#------------------------------------------------------------------------------ #$Date: 2011-07-04 21:24:21 +0300 (Mon, 04 Jul 2011) $ #$Revision: 22560 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2230394.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230394_Fobs loop_ _publ_author_name 'Xu, Xuebin' 'Ding, Shuai' 'Shen, Si' 'Tang, Jinkui' 'Liu, Zhiliang' _publ_section_title ; Bis(\m-2-{[2-(1,3-benzothiazol-2-yl)hydrazinylidene]methyl}-6-methoxyphenolato)bis[dinitratodysprosium(III)] methanol disolvate ; _journal_coeditor_code JJ2083 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m796 _journal_page_last m797 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 112.045 _cell_angle_beta 105.065 _cell_angle_gamma 93.154 _cell_length_a 9.6191 _cell_length_b 10.1002 _cell_length_c 11.6151 _exptl_crystal_F_000 601.84 _reflns_d_resolution_high 0.8369 _[local]_cod_data_source_file jj2083Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 88 in P1 New: P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 204.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 339.83 348.75 17.17 o 3 0 0 22567.07 23351.72 178.69 o 4 0 0 10569.80 10812.11 145.02 o 5 0 0 131.44 154.99 36.14 o 6 0 0 1552.44 1564.12 45.16 o 7 0 0 4414.01 4516.04 135.54 o 8 0 0 4280.17 4154.52 84.87 o 9 0 0 18.51 11.96 23.04 o 10 0 0 2107.74 2055.79 126.50 o -11 1 0 1611.58 1604.74 104.81 o -10 1 0 1327.61 1242.48 51.48 o -9 1 0 613.83 685.12 38.72 o -8 1 0 2549.99 2558.46 108.43 o -7 1 0 2781.99 2780.58 63.71 o -6 1 0 3246.57 3367.57 65.01 o -5 1 0 63.55 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