#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:21:56 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181224 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/02/2230216.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230216_Fobs loop_ _publ_author_name 'Cao, Man-Li' _publ_section_title ; catena-Poly[[[4,6-bis(2-pyridyl)-1,3,5-triazin-2-olato]copper(II)]-\m-chlorido] ; _journal_coeditor_code AA2005 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m739 _journal_volume 67 _journal_year 2011 _space_group_IT_number 11 _symmetry_space_group_name_Hall '-P 2yb' _symmetry_space_group_name_H-M 'P 1 21/m 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.851 _cell_angle_gamma 90.000 _cell_length_a 3.7687 _cell_length_b 13.6985 _cell_length_c 11.8523 _exptl_crystal_F_000 350.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file aa2005Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P2(1)/m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 223.39 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' '-x, -y, -z' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 7756.41 8653.74 245.08 o 2 0 0 1442.64 1611.12 55.08 o 3 0 0 683.88 667.46 32.42 o 4 0 0 265.23 249.19 23.45 o 1 1 0 2.78 2.96 1.83 o 2 1 0 883.09 925.33 19.72 o 3 1 0 589.26 616.06 25.40 o 4 1 0 32.95 32.78 8.51 o 1 2 0 1857.89 2214.76 38.59 o 2 2 0 764.34 780.18 21.52 o 3 2 0 145.39 157.63 11.13 o 4 2 0 1.89 9.76 7.57 o 1 3 0 479.25 469.06 9.16 o 2 3 0 470.53 456.82 12.27 o 3 3 0 444.54 415.70 37.91 o 4 3 0 16.25 17.31 7.75 o 0 4 0 5569.08 5777.09 95.11 o 1 4 0 69.74 81.42 3.49 o 2 4 0 415.31 393.46 11.37 o 3 4 0 943.03 895.45 28.29 o 4 4 0 70.26 50.97 14.15 o 1 5 0 2372.53 2526.72 38.47 o 2 5 0 312.45 306.10 13.57 o 3 5 0 160.78 159.88 11.75 o 4 5 0 2.13 -3.50 9.13 o 0 6 0 7662.31 8216.81 135.35 o 1 6 0 1108.15 1222.18 20.69 o 2 6 0 2594.81 2659.81 49.62 o 3 6 0 101.26 96.24 11.53 o 1 7 0 578.92 566.45 11.71 o 2 7 0 262.00 227.54 15.06 o 3 7 0 372.81 409.14 27.74 o 4 7 0 53.04 64.16 17.20 o 0 8 0 3177.05 3326.76 58.59 o 1 8 0 15.40 13.32 2.48 o 2 8 0 543.52 509.13 15.05 o 3 8 0 197.25 163.22 19.62 o 1 9 0 692.75 696.09 15.26 o 2 9 0 874.57 900.01 22.33 o 3 9 0 326.45 360.54 28.41 o 0 10 0 2465.45 2556.67 47.67 o 1 10 0 38.31 36.11 6.80 o 2 10 0 36.79 39.85 7.29 o 3 10 0 241.88 239.04 24.64 o 1 11 0 102.33 90.58 6.88 o 2 11 0 3.15 2.75 4.67 o 3 11 0 15.84 9.19 10.15 o 0 12 0 3500.01 3572.54 81.82 o 1 12 0 219.93 220.28 14.73 