#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:21:56 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181224 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/02/2230222.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230222_Fobs loop_ _publ_author_name 'Chang, Liu-Shuan' 'Duan, Hong-Quan' _publ_section_title ; (S,E)-N-Methyl-4-[(S)2,6,6-trimethyl-4-oxocyclohex-2-enyl]but-3-en-2-aminium chloride ; _journal_coeditor_code BH2347 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1289 _journal_volume 67 _journal_year 2011 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.460 _cell_angle_gamma 90.000 _cell_length_a 14.5470 _cell_length_b 12.2470 _cell_length_c 19.0350 _exptl_crystal_F_000 1120.00 _reflns_d_resolution_high 0.7689 _cod_data_source_file bh2347Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' r90923i in P2(1) P21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 250.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -15 0 50.48 41.20 10.44 o 2 -15 0 32.16 42.70 12.98 o 3 -15 0 46.77 30.24 11.36 o 4 -15 0 180.71 133.51 38.86 o 5 -15 0 88.11 71.07 20.73 o 0 -14 0 26.82 19.81 35.94 o 1 -14 0 113.18 87.48 20.90 o 2 -14 0 44.51 45.75 13.92 o 3 -14 0 30.28 24.90 11.40 o 4 -14 0 45.90 35.14 13.43 o 5 -14 0 96.82 105.48 22.24 o 6 -14 0 43.84 52.26 13.93 o 7 -14 0 41.47 47.04 11.08 o 8 -14 0 40.32 51.12 15.93 o 1 -13 0 239.91 220.17 29.88 o 2 -13 0 27.28 19.39 6.27 o 3 -13 0 475.67 504.82 16.71 o 4 -13 0 57.88 60.73 17.37 o 5 -13 0 129.73 126.30 27.64 o 6 -13 0 16.13 18.86 21.40 o 7 -13 0 234.34 207.28 45.27 o 8 -13 0 54.30 52.40 19.45 o 9 -13 0 11.05 13.07 8.33 o 10 -13 0 11.51 22.52 17.55 o 0 -12 0 10.67 5.87 15.48 o 1 -12 0 91.07 100.39 15.97 o 2 -12 0 239.45 230.55 25.53 o 3 -12 0 146.90 166.03 25.87 o 4 -12 0 65.17 71.31 13.14 o 5 -12 0 176.22 196.05 12.06 o 6 -12 0 91.97 90.71 21.74 o 7 -12 0 23.98 18.18 8.76 o 8 -12 0 34.20 39.36 13.62 o 9 -12 0 78.50 91.77 23.14 o 10 -12 0 26.99 34.40 14.60 o 11 -12 0 42.03 38.45 23.25 o 1 -11 0 274.36 297.74 30.57 o 2 -11 0 432.61 504.26 41.46 o 3 -11 0 1100.32 1143.46 31.53 o 4 -11 0 327.72 336.67 22.56 o 5 -11 0 794.95 867.22 22.57 o 6 -11 0 112.37 127.07 17.01 o 7 -11 0 318.69 282.58 43.43 o 8 -11 0 167.44 163.19 28.94 o 9 -11 0 305.11 319.59 