#------------------------------------------------------------------------------ #$Date: 2011-07-04 21:24:21 +0300 (Mon, 04 Jul 2011) $ #$Revision: 22560 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2230299.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230299_Fobs loop_ _publ_author_name 'Gelbrich, Thomas' 'Haddow, Mairi F.' 'Griesser, Ulrich J.' _publ_section_title ; Benzylsulfamide ; _journal_coeditor_code EZ2246 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1551 _journal_page_last o1552 _journal_volume 67 _journal_year 2011 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.8426 _cell_length_b 10.5549 _cell_length_c 14.6694 _exptl_crystal_F_000 552.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file ez2246Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' s92 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 81.09 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 6.60 5.02 1.27 o 6 0 0 93.12 79.66 3.69 o 8 0 0 81.54 81.73 6.39 o 1 1 0 1948.74 1835.33 57.03 o 2 1 0 3456.78 3178.50 56.81 o 3 1 0 199.71 236.49 3.50 o 4 1 0 168.78 157.29 2.53 o 5 1 0 18.80 24.80 1.26 o 6 1 0 1282.38 1324.96 14.96 o 7 1 0 537.66 535.85 8.03 o 8 1 0 597.75 625.86 14.65 o 9 1 0 109.31 105.00 5.49 o 3 2 0 321.44 285.88 3.85 o 4 2 0 128.38 134.70 4.13 o 5 2 0 1018.23 1000.71 12.03 o 6 2 0 0.00 3.09 1.12 o 7 2 0 43.14 42.58 1.86 o 8 2 0 520.70 539.66 13.13 o 9 2 0 5.47 10.90 2.49 o 1 3 0 689.78 626.06 7.47 o 2 3 0 89.71 112.23 1.79 o 3 3 0 1490.70 1468.57 16.06 o 4 3 0 7.71 6.69 0.86 o 5 3 0 34.91 37.52 1.72 o 6 3 0 1.70 4.45 1.12 o 7 3 0 741.74 765.24 12.94 o 8 3 0 5.08 4.08 1.44 o 9 3 0 49.41 39.72 2.77 o 0 4 0 1665.97 1620.52 42.98 o 1 4 0 73.94 76.44 1.42 o 2 4 0 507.84 526.89 6.86 o 3 4 0 1631.51 1722.90 18.81 o 4 4 0 3157.23 3272.71 30.93 o 5 4 0 520.45 544.84 6.52 o 6 4 0 1980.28 2097.09 27.78 o 7 4 0 57.34 52.87 2.29 o 8 4 0 18.25 17.26 1.35 o 9 4 0 343.18 360.45 24.20 o 1 5 0 456.78 444.32 5.47 o 2 5 0 3723.55 3724.65 40.90 o 3 5 0 247.00 260.41 4.07 o 4 5 0 1276.28 1279.95 13.70 o 5 5 0 53.49 55.15 1.53 o 6 5 0 212.83 209.69 4.48 o 7 5 0 3.55 1.94 0.96 o 8 5 0 98.55 111.81 4.93 o 0 6 0 1565.87 1678.66 25.91 o 1 6 0 715.49 645.96 7.03 o 2 6 0 1.36 4.24 0.72 o 3 6 0 106.15 127.67 3.69 o 4 6 0 2639.92 2657.70 31.37 o 5 6 0 2767.74 2861.17 