o 2 12 0 303.15 287.44 13.63 o 3 12 0 57.16 56.20 18.58 o 1 13 0 186.41 201.56 14.19 o 2 13 0 416.52 406.43 16.20 o 0 14 0 1114.87 1078.44 52.71 o 1 14 0 33.83 45.09 9.31 o 2 14 0 89.63 94.75 13.36 o 1 15 0 55.49 90.98 23.17 o -4 0 1 83.74 83.72 16.80 o -3 0 1 5.66 12.57 7.89 o -2 0 1 2398.36 2637.89 84.34 o -1 0 1 794.92 830.62 28.92 o 1 0 1 2.96 -3.38 3.61 o 2 0 1 49.67 34.00 7.39 o 3 0 1 1058.09 1110.20 45.16 o 4 0 1 1.21 -0.23 9.25 o -4 1 1 161.90 151.89 13.93 o -3 1 1 755.71 805.83 26.47 o -2 1 1 8.09 10.33 2.56 o -1 1 1 26.30 28.84 2.57 o 0 1 1 6703.56 7260.92 144.54 o 1 1 1 8546.11 9947.19 198.13 o 2 1 1 264.09 263.08 11.02 o 3 1 1 5.77 5.49 4.96 o 4 1 1 100.09 110.10 14.71 o -4 2 1 181.65 169.15 14.38 o -3 2 1 70.72 76.25 8.83 o -2 2 1 2131.85 2320.49 42.61 o -1 2 1 207.89 186.24 6.96 o 0 2 1 15.65 17.76 1.68 o 1 2 1 5.45 6.18 3.68 o 2 2 1 8.54 8.39 2.66 o 3 2 1 830.36 883.28 25.26 o 4 2 1 34.74 37.28 9.14 o -4 3 1 39.50 33.25 8.95 o -3 3 1 491.75 458.13 23.34 o -2 3 1 14.39 12.13 3.37 o -1 3 1 511.82 536.81 14.29 o 0 3 1 2334.10 2431.13 32.01 o 1 3 1 2573.34 2724.92 47.23 o 2 3 1 441.66 417.12 11.53 o 3 3 1 19.32 14.22 4.52 o 4 3 1 65.03 58.52 14.38 o -4 4 1 17.75 15.55 8.14 o -3 4 1 1.17 1.45 5.20 o -2 4 1 718.96 697.16 16.67 o -1 4 1 272.03 260.60 6.56 o 0 4 1 1502.95 1613.63 22.35 o 1 4 1 409.69 424.35 11.86 o 2 4 1 158.85 167.31 7.17 o 3 4 1 371.82 361.03 15.79 o 4 4 1 0.75 -0.28 10.09 o -4 5 1 38.07 31.93 9.46 o -3 5 1 384.62 375.20 17.27 o -2 5 1 19.66 19.36 3.02 o -1 5 1 963.27 1004.53 17.58 o 0 5 1 1003.72 917.65 12.65 o 1 5 1 882.18 830.73 17.58 o 2 5 1 639.19 618.65 15.55 o 3 5 1 27.36 29.54 5.32 o 4 5 1 62.33 63.20 16.41 o -4 6 1 0.26 2.42 9.47 o -3 6 1 16.12 12.55 6.05 o -2 6 1 1145.20 1067.10 20.17 o -1 6 1 1258.19 1328.78 29.35 o 0 6 1 2681.41 2831.24 34.71 o 1 6 1 690.32 742.46 12.31 o 2 6 1 591.14 561.81 23.15 o 3 6 1 555.30 602.20 22.26 o 4 6 1 7.93 21.31 11.56 o -3 7 1 443.76 441.25 19.23 o -2 7 1 7.60 11.83 3.12 o -1 7 1 1230.54 1357.77 20.99 o 0 7 1 1597.83 1727.29 22.82 o 1 7 1 1341.33 1348.10 23.54 o 2 7 1 813.13 781.10 22.51 o 3 7 1 94.48 92.63 9.92 o 4 7 1 50.32 52.66 16.12 o -3 8 1 36.07 34.30 8.22 o -2 8 1 789.71 753.82 21.54 o -1 8 1 228.38 223.32 6.52 o 0 8 1 422.95 401.16 8.54 o 1 8 1 124.07 114.89 5.49 o 2 8 1 61.42 48.57 7.16 o 3 8 1 364.95 363.42 37.18 o -3 9 1 209.16 202.91 22.44 o -2 9 1 1.51 2.15 4.52 o -1 9 1 72.60 69.64 4.37 o 0 9 1 1040.37 1052.89 15.87 o 1 9 1 1270.83 