49.72 o 10 -11 0 41.77 16.83 12.27 o 11 -11 0 253.88 187.87 46.47 o 12 -11 0 151.20 144.35 33.09 o 0 -10 0 270.46 269.26 45.55 o 1 -10 0 186.51 192.53 23.47 o 2 -10 0 551.15 554.84 33.34 o 3 -10 0 166.54 179.56 23.46 o 4 -10 0 793.46 799.94 44.48 o 5 -10 0 484.43 499.92 23.58 o 6 -10 0 33.20 24.06 12.04 o 7 -10 0 93.35 98.91 12.75 o 8 -10 0 161.37 130.41 28.67 o 9 -10 0 66.23 84.17 20.96 o 10 -10 0 31.05 40.66 11.54 o 11 -10 0 85.98 86.85 18.72 o 12 -10 0 231.49 209.42 43.15 o 13 -10 0 37.68 64.90 20.40 o 1 -9 0 659.23 674.96 18.65 o 2 -9 0 381.62 398.85 31.41 o 3 -9 0 1692.86 1871.93 32.77 o 4 -9 0 601.31 601.05 15.66 o 5 -9 0 1435.30 1570.89 39.64 o 6 -9 0 170.23 223.37 16.55 o 7 -9 0 482.61 538.47 17.80 o 8 -9 0 470.52 456.70 18.18 o 9 -9 0 429.88 457.69 45.92 o 10 -9 0 79.93 75.13 16.72 o 11 -9 0 266.13 263.46 51.31 o 12 -9 0 179.96 183.62 28.21 o 13 -9 0 198.26 171.15 44.99 o 14 -9 0 220.90 193.47 67.16 o 0 -8 0 176.47 226.62 30.53 o 1 -8 0 138.21 151.65 14.87 o 2 -8 0 268.47 304.02 15.06 o 3 -8 0 49.04 49.02 7.31 o 4 -8 0 2084.47 2269.57 48.90 o 5 -8 0 611.90 637.51 12.29 o 6 -8 0 61.27 66.73 8.59 o 7 -8 0 63.63 55.26 8.19 o 8 -8 0 92.99 112.38 15.10 o 9 -8 0 228.97 256.26 27.81 o 10 -8 0 46.87 38.30 11.28 o 11 -8 0 221.99 222.94 33.23 o 12 -8 0 519.20 575.47 26.07 o 13 -8 0 113.40 135.20 46.25 o 14 -8 0 223.49 174.80 49.49 o 15 -8 0 125.06 154.94 50.20 o 1 -7 0 510.78 508.64 15.74 o 2 -7 0 471.67 490.83 16.41 o 3 -7 0 1452.06 1391.80 25.07 o 4 -7 0 429.47 491.23 12.46 o 5 -7 0 250.14 265.25 17.78 o 6 -7 0 199.99 198.65 8.76 o 7 -7 0 188.33 197.88 15.29 o 8 -7 0 333.74 335.83 21.29 o 9 -7 0 432.28 458.96 39.19 o 10 -7 0 120.37 116.97 18.45 o 11 -7 0 251.26 270.60 45.88 o 12 -7 0 55.93 59.62 13.76 o 13 -7 0 337.83 409.66 60.59 o 14 -7 0 477.09 482.06 62.83 o 15 -7 0 79.97 39.64 21.80 o 0 -6 0 8452.58 8322.12 127.09 o 1 -6 0 717.51 736.57 33.21 o 2 -6 0 794.23 878.85 23.55 o 3 -6 0 324.13 344.51 12.10 o 4 -6 0 884.78 925.60 23.66 o 5 -6 0 1090.60 1096.04 38.13 o 6 -6 0 1009.38 1014.82 15.17 o 7 -6 0 401.00 412.54 17.66 o 8 -6 0 54.40 60.74 14.25 o 9 -6 0 626.98 754.95 28.11 o 10 -6 0 1209.25 1215.26 36.83 o 11 -6 0 341.94 394.17 28.50 o 12 -6 0 705.50 732.56 32.23 o 13 -6 0 205.06 224.14 34.96 o 14 -6 0 295.74 223.90 40.53 