36.68 o 6 6 0 1576.24 1593.60 29.65 o 7 6 0 13.76 10.03 1.54 o 8 6 0 24.76 32.45 2.74 o 1 7 0 670.00 711.06 9.99 o 2 7 0 1020.10 990.27 11.21 o 3 7 0 5218.99 5470.77 63.57 o 4 7 0 149.47 161.09 3.59 o 5 7 0 21.40 25.34 1.71 o 6 7 0 0.47 3.61 1.11 o 7 7 0 266.79 261.77 8.44 o 8 7 0 35.27 33.78 3.19 o 0 8 0 139.33 142.91 5.94 o 1 8 0 175.35 147.74 5.27 o 2 8 0 1426.95 1493.10 17.89 o 3 8 0 915.13 936.00 12.84 o 4 8 0 50.25 42.40 1.94 o 5 8 0 1445.81 1488.79 31.02 o 6 8 0 39.68 39.56 1.92 o 7 8 0 143.61 115.62 6.13 o 1 9 0 680.39 688.15 11.59 o 2 9 0 1175.34 1219.34 20.25 o 3 9 0 1406.01 1425.94 26.50 o 4 9 0 707.87 703.88 15.42 o 5 9 0 17.33 17.17 1.36 o 6 9 0 24.20 18.88 2.04 o 0 10 0 1294.51 1388.26 51.12 o 1 10 0 16.02 20.64 1.89 o 2 10 0 270.25 271.95 9.19 o 3 10 0 350.62 328.77 7.75 o 4 10 0 171.34 166.15 4.36 o 5 10 0 3.80 2.00 1.34 o 6 10 0 0.67 0.00 2.39 o 1 11 0 54.00 67.46 5.75 o 2 11 0 1058.76 1010.07 33.17 o 3 11 0 751.18 748.77 24.34 o 4 11 0 119.41 123.01 4.99 o 5 11 0 15.27 10.63 1.68 o 0 12 0 484.77 445.66 31.47 o 1 12 0 830.92 877.89 36.53 o 2 12 0 25.92 18.50 2.58 o 3 12 0 133.37 128.28 7.59 o 3 0 1 0.12 0.00 1.55 o 4 0 1 61.44 61.53 2.07 o 5 0 1 24.73 29.41 2.18 o 6 0 1 2823.93 2901.89 30.16 o 7 0 1 60.21 61.33 2.13 o 8 0 1 168.06 171.06 4.70 o 9 0 1 36.09 39.47 3.21 o -9 1 1 516.12 538.88 18.13 o -8 1 1 915.48 966.52 16.89 o -7 1 1 126.90 131.36 3.64 o -6 1 1 505.00 509.80 7.66 o -5 1 1 715.44 697.63 7.46 o -4 1 1 1584.19 1600.20 17.21 o -3 1 1 439.90 466.92 5.74 o -1 1 1 1897.92 1755.44 75.91 o 1 1 1 1862.09 1699.10 67.05 o 3 1 1 450.11 475.44 6.57 o 4 1 1 1597.35 1642.23 22.94 o 5 1 1 707.59 681.66 7.50 o 6 1 1 497.77 501.41 6.28 o 7 1 1 127.84 139.76 3.27 o 8 1 1 915.31 934.61 18.66 o 9 1 1 531.17 523.28 19.54 o -9 2 1 13.02 10.65 3.68 o -8 2 1 71.87 80.99 3.61 o -7 2 1 1129.95 1175.12 18.51 o -6 2 1 56.95 64.11 2.37 o -5 2 1 521.93 528.87 7.04 o -4 2 1 419.03 437.58 5.56 o -3 2 1 51.10 66.49 1.83 o -2 2 1 1623.59 1599.76 19.59 o 0 2 1 707.93 603.17 73.29 o 2 2 1 1626.90 1602.64 22.70 o 3 2 1 57.21 70.30 1.52 o 4 2 1 415.00 436.76 4.93 o 5 2 1 524.27 534.75 6.31 o 6 2 1 55.04 61.37 2.26 o 7 2 1 1121.54 1147.37 18.36 o 8 2 1 69.27 70.03 3.04 o 9 2 1 12.90 15.12 3.20 o -9 3 1 590.99 638.07 26.54 o -8 3 1 112.58 114.25 4.06 o -7 3 1 519.11 513.28 