#------------------------------------------------------------------------------ #$Date: 2011-07-04 21:24:21 +0300 (Mon, 04 Jul 2011) $ #$Revision: 22560 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2230437.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230437_Fobs loop_ _publ_author_name 'Ha, Kwang' _publ_section_title ; cis-(Acetonitrile-\kN)aquabis(2,2'-bipyrimidine-\k^2^N^1^,N^1'^)manganese(II) cis-diaquabis(2,2'-bipyrimidine-\k^2^N^1^,N^1'^)manganese(II) tetrakis(perchlorate) dihydrate ; _journal_coeditor_code OM2423 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m656 _journal_page_last m657 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 111.201 _cell_angle_beta 104.147 _cell_angle_gamma 91.419 _cell_length_a 12.0386 _cell_length_b 13.1878 _cell_length_c 17.5378 _exptl_crystal_F_000 1292.00 _reflns_d_resolution_high 0.7501 _[local]_cod_data_source_file om2423Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Mn(bpym)2(H2O)(CH3CN)][Mn(bpym)2(H2O)2](ClO4)4.2H2O' _shelx_refln_list_code 4 _shelx_f_calc_maximum 365.35 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 110.54 81.98 16.42 o 2 0 0 17049.93 19674.45 144.41 o 3 0 0 884.23 740.47 32.30 o 4 0 0 56169.27 59929.46 366.87 o 5 0 0 1329.49 1401.10 54.99 o 6 0 0 221.52 281.85 36.16 o 7 0 0 2838.36 2607.10 88.00 o 8 0 0 6270.88 6393.27 166.48 o 9 0 0 337.54 378.15 47.82 o 10 0 0 38.01 33.08 33.12 o 11 0 0 33.46 7.44 35.24 o 12 0 0 1127.11 1155.02 134.77 o 13 0 0 1.81 0.90 46.58 o 14 0 0 8.39 -43.78 66.61 o 15 0 0 35.50 82.72 87.55 o -15 1 0 207.53 199.99 113.17 o -14 1 0 21.12 -34.11 70.42 o -13 1 0 60.58 58.71 76.28 o -12 1 0 0.08 3.94 37.06 o -11 1 0 1148.20 1040.15 102.70 o -10 1 0 191.25 272.56 56.64 o -9 1 0 84.14 124.14 32.40 o -8 1 0 262.06 308.47 39.37 o -7 1 0 136.02 155.04 27.71 o -6 1 0 961.13 1067.50 53.72 o -5 1 0 2272.25 2185.66 76.47 o -4 1 0 62.09 71.39 15.00 o -3 1 0 67.07 60.37 12.64 o -2 1 0 155.99 140.31 14.55 o -1 1 0 586.35 556.80 16.40 o 1 1 0 539.29 519.97 17.03 o 2 1 0 3.43 18.80 7.13 o 3 1 0 20.10 23.79 10.47 o 4 1 0 9892.52 10582.66 140.72 o 5 1 0 137.01 135.67 22.79 o 6 1 0 322.49 328.75 42.32 o 7 1 0 509.94 460.80 41.91 o 8 1 0 3415.99 3729.83 166.29 o 9 1 0 51.97 69.31 27.60 o 10 1 0 16.63 15.76 32.11 o 11 1 0 7.17 47.03 