#------------------------------------------------------------------------------ #$Date: 2011-07-04 21:24:21 +0300 (Mon, 04 Jul 2011) $ #$Revision: 22560 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2230256.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230256_Fobs loop_ _publ_author_name 'Wang, Jing-Yi' 'Wang, Xiu-Guang' 'Zhao, Xiao-Jun' _publ_section_title ; Tetraaquabis[2-(4-pyridylsulfanyl)acetato-\kN]nickel(II) ; _journal_coeditor_code BT5549 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m795 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 92.713 _cell_angle_beta 103.440 _cell_angle_gamma 115.120 _cell_length_a 6.3577 _cell_length_b 7.0330 _cell_length_c 11.7624 _exptl_crystal_F_000 242.00 _reflns_d_resolution_high 0.8407 _[local]_cod_data_source_file bt5549Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 90820A in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 120.46 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 12.05 12.36 0.37 o 2 0 0 24.32 24.62 0.49 o 3 0 0 6.07 2.99 0.26 o 4 0 0 864.83 866.16 6.10 o 5 0 0 29.94 31.01 0.98 o 6 0 0 0.35 1.34 0.77 o -6 1 0 361.71 369.91 5.74 o -5 1 0 254.03 268.17 2.72 o -4 1 0 90.63 101.14 2.95 o -3 1 0 79.66 134.13 2.95 o -2 1 0 1863.02 1893.49 11.33 o -1 1 0 25.48 25.56 0.37 o 0 1 0 370.71 371.06 3.63 o 1 1 0 2398.36 2137.52 19.05 o 2 1 0 1.12 4.05 0.47 o 3 1 0 140.53 154.38 2.64 o 4 1 0 159.56 162.65 2.01 o 5 1 0 281.15 293.93 4.83 o 6 1 0 32.11 32.73 1.82 o -7 2 0 0.72 0.69 0.78 o -6 2 0 4.78 4.61 0.84 o -5 2 0 484.66 458.00 3.84 o -4 2 0 170.84 165.65 1.81 o -3 2 0 477.44 514.94 2.98 o -2 2 0 387.03 366.22 2.68 o -1 2 0 14511.67 13550.52 204.90 o 0 2 0 1984.32 1988.04 31.53 o 1 2 0 357.60 365.47 4.16 o 2 2 0 777.52 783.18 8.11 o 3 2 0 659.14 615.36 7.12 o 4 2 0 41.28 40.19 1.71 o 5 2 0 3.18 1.25 0.91 o -7 3 0 143.15 149.81 3.65 o -6 3 0 1.83 3.03 0.72 o -5 3 0 8.36 8.85 0.60 o -4 3 0 63.56 54.20 1.02 o -3 3 0 2390.05 2452.45 21.91 o -2 3 0 10.02 13.08 0.61 o -1 3 0 154.69 142.87 1.50 o 0 3 0 798.68 744.58 5.29 o 1 3 0 3.04 1.59 0.60 o 2 3 0 132.60 128.31 1.77 o 3 3 0 208.90 216.15 2.63 o 4 3 0 318.02 321.90 3.60 o -7 4 0 17.46 19.51 1.46 o -6 4 0 339.48 350.48 5.49 o -5 4 0 41.08 43.64 1.61 o -4 4 0 18.07 19.37 1.02 o -3 4 0 222.08 208.79 2.11 o -2 4 0 4744.27 4887.85 35.57 o -1 4 0 35.01 47.08 1.72 o 