#------------------------------------------------------------------------------ #$Date: 2011-07-04 21:24:21 +0300 (Mon, 04 Jul 2011) $ #$Revision: 22560 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2230205.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230205_Fobs loop_ _publ_author_name 'Cao, Man-Li' 'Shi, Lei' _publ_section_title ; [2-Amino-4,6-bis(2-pyridyl)-1,3,5-triazine-\k^3^N^4^,N^5^,N^6^]dichloridocadmium(II) ; _journal_coeditor_code ZQ2094 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m638 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 82.515 _cell_angle_beta 65.636 _cell_angle_gamma 82.798 _cell_length_a 8.8750 _cell_length_b 9.2010 _cell_length_c 10.2677 _exptl_crystal_F_000 424.00 _reflns_d_resolution_high 0.8411 _[local]_cod_data_source_file zq2094Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 209.47 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3537.45 3463.50 70.10 o 2 0 0 7590.90 7236.13 93.04 o 3 0 0 2601.44 2671.82 35.03 o 4 0 0 1622.16 1677.33 22.98 o 5 0 0 2666.57 2681.58 44.92 o 6 0 0 1661.37 1680.81 30.42 o 7 0 0 760.10 707.78 22.83 o 8 0 0 72.28 70.13 6.47 o 9 0 0 225.41 230.20 12.32 o -9 1 0 469.25 474.29 13.58 o -8 1 0 37.30 58.18 13.31 o -7 1 0 277.09 267.65 8.45 o -6 1 0 1503.55 1549.23 28.48 o -5 1 0 417.33 436.40 12.65 o -4 1 0 8019.16 8109.80 103.61 o -3 1 0 60.85 56.41 2.07 o -2 1 0 3476.90 3599.61 46.33 o -1 1 0 50.02 61.13 2.36 o 1 1 0 4941.35 4966.14 110.40 o 2 1 0 356.08 386.78 5.93 o 3 1 0 4079.77 4193.85 79.66 o 4 1 0 2293.71 2442.85 32.60 o 5 1 0 577.96 507.36 11.22 o 6 1 0 249.13 216.19 6.83 o 7 1 0 716.23 733.87 18.56 o 8 1 0 343.91 328.67 19.68 o 9 1 0 1.16 3.55 2.36 o -9 2 0 8.11 12.15 2.49 o -8 2 0 335.90 331.40 10.37 o -7 2 0 74.37 74.94 4.31 o -6 2 0 512.98 506.74 12.14 o -5 2 0 895.17 919.92 16.05 o -4 2 0 1874.74 1902.67 26.23 o -3 2 0 2820.62 2975.80 39.22 o -2 2 0 741.35 750.24 10.85 o -1 2 0 4481.53 4692.67 73.75 o 0 2 0 7749.77 7279.82 163.97 o 1 2 0 8411.08 8097.22 106.99 o 2 2 0 374.19 375.49 7.37 o 3 2 0 2595.66 2632.48 42.59 o 4 2 0 3052.49 3221.72 42.49 o 5 2 0 196.22 203.03 4.45 o 6 2 0 3246.90 3311.89 55.41 o 7 2 0 53.36 50.95 3.64 o 8 2 0 441.60 431.17 11.95 o 9 2 0 99.66 94.82 5.41 o -8 3 0 250.41 261.39 9.18 o -7 3 0 24.31 23.94 4.11 o -6 3 0 253.75 265.36 15.52 o -5 3 0 810.47 876.73 14.07 o -4 3 0 117.01 135.84 6.05 o -3 3 0 