#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/03/2230347.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230347_Fobs loop_ _publ_author_name 'Zhou, Fu-Lin' 'Du, Zhi-Hua' 'Ng, Seik Weng' _publ_section_title ; catena-Poly[[bis(dimethyl sulfoxide-\kO)cerium(III)]tris(\m~2~-3,5-dinitrobenzoato-\k^2^O:O')] ; _journal_coeditor_code HG5026 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m673 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 101.880 _cell_angle_beta 103.676 _cell_angle_gamma 119.683 _cell_length_a 14.3025 _cell_length_b 14.3752 _cell_length_c 21.9143 _exptl_crystal_F_000 1852.00 _reflns_d_resolution_high 0.8325 _[local]_cod_data_source_file hg5026Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 422.02 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1090.95 997.60 39.05 o 2 0 0 398.28 391.50 49.21 o 3 0 0 1551.23 1676.90 57.16 o 4 0 0 5208.13 5532.14 133.11 o 5 0 0 8267.40 8446.66 190.31 o 6 0 0 11152.91 11322.24 248.29 o 7 0 0 9847.69 9625.35 234.98 o 8 0 0 245.76 163.31 37.84 o 9 0 0 7068.32 6273.41 202.14 o 10 0 0 2.45 19.79 50.18 o 11 0 0 213.87 171.21 79.69 o 12 0 0 701.70 545.80 125.63 o 13 0 0 2626.52 3298.11 267.86 o -14 1 0 747.57 515.41 142.24 o -13 1 0 3149.58 2909.39 249.84 o -12 1 0 1009.98 895.29 144.53 o -11 1 0 683.26 728.50 121.56 o -10 1 0 13366.19 13019.24 326.95 o -9 1 0 471.99 339.34 107.25 o -8 1 0 3640.42 3591.46 146.83 o -7 1 0 419.49 361.62 44.62 o -6 1 0 6054.84 6142.93 162.03 o -5 1 0 2696.02 2617.88 89.87 o -4 1 0 28306.26 28236.47 460.81 o -3 1 0 12222.59 11894.06 212.53 o -2 1 0 8904.37 9584.39 165.80 o 1 1 0 46308.52 49108.52 1041.24 o 2 1 0 8512.96 9496.71 139.92 o 3 1 0 26323.51 25231.40 335.19 o 4 1 0 31.19 109.06 99.48 o 6 1 0 1314.40 1340.02 116.79 o 8 1 0 5416.62 5615.76 276.87 o 9 1 0 2343.83 1968.33 174.75 o 10 1 0 16.70 -25.27 56.54 o 11 1 0 73.96 179.69 80.92 o 12 1 0 2766.00 2466.60 238.36 o 13 1 0 370.39 638.91 155.66 o -14 2 0 3289.18 3684.88 280.58 o -13 2 0 308.17 54.07 77.04 o -12 2 0 467.70 554.50 79.50 o -11 2 0 9292.13 9647.14 281.91 o -10 2 0 1004.75 1007.08 84.69 o -9 2 0 953.74 901.53 74.12 o -8 2 0 848.60 806.31 71.47 o -7 2 0 3473.06 3426.64 120.45 o -6 2 0 190.03 180.57 30.81 o -5 2 0 57065.88 55531.45 1549.14 o -4 2 0 31123.53 32882.18 808.63 o -3 2 0 7585.50 8105.31 154.45 o -2 2 0 11996.28 12204.91 302.14 o -1 2 0 19163.85 19012.01 303.04 o 0 2 0 672.10 665.28 29.42 o 1 2 0 7862.08 9185.33 174.32 o 2 2 0 33836.83 34256.12 436.73 o 3 2 0 435.62 348.18 25.64 o 4 2 0 24840.32 24358.72 342.37 o 5 2 0 8.22 14.11 12.88 o 6 2 0 5362.82 5462.23 155.98 o 7 2 0 5525.41 5439.60 267.86 o 8 2 0 1669.96 1595.69 159.02 o 9 2 0 829.54 1041.59 143.65 o 10 2 0 967.26 1002.01 148.77 o 11 2 0 2605.09 2588.34 239.24 o 12 2 0 109.35 -27.56 64.67 o -15 3 0 3367.38 3520.03 279.88 o -14 3 0 116.05 -59.37 65.02 o -13 3 0 348.65 239.90 