0 4 0 162.76 176.89 2.03 o 1 4 0 46.29 46.24 2.19 o 2 4 0 115.73 107.81 2.46 o 3 4 0 1.05 0.80 0.66 o 4 4 0 42.27 41.16 1.82 o -7 5 0 34.53 35.17 1.89 o -6 5 0 111.97 100.43 2.75 o -5 5 0 34.83 34.01 1.51 o -4 5 0 226.35 231.30 3.81 o -3 5 0 83.48 79.01 2.57 o -2 5 0 502.16 508.60 5.55 o -1 5 0 571.65 566.55 10.58 o 0 5 0 0.47 0.46 0.42 o 1 5 0 16.03 17.57 1.18 o 2 5 0 119.92 124.19 3.06 o 3 5 0 182.15 177.96 3.94 o -6 6 0 21.24 22.29 1.47 o -5 6 0 22.23 25.36 1.42 o -4 6 0 185.34 184.98 3.51 o -3 6 0 946.82 930.80 12.42 o -2 6 0 134.93 127.52 1.92 o -1 6 0 35.32 36.95 1.10 o 0 6 0 97.70 96.93 1.81 o 1 6 0 125.38 130.08 3.26 o 2 6 0 0.68 0.45 0.73 o -6 7 0 5.46 7.61 1.03 o -5 7 0 167.76 161.48 3.58 o -4 7 0 9.23 9.53 1.05 o -3 7 0 160.22 164.09 2.36 o -2 7 0 19.22 23.83 1.50 o -1 7 0 4.47 4.08 0.76 o 0 7 0 47.07 44.10 2.01 o -5 8 0 83.85 85.22 2.71 o -4 8 0 209.94 192.71 4.02 o -3 8 0 38.82 33.60 1.18 o -2 8 0 29.70 29.80 1.68 o 2 -8 1 3.05 1.64 0.81 o 3 -8 1 292.19 269.06 4.85 o 4 -8 1 37.21 45.12 1.97 o 0 -7 1 23.70 26.37 1.57 o 1 -7 1 67.22 68.36 2.33 o 2 -7 1 0.55 0.69 0.45 o 3 -7 1 32.95 28.29 1.47 o 4 -7 1 198.29 196.10 3.80 o 5 -7 1 65.78 68.43 2.31 o 6 -7 1 0.57 0.77 0.77 o -2 -6 1 162.72 165.84 3.92 o -1 -6 1 59.53 64.28 2.26 o 0 -6 1 15.27 15.75 1.20 o 1 -6 1 4.46 5.00 0.61 o 2 -6 1 941.28 971.98 7.34 o 3 -6 1 81.71 85.52 1.55 o 4 -6 1 3.65 5.13 0.78 o 5 -6 1 49.57 57.75 2.02 o 6 -6 1 169.35 175.80 3.84 o -3 -5 1 36.71 36.00 1.82 o -2 -5 1 14.65 19.02 1.23 o -1 -5 1 10.51 9.83 0.68 o 0 -5 1 178.38 182.22 3.46 o 1 -5 1 79.04 81.78 1.41 o 2 -5 1 365.77 372.23 3.74 o 3 -5 1 207.77 210.33 2.33 o 4 -5 1 0.89 0.36 0.55 o 5 -5 1 1.22 1.90 0.59 o 6 -5 1 222.96 219.03 4.28 o 7 -5 1 192.04 197.20 4.35 o -4 -4 1 3.53 5.89 0.94 o -3 -4 1 541.04 551.77 7.23 o -2 -4 1 2.41 2.65 0.44 o -1 -4 1 13.85 14.10 0.67 o 0 -4 1 293.63 275.84 2.63 o 1 -4 1 4354.52 4441.87 29.87 o 2 -4 1 275.83 268.13 2.51 o 3 -4 1 15.79 15.64 0.59 o 4 -4 1 181.36 183.62 3.18 o 5 -4 1 223.74 215.39 3.81 o 6 -4 1 0.90 1.03 0.66 o 7 -4 1 6.59 7.08 1.07 o -5 -3 1 118.43 112.43 2.75 o -4 -3 1 25.63 24.49 1.28 o -3 -3 1 36.60 39.40 1.05 o -2 -3 1 136.77 104.90 1.51 o -1 -3 1 408.10 424.54 3.45 o 0 -3 1 3.04 3.54 0.33 o 1 -3 1 305.92 302.48 2.50 o 2 -3 1 670.33 671.92 4.75 o 3 -3 1 316.70 300.31 2.59 o 4 -3 1 57.34 57.97 1.64 o 5 -3 1 320.15 327.12 3.05 o 6 -3 1 152.05 156.10 3.43 o 7 -3 1 13.74 14.56 1.36 o -5 -2 1 3.41 2.04 0.56 o -4 -2 1 461.03 441.75 4.06 o -3 -2 1 14.17 13.26 0.60 o -2 -2 1 539.90 542.35 4.21 o -1 -2 1 2227.12 2133.17 14.51 o 0 -2 1 4993.62 4956.10 32.06 o 1 -2 1 337.21 343.86 6.42 o 2 -2 1 13.94 16.34 0.43 o 3 -2 1 1398.69 1409.13 7.20 o 4 -2 1 387.71 382.50 2.51 o 5 -2 1 5.70 5.20 0.78 o 6 -2 1 13.79 17.01 1.28 o 7 -2 1 198.13 200.77 4.38 o -5 -1 1 0.43 0.62 0.50 o -4 -1 1 39.45 39.41 0.75 o -3 -1 1 257.09 212.84 3.07 o -2 -1 1 382.63 399.11 3.02 o -1 -1 1 63.02 51.19 0.68 o 0 -1 1 1716.37 1768.42 12.29 o 1 -1 1 1567.61 1590.98 10.68 o 2 -1 1 1.91 3.57 0.54 o 3 -1 1 6.98 8.62 0.42 o 4 -1 1 930.47 973.26 6.56 o 5 -1 1 692.98 709.82 8.45 o 6 -1 1 43.18 43.21 1.93 o -6 0 1 9.41 14.45 1.20 o -5 0 1 1081.63 1057.22 7.53 o -4 0 1 40.51 46.24 0.96 o -3 0 1 46.39 46.90 0.81 o -2 0 1 718.84 724.91 7.20 o -1 0 1 8368.22 6796.60 44.09 o 0 0 1 658.84 675.06 7.27 o 1 0 1 109.57 107.35 1.02 o 2 0 1 379.85 346.46 2.53 o 3 0 1 0.93 1.64 0.24 o 4 0 1 0.84 0.72 0.33 o 5 0 1 188.64 196.65 3.77 o 6 0 1 327.10 336.05 5.69 o -7 1 1 49.51 58.19 2.30 o -6 1 1 7.36 7.55 0.58 o -5 1 1 325.55 321.82 5.16 o -4 1 1 309.16 262.57 2.46 o -3 1 1 9.55 9.11 0.37 o -2 1 1 1.25 0.45 0.19 o -1 1 1 1831.41 1831.85 26.11 o 0 1 1 1463.75 1424.73 13.67 o 1 1 1 3.73 3.40 0.45 o 2 1 1 205.85 211.68 3.00 o 3 1 1 1389.03 1416.54 13.75 o 4 1 1 463.25 455.61 3.89 o 5 1 1 1.58 0.15 0.69 o -7 2 1 28.27 34.88 1.80 o -6 2 1 549.09 526.29 4.56 o -5 2 1 7.68 6.28 0.46 o -4 2 1 339.23 317.82 2.79 o -3 2 1 2769.61 2739.26 22.69 o -2 2 1 4028.78 4208.34 41.80 o -1 2 1 535.06 492.26 4.98 o 0 2 1 694.26 724.56 7.13 o 1 2 1 995.38 939.12 9.26 o 2 2 1 291.64 300.58 4.13 o 3 2 1 28.58 28.47 1.38 o 4 2 1 89.12 88.63 2.49 o 5 2 1 145.55 153.33 2.57 o -7 3 1 6.41 6.00 0.98 o -6 3 1 63.42 65.77 1.36 o -5 3 1 19.12 17.26 1.18 o -4 3 1 117.99 145.87 1.76 o -3 3 1 545.44 558.45 4.03 o -2 3 1 1257.99 1268.82 8.24 o -1 3 1 145.62 134.94 1.48 o 0 3 1 26.06 32.87 1.13 o 1 3 1 356.30 356.26 4.63 o 2 3 1 997.27 980.61 10.42 o 3 3 1 311.78 308.63 4.91 o 4 3 1 1.88 1.80 0.81 o -7 4 1 289.29 283.23 5.11 o -6 4 1 0.56 0.50 0.41 o -5 4 1 213.73 201.40 3.58 o -4 4 1 567.88 572.54 6.77 o -3 4 1 374.54 420.92 3.43 o -2 4 1 14.07 15.42 0.59 o -1 4 1 152.14 137.68 3.45 o 0 4 1 