o 15 -6 0 124.47 72.58 41.65 o 16 -6 0 30.95 36.74 17.72 o 1 -5 0 445.39 427.65 21.87 o 2 -5 0 2206.38 2369.24 35.16 o 3 -5 0 1084.02 1122.95 34.37 o 4 -5 0 3441.42 3605.92 72.33 o 5 -5 0 604.07 593.09 20.98 o 6 -5 0 1168.92 1202.80 30.12 o 7 -5 0 816.18 795.91 20.75 o 8 -5 0 701.62 697.33 29.63 o 9 -5 0 351.57 332.48 33.03 o 10 -5 0 45.85 46.88 10.08 o 11 -5 0 443.88 418.43 25.85 o 12 -5 0 21.31 26.38 10.79 o 13 -5 0 155.85 153.97 24.85 o 14 -5 0 417.55 386.02 20.77 o 15 -5 0 196.80 183.93 35.44 o 16 -5 0 19.67 24.20 12.38 o 0 -4 0 2039.56 2115.67 62.09 o 1 -4 0 2157.69 2069.87 50.84 o 2 -4 0 3618.59 3585.36 47.95 o 3 -4 0 954.64 961.87 22.76 o 4 -4 0 2658.37 2798.70 60.32 o 5 -4 0 493.72 499.45 12.10 o 6 -4 0 3124.57 3085.54 37.52 o 7 -4 0 407.82 402.24 17.97 o 8 -4 0 446.93 485.23 31.33 o 9 -4 0 277.44 285.15 15.79 o 10 -4 0 891.90 908.70 14.12 o 11 -4 0 672.68 684.75 17.15 o 12 -4 0 46.59 29.74 10.56 o 13 -4 0 261.38 236.80 37.23 o 14 -4 0 492.65 543.45 33.97 o 15 -4 0 164.91 116.69 26.51 o 16 -4 0 16.25 -1.47 15.20 o 1 -3 0 1899.86 1784.52 31.55 o 2 -3 0 3612.85 3247.92 41.63 o 3 -3 0 1803.06 1747.09 29.51 o 4 -3 0 279.06 275.48 15.82 o 5 -3 0 597.91 571.46 18.46 o 6 -3 0 836.60 889.90 20.20 o 7 -3 0 1504.19 1552.38 55.30 o 8 -3 0 2627.11 2710.29 49.19 o 9 -3 0 62.21 59.81 10.69 o 10 -3 0 147.67 144.21 14.98 o 11 -3 0 186.60 205.10 30.12 o 12 -3 0 178.47 204.98 24.44 o 13 -3 0 209.17 186.00 28.44 o 14 -3 0 195.95 163.89 23.17 o 15 -3 0 87.64 73.21 20.27 o 16 -3 0 9.20 20.53 10.06 o 17 -3 0 13.32 47.80 24.91 o 1 -2 0 455.05 439.18 13.28 o 2 -2 0 1626.13 1647.08 31.11 o 3 -2 0 2083.29 2006.26 31.80 o 4 -2 0 3551.07 3251.05 25.21 o 5 -2 0 1336.19 1363.96 26.65 o 6 -2 0 2448.61 2272.92 18.09 o 7 -2 0 216.54 233.48 15.68 o 8 -2 0 5335.83 5452.78 150.81 o 9 -2 0 28.62 23.94 6.86 o 10 -2 0 56.96 56.15 12.55 o 11 -2 0 219.85 195.16 44.99 o 12 -2 0 167.45 147.87 47.28 o 13 -2 0 53.00 38.78 12.97 o 14 -2 0 561.49 609.44 119.28 o 15 -2 0 70.52 36.49 39.49 o 16 -2 0 29.76 74.62 41.53 o 17 -2 0 39.75 27.09 11.08 o 1 -1 0 911.47 820.75 17.59 o 2 -1 0 6982.65 5755.01 131.36 o 3 -1 0 683.20 647.20 23.82 o 4 -1 0 6177.18 5712.13 84.59 o 5 -1 0 104.91 107.96 13.96 o 6 -1 0 429.36 463.12 10.10 o 7 -1 0 289.26 289.25 11.49 o 8 -1 0 1419.17 