4565.69 4768.25 61.96 o -2 3 0 9.69 6.47 0.92 o -1 3 0 203.50 184.37 3.58 o 0 3 0 1929.84 1980.39 26.20 o 1 3 0 490.46 480.27 7.37 o 2 3 0 8813.88 8917.00 137.95 o 3 3 0 285.44 271.90 6.42 o 4 3 0 1198.92 1236.09 22.13 o 5 3 0 581.29 589.86 12.42 o 6 3 0 822.08 830.61 17.21 o 7 3 0 474.03 482.57 12.25 o 8 3 0 396.55 388.75 11.22 o 9 3 0 88.72 92.27 5.67 o -8 4 0 91.64 101.02 7.98 o -7 4 0 437.69 441.04 13.86 o -6 4 0 386.29 395.01 10.51 o -5 4 0 540.36 559.52 11.66 o -4 4 0 62.41 59.17 2.45 o -3 4 0 2245.95 2337.04 31.91 o -2 4 0 2694.97 2890.71 38.48 o -1 4 0 1515.23 1592.95 35.28 o 0 4 0 3648.98 3903.08 50.68 o 1 4 0 221.86 245.04 4.64 o 2 4 0 5754.00 5893.25 92.23 o 3 4 0 238.42 243.12 6.11 o 4 4 0 661.09 639.77 14.54 o 5 4 0 408.78 416.90 7.88 o 6 4 0 27.48 28.35 4.01 o 7 4 0 186.42 175.68 6.64 o 8 4 0 47.20 44.60 3.74 o 9 4 0 61.09 72.11 4.86 o -8 5 0 5.54 2.87 2.73 o -7 5 0 746.83 752.59 25.58 o -6 5 0 48.91 44.72 5.18 o -5 5 0 563.36 548.11 30.65 o -4 5 0 974.67 974.49 44.91 o -3 5 0 13.69 20.54 5.95 o -2 5 0 3186.21 3293.50 45.25 o -1 5 0 272.96 270.20 8.75 o 0 5 0 2116.03 2146.55 29.10 o 1 5 0 218.00 226.46 4.63 o 2 5 0 151.51 133.44 3.99 o 3 5 0 1688.44 1706.00 31.33 o 4 5 0 73.52 66.10 5.21 o 5 5 0 1.39 0.72 0.96 o 6 5 0 27.73 30.10 2.76 o 7 5 0 73.80 74.97 4.39 o 8 5 0 211.94 221.24 8.14 o -7 6 0 98.59 92.80 7.84 o -6 6 0 1240.24 1247.89 36.60 o -5 6 0 113.21 120.66 5.46 o -4 6 0 864.21 886.01 18.75 o -3 6 0 139.90 134.49 5.31 o -2 6 0 2915.09 2956.95 50.24 o -1 6 0 1374.81 1402.77 25.89 o 0 6 0 1631.85 1632.70 29.44 o 1 6 0 748.64 806.40 12.64 o 2 6 0 51.92 64.11 2.77 o 3 6 0 1706.28 1711.16 29.63 o 4 6 0 99.01 85.51 5.16 o 5 6 0 674.59 642.72 14.15 o 6 6 0 173.64 175.02 7.44 o 7 6 0 180.04 161.50 6.48 o 8 6 0 381.55 365.54 11.13 o -6 7 0 841.54 918.20 30.79 o -5 7 0 328.15 337.37 10.42 o -4 7 0 590.51 561.03 13.89 o -3 7 0 574.07 573.34 14.08 o -2 7 0 31.80 30.55 2.99 o -1 7 0 1311.26 1344.23 25.80 o 0 7 0 4.42 3.91 1.40 o 1 7 0 2129.41 2176.27 53.47 o 2 7 0 880.91 873.31 25.12 o 3 7 0 159.52 168.20 8.50 o 4 7 0 922.08 886.98 19.44 o 5 7 0 176.34 175.93 6.21 o 6 7 0 318.63 336.95 9.75 o 7 7 0 2.90 5.31 2.12 o -5 8 0 920.06 953.53 21.67 o -4 8 0 126.24 115.33 5.83 o -3 8 0 2007.05 1991.28 37.27 o -2 8 0 2444.60 2418.43 43.45 o -1 8 0 333.18 316.85 13.80 o 0 8 0 1835.93 1862.37 47.73 o 1 8 0 657.39 715.88 22.39 o 2 