35.35 o 12 1 0 1110.48 1335.53 115.74 o 13 1 0 2.38 63.01 46.91 o 14 1 0 42.50 65.73 57.68 o -15 2 0 122.40 340.68 123.13 o -14 2 0 16.93 -22.11 58.56 o -13 2 0 2.17 118.00 71.88 o -12 2 0 1503.37 1433.30 180.37 o -11 2 0 2264.08 2102.79 132.81 o -10 2 0 0.41 -26.08 26.08 o -9 2 0 112.37 99.05 27.08 o -8 2 0 1274.29 1139.66 63.26 o -7 2 0 5652.96 5468.85 126.22 o -6 2 0 7.12 -5.16 11.72 o -5 2 0 5022.21 5911.76 110.90 o -4 2 0 270.51 298.31 24.40 o -3 2 0 38345.77 40899.07 261.66 o -2 2 0 22823.63 23378.96 168.94 o -1 2 0 3525.37 4135.83 79.45 o 0 2 0 375.69 354.12 16.67 o 1 2 0 30530.06 34661.37 311.18 o 2 2 0 14.81 12.54 7.57 o 3 2 0 4256.46 3901.18 65.30 o 4 2 0 6235.80 6200.03 106.44 o 5 2 0 10294.28 9444.16 150.84 o 6 2 0 424.17 365.89 38.12 o 7 2 0 10.90 18.73 18.25 o 8 2 0 379.63 367.77 46.04 o 9 2 0 1707.16 1796.34 88.39 o 10 2 0 239.77 185.27 53.01 o 11 2 0 118.58 115.08 46.91 o 12 2 0 26.88 39.63 41.80 o 13 2 0 30.87 1.02 56.37 o 14 2 0 1.40 -9.22 71.30 o 15 2 0 19.47 -38.65 79.06 o -15 3 0 20.59 -22.69 84.18 o -14 3 0 182.51 407.44 126.79 o -13 3 0 33.21 104.97 75.25 o -12 3 0 146.41 74.23 69.25 o -11 3 0 33.78 130.45 64.86 o -10 3 0 260.26 297.35 59.13 o -9 3 0 265.25 330.30 42.69 o -8 3 0 204.23 222.47 35.34 o -7 3 0 428.86 461.86 49.77 o -6 3 0 155.41 130.07 23.38 o -5 3 0 9.75 59.62 15.06 o -4 3 0 725.60 593.13 32.48 o -3 3 0 781.20 726.94 74.08 o -2 3 0 3220.90 3239.03 89.78 o -1 3 0 20582.01 21190.44 169.38 o 0 3 0 15304.88 16864.80 142.06 o 1 3 0 1495.47 1659.60 66.57 o 2 3 0 2150.13 1801.51 74.17 o 3 3 0 4.14 2.95 10.56 o 4 3 0 2179.63 2265.65 57.87 o 5 3 0 5604.06 6019.17 129.94 o 6 3 0 62.60 105.02 27.79 o 7 3 0 9.34 -6.23 15.00 o 8 3 0 211.30 233.20 39.49 o 9 3 0 932.58 813.73 63.76 o 10 3 0 419.29 413.23 73.93 o 11 3 0 342.77 337.24 67.70 o 12 3 0 26.32 19.03 56.07 o 13 3 0 131.64 158.70 85.94 o 14 3 0 4.32 33.38 75.69 o -15 4 0 174.57 158.41 109.07 o -14 4 0 125.60 40.11 84.33 o -13 4 0 3.49 37.48 72.18 o -12 4 0 151.10 369.23 109.07 o -11 4 0 1726.64 1853.78 197.94 o -10 4 0 2329.35 2401.62 211.85 o -9 4 0 35.86 43.65 22.58 o -8 4 0 5.13 18.47 17.82 o -7 4 0 52.95 59.22 19.03 o -6 4 0 10805.45 11463.29 170.51 o -5 4 0 1097.28 1093.38 68.26 o -4 4 0 3235.13 3817.34 83.03 o -3 4 0 2544.77 2257.00 88.94 o -2 