1378.09 23.71 o 9 -1 0 355.56 356.07 11.27 o 10 -1 0 173.59 182.21 10.07 o 11 -1 0 202.29 90.60 41.59 o 12 -1 0 457.06 501.21 40.36 o 13 -1 0 174.86 93.70 42.88 o 14 -1 0 217.54 268.54 49.57 o 15 -1 0 56.43 21.83 20.32 o 16 -1 0 74.30 51.33 19.03 o 17 -1 0 11.05 30.17 21.05 o 2 0 0 11229.25 10073.09 76.21 o 3 0 0 242.41 218.27 12.14 o 4 0 0 3875.36 3488.16 83.45 o 5 0 0 1042.89 1048.31 16.91 o 6 0 0 563.32 508.03 11.09 o 7 0 0 100.73 120.08 14.51 o 8 0 0 9159.94 9268.48 147.98 o 9 0 0 47.38 -1.85 32.35 o 10 0 0 228.48 258.44 57.26 o 11 0 0 111.98 149.18 67.56 o 12 0 0 696.27 680.67 53.07 o 13 0 0 295.46 219.43 43.38 o 14 0 0 458.10 610.53 66.39 o 15 0 0 10.54 10.92 21.94 o 16 0 0 28.34 -3.47 18.70 o 1 1 0 910.44 812.54 32.47 o 2 1 0 7017.16 5901.63 47.17 o 3 1 0 681.23 627.43 12.67 o 4 1 0 6245.21 5803.69 101.46 o 5 1 0 104.75 110.09 9.91 o 6 1 0 429.15 447.28 21.56 o 7 1 0 285.30 303.90 14.34 o 8 1 0 1432.47 1316.98 43.92 o 9 1 0 357.25 307.81 85.08 o 10 1 0 174.67 159.25 89.51 o 11 1 0 204.16 260.57 77.58 o 12 1 0 464.46 399.28 52.51 o 13 1 0 176.06 260.18 44.67 o 1 2 0 451.44 429.08 6.92 o 2 2 0 1612.56 1606.35 28.80 o 3 2 0 2082.31 2021.13 33.70 o 4 2 0 3487.34 3283.49 31.64 o 5 2 0 1320.71 1263.25 31.57 o 6 2 0 2405.12 2284.34 22.37 o 7 2 0 218.07 223.75 33.19 o 8 2 0 5332.21 5505.59 95.51 o 9 2 0 28.04 34.80 14.50 o 10 2 0 62.53 57.66 33.70 o 11 2 0 222.21 204.03 41.70 o 12 2 0 163.61 220.27 66.28 o 1 3 0 1892.33 1809.63 36.95 o 2 3 0 3565.53 3214.72 42.96 o 3 3 0 1801.13 1734.15 27.62 o 4 3 0 262.94 243.34 10.22 o 5 3 0 606.90 581.08 13.83 o 6 3 0 871.09 923.54 30.45 o 7 3 0 1508.01 1558.64 32.97 o 8 3 0 2637.07 2816.84 149.68 o 9 3 0 65.77 64.33 18.27 o 10 3 0 147.07 205.99 64.88 o 0 4 0 2040.06 2017.31 49.78 o 1 4 0 2146.21 2096.02 37.76 o 2 4 0 3531.99 3638.29 43.66 o 3 4 0 952.73 951.54 19.97 o 4 4 0 2559.07 2839.88 32.24 o 5 4 0 486.64 473.19 11.52 o 6 4 0 3120.28 3005.22 45.16 o 7 4 0 410.06 395.41 9.63 o 8 4 0 466.79 457.44 12.20 o 9 4 0 281.87 261.63 9.40 o 10 4 0 884.51 884.42 32.86 o 1 5 0 425.05 410.29 11.82 o 2 5 0 2283.24 2399.53 25.59 o 3 5 0 1049.79 1008.63 48.70 o 4 5 0 3388.15 3590.53 115.23 o 5 5 0 614.69 623.39 12.90 o 6 5 0 1196.61 1328.15 30.76 o 7 5 0 809.01 766.31 13.15 o 8 5 0 701.58 712.80 12.76 