8.59 o -6 3 1 274.49 261.42 4.42 o -5 3 1 539.04 558.96 6.88 o -4 3 1 2310.99 2438.30 25.05 o -3 3 1 1467.99 1421.28 16.08 o -2 3 1 1543.99 1563.65 17.72 o -1 3 1 4842.39 4914.13 85.10 o 0 3 1 3482.26 3527.88 74.68 o 1 3 1 4934.34 5040.64 70.84 o 2 3 1 1545.69 1532.39 22.46 o 3 3 1 1446.53 1404.51 18.68 o 4 3 1 2329.91 2415.41 26.74 o 5 3 1 534.45 563.31 7.00 o 6 3 1 275.57 261.51 4.32 o 7 3 1 524.58 521.80 9.71 o 8 3 1 116.36 112.25 5.33 o 9 3 1 590.84 613.87 35.71 o -9 4 1 13.35 9.35 1.85 o -8 4 1 223.95 217.61 6.75 o -7 4 1 91.18 91.01 2.76 o -6 4 1 1505.54 1511.76 19.96 o -5 4 1 104.16 99.68 2.35 o -4 4 1 432.46 457.49 4.81 o -3 4 1 1640.54 1641.69 15.52 o -2 4 1 252.65 242.27 2.73 o -1 4 1 369.31 397.77 5.29 o 0 4 1 147.48 154.85 2.20 o 1 4 1 362.28 389.77 5.63 o 2 4 1 273.28 255.69 3.43 o 3 4 1 1641.53 1629.12 19.63 o 4 4 1 423.25 445.06 5.41 o 5 4 1 100.75 102.84 2.92 o 6 4 1 1514.97 1482.35 24.68 o 7 4 1 83.88 83.81 2.75 o 8 4 1 220.29 211.00 7.76 o 9 4 1 13.39 5.56 6.12 o -8 5 1 355.23 359.89 10.44 o -7 5 1 77.08 81.66 2.66 o -6 5 1 12.00 14.86 1.38 o -5 5 1 930.04 897.10 10.22 o -4 5 1 1084.68 1060.48 10.68 o -3 5 1 2034.94 2089.50 22.95 o -2 5 1 288.38 325.83 4.04 o -1 5 1 867.24 907.00 11.22 o 0 5 1 1318.07 1265.98 16.16 o 1 5 1 872.32 913.74 12.83 o 2 5 1 293.31 329.39 4.86 o 3 5 1 2038.28 2084.37 22.61 o 4 5 1 1096.31 1081.51 11.32 o 5 5 1 933.38 902.49 11.32 o 6 5 1 9.72 10.86 1.35 o 7 5 1 78.00 79.37 2.54 o 8 5 1 357.01 387.56 10.93 o -8 6 1 282.36 289.58 10.20 o -7 6 1 1070.07 1064.63 24.79 o -6 6 1 95.96 106.40 2.65 o -5 6 1 1352.50 1344.61 17.41 o -4 6 1 139.91 138.97 3.16 o -3 6 1 67.10 63.25 2.01 o -2 6 1 758.21 706.12 9.46 o -1 6 1 344.06 346.42 5.98 o 0 6 1 15.08 15.17 0.91 o 1 6 1 350.18 356.05 6.45 o 2 6 1 744.63 696.41 8.46 o 3 6 1 65.05 66.89 1.80 o 4 6 1 139.01 142.90 3.22 o 5 6 1 1357.84 1366.00 18.61 o 6 6 1 94.29 102.99 2.64 o 7 6 1 1075.69 1079.45 27.17 o 8 6 1 281.47 295.43 8.18 o -8 7 1 134.75 126.63 7.41 o -7 7 1 265.62 252.42 8.44 o -6 7 1 61.99 52.57 2.06 o -5 7 1 828.26 832.93 13.99 o -4 7 1 1105.68 1153.51 15.13 o -3 7 1 1089.33 1098.47 13.44 o -2 7 1 20.54 24.02 0.95 o -1 7 1 703.00 758.63 8.43 o 0 7 1 0.13 1.01 0.74 o 1 7 1 694.24 727.06 10.67 o 2 7 1 19.51 23.40 1.39 o 3 7 1 1090.87 1074.06 13.13 o 4 7 1 1094.18 1174.09 