63.35 o -12 3 0 2670.38 2808.30 150.79 o -11 3 0 5021.16 5057.95 190.19 o -10 3 0 2326.82 2369.54 119.99 o -9 3 0 4846.26 5285.64 174.19 o -8 3 0 5042.05 4867.54 156.32 o -7 3 0 154.94 132.49 29.42 o -6 3 0 36842.22 35865.56 1187.10 o -5 3 0 20932.30 21102.86 368.17 o -4 3 0 35760.76 36007.56 563.49 o -3 3 0 2006.30 2210.75 99.83 o -2 3 0 20551.21 20492.48 338.08 o -1 3 0 520.38 490.26 21.14 o 0 3 0 4049.44 4393.61 104.76 o 1 3 0 18681.93 19928.62 343.68 o 2 3 0 2193.52 2227.76 82.14 o 3 3 0 30990.80 31469.39 420.59 o 4 3 0 1701.43 1694.13 62.85 o 5 3 0 24.11 41.43 21.93 o 6 3 0 11919.21 12004.14 374.58 o 7 3 0 3549.92 4027.66 238.18 o 8 3 0 4184.64 4237.57 258.68 o 9 3 0 5726.96 6289.66 343.13 o 10 3 0 3232.06 3462.25 266.45 o 11 3 0 67.30 -14.31 85.16 o -15 4 0 78.85 162.20 95.59 o -14 4 0 1373.13 1612.79 132.32 o -13 4 0 145.02 70.18 102.39 o -12 4 0 3003.36 2761.60 194.62 o -10 4 0 5785.07 5935.78 194.37 o -9 4 0 3176.43 3305.56 130.92 o -8 4 0 15.36 17.52 26.50 o -7 4 0 16521.87 16554.97 326.15 o -6 4 0 11866.36 11471.14 237.04 o -5 4 0 41908.19 42234.86 664.44 o -4 4 0 441.57 300.57 85.25 o -3 4 0 69000.98 69178.06 1056.02 o -2 4 0 12641.51 13823.81 197.84 o -1 4 0 9086.31 9427.38 146.31 o 0 4 0 7243.47 7797.70 170.46 o 1 4 0 7.27 -4.93 11.05 o 2 4 0 30510.29 30668.05 525.15 o 3 4 0 1105.86 1311.74 95.06 o 4 4 0 730.46 616.30 78.45 o 5 4 0 1615.83 1664.79 112.11 o 6 4 0 4728.52 4296.06 244.36 o 7 4 0 3375.29 3774.11 242.95 o 8 4 0 10962.60 11404.32 474.77 o 9 4 0 1183.08 1269.17 174.39 o 10 4 0 279.81 374.05 121.56 o -15 5 0 779.36 911.52 111.38 o -14 5 0 27.73 -10.03 43.64 o -13 5 0 1627.87 1651.72 121.44 o -12 5 0 284.96 240.90 58.29 o -11 5 0 7238.54 7609.53 231.61 o -10 5 0 392.93 392.95 57.12 o -9 5 0 1328.46 1361.72 84.12 o -8 5 0 1086.03 1012.03 67.80 o -7 5 0 2018.45 2234.82 88.39 o -6 5 0 20325.28 20798.97 368.15 o -5 5 0 2072.91 2116.37 80.04 o -4 5 0 72864.12 71325.35 1426.69 o -3 5 0 2507.37 2271.33 184.17 o -2 5 0 52692.43 51094.48 642.62 o -1 5 0 1197.36 1128.79 39.68 o 0 5 0 2670.81 2941.63 100.58 o 1 5 0 15400.23 16541.79 404.53 o 2 5 0 3480.67 3284.22 211.32 o 3 5 0 246.07 278.66 98.95 o 4 5 0 5899.15 5864.54 186.21 o 5 5 0 3832.48 3377.76 274.93 o 6 5 0 994.11 817.61 84.38 o 7 5 0 6720.22 7062.17 270.16 o 8 5 0 91.49 -39.40 49.30 o 9 5 0 78.22 77.57 87.46 o 10 5 0 883.09 918.08 173.51 o -16 6 0 349.17 365.57 138.17 o -15 6 0 1963.32 2016.22 222.81 o -14 6 0 3044.29 3283.39 189.77 o -13 6 0 167.44 112.90 94.09 o -12 6 0 5095.18 5246.32 194.50 o -11 6 0 455.14 402.81 69.26 o -10 6 0 4450.24 4420.59 157.93 o -9 6 0 3840.32 3663.22 233.23 o -8 6 0 6507.80 6991.18 207.62 o -7 6 0 402.73 287.60 107.52 o -6 6 0 236.25 320.22 37.95 o -5 6 0 53083.99 54484.03 874.99 o -4 6 0 15.04 12.47 12.56 o -3 6 0 48684.05 47647.81 611.19 o -2 6 0 5170.81 5689.86 198.84 o -1 6 0 3087.46 3188.10 287.93 o 0 6 0 