o 9 5 0 338.33 287.88 24.74 o 0 6 0 8452.27 7818.44 171.17 o 1 6 0 705.04 668.58 25.92 o 2 6 0 761.83 752.32 34.71 o 3 6 0 321.67 331.83 16.62 o 4 6 0 828.75 868.13 32.35 o 5 6 0 1103.52 1153.06 28.82 o 6 6 0 996.99 996.23 13.99 o 7 6 0 395.76 383.32 11.42 o 8 6 0 47.26 43.94 9.74 o 1 7 0 500.34 480.33 19.93 o 2 7 0 488.03 470.09 38.06 o 3 7 0 1431.96 1372.92 25.53 o 4 7 0 418.35 456.26 15.51 o 5 7 0 251.74 249.11 5.44 o 6 7 0 208.97 217.27 5.94 o 7 7 0 204.05 151.86 19.48 o 8 7 0 340.73 352.42 10.52 o 3 8 0 48.66 34.76 8.47 o 4 8 0 2073.44 2178.40 65.63 o 5 8 0 602.18 589.94 45.84 o 6 8 0 57.27 56.02 8.25 o 4 9 0 594.99 588.87 22.95 o 5 9 0 1442.39 1426.38 28.24 o 6 9 0 172.65 189.31 14.95 o 6 10 0 33.74 30.06 9.40 o -6 -15 1 69.13 44.57 14.24 o -5 -15 1 60.94 67.47 17.25 o -4 -15 1 88.73 55.23 18.93 o -3 -15 1 86.24 39.28 11.96 o -2 -15 1 82.29 76.07 19.33 o -1 -15 1 34.24 34.04 9.25 o 0 -15 1 7.66 23.53 9.68 o 1 -15 1 71.81 64.39 13.82 o 2 -15 1 10.93 -7.49 17.54 o 3 -15 1 53.13 59.88 20.16 o 4 -15 1 57.10 39.20 12.63 o 5 -15 1 44.16 54.95 18.08 o -8 -14 1 109.27 94.09 20.91 o -7 -14 1 112.02 87.62 25.85 o -6 -14 1 84.92 61.63 23.62 o -5 -14 1 117.51 123.98 28.63 o -4 -14 1 27.31 24.18 11.86 o -3 -14 1 295.10 300.67 60.78 o -2 -14 1 71.02 62.71 11.18 o -1 -14 1 147.75 158.15 21.10 o 0 -14 1 100.36 87.11 16.59 o 1 -14 1 113.08 90.61 15.99 o 2 -14 1 23.16 27.53 11.90 o 3 -14 1 139.52 109.59 20.37 o 4 -14 1 6.02 18.14 9.37 o 5 -14 1 79.92 79.75 14.80 o 6 -14 1 44.25 22.84 10.65 o 7 -14 1 185.68 199.40 44.08 o 8 -14 1 53.18 59.00 34.26 o -10 -13 1 88.04 72.57 39.46 o -9 -13 1 27.47 16.65 11.78 o -8 -13 1 144.97 147.27 37.89 o -7 -13 1 180.14 169.95 42.51 o -6 -13 1 45.67 43.84 12.85 o -5 -13 1 84.62 63.21 14.98 o -4 -13 1 93.92 56.94 14.86 o -3 -13 1 94.71 82.08 15.60 o -2 -13 1 287.91 241.08 34.77 o -1 -13 1 223.56 217.38 28.75 o 0 -13 1 6.50 6.80 10.15 o 1 -13 1 96.11 95.26 17.18 o 2 -13 1 28.30 41.65 9.89 o 3 -13 1 148.51 169.44 20.04 o 4 -13 1 4.82 17.02 12.13 o 5 -13 1 139.16 158.87 27.90 o 6 -13 1 74.18 62.12 14.90 o 7 -13 1 151.38 127.97 24.45 o 8 -13 1 26.69 31.15 15.81 o 9 -13 1 16.49 26.24 9.06 o -11 -12 1 73.47 56.21 22.80 o -10 -12 1 69.09 70.08 17.85 o -9 -12 1 271.05 253.54 39.39 o -8 -12 1 16.40 21.08 11.11 o -7 -12 1 190.83 165.57 32.04 o -6 -12 1 8.78 22.08 9.05 o -5 -12 1 84.25 95.92 18.62 o -4 -12 1 96.43 72.87 21.04 o -3 -12 1 312.97 342.30 28.88 o -2 -12 1 4.04 4.80 7.04 o -1 -12 1 69.01 64.35 14.01 o 0 -12 1 56.24 31.06 9.57 o 1 -12 1 276.52 321.87 37.40 o 2 -12 1 319.87 414.68 33.65 o 3 -12 1 413.00 522.43 22.44 o 4 -12 1 20.36 22.06 7.48 o 5 -12 1 236.83 252.44 34.57 o 6 -12 1 78.10 58.60 19.44 o 7 -12 1 164.93 136.33 27.87 o 8 -12 1 10.16 12.06 10.85 o 9 -12 1 160.57 169.96 27.89 o 10 -12 1 69.24 66.67 18.87 o 11 -12 1 300.68 298.12 59.94 o -12 -11 1 29.06 15.30 11.76 o -11 -11 1 226.56 237.16 76.32 o -10 -11 1 77.40 76.21 20.07 o -9 -11 1 296.63 328.48 39.04 o -8 -11 1 38.74 40.34 12.84 o -7 -11 1 602.18 621.10 36.82 o -6 -11 1 101.36 91.63 11.46 o -5 -11 1 351.77 383.14 21.60 o -4 -11 1 604.96 603.97 28.96 o -3 -11 1 61.22 46.68 9.19 o -2 -11 1 10.47 5.20 9.32 o -1 -11 1 378.94 451.32 28.82 o 0 -11 1 136.43 134.28 18.12 o 1 -11 1 131.95 137.21 16.59 o 2 -11 1 142.52 163.77 20.41 o 3 -11 1 369.92 429.84 29.43 o 4 -11 1 814.84 798.87 29.73 o 5 -11 1 377.77 427.01 14.69 o 6 -11 1 6.20 11.45 7.34 o 7 -11 1 75.30 72.20 26.62 o 8 -11 1 77.29 50.92 13.58 o 9 -11 1 241.61 234.15 39.05 o 10 -11 1 84.74 66.15 18.33 o 11 -11 1 51.18 37.13 11.21 o 12 -11 1 22.52 26.38 18.16 o -13 -10 1 66.54 74.01 27.81 o -12 -10 1 140.98 148.53 42.19 o -11 -10 1 171.18 185.38 32.91 o -10 -10 1 31.47 22.09 10.60 o -9 -10 1 113.41 153.40 24.71 o -8 -10 1 527.16 471.26 25.67 o -7 -10 1 298.59 263.39 21.31 o -6 -10 1 13.30 10.94 4.98 o -5 -10 1 176.60 181.28 14.82 o -4 -10 1 53.16 30.53 9.16 o -3 -10 1 474.06 529.39 16.50 o -2 -10 1 334.88 341.00 17.38 o -1 -10 1 267.16 315.23 38.98 o 0 -10 1 1280.70 1274.32 30.92 o 1 -10 1 819.97 865.77 35.41 o 2 -10 1 858.01 907.63 21.46 o 3 -10 1 423.74 408.79 28.55 o 4 -10 1 162.94 178.16 22.76 o 5 -10 1 457.76 499.93 15.72 o 6 -10 1 130.70 142.78 20.54 o 7 -10 1 157.57 172.76 21.62 o 8 -10 1 41.70 35.96 15.50 o 9 -10 1 77.09 50.79 14.07 o 10 -10 1 6.84 23.96 8.50 o 11 -10 1 377.60 393.93 65.59 o 12 -10 1 139.64 138.84 29.61 o 13 -10 1 119.78 162.26 40.53 o -14 -9 1 50.31 9.40 19.76 o -13 -9 1 100.17 91.83 23.52 o -12 -9 1 20.17 22.85 12.00 o -11 -9 1 313.55 337.43 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