#------------------------------------------------------------------------------
#$Date: 2011-07-04 21:24:21 +0300 (Mon, 04 Jul 2011) $
#$Revision: 22560 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2230515.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2230515_Fobs
loop_
_publ_author_name
'Lamhamdi, Abdellatif'
'Essehli, Rachid'
'El Bali, Brahim'
'Du\<sek, Michal'
'Fejfarov\'a, Karla'
_publ_section_title
;
 The triclinic form of dipotassium cobalt(II)
 bis(dihydrogendiphosphate) dihydrate
;
_journal_coeditor_code           WM2482
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i37
_journal_page_last               i38
_journal_volume                  67
_journal_year                    2011
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                80.740(14)
_cell_angle_beta                 72.397(17)
_cell_angle_gamma                83.484(14)
_cell_length_a                   6.8737(14)
_cell_length_b                   7.3565(11)
_cell_length_c                   7.6141(14)
_exptl_crystal_F_000             261
_reflns_d_resolution_high        0.7950
_[local]_cod_data_source_file    wm2482Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     B95-3
_shelx_refln_list_code           4
_shelx_f_calc_maximum            93.24
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 855.13 798.02 11.83 o
2 0 0 1526.47 1604.04 9.83 o
3 0 0 107.60 100.71 6.14 o
4 0 0 1593.55 1606.42 15.01 o
5 0 0 1215.07 1329.27 16.42 o
6 0 0 207.30 184.43 14.16 o
7 0 0 46.72 39.68 13.97 <
8 0 0 80.23 67.00 19.68 o
-8 1 0 9.59 10.83 11.80 <
-7 1 0 718.77 780.22 27.38 o
-6 1 0 217.08 215.41 15.88 o
-5 1 0 2.96 5.99 5.39 <
-4 1 0 9.39 7.60 4.75 <
-3 1 0 94.93 125.67 5.97 o
-2 1 0 7010.19 6955.39 17.38 o
-1 1 0 425.46 406.17 4.22 o
1 1 0 1893.10 1660.60 7.11 o
2 1 0 519.48 518.01 8.97 o
3 1 0 1152.65 1166.99 11.16 o
4 1 0 78.37 73.19 7.63 o
5 1 0 1493.98 1570.97 17.52 o
6 1 0 314.08 300.50 15.39 o
7 1 0 295.14 284.14 26.74 o
8 1 0 0.39 7.57 14.66 <
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-6 2 0 380.31 416.12 22.43 o
-5 2 0 5.42 13.74 9.06 <
-4 2 0 396.96 406.34 13.76 o
-3 2 0 172.86 176.56 7.00 o
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-1 2 0 2178.81 2251.03 14.53 o
0 2 0 5174.79 4276.06 18.65 o
1 2 0 1.19 2.70 1.59 <
2 2 0 34.29 41.06 4.82 o
3 2 0 669.96 673.97 10.49 o
4 2 0 896.78 958.81 14.46 o
5 2 0 184.07 187.32 14.89 o
6 2 0 169.69 144.70 15.06 o
7 2 0 26.35 26.12 14.16 <
8 2 0 65.06 51.80 21.92 <