712.41 715.83 5.55 o 1 4 1 6.95 6.86 1.37 o 2 4 1 4.82 5.13 0.57 o 3 4 1 178.13 179.96 2.63 o 4 4 1 186.10 185.79 3.95 o -7 5 1 125.27 130.69 3.43 o -6 5 1 134.63 124.70 3.08 o -5 5 1 82.44 82.62 2.29 o -4 5 1 14.52 14.08 0.99 o -3 5 1 127.32 142.17 1.99 o -2 5 1 206.54 202.45 2.30 o -1 5 1 80.13 73.71 1.99 o 0 5 1 220.05 229.87 2.75 o 1 5 1 253.79 254.48 3.07 o 2 5 1 80.72 88.62 1.87 o 3 5 1 1.63 0.78 0.66 o -7 6 1 2.12 0.99 0.80 o -6 6 1 130.73 131.62 3.23 o -5 6 1 213.02 207.54 3.96 o -4 6 1 90.34 88.11 2.37 o -3 6 1 1.09 1.02 0.45 o -2 6 1 33.60 36.85 1.06 o -1 6 1 112.84 113.85 1.91 o 0 6 1 4.04 3.15 0.55 o 1 6 1 29.81 31.05 1.52 o 2 6 1 139.73 141.07 3.65 o -6 7 1 4.82 5.41 0.96 o -5 7 1 51.03 52.61 2.05 o -4 7 1 184.88 190.15 3.77 o -3 7 1 66.49 68.98 1.51 o -2 7 1 2.46 2.78 0.75 o -1 7 1 34.08 38.41 3.32 o 0 7 1 132.28 137.76 3.58 o -5 8 1 24.30 20.91 1.51 o -4 8 1 4.14 2.46 0.83 o -3 8 1 23.86 29.95 1.19 o -2 8 1 34.31 32.86 1.76 o 2 -8 2 102.35 110.58 3.15 o 3 -8 2 15.03 12.72 1.24 o 4 -8 2 12.45 17.78 1.39 o -1 -7 2 33.89 37.08 1.98 o 0 -7 2 42.65 44.31 2.04 o 1 -7 2 2.85 0.76 0.70 o 2 -7 2 93.98 88.79 2.56 o 3 -7 2 15.98 18.00 0.86 o 4 -7 2 53.85 51.67 1.91 o 5 -7 2 32.44 31.40 1.62 o 6 -7 2 41.04 40.57 1.97 o -2 -6 2 2.77 1.94 0.78 o -1 -6 2 31.46 34.63 1.75 o 0 -6 2 379.53 377.22 5.71 o 1 -6 2 172.87 188.89 4.06 o 2 -6 2 23.08 24.97 2.04 o 3 -6 2 20.81 22.09 0.85 o 4 -6 2 59.65 64.24 1.98 o 5 -6 2 73.98 80.43 2.41 o 6 -6 2 1.12 0.52 0.70 o -3 -5 2 88.46 89.05 2.67 o -2 -5 2 69.51 70.29 2.22 o -1 -5 2 1.11 2.79 0.61 o 0 -5 2 4.58 3.76 0.50 o 1 -5 2 822.99 859.43 6.36 o 2 -5 2 187.63 188.92 2.77 o 3 -5 2 43.29 41.62 0.99 o 4 -5 2 1.62 2.63 0.65 o 5 -5 2 156.96 156.76 3.28 o 6 -5 2 338.86 343.73 5.63 o -4 -4 2 238.39 242.49 4.47 o -3 -4 2 46.98 51.11 1.86 o -2 -4 2 29.47 29.40 1.29 o -1 -4 2 529.65 539.67 6.41 o 0 -4 2 204.33 223.09 2.23 o 1 -4 2 454.65 475.58 3.80 o 2 -4 2 121.48 114.20 1.48 o 3 -4 2 113.07 113.85 1.51 o 4 -4 2 48.51 50.16 1.60 o 5 -4 2 1.95 2.68 0.62 o 6 -4 2 205.47 195.33 3.98 o 7 -4 2 115.00 121.66 3.41 o -5 -3 2 1.57 0.51 0.54 o -4 -3 2 174.41 188.67 3.54 o -3 -3 2 130.49 131.41 1.85 o -2 -3 2 0.67 1.35 0.36 o -1 -3 2 182.06 193.72 1.91 o 0 -3 2 1394.53 1468.18 9.44 o 1 -3 2 1.92 5.15 0.39 o 2 -3 2 105.90 106.59 1.29 o 3 -3 2 378.97 357.80 3.03 o 4 -3 2 1225.92 