1298.75 23.89 o 2 9 1 137.78 147.76 9.08 o 3 9 1 4.60 7.30 6.13 o -3 10 1 2.25 4.17 9.70 o -2 10 1 766.45 799.79 21.36 o -1 10 1 321.90 333.24 13.18 o 0 10 1 158.31 154.68 7.52 o 1 10 1 35.69 38.73 4.25 o 2 10 1 54.68 65.58 7.33 o 3 10 1 434.96 446.14 17.27 o -3 11 1 196.18 204.94 23.79 o -2 11 1 0.14 0.24 5.37 o -1 11 1 1.66 -1.66 2.99 o 0 11 1 619.47 611.12 13.03 o 1 11 1 867.33 917.48 25.12 o 2 11 1 33.53 31.50 6.08 o 3 11 1 1.65 6.91 6.05 o -3 12 1 0.67 1.52 10.77 o -2 12 1 245.23 257.32 12.41 o -1 12 1 2.22 1.71 4.20 o 0 12 1 1.05 0.32 3.45 o 1 12 1 0.20 7.58 6.48 o 2 12 1 39.39 45.63 7.13 o -2 13 1 20.60 22.18 6.51 o -1 13 1 22.38 25.38 6.35 o 0 13 1 653.12 672.96 24.46 o 1 13 1 787.21 735.19 26.84 o 2 13 1 82.14 99.35 9.72 o -2 14 1 386.06 382.20 20.87 o -1 14 1 158.77 170.30 20.04 o 0 14 1 163.37 170.93 16.69 o 1 14 1 49.79 50.58 9.25 o 2 14 1 52.87 63.03 8.91 o -1 15 1 107.50 80.19 15.08 o 0 15 1 366.22 344.56 43.35 o 1 15 1 346.85 379.36 20.94 o 0 16 1 124.78 154.25 20.13 o -4 0 2 292.64 276.70 25.20 o -3 0 2 1165.11 1285.88 52.71 o -2 0 2 2618.33 3119.55 66.60 o -1 0 2 450.01 493.90 13.89 o 0 0 2 3412.03 3683.99 103.68 o 1 0 2 49901.99 56365.84 1579.33 o 2 0 2 5597.18 6184.25 181.09 o 3 0 2 967.66 956.91 40.09 o 4 0 2 83.13 116.42 16.86 o -4 1 2 43.88 37.35 22.41 o -3 1 2 12.01 16.28 5.83 o -2 1 2 1587.76 1681.63 31.82 o -1 1 2 862.53 850.02 12.82 o 0 1 2 1683.00 1826.16 37.49 o 1 1 2 585.49 658.01 16.30 o 2 1 2 263.44 297.34 11.65 o 3 1 2 328.69 366.93 17.82 o 4 1 2 116.87 124.15 17.36 o -4 2 2 164.66 167.97 17.62 o -3 2 2 133.50 167.67 19.54 o -2 2 2 437.24 395.18 15.14 o -1 2 2 962.31 1048.83 15.26 o 0 2 2 1908.69 2104.10 27.55 o 1 2 2 1666.14 1715.72 37.15 o 2 2 2 125.59 140.10 7.89 o 3 2 2 213.45 211.25 17.19 o 4 2 2 17.89 27.29 11.44 o -4 3 2 11.14 11.72 9.05 o -3 3 2 17.42 25.47 6.04 o -2 3 2 1233.48 1264.49 22.29 o -1 3 2 187.20 156.27 4.25 o 0 3 2 3147.12 3318.87 48.24 o 1 3 2 71.60 70.87 4.95 o 2 3 2 13.67 11.75 3.28 o 3 3 2 301.82 312.46 18.51 o 4 3 2 82.34 73.57 15.84 o -4 4 2 210.64 191.35 22.66 o -3 4 2 311.09 299.30 15.43 o -2 4 2 2668.35 2844.21 44.74 o -1 4 2 1.04 0.62 1.57 o 0 4 2 96.44 104.00 3.81 o 1 4 2 2740.32 2791.07 42.29 o 2 4 2 17.35 14.51 3.11 o 3 4 2 318.84 331.61 15.45 o 4 4 2 164.01 129.84 19.96 o -4 5 2 20.96 17.42 8.95 o -3 5 2 96.60 98.66 14.60 o -2 5 2 528.14 462.86 11.11 o -1 5 2 4.66 11.08 2.03 o 0 5 2 5279.35 5416.43 78.32 o 1 5 2 44.19 40.30 5.10 o 2 5 2 183.91 