14.74 o 5 7 1 840.18 831.36 13.29 o 6 7 1 63.86 55.61 2.15 o 7 7 1 262.08 244.19 7.71 o 8 7 1 134.24 126.53 6.90 o -7 8 1 662.87 669.10 25.04 o -6 8 1 261.04 235.82 6.77 o -5 8 1 304.22 310.52 7.17 o -4 8 1 121.15 123.91 2.81 o -3 8 1 1338.09 1338.56 17.72 o -2 8 1 100.34 98.95 2.07 o -1 8 1 160.11 157.04 2.94 o 0 8 1 411.12 424.21 6.44 o 1 8 1 152.65 144.85 4.01 o 2 8 1 106.03 103.29 1.97 o 3 8 1 1315.91 1268.73 35.04 o 4 8 1 119.03 124.54 3.05 o 5 8 1 305.82 315.86 7.02 o 6 8 1 265.94 255.82 7.92 o 7 8 1 675.03 667.25 25.50 o -6 9 1 86.26 81.84 5.33 o -5 9 1 218.59 213.54 6.33 o -4 9 1 1022.82 1054.83 19.81 o -3 9 1 248.06 239.61 5.90 o -2 9 1 190.16 190.99 4.16 o -1 9 1 134.47 134.44 2.88 o 0 9 1 10.60 7.94 0.63 o 1 9 1 131.41 131.09 3.52 o 2 9 1 186.81 188.75 5.84 o 3 9 1 247.25 237.79 5.28 o 4 9 1 1012.78 1010.25 23.20 o 5 9 1 218.06 210.85 5.30 o 6 9 1 91.66 87.63 4.27 o -6 10 1 100.25 95.15 6.56 o -5 10 1 13.23 20.41 3.14 o -4 10 1 22.97 19.16 1.99 o -3 10 1 41.31 40.76 1.84 o -2 10 1 403.17 411.05 10.64 o -1 10 1 809.20 820.06 19.33 o 0 10 1 21.12 18.27 1.82 o 1 10 1 811.48 796.22 26.29 o 2 10 1 390.06 378.06 10.94 o 3 10 1 42.27 44.72 2.33 o 4 10 1 20.70 17.71 1.31 o 5 10 1 13.77 16.37 1.41 o 6 10 1 100.94 97.08 6.44 o -5 11 1 133.04 117.08 7.66 o -4 11 1 127.57 111.52 5.21 o -3 11 1 248.76 261.31 7.85 o -2 11 1 40.00 34.78 2.88 o -1 11 1 169.37 161.90 7.73 o 0 11 1 72.78 79.14 3.81 o 1 11 1 161.28 158.54 9.60 o 2 11 1 41.37 40.34 3.25 o 3 11 1 246.05 246.32 11.84 o 4 11 1 129.49 123.40 6.40 o 5 11 1 127.41 115.85 6.02 o -3 12 1 243.41 254.18 12.89 o -2 12 1 75.37 72.08 3.89 o -1 12 1 293.27 296.10 13.94 o 0 12 1 921.14 920.13 46.51 o 1 12 1 305.12 313.52 15.15 o 2 12 1 73.03 62.27 5.02 o 3 12 1 247.59 274.51 26.02 o 0 13 1 20.87 18.47 2.75 o 1 0 2 450.73 417.86 7.84 o 2 0 2 12.93 7.96 0.81 o 3 0 2 0.03 0.32 0.71 o 4 0 2 1022.05 966.16 10.74 o 5 0 2 0.33 1.10 0.98 o 6 0 2 1578.13 1641.48 17.72 o 7 0 2 238.91 247.35 3.89 o 8 0 2 368.28 380.96 8.50 o 9 0 2 4.44 6.71 2.36 o -9 1 2 97.47 108.49 5.86 o -8 1 2 380.11 400.66 9.78 o -7 1 2 1137.30 1172.69 18.95 o -6 1 2 2044.46 2153.64 23.60 o -5 1 2 34.35 34.18 1.29 o -4 1 2 324.94 327.59 4.38 o -3 1 2 24.32 16.12 1.26 o -2 1 2 2150.10 1913.37 24.14 o -1 1 2 1288.50 1199.70 41.62 o 1 1 2 1308.53 1262.38 51.49 o 