8 0 858.19 900.64 26.70 o 3 8 0 18.08 23.90 3.71 o 4 8 0 1224.83 1124.68 32.26 o 5 8 0 194.43 205.29 10.67 o 6 8 0 265.19 268.91 12.81 o 7 8 0 39.18 39.02 5.18 o -4 9 0 158.07 182.38 10.51 o -3 9 0 461.69 444.12 15.24 o -2 9 0 908.90 893.25 20.21 o -1 9 0 23.71 19.94 3.67 o 0 9 0 839.37 807.31 25.26 o 1 9 0 291.89 260.79 12.07 o 2 9 0 152.01 195.32 10.25 o 3 9 0 29.41 43.46 5.14 o 4 9 0 82.41 62.56 6.12 o 5 9 0 331.45 331.86 14.77 o -3 10 0 58.75 69.00 6.96 o -2 10 0 166.07 181.46 10.57 o -1 10 0 154.56 137.62 9.03 o 0 10 0 150.32 138.84 8.99 o 1 10 0 506.14 474.97 18.48 o 2 10 0 59.70 68.76 6.40 o 3 10 0 294.02 298.93 14.10 o 4 10 0 58.71 58.12 6.19 o -3 -10 1 75.24 71.91 7.00 o -2 -10 1 128.00 134.09 9.06 o -1 -10 1 24.12 35.03 5.07 o 0 -10 1 400.06 379.37 16.34 o 1 -10 1 112.94 112.19 8.38 o 2 -10 1 99.26 84.41 5.38 o 3 -10 1 244.26 266.66 9.92 o -5 -9 1 6.84 9.69 3.18 o -4 -9 1 323.33 316.25 14.38 o -3 -9 1 35.33 34.54 4.83 o -2 -9 1 333.84 316.98 14.03 o -1 -9 1 475.84 483.12 18.09 o 0 -9 1 70.74 71.17 4.62 o 1 -9 1 1319.13 1280.19 26.59 o 2 -9 1 2.16 3.08 1.58 o 3 -9 1 405.74 369.13 11.50 o 4 -9 1 151.63 155.25 7.09 o -6 -8 1 139.13 146.72 9.59 o -5 -8 1 326.47 309.22 14.10 o -4 -8 1 551.43 490.50 18.37 o -3 -8 1 1096.91 1021.14 30.23 o -2 -8 1 132.00 120.26 7.63 o -1 -8 1 1199.98 1150.95 23.58 o 0 -8 1 316.90 299.82 9.28 o 1 -8 1 1458.53 1434.74 28.20 o 2 -8 1 17.03 19.03 2.72 o 3 -8 1 349.52 327.97 10.14 o 4 -8 1 93.56 98.36 6.35 o 5 -8 1 31.66 31.95 3.51 o 6 -8 1 442.87 491.52 20.57 o -7 -7 1 164.46 165.64 11.32 o -6 -7 1 108.07 111.03 10.83 o -5 -7 1 559.61 590.96 20.64 o -4 -7 1 24.16 29.95 4.20 o -3 -7 1 1665.97 1707.60 44.58 o -2 -7 1 286.57 268.31 11.37 o -1 -7 1 967.44 984.77 20.23 o 0 -7 1 968.65 976.33 20.01 o 1 -7 1 54.90 50.05 3.43 o 2 -7 1 1121.87 1119.75 29.83 o 3 -7 1 0.49 2.27 1.32 o 4 -7 1 787.48 796.13 18.11 o 5 -7 1 219.34 213.84 7.92 o 6 -7 1 390.07 430.43 18.30 o 7 -7 1 615.68 680.89 26.07 o -7 -6 1 236.32 231.52 8.28 o -6 -6 1 38.47 44.13 3.53 o -5 -6 1 104.16 95.61 5.55 o -4 -6 1 900.41 883.29 17.71 o -3 -6 1 339.20 333.51 10.27 o -2 -6 1 3630.92 3698.22 49.44 o -1 -6 1 2.78 1.65 1.05 o 0 -6 1 2218.47 2288.17 39.74 o 1 -6 1 1944.90 2020.13 51.00 o 2 -6 1 3049.28 3061.17 151.48 o 3 -6 1 1544.42 1611.12 29.92 o 4 -6 1 836.79 845.50 18.06 o 5 -6 1 954.70 1000.63 21.15 o 7 -6 1 1202.27 1252.65 37.65 o -8 -5 1 103.72 105.80 7.63 o -7 -5 1 925.16 932.70 23.01 o -6 -5 1 1485.07 1491.45 28.40 o -5 -5 1 3.27 5.36 1.45 o -4 -5 1 1366.19 1295.96 98.46 o -3 -5 1 444.48 416.72 16.41 o -2 -5 1 3298.86 3355.54 44.72 o -1 -5 1 1278.21 1216.06 17.54 o 0 -5 1 1417.84 1541.49 21.53 o 1 -5 1 3718.49 3753.84 61.59 o 2 -5 1 108.94 131.24 16.94 o 3 -5 1 5761.66 5352.02 336.46 o 4 -5 1 146.34 150.06 5.57 o 5 -5 1 958.97 979.81 19.99 o 6 -5 1 573.80 597.33 20.68 o 7 -5 1 120.66 120.30 8.47 o 8 -5 1 473.44 486.31 19.84 o -8 -4 1 12.36 15.39 2.59 o -7 -4 1 63.89 64.28 4.24 o -6 -4 1 1534.23 1546.40 29.13 o -5 -4 1 107.35 110.75 5.48 o -4 -4 1 206.64 197.67 5.97 o -3 -4 1 3061.75 3148.52 51.37 o -2 -4 1 1832.83 2164.81 29.43 o -1 -4 1 2667.09 2540.65 33.85 o 0 -4 1 5.94 11.36 1.93 o 1 -4 1 2311.36 2328.62 38.93 o 2 -4 1 2691.76 2671.39 35.49 o 3 -4 1 230.87 191.83 4.56 o 4 -4 1 659.16 585.90 9.94 o 5 -4 1 410.38 407.53 9.53 o 6 -4 1 699.69 696.90 15.09 o 7 -4 1 117.18 125.09 8.26 o 8 -4 1 375.91 400.05 16.97 o -9 -3 1 7.48 6.31 1.91 o -8 -3 1 52.76 54.46 4.15 o -7 -3 1 564.59 572.70 14.14 o -6 -3 1 83.51 82.99 7.09 o -5 -3 1 909.73 860.45 17.32 o -4 -3 1 36.23 32.59 2.40 o -3 -3 1 2587.97 2688.40 63.77 o -2 -3 1 3100.70 3225.54 42.34 o -1 -3 1 2059.45 2029.29 27.10 o 0 -3 1 529.55 484.51 7.32 o 1 -3 1 532.12 531.16 15.15 o 2 -3 1 1484.58 1501.17 20.48 o 3 -3 1 3357.08 3737.73 48.94 o 4 -3 1 2230.92 2193.42 30.03 o 5 -3 1 107.46 100.24 3.82 o 6 -3 1 436.07 436.97 10.71 o 7 -3 1 411.28 391.98 10.60 o 8 -3 1 332.25 328.65 13.37 o 9 -3 1 1850.75 1819.73 35.44 o -9 -2 1 96.08 97.55 9.38 o -8 -2 1 64.68 69.49 4.45 o -7 -2 1 318.93 309.77 24.44 o -6 -2 1 54.23 51.21 6.12 o -5 -2 1 2368.28 2457.49 42.00 o -4 -2 1 10.29 13.58 0.99 o -3 -2 1 1031.47 1082.47 19.37 o -2 -2 1 453.08 447.39 12.34 o -1 -2 1 346.93 350.61 5.67 o 0 -2 1 5375.39 5265.26 67.53 o 1 -2 1 696.28 743.90 13.23 o 2 -2 1 2366.12 2415.58 41.45 o 3 -2 1 671.47 656.41 9.97 o 4 -2 1 1982.83 2149.50 29.22 o 5 -2 1 2359.21 2372.57 39.56 o 6 -2 1 233.07 230.11 7.23 o 7 -2 1 161.05 158.51 6.06 o 8 -2 1 56.78 55.14 3.97 o 9 -2 1 284.65 290.09 9.93 o -9 -1 1 633.89 624.09 16.43 o -8 -1 1 1.23 4.07 1.65 o -7 -1 1 356.63 353.12 10.23 o -6 -1 1 211.54 197.64 6.75 o -5 -1 1 1135.08 1140.49 21.69 o -4 -1 1 3890.02 4009.79 64.81 o -3 -1 1 1576.23 1592.61 21.68 o -2 -1 1 3644.82 3563.96 56.50 o -1 -1 1 