 4 10 1 43.69 44.97 10.09 o 6 10 1 19.07 18.10 12.26 o 8 10 1 17.07 31.60 14.37 o 10 10 1 307.77 310.76 24.40 o 12 10 1 72.56 49.62 28.71 o -13 11 1 33.17 47.89 29.68 o -11 11 1 45.69 52.28 26.53 o -9 11 1 3.00 25.81 25.68 o -7 11 1 20.28 10.93 31.52 o -5 11 1 53.97 27.72 13.28 o -3 11 1 1022.81 995.42 44.26 o -1 11 1 80.74 108.01 21.45 o 1 11 1 100.34 159.25 21.37 o 3 11 1 37.75 33.91 25.11 o 5 11 1 209.38 190.52 15.55 o 7 11 1 120.01 119.25 17.93 o 9 11 1 101.74 69.40 26.42 o 11 11 1 2.52 -6.72 27.48 o -12 12 1 17.31 19.55 27.75 o -10 12 1 30.19 22.02 26.74 o -8 12 1 2037.49 2067.11 52.06 o -6 12 1 55.89 47.31 30.44 o -4 12 1 159.12 130.11 32.01 o -2 12 1 261.49 278.79 35.52 o 0 12 1 474.63 480.20 27.94 o 2 12 1 14.28 19.83 25.18 o 4 12 1 256.52 249.74 30.78 o 6 12 1 0.58 -4.40 22.66 o 8 12 1 2.70 10.21 23.30 o 10 12 1 18.82 30.46 26.20 o 12 12 1 16.36 33.11 29.42 o -11 13 1 204.16 231.79 32.59 o -9 13 1 3.56 6.11 26.77 o -7 13 1 431.14 372.30 40.27 o -5 13 1 93.04 95.47 29.53 o -3 13 1 193.74 171.25 33.05 o -1 13 1 4596.24 4482.74 60.07 o 1 13 1 1111.42 1097.06 54.46 o 3 13 1 263.91 222.85 33.38 o 5 13 1 176.24 150.12 31.74 o 7 13 1 166.14 182.39 34.59 o 9 13 1 1.97 2.26 25.04 o 11 13 1 125.32 152.91 30.09 o -10 14 1 37.43 63.76 28.17 o -8 14 1 2036.88 2085.43 54.13 o -6 14 1 529.72 583.19 44.20 o -4 14 1 83.16 70.26 34.30 o -2 14 1 124.28 169.23 27.26 o 0 14 1 131.34 165.14 27.62 o 2 14 1 703.28 691.22 39.32 o 4 14 1 23.82 20.75 27.82 o 6 14 1 38.11 22.58 22.53 o 8 14 1 76.88 133.34 26.98 o 10 14 1 3.80 10.07 26.88 o -11 15 1 3.19 -7.27 29.76 o -9 15 1 5.94 -12.89 28.42 o -7 15 1 32.69 33.98 35.14 o -5 15 1 147.27 154.58 34.48 o -3 15 1 555.54 542.34 32.17 o -1 15 1 895.67 983.98 36.66 o 1 15 1 571.63 473.55 31.23 o 3 15 1 143.55 176.53 33.24 o 5 15 1 9.83 -1.02 28.03 o 7 15 1 78.07 79.38 25.86 o 9 15 1 12.40 -1.25 27.02 o -10 16 1 21.56 20.06 27.57 o -8 16 1 344.54 311.92 32.95 o -6 16 1 4.78 3.94 33.24 o -4 16 1 129.46 73.38 33.32 o -2 16 1 1.06 31.45 24.61 o 0 16 1 23.66 58.64 24.37 o 2 16 1 7.85 8.21 23.52 o 4 16 1 22.56 29.58 29.48 o 6 16 1 0.11 14.54 26.74 o 8 16 1 122.43 99.72 28.38 o 10 16 1 0.72 -7.30 28.24 o -9 17 1 9.38 -8.75 29.21 o -7 17 1 15.83 0.90 34.45 o -5 17 1 6.37 13.85 32.34 o -3 17 1 552.01 487.43 33.44 o -1 17 1 885.32 744.34 35.05 o 1 17 1 239.74 226.09 27.59 o 3 17 1 0.97 7.77 24.47 o 5 17 1 4.09 3.32 23.05 o 7 17 1 13.54 10.51 25.78 o 9 17 1 82.24 112.81 30.42 o -8 18 1 224.55 203.45 32.95 o -6 18 1 63.84 70.42 37.31 o -4 18 1 4.32 -4.40 26.46 o -2 18 1 0.26 -3.39 25.21 o 0 18 1 21.79 36.70 24.54 o 2 18 1 205.07 163.13 28.43 o 4 18 1 9.38 15.17 25.79 o 6 18 1 0.00 7.28 25.02 o 8 18 1 58.47 108.83 30.21 o -7 19 1 11.40 -10.88 28.03 o -5 19 1 8.72 21.74 26.51 o -3 19 1 20.95 3.54 26.25 o -1 19 1 103.70 92.07 26.22 o 1 19 1 0.54 12.54 25.75 