#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/03/2230309.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230309_Fobs loop_ _publ_author_name 'Gao, Guo-Ran' 'Man, Hong-Xue' 'Xiao, Zhi-Chang' 'Deng, Yu-Heng' _publ_section_title ; Chloridobis(1,10-phenanthroline-\k^2^N,N')copper(II) tetrakis(nitrato-\k^2^O,O')(1,10-phenanthroline-\k^2^N,N')terbate(III) ; _journal_coeditor_code FJ2415 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m787 _journal_page_last m788 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 81.103 _cell_angle_beta 75.631 _cell_angle_gamma 84.465 _cell_length_a 10.1556 _cell_length_b 13.4799 _cell_length_c 14.7710 _exptl_crystal_F_000 1034.00 _reflns_d_resolution_high 0.7592 _[local]_cod_data_source_file fj2415Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'a in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 255.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 15439.58 16264.98 317.36 o 2 0 0 15616.91 14937.05 295.33 o 3 0 0 922.32 972.52 28.18 o 4 0 0 227.21 240.13 12.55 o 5 0 0 19921.36 20161.57 210.90 o 6 0 0 2672.43 2809.39 88.12 o 7 0 0 319.16 294.19 36.49 o 8 0 0 80.81 80.28 21.83 o 9 0 0 1687.87 1668.96 62.16 o 10 0 0 0.42 38.55 33.04 o 11 0 0 129.70 31.67 33.73 o 12 0 0 544.94 619.57 60.58 o -10 1 0 616.80 623.01 55.76 o -9 1 0 608.04 666.54 43.00 o -8 1 0 427.13 399.93 33.73 o -7 1 0 811.50 838.07 34.12 o -6 1 0 1283.24 1208.30 31.76 o -5 1 0 9.54 22.58 9.40 o -4 1 0 20555.60 20033.74 202.87 o -3 1 0 13618.29 13591.92 251.96 o -2 1 0 8071.31 7817.55 170.04 o -1 1 0 63229.23 63769.17 1236.38 o 0 1 0 0.56 15.14 4.13 o 2 1 0 4821.37 4875.30 118.41 o 3 1 0 4000.94 4207.30 73.00 o 4 1 0 3069.45 2979.82 57.35 o 5 1 0 4049.27 4148.82 60.48 o 6 1 0 994.20 1037.23 74.59 o 7 1 0 605.96 710.57 43.45 o 8 1 0 812.30 870.66 63.65 o 9 1 0 100.82 109.46 31.67 o 10 1 0 670.58 687.72 59.20 o 11 1 0 340.05 322.86 49.57 o 12 1 0 1.20 15.83 37.86 o -10 2 0 489.62 562.91 42.39 o -9 2 0 332.81 351.94 33.69 o -8 2 0 669.98 780.97 41.90 o -7 2 0 14.64 7.21 11.45 o -6 2 0 105.50 102.94 23.65 o -5 2 0 26453.23 26125.23 232.90 o -4 2 0 920.91 953.00 26.82 o -3 2 0 33926.88 33566.70 474.30 o -2 2 0 2725.87 2821.09 81.92 o 0 2 0 21678.20 22657.53 438.51 o 1 2 0 11316.32 11298.03 163.41 o 2 2 0 40.66 48.19 15.83 o 3 2 0 1971.14 1988.81 72.97 o 4 2 0 5660.88 5906.26 74.82 o 5 2 0 3059.38 3066.09 49.77 o 6 2 0 5925.04 6143.11 116.17 o 7 2 0 980.70 1010.41 41.42 o 8 2 0 942.08 946.26 39.30 o 9 2 0 4369.89 4311.49 139.06 o 