1509.53 1533.96 24.83 o 0 -1 1 2124.41 2126.62 48.18 o 1 -1 1 3821.45 3825.75 85.69 o 2 -1 1 4434.43 4588.31 58.61 o 3 -1 1 217.25 193.06 3.82 o 4 -1 1 17.63 17.66 1.16 o 5 -1 1 2807.23 2884.54 38.66 o 6 -1 1 90.59 101.14 4.33 o 7 -1 1 341.26 333.25 9.35 o 8 -1 1 173.93 172.99 6.80 o 9 -1 1 34.35 35.72 3.54 o -9 0 1 275.70 283.55 10.18 o -8 0 1 284.42 290.32 9.70 o -7 0 1 202.82 193.21 7.18 o -6 0 1 981.65 973.78 21.06 o -5 0 1 238.30 218.99 6.70 o -4 0 1 7113.76 6936.09 109.34 o -3 0 1 740.07 742.92 14.04 o -2 0 1 668.41 664.52 13.31 o 0 0 1 13.69 -0.59 1.01 o 1 0 1 5846.90 5554.51 87.98 o 2 0 1 5536.41 5801.15 73.72 o 3 0 1 2514.64 2516.81 32.96 o 4 0 1 374.76 364.68 6.28 o 5 0 1 1943.80 2005.68 27.52 o 6 0 1 1514.29 1510.21 27.31 o 7 0 1 514.39 501.33 12.22 o 8 0 1 289.36 271.84 8.71 o 9 0 1 11.27 14.66 2.57 o -9 1 1 1.87 4.13 1.86 o -8 1 1 861.10 836.68 19.42 o -7 1 1 72.32 72.64 4.39 o -6 1 1 842.88 842.01 17.86 o -5 1 1 1893.61 1896.79 33.49 o -4 1 1 180.39 200.71 13.07 o -3 1 1 10384.48 10066.20 127.90 o -2 1 1 197.06 200.57 4.33 o 1 1 1 3384.32 3423.46 77.44 o 2 1 1 5809.36 5753.81 89.69 o 3 1 1 8551.46 8411.54 106.68 o 4 1 1 1974.04 1999.88 26.96 o 5 1 1 4.09 7.27 0.88 o 6 1 1 2899.06 2899.97 48.68 o 7 1 1 304.21 306.52 8.77 o 8 1 1 886.63 890.02 19.32 o 9 1 1 234.94 218.94 8.20 o -8 2 1 56.80 49.95 4.20 o -7 2 1 801.27 822.98 18.56 o -6 2 1 117.14 116.82 5.20 o -5 2 1 1577.91 1578.04 28.70 o -4 2 1 2478.73 2590.33 35.00 o -3 2 1 5353.45 5490.37 70.86 o -2 2 1 2333.70 2299.61 30.51 o -1 2 1 3440.98 3512.74 45.36 o 0 2 1 4324.18 4278.24 66.53 o 1 2 1 279.54 261.01 5.07 o 2 2 1 15710.05 14299.70 255.45 o 3 2 1 65.01 68.22 2.02 o 4 2 1 4252.73 4295.46 55.79 o 5 2 1 1961.07 2068.88 28.38 o 6 2 1 335.21 295.08 15.96 o 7 2 1 1443.56 1480.03 35.85 o 8 2 1 332.28 321.27 9.73 o 9 2 1 407.32 396.11 11.66 o -8 3 1 161.57 156.97 7.12 o -7 3 1 820.97 827.05 18.73 o -6 3 1 191.78 197.43 7.06 o -5 3 1 945.47 931.46 31.25 o -4 3 1 2456.49 2490.68 34.09 o -3 3 1 80.80 114.69 13.08 o -2 3 1 7506.86 7463.34 95.41 o -1 3 1 154.90 148.41 3.23 o 0 3 1 3001.49 2921.06 46.06 o 1 3 1 8683.75 8575.38 133.05 o 2 3 1 1871.31 1940.16 31.40 o 3 3 1 9462.52 9282.87 143.75 o 4 3 1 945.34 927.65 13.82 o 5 3 1 1535.47 1559.85 36.39 o 6 3 1 168.19 176.21 5.88 o 7 3 1 1442.04 1481.00 27.84 o 8 3 1 228.19 220.65 7.83 o 9 3 1 255.78 262.58 9.16 o -8 4 1 210.07 