4 0 9057.94 9030.71 165.58 o -1 4 0 11020.60 11284.37 134.19 o 0 4 0 277.40 350.30 23.35 o 1 4 0 60.26 28.55 19.03 o 2 4 0 13434.87 12986.38 222.05 o 3 4 0 2442.72 2623.90 104.89 o 4 4 0 3915.56 4341.02 91.25 o 5 4 0 404.19 359.45 30.58 o 6 4 0 3134.53 3197.61 84.29 o 7 4 0 16.29 4.22 25.29 o 8 4 0 35.45 30.13 25.70 o 9 4 0 445.34 405.78 55.24 o 10 4 0 493.18 369.38 106.73 o 11 4 0 1.16 51.83 50.95 o 12 4 0 43.60 35.43 70.86 o 13 4 0 16.61 54.61 74.81 o 14 4 0 44.93 83.74 90.19 o -15 5 0 34.27 8.78 77.16 o -14 5 0 155.98 222.68 100.43 o -13 5 0 136.56 204.67 96.04 o -12 5 0 54.36 62.81 70.86 o -11 5 0 10.23 15.23 57.83 o -10 5 0 477.29 566.96 78.73 o -9 5 0 66.89 54.34 32.08 o -8 5 0 248.27 262.09 38.30 o -7 5 0 1207.65 1299.78 61.63 o -6 5 0 26.43 17.95 13.58 o -5 5 0 51.56 41.68 14.66 o -4 5 0 4.79 8.64 10.90 o -3 5 0 289.29 175.78 40.26 o -2 5 0 3961.42 5166.72 134.21 o -1 5 0 2492.36 2624.43 70.67 o 0 5 0 4555.37 4450.53 86.65 o 1 5 0 125.40 125.24 44.65 o 2 5 0 1552.37 1374.14 78.95 o 3 5 0 270.24 237.43 44.59 o 4 5 0 894.48 948.07 72.84 o 5 5 0 2017.46 1997.75 66.38 o 6 5 0 2918.70 3075.19 83.29 o 7 5 0 142.66 146.88 27.44 o 8 5 0 87.08 33.49 34.96 o 9 5 0 525.64 536.88 84.47 o 10 5 0 1024.40 1047.38 159.00 o 11 5 0 1.04 8.78 61.05 o 12 5 0 6.63 -30.89 65.59 o 13 5 0 55.98 164.12 87.11 o 14 5 0 504.28 714.46 183.45 o -15 6 0 115.02 362.50 134.69 o -14 6 0 22.56 -32.36 66.91 o -13 6 0 559.98 606.70 157.68 o -12 6 0 113.10 320.04 114.93 o -11 6 0 224.19 312.72 101.31 o -10 6 0 205.62 260.68 58.47 o -9 6 0 846.68 846.05 155.19 o -8 6 0 183.91 127.04 39.19 o -7 6 0 2426.52 2627.98 130.36 o -6 6 0 1230.43 1163.37 84.48 o -5 6 0 4095.32 4193.61 107.11 o -4 6 0 960.89 803.03 64.49 o -3 6 0 1030.08 1030.68 68.42 o -2 6 0 292.26 355.22 53.22 o -1 6 0 9190.96 9718.39 149.57 o 0 6 0 468.16 391.41 31.54 o 1 6 0 6535.67 7030.93 184.79 o 2 6 0 1885.81 1911.89 100.65 o 3 6 0 3747.96 3625.28 191.72 o 4 6 0 162.17 197.99 44.45 o 5 6 0 41.27 39.73 43.04 o 6 6 0 427.45 442.47 54.30 o 7 6 0 29.72 12.70 28.15 o 8 6 0 83.04 87.66 31.13 o 9 6 0 550.88 507.60 84.92 o 10 6 0 4.48 43.48 57.10 o 11 6 0 1.64 43.48 65.15 o 12 6 0 4.69 51.68 65.00 o 13 6 0 3.56 -12.44 76.28 o -14 7 0 23.78 209.94 97.51 o -13 7 0 6.21 -58.27 58.27 o -12 7 0 11.23 -14.20 