o 3 19 1 43.85 32.53 26.68 o 5 19 1 0.17 8.66 21.34 o 7 19 1 21.06 38.51 27.00 o -6 20 1 1.70 16.40 28.38 o -4 20 1 40.10 23.68 27.76 o -2 20 1 72.34 108.37 39.61 o 0 20 1 9.24 9.44 25.61 o 2 20 1 130.56 134.31 28.69 o 4 20 1 14.40 10.71 21.26 o -3 21 1 45.77 42.58 28.75 o -1 21 1 99.68 113.55 38.30 o 1 21 1 46.25 51.88 26.98 o 3 21 1 9.16 -18.60 45.97 o -14 0 2 13.23 -7.83 32.65 o -12 0 2 3922.00 4012.24 87.01 o -10 0 2 1743.92 1557.12 80.59 o -8 0 2 96.98 87.01 23.65 o -6 0 2 1823.23 2112.39 32.77 o -4 0 2 9395.10 9913.55 54.82 o -2 0 2 448.74 366.09 9.56 o 2 0 2 54680.75 56337.46 286.55 o 4 0 2 3474.66 3275.17 28.52 o 6 0 2 40.81 25.43 9.58 o 8 0 2 176.38 132.85 13.17 o 10 0 2 485.70 358.25 28.89 o 12 0 2 63.42 103.10 25.67 o 14 0 2 5.44 -7.82 27.59 o -15 1 2 233.87 247.13 29.50 o -13 1 2 313.09 360.85 28.46 o -11 1 2 2903.23 2813.46 73.07 o -9 1 2 3599.73 3726.99 51.93 o -7 1 2 4642.99 5027.75 45.92 o -5 1 2 6027.60 6246.58 33.09 o -3 1 2 1936.77 1981.24 17.17 o 1 1 2 6428.81 6756.06 39.44 o 3 1 2 12320.83 12400.86 41.24 o 5 1 2 3500.60 4419.60 27.26 o 7 1 2 206.34 161.63 8.62 o 9 1 2 1831.51 1749.30 36.55 o 11 1 2 629.67 595.33 23.64 o 13 1 2 125.08 122.48 20.07 o -14 2 2 16.03 6.23 23.03 o -12 2 2 411.12 437.00 28.35 o -10 2 2 346.71 320.66 21.42 o -8 2 2 0.04 10.72 13.74 o -6 2 2 2568.98 2565.89 27.83 o -4 2 2 36.49 48.47 5.94 o -2 2 2 5130.06 5522.49 34.63 o 0 2 2 488.64 465.67 8.26 o 2 2 2 10.65 21.08 5.35 o 4 2 2 29.58 32.17 5.68 o 6 2 2 6354.73 6782.89 37.50 o 8 2 2 1381.89 1321.35 25.74 o 10 2 2 449.57 399.12 20.57 o 12 2 2 1.10 1.59 17.51 o 14 2 2 57.70 71.51 20.77 o -15 3 2 46.36 45.52 39.43 o -13 3 2 0.29 8.60 22.17 o -11 3 2 950.52 941.92 28.53 o -9 3 2 635.94 627.38 22.40 o -7 3 2 314.00 345.02 16.11 o -5 3 2 3573.68 3828.24 67.44 o -3 3 2 2370.86 2756.31 18.34 o -1 3 2 1128.21 1218.83 21.98 o 1 3 2 674.84 635.67 9.21 o 3 3 2 173.11 148.29 7.34 o 5 3 2 501.61 432.57 12.01 o 7 3 2 3203.42 3082.99 38.45 o 9 3 2 1730.53 1636.42 29.96 o 11 3 2 5.23 9.60 16.36 o 13 3 2 222.69 214.57 21.30 o -14 4 2 137.07 152.42 41.19 o -12 4 2 386.86 386.93 23.13 o -10 4 2 2097.86 2140.26 36.86 o -8 4 2 667.71 643.91 20.09 o -6 4 2 9.21 3.53 8.51 o -4 4 2 4920.47 5053.30 34.87 o -2 4 2 6271.03 6123.36 44.30 o 0 4 2 6857.00 7132.12 42.46 o 2 4 2 15200.83 15551.62 44.56 o 4 4 2 59.74 73.14 8.55 o 6 4 2 385.95 452.95 10.56 o 8 4 2 213.71 204.28 16.81 o 10 4 2 22.68 9.11 15.78 o 12 4 2 245.41 273.41 21.62 o 14 4 2 0.56 3.94 19.90 o -15 5 2 196.43 213.11 47.69 o -13 5 2 213.16 224.75 26.73 o -11 5 2 2397.62 2240.92 39.12 o -9 5 2 2740.34 2778.60 37.80 o -7 5 2 323.86 346.57 13.25 o -5 5 2 807.28 728.11 29.81 o -3 5 2 16463.73 17071.31 42.22 o -1 5 2 5757.09 6675.42 69.13 o 1 5 2 25051.44 24713.67 60.15 o 3 5 2 118.55 82.22 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