216.95 9.13 o -7 4 1 46.45 41.19 3.74 o -6 4 1 979.49 988.35 20.77 o -5 4 1 2.81 8.12 3.62 o -4 4 1 3.70 4.92 1.57 o -3 4 1 1274.59 1263.88 18.59 o -2 4 1 1231.46 1246.65 18.02 o -1 4 1 4661.24 4727.55 61.25 o 0 4 1 265.74 237.53 5.28 o 1 4 1 615.11 648.31 65.33 o 2 4 1 87.59 141.56 3.87 o 3 4 1 3596.19 3536.07 56.49 o 4 4 1 518.88 499.23 10.52 o 5 4 1 863.00 846.84 13.39 o 6 4 1 173.57 174.65 5.91 o 7 4 1 5.41 5.54 1.58 o 8 4 1 381.11 396.89 12.02 o 9 4 1 0.07 0.95 2.15 o -7 5 1 67.92 71.14 6.65 o -6 5 1 632.48 634.77 22.08 o -5 5 1 472.83 474.75 15.20 o -4 5 1 101.68 94.27 3.38 o -3 5 1 583.86 613.16 10.62 o -2 5 1 1.90 2.59 1.01 o -1 5 1 3985.20 3987.92 52.48 o 0 5 1 339.64 372.74 7.75 o 1 5 1 11.71 43.64 2.01 o 2 5 1 347.93 314.18 7.04 o 3 5 1 226.36 218.37 5.72 o 4 5 1 2132.53 2070.44 35.02 o 5 5 1 795.38 747.35 21.29 o 6 5 1 1988.47 1993.54 35.27 o 7 5 1 1352.74 1371.22 26.48 o 8 5 1 239.59 254.13 8.58 o 9 5 1 175.99 202.91 11.69 o -7 6 1 180.74 195.57 11.69 o -6 6 1 48.82 51.51 6.05 o -5 6 1 615.91 641.67 21.94 o -4 6 1 230.50 229.44 7.47 o -3 6 1 733.91 737.15 15.92 o -2 6 1 290.64 280.74 7.89 o -1 6 1 1839.76 1757.78 90.14 o 0 6 1 1126.42 1205.33 21.12 o 1 6 1 1116.52 1191.67 20.92 o 2 6 1 1049.12 1130.91 23.86 o 3 6 1 20.36 16.42 1.65 o 4 6 1 669.48 635.20 13.21 o 5 6 1 13.10 18.39 2.04 o 6 6 1 1393.59 1407.73 26.50 o 7 6 1 202.93 200.54 7.09 o 8 6 1 3.91 2.66 2.06 o -6 7 1 51.22 56.30 6.44 o -4 7 1 157.14 173.56 9.90 o -3 7 1 1045.72 1045.05 21.36 o -2 7 1 68.43 67.50 5.28 o -1 7 1 76.29 80.20 5.28 o 0 7 1 1519.97 1506.82 38.42 o 1 7 1 5.59 9.90 2.27 o 2 7 1 839.95 875.72 24.53 o 3 7 1 227.19 241.39 6.68 o 4 7 1 12.50 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427.72 420.73 12.08 o 4 6 9 8.58 11.87 2.41 o 5 6 9 292.12 278.25 9.49 o 6 6 9 5.56 6.30 1.78 o 7 6 9 276.26 256.15 9.34 o 8 6 9 181.11 184.81 7.91 o 0 7 9 172.97 171.60 10.78 o 1 7 9 210.54 208.79 8.45 o 2 7 9 26.45 26.86 3.23 o 3 7 9 1214.37 1245.47 26.41 o 4 7 9 233.27 239.11 10.53 o 5 7 9 280.65 275.80 9.61 o 6 7 9 57.52 68.49 4.74 o 7 7 9 0.05 1.51 1.38 o 2 8 9 198.30 222.95 8.71 o 3 8 9 3.66 9.90 2.48 o 4 8 9 460.58 503.02 14.31 o 5 8 9 0.03 1.88 1.50 o 3 -5 10 879.03 892.21 20.97 o 1 -4 10 370.54 374.93 15.92 o 2 -4 10 92.91 91.87 5.19 o 3 -4 10 369.00 375.52 16.94 o 4 -4 10 55.91 55.53 6.68 o 5 -4 10 134.12 130.03 9.87 o 6 -4 10 383.58 424.55 