56.66 o -11 7 0 237.20 340.24 115.37 o -10 7 0 175.30 164.61 63.03 o -9 7 0 233.60 202.68 52.74 o -8 7 0 495.02 397.70 70.50 o -7 7 0 118.21 94.57 38.90 o -6 7 0 562.52 429.90 67.34 o -5 7 0 1486.44 1812.12 70.66 o -4 7 0 106.25 74.06 27.33 o -3 7 0 172.56 83.76 26.43 o -2 7 0 1885.54 2034.65 96.21 o -1 7 0 4400.26 5337.10 168.59 o 0 7 0 977.27 1111.93 90.34 o 1 7 0 2377.40 2349.35 116.16 o 2 7 0 254.72 230.07 46.51 o 3 7 0 6458.48 6284.55 239.59 o 4 7 0 1.33 -18.16 18.16 o 5 7 0 295.72 247.08 54.02 o 6 7 0 440.65 646.52 130.59 o 7 7 0 2395.81 2603.89 119.66 o 8 7 0 16.92 -9.44 51.23 o 9 7 0 232.29 276.66 66.71 o 10 7 0 17.24 14.05 58.27 o 11 7 0 566.15 347.42 119.76 o 12 7 0 120.22 88.72 70.86 o 13 7 0 64.93 68.22 85.65 o -14 8 0 159.89 81.84 88.87 o -11 8 0 119.39 39.53 62.22 o -10 8 0 347.69 252.89 65.95 o -9 8 0 378.61 506.94 81.96 o -8 8 0 692.52 687.62 116.68 o -7 8 0 841.06 909.57 104.75 o -6 8 0 191.69 159.97 43.16 o -5 8 0 67.65 18.34 26.71 o -4 8 0 859.68 754.64 69.96 o -3 8 0 218.69 234.31 53.73 o -2 8 0 1759.46 2011.29 101.48 o -1 8 0 687.70 717.81 47.68 o 0 8 0 530.99 583.97 41.56 o 1 8 0 24.95 23.13 21.66 o 2 8 0 861.53 898.27 79.85 o 3 8 0 981.19 1171.20 183.15 o 4 8 0 509.85 402.19 69.98 o 5 8 0 300.37 137.76 45.83 o 6 8 0 199.83 281.76 65.00 o 7 8 0 0.34 0.43 25.15 o 8 8 0 35.21 21.51 30.87 o 9 8 0 34.82 7.97 44.73 o 10 8 0 89.68 77.16 72.03 o 11 8 0 10.91 19.03 50.66 o 12 8 0 3.86 73.93 79.06 o -13 9 0 31.11 155.63 83.60 o -12 9 0 6.43 -8.35 65.74 o -11 9 0 90.36 163.53 93.55 o -10 9 0 4.64 53.96 40.30 o -9 9 0 237.04 279.55 63.74 o -8 9 0 175.78 171.49 90.48 o -7 9 0 446.48 395.22 73.92 o -6 9 0 146.56 117.74 45.81 o -5 9 0 346.06 440.97 71.25 o -4 9 0 513.08 566.17 69.93 o -3 9 0 62.86 84.63 32.57 o -2 9 0 2.74 26.54 27.96 o -1 9 0 15.50 -4.92 16.50 o 0 9 0 1575.77 2092.21 229.42 o 1 9 0 219.28 335.17 103.51 o 2 9 0 47.14 56.70 33.84 o 3 9 0 1589.68 1628.69 117.15 o 4 9 0 3152.49 3346.49 202.92 o 5 9 0 2.33 26.21 30.09 o 6 9 0 30.83 5.64 31.08 o 7 9 0 148.01 79.34 49.59 o 8 9 0 1571.22 1728.44 109.97 o 9 9 0 13.82 12.19 33.04 o 10 9 0 56.16 -26.50 49.78 o 11 9 0 0.01 -23.86 80.23 o -13 10 0 117.90 -27.96 81.55 o -12 10 0 86.07 57.10 76.42 o -11 10 0 185.14 11.71 81.99 o -10 10 0 211.96 288.01 69.08 o -9 10 0 10.58 -3.81 40.85 o -8 10 0 102.34 149.30 52.66 o -7 10 0 858.97 942.96 100.73 o -6 10 0 24.35 19.88 32.77 o -5 10 0 47.13 115.37 40.54 o -4 10 0 36.16 67.94 34.53 o -3 10 0 569.48 585.98 69.09 o -2 10 0 757.16 787.08 71.01 o -1 10 0 1375.08 1448.53 163.68 o 0 10 0 564.59 626.81 94.14 o 1 10 0 695.88 654.37 115.59 o 2 10 0 30.27 42.77 67.79 o 3 10 0 122.33 212.06 60.10 o 4 10 0 0.61 -17.12 28.52 o 5 10 0 115.01 93.96 47.15 o 6 10 0 10.02 -48.39 48.39 o 7 10 0 12.98 48.26 34.14 o 8 10 0 16.64 -23.90 48.51 o 9 10 0 6.80 -8.13 46.81 o 10 10 0 11.68 -54.17 54.17 o 11 10 0 0.03 28.26 71.88 o -12 11 0 3.62 -63.83 81.40 o -11 11 0 2.25 -58.71 72.76 o -10 11 0 90.09 157.39 83.16 o -9 11 0 114.40 166.52 95.16 o -8 11 0 286.23 261.32 86.38 o -7 11 0 470.55 377.21 77.17 o -6 11 0 100.49 105.23 64.78 o -5 11 0 66.24 35.88 37.58 o -4 11 0 497.81 592.83 86.32 o -3 11 0 1371.88 1696.68 184.47 o -2 11 0 675.23 577.86 131.62 o -1 11 0 347.01 308.77 93.55 o 0 11 0 157.24 81.94 43.03 o 1 11 0 3334.50 3800.66 186.94 o 2 11 0 81.20 117.91 84.18 o 3 11 0 13.90 -28.40 28.40 o 4 11 0 81.72 40.97 89.82 o 5 11 0 937.74 969.31 195.16 o 6 11 0 32.08 103.78 49.95 o 7 11 0 93.13 97.45 40.79 o 8 11 0 11.00 -8.85 35.06 o 9 11 0 377.16 501.24 81.32 o 10 11 0 12.50 55.93 72.62 o -11 12 0 59.86 57.98 97.80 o -10 12 0 196.64 158.12 84.77 o -9 12 0 59.40 6.05 48.93 o -8 12 0 10.04 19.38 46.97 o -7 12 0 0.04 -5.06 44.05 o -6 12 0 812.81 1001.92 108.83 o -5 12 0 0.30 30.85 41.02 o -4 12 0 18.36 66.03 55.49 o -3 12 0 162.44 175.54 69.98 o -2 12 0 91.14 123.57 74.67 o -1 12 0 0.01 99.56 54.02 o 0 12 0 11.57 -30.64 30.64 o 1 12 0 47.41 36.59 38.80 o 2 12 0 6.71 -29.61 29.61 o 3 12 0 5.99 45.72 39.32 o 4 12 0 3.66 33.61 85.43 o 5 12 0 150.91 174.83 118.37 o 6 12 0 29.51 0.82 48.05 o 7 12 0 3.64 13.84 57.75 o 8 12 0 18.03 -18.40 37.29 o 9 12 0 76.27 167.27 54.67 o -10 13 0 133.68 156.95 78.33 o -9 13 0 104.19 62.80 63.72 o -8 13 0 1.50 -20.70 110.24 o -7 13 0 69.47 102.40 59.15 o -6 13 0 388.46 502.75 125.91 o -5 13 0 3.30 -45.09 45.09 o -4 13 0 40.10 1.46 53.00 o -3 13 0 128.19 -4.54 68.22 o -2 13 0 1414.26 2014.24 224.88 o -1 13 0 0.28 -4.68 57.24 o 0 13 0 44.20 136.89 73.35 o 1 13 0 7.30 32.09 42.62 o 2 13 0 1326.44 1418.13 129.54 o 3 13 0 0.07 33.49 41.21 o 4 13 0 3.81 0.22 45.75 