181.85 7.66 o 3 5 2 370.98 375.76 17.73 o 4 5 2 21.07 32.47 13.02 o -3 6 2 153.76 149.00 12.17 o -2 6 2 523.48 517.15 12.42 o -1 6 2 2047.43 2337.33 32.98 o 0 6 2 1820.45 1978.91 31.82 o 1 6 2 4473.27 4749.69 70.33 o 2 6 2 543.91 561.25 17.38 o 3 6 2 1284.38 1263.51 36.63 o 4 6 2 0.49 -4.79 10.37 o -4 7 2 10.81 4.51 11.22 o -3 7 2 23.60 21.57 7.29 o -2 7 2 1286.99 1344.10 28.35 o -1 7 2 138.27 118.03 4.77 o 0 7 2 1835.61 1801.89 36.23 o 1 7 2 2.04 -0.66 1.89 o 2 7 2 15.33 13.10 4.22 o 3 7 2 209.11 213.30 13.96 o -3 8 2 141.50 153.45 12.94 o -2 8 2 601.91 644.15 15.01 o -1 8 2 247.96 238.87 6.86 o 0 8 2 19.70 19.63 2.42 o 1 8 2 1828.86 1775.28 29.99 o 2 8 2 43.87 36.80 5.59 o 3 8 2 290.81 311.61 17.24 o -3 9 2 42.72 39.44 11.42 o -2 9 2 533.74 526.10 16.19 o -1 9 2 827.87 830.06 36.82 o 0 9 2 2289.06 2239.84 69.65 o 1 9 2 2.47 2.59 3.39 o 2 9 2 17.10 20.64 4.98 o 3 9 2 467.05 434.01 31.85 o -3 10 2 180.84 182.95 21.71 o -2 10 2 587.50 621.39 18.64 o -1 10 2 1.06 -0.21 3.00 o 0 10 2 161.17 152.37 6.90 o 1 10 2 1392.50 1372.85 32.06 o 2 10 2 12.56 7.52 4.39 o 3 10 2 30.53 29.76 6.98 o -3 11 2 0.08 2.37 11.78 o -2 11 2 85.91 84.09 8.01 o -1 11 2 10.82 5.37 3.52 o 0 11 2 3.16 3.96 3.24 o 1 11 2 121.04 113.28 8.26 o 2 11 2 210.28 214.85 11.76 o 3 11 2 3.35 1.90 6.00 o -2 12 2 220.96 189.15 13.93 o -1 12 2 173.82 178.33 12.50 o 0 12 2 101.97 110.09 10.24 o 1 12 2 2338.93 2412.32 48.84 o 2 12 2 332.97 347.10 14.99 o -2 13 2 445.56 467.43 21.57 o -1 13 2 474.75 464.17 13.78 o 0 13 2 691.28 641.50 24.08 o 1 13 2 0.17 10.79 9.00 o 2 13 2 1.51 2.09 5.48 o -2 14 2 194.28 210.23 15.82 o -1 14 2 20.36 19.55 7.39 o 0 14 2 10.85 4.93 6.07 o 1 14 2 737.17 753.63 28.46 o 2 14 2 64.14 79.36 9.65 o 0 15 2 188.84 192.04 14.80 o 1 15 2 0.13 4.53 7.61 o 0 16 2 1.51 -0.82 7.37 o -4 0 3 248.49 217.73 23.68 o -3 0 3 59.18 55.42 11.50 o -2 0 3 125.30 142.64 12.97 o -1 0 3 2563.70 2572.74 54.99 o 0 0 3 1277.16 1285.78 28.22 o 1 0 3 558.08 499.56 13.37 o 2 0 3 17.71 19.45 6.03 o -4 1 3 282.38 263.23 25.26 o -3 1 3 258.91 294.92 15.96 o -2 1 3 3322.30 3453.63 95.24 o -1 1 3 103.78 85.50 2.88 o 0 1 3 126.16 122.34 3.75 o 1 1 3 1542.27 1662.02 25.52 o 2 1 3 3081.76 3277.48 71.01 o 3 1 3 351.93 369.21 15.64 o 4 1 3 3.82 5.24 9.42 o -4 2 3 223.34 241.39 20.18 o -3 2 3 135.14 119.53 11.10 o -2 2 3 50.76 55.50 3.38 o -1 2 3 3386.82 3581.76 47.17 o 0 2 3 414.71 342.90 6.16 o 1 2 3 480.23 464.01 12.22 o 2 2 3 33.66 42.00 6.26 o 3 2 3 38.89 30.90 5.42 o 4 