2233.75 2633.04 104.07 o 1 6 0 7373.99 7449.70 199.67 o 2 6 0 2972.92 2674.60 116.63 o 3 6 0 15000.97 15919.98 437.31 o 4 6 0 1958.42 2128.79 211.94 o 5 6 0 34.46 -3.01 33.95 o 6 6 0 5494.74 5528.11 210.31 o 7 6 0 240.24 144.89 71.38 o 8 6 0 117.57 108.49 89.94 o 9 6 0 589.86 673.19 160.26 o -16 7 0 961.78 1150.43 190.30 o -15 7 0 1861.58 2195.91 230.40 o -14 7 0 4.90 -6.36 62.20 o -13 7 0 4532.11 4745.03 297.19 o -12 7 0 339.92 205.59 88.52 o -11 7 0 21.88 33.58 29.96 o -10 7 0 322.88 333.74 50.04 o -9 7 0 3277.83 3009.58 101.37 o -8 7 0 1472.09 1479.78 125.98 o -7 7 0 15301.95 14982.34 313.50 o -6 7 0 3800.58 3903.37 322.55 o -5 7 0 5820.25 5865.76 161.98 o -4 7 0 15000.33 15103.28 238.67 o -3 7 0 316.81 353.83 30.59 o -2 7 0 394.06 336.95 28.85 o -1 7 0 76.98 86.16 17.36 o 0 7 0 22979.54 23215.21 447.16 o 1 7 0 752.29 704.90 67.23 o 2 7 0 8236.28 7665.69 224.02 o 3 7 0 29.70 -13.61 26.54 o 4 7 0 2160.47 2009.54 123.08 o 5 7 0 7069.83 6948.30 240.11 o 6 7 0 358.03 332.23 74.21 o 7 7 0 99.83 18.82 49.28 o 8 7 0 4.54 78.63 95.06 o -16 8 0 4.50 -25.27 75.09 o -15 8 0 1.11 21.38 70.32 o -14 8 0 1970.58 2587.46 239.77 o -13 8 0 1832.70 2023.64 199.84 o -12 8 0 44.37 6.71 54.95 o -11 8 0 1329.82 1418.42 128.37 o -10 8 0 4906.14 5059.54 274.40 o -8 8 0 5855.20 5646.77 172.22 o -7 8 0 94.72 74.00 21.00 o -6 8 0 1665.04 1750.79 87.49 o -5 8 0 3144.97 2883.21 353.20 o -4 8 0 1542.45 1433.19 95.84 o -3 8 0 1261.88 1192.81 81.50 o -2 8 0 5707.44 5511.39 445.02 o -1 8 0 7446.68 7866.30 405.33 o 0 8 0 32.99 3.01 26.06 o 1 8 0 8287.66 8114.25 237.23 o 2 8 0 319.35 270.95 54.32 o 3 8 0 3135.25 2947.40 147.22 o 4 8 0 4801.00 5011.12 203.33 o 5 8 0 1617.09 1639.17 127.05 o 6 8 0 22.06 -31.11 42.94 o 7 8 0 823.25 767.77 108.45 o -16 9 0 14.35 -71.21 80.39 o -15 9 0 88.44 19.97 72.44 o -14 9 0 1179.49 1340.02 185.53 o -13 9 0 252.73 163.79 78.63 o -12 9 0 1734.87 2185.49 193.83 o -10 9 0 374.04 435.90 98.59 o -9 9 0 12821.47 12243.13 880.27 o -8 9 0 2.36 -13.11 17.12 o -7 9 0 3510.35 3071.72 124.89 o -6 9 0 854.84 694.67 165.56 o -5 9 0 5310.44 5139.65 126.28 o -4 9 0 101.57 63.84 21.29 o -3 9 0 4659.54 4771.22 183.21 o -2 9 0 2226.43 2366.67 113.58 o -1 9 0 1981.77 2052.88 111.03 o 0 9 0 7756.76 8029.19 241.54 o 1 9 0 190.08 145.20 47.46 o 2 9 0 546.69 620.74 112.73 o 3 9 0 1557.53 1415.36 115.07 o 4 9 0 3809.23 3774.75 185.26 o 5 9 0 18.98 39.32 51.90 o 6 9 0 2079.55 2314.55 166.32 o -16 10 0 0.82 -38.87 79.86 o -15 10 0 1590.78 1808.43 214.15 o -14 10 0 56.57 17.49 64.32 o -13 10 0 7724.55 7379.66 385.19 o -12 10 0 777.41 874.27 136.76 o -11 10 0 688.37 655.52 121.03 o -10 10 0 9349.89 9647.67 405.33 o -9 10 0 412.41 320.31 81.45 o -8 10 0 173.23 150.42 40.44 o -7 10 0 357.86 337.80 52.96 o -6 10 0 8438.70 8369.97 178.76 o -5 10 0 57.82 48.66 22.28 o -4 10 0 7631.99 8074.05 174.55 o -3 10 0 2445.77 2292.73 114.01 o -2 10 0 3.25 