o 5 13 0 21.37 7.55 46.25 o 6 13 0 321.67 530.72 98.10 o 7 13 0 55.77 33.07 69.84 o -9 14 0 67.94 179.64 98.09 o -8 14 0 65.46 193.55 108.49 o -7 14 0 5.52 69.98 80.67 o -6 14 0 11.48 64.27 80.23 o -5 14 0 2.96 27.52 68.22 o -4 14 0 5.99 91.36 68.96 o -3 14 0 7.76 55.49 59.15 o -2 14 0 1.77 46.41 62.95 o -1 14 0 68.19 125.18 80.23 o 0 14 0 37.65 97.65 70.27 o 1 14 0 97.36 -14.79 58.12 o 2 14 0 28.61 58.98 85.87 o 3 14 0 18.93 22.94 58.34 o 4 14 0 6.66 17.01 47.14 o 5 14 0 1.92 -10.74 85.13 o 6 14 0 207.17 241.05 74.00 o -8 15 0 22.26 99.56 96.19 o -7 15 0 0.87 33.97 89.60 o -6 15 0 62.83 -43.78 80.38 o -5 15 0 297.19 196.48 117.56 o -4 15 0 23.69 58.85 75.11 o -3 15 0 0.40 32.21 73.93 o -2 15 0 16.92 59.73 73.06 o -1 15 0 305.99 437.31 143.48 o 0 15 0 0.06 -1.76 48.75 o 1 15 0 10.03 -52.85 60.17 o 2 15 0 24.95 81.40 69.40 o 3 15 0 309.95 169.27 87.84 o 4 15 0 38.82 30.35 52.53 o -5 16 0 13.52 88.43 94.58 o -4 16 0 71.37 7.91 83.30 o -3 16 0 22.79 124.15 88.72 o -2 16 0 62.32 136.45 103.95 o -1 16 0 32.80 24.16 79.06 o 0 16 0 1.12 42.16 78.47 o 1 16 0 4.17 -53.29 68.37 o -2 -16 1 12.91 -47.58 63.54 o -1 -16 1 27.44 36.31 74.08 o 0 -16 1 0.33 -27.52 75.69 o 1 -16 1 0.07 10.25 76.42 o 2 -16 1 265.00 225.61 104.09 o 3 -16 1 252.29 336.44 118.88 o 4 -16 1 6.20 107.90 84.04 o 5 -16 1 18.07 -16.40 70.71 o -5 -15 1 10.94 -50.22 50.22 o -4 -15 1 0.42 -28.55 48.75 o -3 -15 1 15.09 36.60 55.19 o -2 -15 1 104.98 -16.10 60.17 o -1 -15 1 38.58 50.95 57.98 o 0 -15 1 0.40 -65.74 65.74 o 1 -15 1 2.48 -56.51 56.51 o 2 -15 1 3.51 18.01 63.98 o 3 -15 1 9.41 57.68 74.96 o 4 -15 1 38.67 105.85 77.45 o 5 -15 1 0.19 -55.19 69.25 o 6 -15 1 5.71 -52.56 75.40 o 7 -15 1 7.18 -45.53 69.69 o 8 -15 1 9.55 106.88 91.65 o -6 -14 1 61.93 35.87 80.96 o -5 -14 1 126.34 103.08 100.87 o -4 -14 1 25.42 75.93 45.22 o -3 -14 1 58.82 43.84 40.83 o -2 -14 1 3.24 27.77 71.01 o -1 -14 1 254.09 376.55 122.25 o 0 -14 1 48.40 -5.71 54.90 o 1 -14 1 3.68 -15.23 57.10 o 2 -14 1 0.58 -8.49 60.17 o 3 -14 1 217.62 374.65 125.32 o 4 -14 1 112.48 -18.01 76.42 o 5 -14 1 13.27 137.77 81.69 o 6 -14 1 6.26 -61.05 61.05 o 7 -14 1 95.22 110.83 75.11 o 8 -14 1 118.11 183.15 77.16 o 9 -14 1 15.43 1.95 73.20 o -8 -13 1 61.14 44.91 46.49 o -7 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