2 3 214.59 171.90 19.28 o -4 3 3 152.10 149.08 15.02 o -3 3 3 45.42 50.90 8.26 o -2 3 3 1834.81 1826.28 30.34 o -1 3 3 217.28 210.50 5.89 o 0 3 3 33.70 35.05 2.01 o 1 3 3 901.79 864.63 13.12 o 2 3 3 854.92 833.06 22.72 o 3 3 3 242.87 248.62 13.49 o -4 4 3 94.36 77.04 18.83 o -3 4 3 1.66 0.49 6.91 o -2 4 3 15.85 18.17 3.23 o -1 4 3 1037.39 1011.29 23.21 o 0 4 3 59.45 37.01 2.57 o 1 4 3 1969.42 1956.37 30.52 o 2 4 3 46.44 46.03 3.81 o 3 4 3 9.15 3.09 5.57 o 4 4 3 140.08 159.78 21.14 o -4 5 3 492.44 501.03 34.33 o -3 5 3 91.39 82.27 10.16 o -2 5 3 1221.75 1217.02 22.44 o -1 5 3 262.55 268.45 7.40 o 0 5 3 243.17 257.54 7.49 o 1 5 3 814.60 752.09 14.98 o 2 5 3 292.32 269.65 13.11 o 3 5 3 264.51 282.84 20.07 o 4 5 3 34.00 41.33 14.88 o -4 6 3 218.09 176.42 15.95 o -3 6 3 64.97 68.55 14.55 o -2 6 3 0.63 1.93 2.72 o -1 6 3 1628.47 1487.75 22.58 o 0 6 3 752.90 709.70 13.73 o 1 6 3 3110.61 3057.17 46.86 o 2 6 3 38.78 46.98 5.78 o 3 6 3 88.86 101.17 8.68 o 4 6 3 204.68 163.16 22.49 o -3 7 3 459.67 451.26 20.76 o -2 7 3 1667.33 1725.02 30.43 o -1 7 3 84.47 82.08 4.37 o 0 7 3 486.10 560.76 12.06 o 1 7 3 1132.57 1052.14 37.99 o 2 7 3 477.78 473.08 17.43 o 3 7 3 345.03 358.89 14.68 o -3 8 3 87.10 74.20 10.86 o -2 8 3 40.43 34.43 4.53 o -1 8 3 1125.72 1034.83 17.96 o 0 8 3 219.02 194.72 14.17 o 1 8 3 723.08 668.09 17.54 o 2 8 3 24.07 19.57 4.95 o 3 8 3 0.36 1.19 4.80 o -3 9 3 5.57 10.01 7.66 o -2 9 3 726.85 717.91 16.71 o -1 9 3 35.09 34.08 3.69 o 0 9 3 1.97 3.62 2.55 o 1 9 3 424.04 388.61 13.06 o 2 9 3 576.99 525.34 29.90 o 3 9 3 122.34 153.66 12.90 o -3 10 3 0.11 5.69 7.82 o -2 10 3 33.17 24.14 5.35 o -1 10 3 731.17 747.18 18.97 o 0 10 3 446.34 457.19 25.71 o 1 10 3 374.40 359.27 22.01 o 2 10 3 8.80 8.54 4.80 o 3 10 3 1.75 1.91 5.98 o -3 11 3 73.40 75.83 18.83 o -2 11 3 715.31 661.12 19.68 o -1 11 3 10.56 8.24 4.13 o 0 11 3 31.51 45.76 6.10 o 1 11 3 212.52 227.12 15.93 o 2 11 3 471.97 461.04 20.36 o 3 11 3 64.39 78.66 10.06 o -2 12 3 0.38 -5.53 5.14 o -1 12 3 296.89 289.46 20.67 o 0 12 3 13.46 20.00 5.20 o 1 12 3 14.25 9.93 4.90 o 2 12 3 4.84 6.68 5.61 o -2 13 3 610.61 588.83 19.81 o -1 13 3 84.57 73.00 15.79 o 0 13 3 10.81 9.59 6.77 o 1 13 3 290.72 290.14 13.61 o 2 13 3 447.15 477.76 18.99 o -2 14 3 24.81 33.66 12.49 o -1 14 3 450.86 403.03 18.85 o 0 14 3 195.30 193.58 14.44 o 1 14 3 261.62 269.08 21.05 o 2 14 3 6.30 2.34 6.18 o -1 15 3 17.66 9.12 7.77 o 0 15 3 17.81 22.31 8.68 o 1 15 3 236.44 239.72 18.52 o -4 0 4 6.10 0.79 