10 2 0 397.83 360.73 47.50 o 11 2 0 102.04 53.01 34.42 o 12 2 0 629.29 687.03 68.84 o -12 3 0 124.33 142.50 55.76 o -11 3 0 81.11 102.57 48.19 o -10 3 0 404.06 392.39 67.46 o -9 3 0 1786.35 1807.07 111.52 o -8 3 0 166.24 170.59 30.13 o -7 3 0 2140.57 2131.78 59.40 o -6 3 0 8553.11 8419.02 124.46 o -5 3 0 4543.71 4445.86 71.64 o -4 3 0 19595.28 18746.72 291.94 o -3 3 0 341.43 411.91 25.47 o -2 3 0 650.38 730.17 30.18 o -1 3 0 8081.78 8318.02 187.25 o 0 3 0 673.43 646.49 24.78 o 1 3 0 12201.72 11915.61 244.04 o 2 3 0 13126.78 13118.28 192.79 o 3 3 0 10735.93 10629.01 307.03 o 4 3 0 55.93 42.54 7.72 o 5 3 0 5059.38 5298.24 63.11 o 6 3 0 516.47 557.29 26.33 o 7 3 0 548.87 532.54 37.74 o 8 3 0 8183.56 8487.33 162.46 o 9 3 0 758.78 810.63 171.07 o 10 3 0 1098.10 1162.03 75.04 o 11 3 0 813.39 855.00 69.53 o 12 3 0 0.03 4.13 38.55 o -12 4 0 9.56 52.32 53.01 o -11 4 0 167.32 134.93 55.76 o -10 4 0 1443.92 1474.57 112.21 o -9 4 0 60.73 17.90 34.42 o -8 4 0 4327.97 4331.43 120.04 o -7 4 0 553.88 573.98 33.59 o -6 4 0 1250.58 1132.27 34.38 o -5 4 0 5580.28 5190.32 76.69 o -4 4 0 57.11 58.01 15.53 o -3 4 0 5988.33 5912.57 170.04 o -2 4 0 2600.24 2791.16 150.76 o -1 4 0 60.54 81.13 11.68 o 0 4 0 20.27 36.62 10.94 o 1 4 0 127.84 135.81 19.84 o 2 4 0 673.38 763.06 22.57 o 3 4 0 4209.85 4347.74 66.49 o 4 4 0 17640.69 17645.02 391.01 o 5 4 0 864.85 881.87 45.75 o 6 4 0 419.32 407.87 22.53 o 7 4 0 3092.62 3057.77 77.69 o 8 4 0 540.89 591.50 35.08 o 9 4 0 1747.63 1849.48 112.55 o 10 4 0 1126.37 980.98 71.59 o 11 4 0 69.22 82.61 39.93 o 12 4 0 583.01 576.88 66.09 o -12 5 0 136.70 128.73 55.76 o -11 5 0 309.52 271.23 67.46 o -10 5 0 231.34 240.94 60.58 o -9 5 0 1742.33 2037.41 86.50 o -8 5 0 9.92 -3.95 16.90 o -7 5 0 111.31 119.89 21.34 o -6 5 0 1657.68 1649.62 49.23 o -5 5 0 380.79 414.45 30.02 o -4 5 0 6946.54 6970.27 114.26 o -3 5 0 1236.31 1149.70 41.07 o -2 5 0 20.23 16.09 8.12 o -1 5 0 3706.40 3795.98 56.16 o 0 5 0 2433.00 2581.99 50.18 o 1 5 0 768.91 783.54 26.41 o 2 5 0 3816.84 3684.12 62.85 o 3 5 0 8772.62 8153.61 124.64 o 4 5 0 236.57 293.53 28.22 o 5 5 0 5432.43 5232.68 88.01 o 6 5 0 4336.64 4503.40 83.83 o 7 5 0 53.07 57.64 16.89 o 8 5 0 2481.56 2732.86 152.48 o 9 5 0 237.58 263.67 37.17 o 10 5 0 520.06 578.26 58.51 o 11 5 0 797.74 810.25 69.53 o 12 5 0 13.38 -0.69 39.24 o -11 6 0 210.29 249.20 66.78 o -10 6 0 529.31 401.34 70.91 o -9 6 0 2.45 -10.70 22.05 o -8 6 0 2018.21 1978.04 68.09 o -7 6 0 2807.40 2787.27 124.63 o -6 6 0 168.84 177.74 23.07 o -5 6 0 