19.66 o 0 -3 10 17.16 15.36 3.60 o 1 -3 10 49.57 57.84 5.46 o 2 -3 10 255.70 247.81 12.53 o 3 -3 10 4.09 6.37 2.73 o 4 -3 10 120.24 131.36 9.31 o 5 -3 10 12.87 17.85 4.37 o 6 -3 10 163.64 163.55 11.02 o 7 -3 10 139.61 135.00 10.08 o -1 -2 10 50.68 55.69 4.17 o 0 -2 10 48.40 50.88 3.85 o 2 -2 10 134.27 132.76 8.68 o 3 -2 10 65.32 59.31 6.23 o 4 -2 10 606.68 655.31 24.00 o 5 -2 10 246.82 235.49 13.12 o 6 -2 10 256.10 284.97 14.94 o 7 -2 10 192.69 201.51 12.49 o 8 -2 10 0.16 -2.03 2.03 o -1 -1 10 40.29 37.69 5.25 o 0 -1 10 747.81 762.25 25.23 o 1 -1 10 11.34 17.60 3.60 o 2 -1 10 259.70 273.55 8.94 o 3 -1 10 172.70 165.68 6.73 o 4 -1 10 641.62 684.09 16.31 o 5 -1 10 414.51 392.53 17.29 o 6 -1 10 244.26 263.17 13.96 o 7 -1 10 121.23 133.91 9.87 o 8 -1 10 23.02 21.59 4.76 o -1 0 10 48.34 54.69 6.44 o 0 0 10 641.75 612.83 22.18 o 1 0 10 692.32 692.16 23.62 o 2 0 10 216.81 232.43 8.21 o 3 0 10 250.34 262.87 8.80 o 4 0 10 34.86 30.69 3.20 o 5 0 10 264.65 277.08 9.11 o 6 0 10 22.45 23.31 2.94 o 7 0 10 917.32 941.27 27.49 o 8 0 10 153.69 140.74 6.56 o -1 1 10 223.42 221.91 12.35 o 0 1 10 0.69 0.24 1.82 o 1 1 10 1441.29 1451.81 41.22 o 2 1 10 1.78 4.99 4.23 o 3 1 10 613.42 612.26 15.20 o 4 1 10 506.16 517.11 13.58 o 5 1 10 31.57 37.61 3.48 o 6 1 10 345.82 349.89 10.80 o 7 1 10 387.66 395.82 11.80 o 8 1 10 636.48 615.14 19.16 o 9 1 10 22.73 24.14 3.14 o -1 2 10 136.09 140.45 9.69 o 0 2 10 241.44 244.38 12.88 o 1 2 10 182.07 184.82 10.78 o 2 2 10 601.77 580.27 14.77 o 3 2 10 186.57 194.86 9.90 o 4 2 10 944.96 966.29 21.15 o 5 2 10 322.88 321.63 10.16 o 6 2 10 1438.85 1469.66 29.58 o 7 2 10 399.40 372.93 11.47 o 8 2 10 460.47 444.95 13.06 o 9 2 10 166.50 167.53 15.92 o -1 3 10 8.85 13.16 3.71 o 0 3 10 255.36 273.95 14.00 o 1 3 10 319.25 318.87 15.01 o 2 3 10 801.99 829.08 19.11 o 3 3 10 97.98 99.99 5.41 o 4 3 10 610.15 636.72 16.60 o 5 3 10 384.79 372.84 11.23 o 6 3 10 35.33 42.70 4.01 o 7 3 10 635.98 677.77 17.09 o 8 3 10 1.02 0.91 1.40 o -1 4 10 22.19 24.98 4.79 o 0 4 10 73.93 75.86 7.03 o 1 4 10 210.20 209.70 11.86 o 2 4 10 32.00 37.63 3.56 o 3 4 10 615.04 584.37 14.97 o 4 4 10 55.90 55.65 4.15 o 5 4 10 185.13 186.53 7.56 o 6 4 10 255.18 252.67 9.11 o 7 4 10 289.70 305.17 11.04 o 8 4 10 247.38 251.79 9.52 o 0 5 10 16.66 20.82 4.37 o 1 5 10 26.88 31.98 5.00 o 2 5 10 15.52 18.92 2.80 o 3 5 10 414.27 409.23 12.06 o 4 5 10 23.76 20.46 2.86 o 