11.50 o -3 0 4 284.30 277.04 22.38 o -2 0 4 2942.48 3329.08 73.72 o -1 0 4 5277.30 5557.39 113.81 o 0 0 4 238.00 224.03 8.05 o 1 0 4 334.84 393.87 17.82 o 2 0 4 7845.86 8311.90 168.75 o 3 0 4 2595.25 2285.92 77.52 o -4 1 4 352.89 373.74 31.88 o -3 1 4 4.93 0.78 5.10 o -2 1 4 2.01 4.38 3.29 o -1 1 4 1719.12 1740.81 24.62 o 0 1 4 514.72 489.26 9.48 o 1 1 4 2609.88 2635.13 39.35 o 2 1 4 159.51 162.34 6.08 o 3 1 4 182.37 168.29 15.90 o -4 2 4 26.03 17.99 9.20 o -3 2 4 278.56 287.49 16.37 o -2 2 4 687.01 608.88 22.70 o -1 2 4 675.49 576.42 10.10 o 0 2 4 132.73 150.35 4.57 o 1 2 4 155.95 161.87 4.77 o 2 2 4 238.05 213.58 13.75 o 3 2 4 1.78 1.41 7.05 o -4 3 4 448.59 466.93 34.50 o -3 3 4 159.00 162.94 12.75 o -2 3 4 336.97 349.24 18.82 o -1 3 4 1194.83 1151.50 17.63 o 0 3 4 64.30 51.16 4.05 o 1 3 4 2643.61 2649.46 46.27 o 2 3 4 1.13 4.77 2.38 o 3 3 4 81.24 84.24 7.78 o 4 3 4 74.89 79.60 11.15 o -4 4 4 7.40 -4.50 7.57 o -3 4 4 320.38 337.87 17.42 o -2 4 4 835.97 779.50 48.21 o -1 4 4 3561.38 3767.24 56.57 o 0 4 4 1021.12 1141.90 16.93 o 1 4 4 10.07 10.91 3.00 o 2 4 4 511.98 498.34 12.40 o 3 4 4 38.39 62.16 8.96 o 4 4 4 87.16 91.69 30.16 o -4 5 4 30.81 31.62 10.08 o -3 5 4 56.89 57.01 12.15 o -2 5 4 526.38 531.90 15.51 o -1 5 4 526.16 466.73 10.69 o 0 5 4 75.52 120.15 9.34 o 1 5 4 2839.28 2887.04 52.70 o 2 5 4 127.95 130.62 7.90 o 3 5 4 3.53 3.64 4.60 o 4 5 4 150.63 137.74 14.56 o 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187.74 20.52 o 2 3 12 299.01 289.05 26.39 o -2 4 12 16.21 35.22 7.83 o -1 4 12 629.64 641.60 30.42 o 0 4 12 252.03 256.27 12.98 o 1 4 12 260.56 238.19 21.96 o -2 5 12 45.86 59.30 8.97 o -1 5 12 15.68 32.03 12.77 o 0 5 12 70.37 76.81 11.71 o 1 5 12 28.50 22.19 15.73 o -1 6 12 444.77 455.00 22.96 o 0 6 12 73.17 88.17 9.26 o 1 6 12 8.02 10.85 6.18 o -1 7 12 3.72 3.04 7.64 o 0 7 12 145.34 141.38 14.05 o 1 7 12 2.18 -2.53 5.90 o -1 8 12 363.82 380.98 22.42 o 0 8 12 46.39 42.89 8.25 o -1 0 13 83.65 117.49 18.04 o 0 0 13 4.80 10.66 10.37 o -1 1 13 290.57 296.41 17.59 o 0 1 13 45.38 60.21 9.84 o 1 1 13 0.64 4.51 10.99 o -1 2 13 288.44 288.53 15.66 o 0 2 13 22.21 21.20 11.90 o 1 2 13 45.38 43.58 14.15 o -1 3 13 381.16 358.65 15.90 o 0 3 13 459.54 446.57 20.86 o 1 3 13 379.09 378.75 28.70 o -1 4 13 132.15 149.77 15.19 o 0 4 13 70.45 67.66 10.36 o 1 4 13 4.62 5.74 8.05 o -1 5 13 136.18 168.34 15.84 o 0 5 13 60.46 93.51 10.03 o 0 6 13 67.80 71.40 9.42 o 0 0 14 341.81 355.24 27.74 o 0 1 14 50.89 57.11 15.73 o