3159.52 3124.50 67.85 o -4 6 0 910.85 893.42 45.24 o -3 6 0 1535.88 1706.97 86.06 o -2 6 0 2854.93 3064.07 52.14 o -1 6 0 8352.22 8685.51 108.04 o 0 6 0 486.28 447.40 23.08 o 1 6 0 7012.65 6955.83 84.27 o 2 6 0 3923.38 3603.64 114.76 o 3 6 0 1.98 -0.43 8.60 o 4 6 0 13484.13 13087.28 174.36 o 5 6 0 1945.65 1920.04 48.85 o 6 6 0 1235.06 1190.28 49.65 o 7 6 0 4386.27 4500.54 79.65 o 8 6 0 150.95 127.65 27.46 o 9 6 0 1386.97 1550.98 83.99 o 10 6 0 316.77 363.98 40.73 o 11 6 0 22.72 41.30 37.17 o 12 6 0 117.12 74.35 46.12 o -11 7 0 61.64 60.58 50.94 o -10 7 0 31.04 44.06 39.93 o -9 7 0 886.52 1015.38 51.95 o -8 7 0 749.50 638.79 61.18 o -7 7 0 85.30 58.21 20.25 o -6 7 0 422.92 460.44 32.45 o -5 7 0 847.07 821.41 50.62 o -4 7 0 25.39 57.05 16.26 o -3 7 0 1288.08 1365.00 34.79 o -2 7 0 1823.96 1793.53 40.39 o -1 7 0 860.89 919.94 28.45 o 0 7 0 8539.40 8155.98 105.19 o 1 7 0 3549.52 3443.16 51.80 o 2 7 0 644.69 660.00 28.39 o 3 7 0 7999.75 8015.26 164.01 o 4 7 0 9.43 8.21 21.34 o 5 7 0 7664.47 7586.92 233.71 o 6 7 0 4126.77 4089.60 82.45 o 7 7 0 93.02 48.12 19.49 o 8 7 0 752.82 756.91 40.64 o 9 7 0 78.70 70.44 35.11 o 10 7 0 63.97 26.64 27.28 o 11 7 0 219.42 232.10 39.35 o 12 7 0 303.81 287.07 57.83 o -11 8 0 25.79 15.83 44.75 o -10 8 0 274.36 242.09 35.18 o -9 8 0 141.66 105.60 27.15 o -8 8 0 192.99 217.96 30.80 o -7 8 0 1100.53 1185.48 129.08 o -6 8 0 424.92 350.14 54.73 o -5 8 0 11.93 9.80 15.63 o -4 8 0 1496.53 1475.76 51.87 o -3 8 0 931.25 940.12 48.78 o -2 8 0 384.16 475.79 26.03 o -1 8 0 7552.65 7497.80 111.09 o 0 8 0 371.78 385.22 20.91 o 1 8 0 9497.50 9481.04 101.68 o 2 8 0 9667.14 9459.45 174.44 o 3 8 0 727.26 843.19 49.14 o 4 8 0 5725.12 5748.30 139.45 o 5 8 0 2548.34 2497.65 99.13 o 6 8 0 2850.55 2702.70 96.86 o 7 8 0 3067.79 3192.71 108.55 o 8 8 0 820.58 849.42 65.37 o 9 8 0 22.32 74.72 26.86 o 10 8 0 297.53 271.78 40.37 o 11 8 0 119.84 94.31 44.75 o -10 9 0 15.85 37.29 31.46 o -9 9 0 179.60 225.72 40.26 o -8 9 0 226.24 149.76 38.22 o -7 9 0 46.61 43.44 27.14 o -6 9 0 302.26 461.81 77.10 o -5 9 0 1623.14 1685.62 119.44 o -4 9 0 381.58 392.61 32.99 o -3 9 0 390.45 412.52 30.69 o -2 9 0 4991.31 4953.94 82.04 o -1 9 0 17.25 15.76 10.91 o 0 9 0 12761.14 13364.60 163.85 o 1 9 0 3518.51 3504.44 62.52 o 2 9 0 353.07 387.23 26.96 o 3 9 0 4217.60 4143.35 175.54 o 4 9 0 57.88 43.97 39.93 o 5 9 0 1303.13 1287.08 85.36 o 6 9 0 1118.73 999.19 64.65 o 7 9 0 523.55 552.66 82.61 o 8 9 0 18.11 11.33 28.71 o 9 9 0 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