5 5 10 74.31 78.91 4.88 o 6 5 10 48.97 52.35 4.25 o 7 5 10 25.99 22.53 3.11 o 8 5 10 344.97 345.23 11.57 o 1 6 10 95.14 85.06 7.52 o 2 6 10 48.23 54.98 4.35 o 3 6 10 10.10 9.63 2.18 o 4 6 10 473.91 480.20 13.61 o 5 6 10 11.44 11.28 2.41 o 6 6 10 141.76 154.35 7.20 o 7 6 10 73.09 73.21 5.07 o 3 7 10 56.35 56.54 4.55 o 4 7 10 434.92 442.89 13.27 o 5 7 10 17.56 22.84 3.13 o 3 -3 11 184.11 178.21 11.02 o 4 -3 11 299.67 291.20 15.05 o 5 -3 11 902.37 891.61 31.07 o 2 -2 11 3.69 4.62 2.76 o 3 -2 11 147.21 141.19 9.62 o 4 -2 11 272.80 238.81 13.23 o 5 -2 11 563.90 544.53 22.29 o 6 -2 11 150.45 137.37 10.32 o 1 -1 11 208.45 215.79 11.65 o 2 -1 11 9.84 11.18 2.36 o 3 -1 11 160.59 172.86 7.28 o 4 -1 11 98.69 95.18 8.12 o 5 -1 11 210.66 226.67 12.98 o 6 -1 11 364.31 373.63 17.81 o 7 -1 11 2.59 7.31 3.22 o 0 0 11 19.88 23.30 4.83 o 1 0 11 153.82 169.57 10.43 o 2 0 11 46.18 48.69 4.44 o 3 0 11 172.01 185.17 7.56 o 4 0 11 1.31 3.04 1.75 o 5 0 11 4.32 5.41 1.86 o 6 0 11 525.11 545.63 14.74 o 7 0 11 116.69 109.70 9.13 o 0 1 11 90.45 101.79 8.29 o 1 1 11 5.46 11.06 3.39 o 2 1 11 551.91 584.41 15.29 o 3 1 11 26.39 24.44 3.14 o 4 1 11 660.72 677.81 16.93 o 5 1 11 376.98 384.52 11.71 o 6 1 11 71.48 74.25 5.34 o 7 1 11 628.74 668.46 17.13 o 8 1 11 49.33 55.56 4.55 o 0 2 11 240.73 235.87 13.16 o 1 2 11 47.04 51.68 6.23 o 2 2 11 306.38 312.64 10.40 o 3 2 11 265.14 259.14 9.47 o 4 2 11 470.24 496.72 13.78 o 5 2 11 440.30 438.20 12.78 o 6 2 11 15.26 23.56 3.17 o 7 2 11 583.64 586.63 15.84 o 8 2 11 41.93 54.28 4.55 o 1 3 11 168.72 173.87 11.09 o 2 3 11 20.78 19.29 3.45 o 3 3 11 935.71 953.54 21.72 o 4 3 11 51.51 60.66 5.98 o 5 3 11 329.77 351.69 15.64 o 6 3 11 55.68 60.19 4.59 o 7 3 11 51.85 53.96 4.44 o 1 4 11 220.39 205.47 12.28 o 2 4 11 308.86 315.66 12.33 o 3 4 11 98.53 106.81 6.75 o 4 4 11 617.18 605.99 16.02 o 5 4 11 107.36 106.78 8.78 o 6 4 11 396.18 406.82 20.94 o 7 4 11 143.12 146.43 7.21 o 2 5 11 338.04 339.34 16.24 o 3 5 11 58.28 57.80 4.49 o 4 5 11 371.16 379.50 14.15 o 5 5 11 74.29 77.70 5.08 o 6 5 11 411.57 406.24 12.75 o 3 0 12 98.21 112.35 6.15 o 4 0 12 12.90 18.63 3.02 o 5 0 12 110.56 125.95 6.48 o 3 1 12 328.71 334.61 11.22 o 4 1 12 129.40 126.85 6.56 o 5 1 12 5.44 10.76 7.05 o 3 2 12 130.58 138.83 9.50 o 4 2 12 414.36 428.22 13.13 o 5 2 12 0.73 2.55 1.64 o 6 2 12 38.20 37.32 4.00 o 4 3 12 596.54 604.63 16.48 o 5 3 12 19.33 22.48 3.30 o