1269.50 12.68 o 5 -3 2 367.25 360.31 5.24 o 6 -3 2 25.15 27.43 1.50 o -5 -2 2 163.48 150.96 3.08 o -4 -2 2 2.17 2.30 1.06 o -3 -2 2 125.37 113.62 1.54 o -2 -2 2 3393.90 3405.58 22.95 o -1 -2 2 694.95 696.73 5.56 o 0 -2 2 83.17 94.19 0.97 o 1 -2 2 681.99 723.14 5.94 o 2 -2 2 138.78 126.18 1.35 o 3 -2 2 336.98 345.46 2.93 o 4 -2 2 23.12 27.20 0.57 o 5 -2 2 550.50 556.48 7.13 o 6 -2 2 83.63 90.80 2.66 o -6 -1 2 15.69 16.57 1.13 o -5 -1 2 165.34 159.74 2.16 o -4 -1 2 79.68 81.18 1.06 o -3 -1 2 12.01 13.61 0.40 o -2 -1 2 989.89 1059.44 6.88 o -1 -1 2 1921.68 1992.03 17.77 o 0 -1 2 70.35 68.74 0.65 o 1 -1 2 518.40 558.85 3.83 o 2 -1 2 444.10 458.66 7.41 o 3 -1 2 1048.14 1058.44 5.60 o 4 -1 2 316.03 324.48 4.63 o 5 -1 2 10.90 9.57 1.02 o 6 -1 2 274.14 283.18 5.09 o -6 0 2 136.23 143.20 2.17 o -5 0 2 102.05 105.68 1.65 o -4 0 2 590.74 579.74 3.60 o -3 0 2 1786.66 1886.05 9.42 o -2 0 2 670.57 728.87 5.95 o -1 0 2 223.58 238.30 3.17 o 0 0 2 363.43 351.95 2.50 o 1 0 2 1640.30 1549.95 10.41 o 2 0 2 1.19 2.31 0.43 o 3 0 2 57.87 57.67 0.89 o 4 0 2 945.75 957.64 10.38 o 5 0 2 137.88 143.37 3.26 o 6 0 2 5.06 3.08 0.96 o -7 1 2 1.35 1.21 0.87 o -6 1 2 238.37 236.38 2.78 o -5 1 2 315.62 321.92 3.09 o -4 1 2 3.99 3.17 0.34 o -3 1 2 713.27 682.60 4.69 o -2 1 2 306.12 333.87 2.48 o -1 1 2 203.47 186.08 1.49 o 0 1 2 907.16 995.11 9.31 o 1 1 2 750.96 776.55 5.47 o 2 1 2 1619.67 1588.54 14.88 o 3 1 2 268.57 268.18 4.06 o 4 1 2 3.67 2.78 0.69 o 5 1 2 132.77 138.02 3.36 o -7 2 2 93.61 86.20 2.70 o -6 2 2 39.94 39.28 1.58 o -5 2 2 253.33 258.84 3.09 o -4 2 2 972.21 988.99 6.73 o -3 2 2 19.30 20.54 0.56 o -2 2 2 1252.03 1318.07 12.52 o -1 2 2 67.29 75.16 1.45 o 0 2 2 7.36 10.60 0.73 o 1 2 2 2.71 3.59 0.55 o 2 2 2 413.66 403.58 5.27 o 4 2 2 4.40 4.20 0.64 o 5 2 2 5.99 6.07 0.94 o -7 3 2 229.14 219.36 5.13 o -6 3 2 21.80 23.83 0.87 o -5 3 2 84.98 82.03 1.42 o -4 3 2 750.50 777.55 5.66 o -3 3 2 1075.10 1078.55 8.38 o -2 3 2 539.36 525.90 6.05 o -1 3 2 149.91 163.93 2.62 o 0 3 2 199.66 177.81 2.95 o 1 3 2 1072.53 1057.68 10.90 o 2 3 2 107.70 105.41 2.56 o 3 3 2 24.12 24.81 1.43 o 4 3 2 102.73 112.54 3.15 o -7 4 2 45.02 51.36 1.38 o -6 4 2 205.36 206.93 3.22 o -5 4 2 249.80 251.42 2.76 o -4 4 2 10.99 12.86 0.95 o -3 4 2 147.53 144.96 2.11 o -2 4 2 26.36 22.59 0.66 o -1 4 2 368.00 363.11 4.76 o 0 4 2 67.33 71.07 2.04 o 1 4 2 