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-6 3 0 66.45 51.04 15.21 o
-5 3 0 437.08 435.82 18.80 o
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-3 3 0 508.08 534.38 8.94 o
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-1 3 0 2036.77 2221.39 14.58 o
0 3 0 109.61 149.16 7.13 o
1 3 0 558.85 578.75 6.91 o
2 3 0 4348.19 4587.92 16.65 o
3 3 0 323.44 330.43 8.73 o
4 3 0 104.79 100.72 10.19 o
5 3 0 255.52 235.91 17.19 o
6 3 0 3.29 5.38 7.46 <
7 3 0 651.03 656.21 24.59 o
-7 4 0 49.25 42.81 17.50 <
-6 4 0 107.95 104.06 18.59 o
-5 4 0 63.45 57.26 11.98 o
-4 4 0 58.94 47.54 8.91 o
-3 4 0 578.12 564.35 11.49 o
-2 4 0 271.60 242.60 8.76 o
-1 4 0 181.64 177.97 6.91 o
0 4 0 2842.48 2608.65 21.91 o
1 4 0 1644.99 1835.36 18.81 o
2 4 0 1463.03 1443.53 12.39 o
3 4 0 0.29 7.00 5.50 <
4 4 0 0.41 6.32 6.34 <
5 4 0 1299.92 1472.48 24.03 o
6 4 0 45.56 44.89 14.01 o
7 4 0 29.82 12.17 12.40 <
-6 5 0 168.90 163.80 17.75 o
-5 5 0 126.76 107.60 13.39 o
-4 5 0 84.46 67.06 10.88 o
-3 5 0 63.52 49.68 8.27 o
-2 5 0 1648.73 1701.26 15.98 o
-1 5 0 465.01 466.22 16.31 o
0 5 0 150.28 126.96 9.71 o
1 5 0 126.64 128.86 9.75 o
2 5 0 29.16 16.97 7.84 <
3 5 0 1017.79 1105.53 16.94 o
4 5 0 4.56 7.34 5.69 <
5 5 0 164.39 146.45 15.95 o
6 5 0 364.38 367.79 23.00 o
7 5 0 3.30 3.32 24.46 <
-5 6 0 3.59 7.44 12.88 <
-4 6 0 676.94 688.35 30.99 o
-3 6 0 105.46 97.46 14.32 o
-2 6 0 129.50 127.64 14.34 o
-1 6 0 442.47 451.66 20.28 o
0 6 0 7.80 6.36 6.17 <
1 6 0 27.56 20.35 8.26 <
2 6 0 107.88 106.60 14.71 o
3 6 0 196.49 193.46 16.25 o
4 6 0 633.97 756.99 29.90 o
5 6 0 32.29 22.11 20.26 <
6 6 0 6.54 5.15 19.36 <
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-3 7 0 934.23 986.86 27.16 o
-2 7 0 23.43 21.20 10.50 <
-1 7 0 31.67 22.97 10.49 <
0 7 0 25.21 22.42 10.63 <
1 7 0 369.45 346.20 16.55 o
2 7 0 211.90 220.96 15.81 o
3 7 0 24.00 14.21 10.21 <
4 7 0 90.94 82.73 22.63 o
5 7 0 6.43 3.97 20.30 <
-3 8 0 42.70 46.61 16.67 <
-2 8 0 0.26 3.63 8.20 <
-1 8 0 0.29 6.30 9.05 <
0 8 0 72.09 53.76 15.07 o
1 8 0 147.60 179.17 17.91 o
2 8 0 514.08 609.38 24.25 o
3 8 0 8.04 11.04 10.37 <
0 9 0 197.09 217.51 29.49 o
1 9 0 3.16 6.59 13.82 <
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0 -8 1 174.66 189.59 18.38 o
1 -8 1 155.91 178.47 18.80 o
2 -8 1 69.31 66.11 18.79 o
3 -8 1 494.06 588.09 33.36 o
-4 -7 1 325.26 314.21 30.53 o
-3 -7 1 47.00 48.24 21.14 <
-2 -7 1 27.75 27.59 11.07 <
-1 -7 1 7.85 14.64 8.81 <
0 -7 1 53.64 50.50 10.35 o
1 -7 1 36.22 39.20 10.22 o
2 -7 1 0.27 4.32 7.83 <
3 -7 1 469.99 505.20 24.82 o