2 1 2 2191.11 1951.17 26.62 o 3 1 2 22.34 14.00 0.92 o 4 1 2 329.41 330.64 3.85 o 5 1 2 31.74 34.70 1.78 o 6 1 2 2059.87 2145.39 21.71 o 7 1 2 1129.97 1148.22 16.37 o 8 1 2 380.42 391.27 10.14 o 9 1 2 96.78 102.12 6.77 o -9 2 2 54.09 47.26 3.65 o -8 2 2 345.41 330.08 8.93 o -7 2 2 87.80 88.08 2.50 o -6 2 2 333.98 352.98 5.24 o -5 2 2 1243.57 1242.38 13.12 o -4 2 2 1986.52 2134.90 23.45 o -3 2 2 336.93 380.23 4.70 o -2 2 2 1381.72 1359.21 14.61 o -1 2 2 801.34 739.66 16.41 o 1 2 2 779.76 739.71 22.54 o 2 2 2 1396.27 1378.87 18.92 o 3 2 2 338.65 387.40 4.53 o 4 2 2 1994.59 2125.35 23.38 o 5 2 2 1232.93 1222.08 11.59 o 6 2 2 334.67 350.64 6.32 o 7 2 2 85.81 85.64 2.23 o 8 2 2 337.81 326.88 13.05 o 9 2 2 46.04 52.28 4.54 o -9 3 2 17.12 23.15 3.06 o -8 3 2 209.58 221.58 6.23 o -7 3 2 457.80 474.46 8.89 o -6 3 2 349.55 327.92 5.14 o -5 3 2 108.74 120.45 2.90 o -4 3 2 778.74 787.77 8.63 o -3 3 2 2073.50 2168.65 22.70 o -2 3 2 55.65 66.08 1.58 o -1 3 2 696.61 666.22 9.02 o 0 3 2 0.45 0.00 0.49 o 1 3 2 718.57 662.28 12.81 o 2 3 2 56.42 67.51 1.66 o 3 3 2 2134.60 2202.38 29.63 o 4 3 2 785.32 800.92 10.11 o 5 3 2 107.65 114.75 2.33 o 6 3 2 347.33 324.45 5.77 o 7 3 2 461.04 497.28 10.19 o 8 3 2 205.66 203.24 6.58 o 9 3 2 16.69 20.11 4.94 o -9 4 2 64.43 75.46 5.34 o -8 4 2 349.26 322.81 9.43 o -7 4 2 538.73 524.46 10.83 o -6 4 2 400.95 430.52 7.28 o -5 4 2 190.84 188.15 3.08 o -4 4 2 545.52 594.36 7.14 o -3 4 2 1552.72 1617.66 17.40 o -2 4 2 441.70 472.72 4.89 o -1 4 2 3.14 2.36 0.49 o 0 4 2 5104.99 4971.83 73.76 o 1 4 2 3.07 1.78 0.59 o 2 4 2 442.91 474.03 6.44 o 3 4 2 1567.80 1632.79 21.47 o 4 4 2 522.85 544.83 7.28 o 5 4 2 202.14 198.32 3.34 o 6 4 2 386.88 399.71 6.93 o 7 4 2 532.30 511.74 12.99 o 8 4 2 346.76 342.07 11.80 o 9 4 2 58.75 59.68 10.53 o -8 5 2 105.18 112.90 3.45 o -7 5 2 442.53 406.12 8.64 o -6 5 2 61.16 63.78 1.96 o -5 5 2 542.16 579.21 7.40 o -4 5 2 107.47 111.16 2.28 o -3 5 2 221.67 245.40 3.58 o -2 5 2 2280.75 2246.49 22.43 o -1 5 2 762.09 792.00 8.89 o 0 5 2 87.41 90.03 2.48 o 1 5 2 753.45 763.00 11.70 o 2 5 2 2302.47 2256.21 24.02 o 3 5 2 222.85 245.98 3.73 o 4 5 2 110.40 115.83 4.29 o 5 5 2 545.35 576.04 8.59 o 6 5 2 69.82 71.05 2.22 o 7 5 2 443.63 412.91 8.57 o 8 5 2 106.01 117.17 4.57 o -8 6 2 96.05 114.19 7.65 o -7 6 2 492.68 490.25 12.98 o -6 6 2 