138.05 133.32 2.95 o 2 4 2 350.22 344.48 5.38 o 3 4 2 0.69 0.94 0.78 o -7 5 2 19.58 20.76 1.39 o -6 5 2 31.41 31.40 1.58 o -5 5 2 567.97 558.21 7.19 o -4 5 2 53.14 47.16 1.64 o -3 5 2 5.25 6.52 0.50 o -2 5 2 136.52 129.13 1.80 o -1 5 2 500.06 490.36 5.03 o 0 5 2 480.52 506.66 4.68 o 1 5 2 0.49 0.67 0.45 o 2 5 2 9.98 11.26 0.81 o -7 6 2 83.41 75.16 2.66 o -6 6 2 73.05 63.54 2.27 o -5 6 2 1.81 0.73 0.58 o -4 6 2 113.16 110.37 2.63 o -3 6 2 37.29 37.78 1.04 o -2 6 2 60.17 62.49 1.38 o -1 6 2 2.78 2.44 0.54 o 0 6 2 132.08 133.27 2.27 o 1 6 2 244.41 248.90 3.38 o -6 7 2 75.93 77.04 2.59 o -5 7 2 17.04 18.49 1.38 o -4 7 2 100.47 95.04 2.66 o -3 7 2 89.11 79.31 1.64 o -2 7 2 47.62 51.63 1.40 o -1 7 2 42.28 44.60 1.39 o 0 7 2 1.87 0.45 0.56 o -4 8 2 27.40 28.51 1.65 o -3 8 2 27.39 29.24 1.65 o -2 8 2 5.01 5.54 0.72 o 2 -8 3 24.34 25.77 1.67 o 3 -8 3 12.78 15.02 1.34 o -1 -7 3 0.20 -0.21 0.73 o 0 -7 3 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1.58 o -3 5 10 104.65 108.02 3.47 o -2 5 10 57.20 52.47 2.66 o -1 -5 11 0.29 -0.95 0.72 o 0 -5 11 17.08 15.94 1.45 o 1 -5 11 0.44 1.42 0.84 o 2 -5 11 83.78 89.14 3.06 o -2 -4 11 254.13 244.92 3.14 o -1 -4 11 203.28 189.08 4.14 o 0 -4 11 1.93 0.89 0.74 o 1 -4 11 10.85 9.92 1.21 o 2 -4 11 81.70 80.66 2.79 o -3 -3 11 143.74 134.70 3.68 o -2 -3 11 0.63 0.44 0.37 o -1 -3 11 75.74 75.92 2.46 o 0 -3 11 3.58 3.65 0.87 o 1 -3 11 196.30 187.61 4.12 o 2 -3 11 2.00 2.20 0.81 o 3 -3 11 72.40 71.10 2.68 o -4 -2 11 23.04 22.78 1.34 o -3 -2 11 366.54 344.09 4.93 o -2 -2 11 41.14 41.05 1.12 o -1 -2 11 1.20 3.01 0.78 o 0 -2 11 209.69 205.23 4.13 o 1 -2 11 423.06 411.36 6.46 o 2 -2 11 202.91 184.26 4.12 o 3 -2 11 33.37 31.55 1.28 o -5 -1 11 246.90 248.33 4.56 o -4 -1 11 184.32 179.50 3.51 o -3 -1 11 46.42 44.48 1.19 o -2 -1 11 50.63 54.13 1.24 o -1 -1 11 4.43 3.11 0.76 o 0 -1 11 387.33 379.32 5.93 o 1 -1 11 12.92 13.61 0.84 o 2 -1 11 226.60 215.77 3.13 o -5 0 11 18.55 21.07 1.35 o -4 0 11 491.94 489.33 6.35 o -3 0 11 80.77 84.43 1.57 o -2 0 11 37.50 38.10 1.04 o -1 0 11 134.65 139.17 3.19 o 0 0 11 249.34 250.62 3.22 o 1 0 11 139.89 124.65 4.83 o 2 0 11 0.66 0.16 0.50 o -5 1 11 9.48 9.07 0.98 o -4 1 11 17.60 16.79 1.10 o -3 1 11 344.83 360.62 3.59 o -2 1 11 57.50 58.53 2.05 o -1 1 11 223.98 220.61 2.97 o 0 1 11 2.88 2.77 0.58 o 1 1 11 296.79 292.90 3.81 o 2 1 11 142.70 142.42 