0.77 27.10 o -1 10 0 4227.51 4349.45 174.73 o 0 10 0 550.17 603.96 77.63 o 1 10 0 10.42 -12.15 33.31 o 2 10 0 100.65 106.23 46.74 o 3 10 0 3663.43 3601.72 185.96 o 4 10 0 42.84 46.68 50.10 o 5 10 0 1793.19 1251.21 133.25 o -16 11 0 2974.55 3276.91 289.07 o -15 11 0 2.55 56.01 86.93 o -14 11 0 3240.09 3197.93 260.09 o -13 11 0 1205.06 913.31 151.42 o -12 11 0 293.01 290.48 96.65 o -11 11 0 570.01 687.33 125.63 o -10 11 0 2343.01 2425.41 127.17 o -9 11 0 1057.99 1007.81 87.43 o -8 11 0 1681.79 1908.21 111.19 o -7 11 0 6151.37 6419.77 279.35 o -6 11 0 99.61 77.28 28.00 o -5 11 0 8770.65 8731.42 239.68 o -4 11 0 2669.37 2755.09 129.90 o -3 11 0 62.92 74.01 38.72 o -2 11 0 818.82 881.25 87.26 o -1 11 0 6424.49 6677.88 233.86 o 0 11 0 80.62 44.33 43.05 o 1 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0 560.08 767.01 125.45 o -6 13 0 5144.27 5225.27 301.26 o -5 13 0 18.38 26.15 56.19 o -4 13 0 112.76 163.26 83.93 o -3 13 0 2368.75 2337.70 145.65 o -2 13 0 217.61 122.19 58.79 o -1 13 0 3376.48 3288.36 280.85 o 0 13 0 1081.46 1123.07 165.21 o 1 13 0 0.03 -11.21 60.89 o -15 14 0 63.70 22.26 84.81 o -14 14 0 217.93 441.37 136.05 o -13 14 0 3347.84 3304.12 271.40 o -12 14 0 17.82 7.24 66.97 o -11 14 0 3805.97 3848.15 271.04 o -10 14 0 15.69 25.80 46.74 o -9 14 0 105.92 44.83 49.19 o -8 14 0 260.08 222.63 83.57 o -7 14 0 2530.09 2918.05 235.18 o -6 14 0 0.46 10.42 64.32 o -5 14 0 427.72 423.00 120.33 o -4 14 0 1815.49 1910.38 213.09 o -3 14 0 166.16 114.85 84.46 o -2 14 0 4164.06 3813.87 293.66 o -1 14 0 70.67 72.69 59.77 o -14 15 0 1846.70 1793.76 222.10 o -13 15 0 10.56 10.78 73.33 o -12 15 0 1327.72 1503.99 191.36 o -11 15 0 486.24 343.66 118.74 o -10 15 0 94.72 57.60 73.50 o -9 15 0 106.15 63.26 71.38 o -8 15 0 4379.96 5066.43 322.11 o -7 15 0 0.13 -33.75 68.56 o -6 15 0 1439.99 1970.63 218.04 o -5 15 0 2057.90 2123.12 229.87 o -4 15 0 367.02 168.39 100.18 o -3 15 0 1062.58 1126.40 187.29 o -13 16 0 192.28 87.64 92.76 o -12 16 0 1089.35 1179.06 181.64 o -10 16 0 85.81 43.82 90.11 o -9 16 0 2491.56 2824.93 257.44 o -8 16 0 90.46 65.73 93.65 o -7 16 0 2468.41 2473.85 247.37 o -6 16 0 216.85 326.52 124.92 o -5 16 0 319.00 258.50 114.14 o 9 -17 1 2185.14 2123.12 239.06 o 10 -17 1 860.12 1086.29 184.29 o 5 -16 1 1282.09 923.21 171.74 o 6 -16 1 1632.40 2063.39 230.58 o 7 -16 1 298.43 181.46 106.90 o 8 -16 1 2616.90 3006.39 261.15 o 9 -16 1 465.10 412.75 128.63 o 10 -16 1 44.28 1.77 79.86 o 12 -16 1 1362.96 1491.45 196.83 o 13 -16 1 0.39 43.11 83.22 o 2 -15 1 1466.63 1857.02 227.05 o 3 -15 1 47.10 17.14 89.58 o 4 -15 1 3897.69 4279.27 314.86 o 5 -15 1 797.26 772.14 153.72 o 6 -15 1 7.55 23.68 68.03 o 7 -15 1 2019.74 1978.23 208.49 o 8 -15 1 3.60 46.29 70.15 o 9 -15 1 91.35 107.96 84.81 o 10 -15 1 30.16 31.48 51.62 o 11 -15 1 1592.39 1888.29 205.84 o 12 -15 1 51.75 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