67.98 73.87 1.99 o -5 6 2 698.60 715.51 9.77 o -4 6 2 538.43 550.07 6.27 o -3 6 2 239.89 221.96 2.83 o -2 6 2 279.33 285.36 4.14 o -1 6 2 1256.68 1259.04 16.61 o 0 6 2 595.28 617.58 8.42 o 1 6 2 1258.56 1274.50 16.53 o 2 6 2 276.80 265.90 3.93 o 3 6 2 233.59 228.03 3.26 o 4 6 2 542.87 567.21 7.94 o 5 6 2 674.34 689.25 11.04 o 6 6 2 71.28 69.78 2.34 o 7 6 2 490.44 474.96 13.49 o 8 6 2 97.56 105.23 4.81 o -8 7 2 172.09 167.00 9.48 o -7 7 2 90.81 85.98 3.27 o -6 7 2 38.98 38.61 2.15 o -5 7 2 120.81 119.08 2.91 o -4 7 2 61.13 67.25 1.90 o -3 7 2 1792.45 1824.25 21.60 o -2 7 2 199.11 192.17 2.83 o -1 7 2 820.19 846.65 9.37 o 0 7 2 182.87 199.91 3.22 o 1 7 2 817.81 827.10 21.00 o 2 7 2 201.59 194.97 3.08 o 3 7 2 1786.33 1795.28 22.02 o 4 7 2 62.20 65.83 1.79 o 5 7 2 122.98 117.21 2.77 o 6 7 2 36.95 36.84 1.53 o 7 7 2 99.81 101.83 3.78 o 8 7 2 176.02 176.63 8.31 o -7 8 2 63.71 47.73 2.75 o -6 8 2 216.74 198.47 5.86 o -5 8 2 255.87 271.27 6.09 o -4 8 2 165.91 166.55 3.76 o -3 8 2 334.10 340.53 5.17 o -2 8 2 227.56 240.43 4.07 o -1 8 2 506.58 499.70 6.09 o 0 8 2 15.65 20.52 1.37 o 1 8 2 512.09 506.83 9.12 o 2 8 2 221.79 228.96 4.22 o 3 8 2 329.67 333.18 5.69 o 4 8 2 162.53 168.77 3.63 o 5 8 2 253.87 282.91 6.84 o 6 8 2 211.39 199.01 6.52 o 7 8 2 65.52 55.65 3.31 o -6 9 2 13.12 9.33 2.82 o -5 9 2 29.79 26.31 1.39 o -4 9 2 14.89 19.50 1.20 o -3 9 2 304.09 314.19 5.96 o -2 9 2 739.42 756.21 14.07 o -1 9 2 12.01 8.83 0.97 o 0 9 2 36.40 38.77 1.90 o 1 9 2 13.53 11.01 1.58 o 2 9 2 734.10 720.62 18.46 o 3 9 2 302.29 314.42 7.01 o 4 9 2 14.25 16.69 1.11 o 5 9 2 30.31 29.18 2.49 o 6 9 2 14.31 17.49 2.03 o -6 10 2 194.48 213.01 13.58 o -5 10 2 48.75 42.03 2.91 o -4 10 2 476.89 505.89 16.77 o -3 10 2 233.71 224.52 6.64 o -2 10 2 33.91 28.16 1.27 o -1 10 2 116.99 106.80 2.63 o 0 10 2 35.11 36.23 1.91 o 1 10 2 114.61 103.86 3.18 o 2 10 2 34.20 35.04 2.45 o 3 10 2 230.27 222.13 8.40 o 4 10 2 478.37 506.13 15.11 o 5 10 2 47.64 45.06 7.13 o 6 10 2 197.13 216.14 15.42 o -5 11 2 6.33 8.32 4.18 o -4 11 2 94.68 91.29 4.34 o -3 11 2 461.19 456.28 13.78 o -2 11 2 32.86 30.81 1.67 o -1 11 2 45.83 47.05 2.44 o 0 11 2 7.75 11.92 4.72 o 1 11 2 46.33 45.03 2.55 o 2 11 2 38.94 32.58 2.46 o 3 11 2 458.74 451.68 25.78 o 4 11 2 93.93 95.72 4.76 o 5 11 2 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