3.87 o -5 2 11 377.00 365.08 5.53 o -4 2 11 8.05 10.48 0.96 o -3 2 11 24.02 27.00 0.82 o -2 2 11 162.55 160.79 2.53 o -1 2 11 412.26 417.91 6.57 o 0 2 11 97.50 89.12 2.93 o 1 2 11 20.60 15.76 1.56 o -5 3 11 3.81 5.18 0.88 o -4 3 11 105.98 110.69 2.02 o -3 3 11 0.86 1.84 0.98 o -2 3 11 178.66 180.71 4.23 o -1 3 11 54.45 53.56 2.51 o 0 3 11 376.62 388.39 6.87 o -5 4 11 2.24 3.80 1.33 o -4 4 11 28.85 29.25 1.86 o -3 4 11 82.15 85.77 3.04 o -2 4 11 169.27 192.45 4.65 o -1 4 11 15.61 16.61 1.80 o -1 -4 12 12.82 13.56 1.34 o 0 -4 12 107.72 107.48 3.23 o 1 -4 12 108.17 115.38 3.40 o -3 -3 12 5.07 5.68 0.64 o -2 -3 12 183.54 182.33 2.56 o -1 -3 12 46.82 49.06 2.15 o 0 -3 12 28.16 27.68 1.64 o 1 -3 12 78.33 80.39 2.78 o 2 -3 12 225.75 231.88 4.96 o -3 -2 12 7.52 9.28 0.71 o -2 -2 12 2.20 2.56 0.88 o -1 -2 12 171.86 177.48 3.94 o 0 -2 12 334.86 321.65 5.63 o 1 -2 12 28.29 27.76 1.68 o 2 -2 12 3.40 4.54 1.00 o -4 -1 12 9.89 11.44 1.05 o -3 -1 12 218.64 232.19 2.91 o -2 -1 12 4.95 7.53 0.95 o -1 -1 12 18.22 23.54 1.51 o 0 -1 12 240.83 242.63 4.72 o 1 -1 12 422.45 433.50 6.98 o 2 -1 12 17.37 13.63 0.97 o -5 0 12 245.01 237.93 4.42 o -4 0 12 0.49 1.47 0.61 o -3 0 12 27.66 27.71 0.99 o -2 0 12 439.73 451.09 6.58 o -1 0 12 189.37 191.03 4.03 o 0 0 12 15.65 13.45 1.27 o 1 0 12 2.42 3.97 0.66 o -5 1 12 2.85 2.86 0.76 o -4 1 12 214.44 217.35 3.90 o -3 1 12 78.21 86.92 1.68 o -2 1 12 110.53 110.00 2.92 o -1 1 12 242.66 241.83 3.96 o 0 1 12 202.60 216.19 3.21 o 1 1 12 0.53 1.40 1.00 o -5 2 12 2.25 0.55 0.66 o -4 2 12 36.47 40.19 1.72 o -2 2 12 80.32 82.11 1.99 o -1 2 12 0.37 -0.26 1.13 o 0 2 12 38.41 33.95 2.09 o -4 3 12 8.54 8.73 0.98 o -3 3 12 4.77 4.32 1.25 o -2 3 12 179.18 187.46 4.46 o -1 3 12 254.57 279.77 5.73 o -1 -3 13 17.94 19.16 1.54 o 0 -3 13 224.56 226.49 4.89 o -3 -2 13 51.90 50.12 1.41 o -2 -2 13 169.81 179.22 4.07 o -1 -2 13 6.18 5.16 0.96 o 0 -2 13 4.58 4.67 0.99 o 1 -2 13 192.39 186.12 4.40 o -3 -1 13 30.29 28.60 1.67 o -2 -1 13 1.32 2.17 0.77 o -1 -1 13 288.77 298.13 5.41 o 0 -1 13 212.40 228.79 4.79 o -4 0 13 53.85 58.32 2.02 o -3 0 13 283.24 293.31 5.13 o -2 0 13 5.81 5.91 0.94 o -1 0 13 1.71 0.89 0.77 o 0 0 13 130.01 131.25 3.52 o -4 1 13 3.10 3.30 0.77 o -2 1 13 557.55 550.60 7.80 o -1 1 13 110.52 118.13 3.28 o 0 1 13 70.16 88.45 2.11 o -4 2 13 175.73 189.82 3.77 o -2 2 13 5.01 4.78 0.91 o