4 -7 1 1.83 5.61 12.39 <
-5 -6 1 28.33 11.88 20.09 <
-4 -6 1 31.10 28.41 13.91 <
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-2 -6 1 134.72 163.75 16.92 o
-1 -6 1 28.08 18.52 8.24 <
0 -6 1 39.11 28.78 8.25 o
1 -6 1 1480.63 1582.02 19.49 o
2 -6 1 107.88 105.29 13.34 o
3 -6 1 159.05 157.42 16.09 o
4 -6 1 10.38 16.06 13.11 <
5 -6 1 31.76 24.03 16.10 <
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-5 -5 1 27.57 23.80 22.15 <
-4 -5 1 12.64 22.57 15.78 <
-3 -5 1 11.78 26.04 14.61 <
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0 -5 1 144.37 152.12 11.03 o
1 -5 1 19.25 15.29 5.92 <
2 -5 1 627.64 612.63 17.21 o
3 -5 1 33.91 35.75 8.31 o
4 -5 1 316.46 319.11 14.80 o
5 -5 1 27.04 21.79 8.77 <
6 -5 1 151.43 141.62 16.43 o
-7 -4 1 91.92 65.67 19.77 o
-6 -4 1 4.82 3.75 8.26 <
-5 -4 1 144.39 122.25 16.25 o
-4 -4 1 30.74 24.16 9.02 <
-3 -4 1 1256.85 1359.87 16.71 o
-2 -4 1 149.07 140.92 7.61 o
-1 -4 1 12.21 4.42 2.97 <
0 -4 1 794.74 763.47 13.98 o
1 -4 1 266.52 272.37 6.44 o
2 -4 1 623.21 631.60 8.60 o
3 -4 1 255.42 269.23 9.67 o
4 -4 1 724.22 750.53 14.33 o
5 -4 1 957.80 1037.67 19.38 o
6 -4 1 94.67 77.62 12.51 o
7 -4 1 8.13 17.97 12.83 <
-7 -3 1 104.22 105.39 20.23 o
-6 -3 1 1.95 6.25 7.81 <
-5 -3 1 57.91 52.44 14.71 o
-4 -3 1 296.92 295.57 15.14 o
-3 -3 1 2507.05 2707.85 21.31 o
-2 -3 1 864.48 842.34 11.01 o
-1 -3 1 620.15 592.25 7.92 o
0 -3 1 83.50 64.91 5.32 o
1 -3 1 870.40 829.62 7.23 o
2 -3 1 462.17 434.45 6.71 o
3 -3 1 578.41 593.03 11.02 o
4 -3 1 102.39 93.34 9.20 o
5 -3 1 92.56 87.94 11.10 o
6 -3 1 65.78 57.42 18.88 o
7 -3 1 3.12 6.67 11.05 <
-7 -2 1 23.10 18.35 12.68 <
-6 -2 1 27.45 26.41 12.81 <
-5 -2 1 2013.69 2142.92 32.24 o
-4 -2 1 1679.08 1816.54 22.47 o
-3 -2 1 207.60 189.75 11.44 o
-2 -2 1 269.66 234.04 7.68 o
-1 -2 1 1062.83 982.53 8.54 o
0 -2 1 875.78 872.66 7.22 o
1 -2 1 355.81 348.74 4.32 o
2 -2 1 4.78 4.22 2.57 <
3 -2 1 333.20 350.05 11.46 o
4 -2 1 155.35 145.74 12.06 o
5 -2 1 511.50 516.90 15.98 o
6 -2 1 701.14 783.17 20.60 o
7 -2 1 316.36 326.35 24.56 o
8 -2 1 6.74 13.24 13.57 <
-7 -1 1 0.69 7.24 11.56 <
-6 -1 1 121.13 113.10 14.83 o
-5 -1 1 222.22 233.30 13.95 o
-4 -1 1 995.51 984.47 14.81 o
-3 -1 1 1242.81 1265.42 13.71 o
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-1 -1 1 4916.70 4930.31 17.41 o
0 -1 1 4426.91 4355.08 13.64 o
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2 -1 1 433.56 427.37 7.17 o
3 -1 1 14.02 23.53 4.53 o
4 -1 1 2441.46 2606.69 20.02 o
5 -1 1 230.24 210.13 12.35 o
6 -1 1 66.52 57.99 11.97 o
7 -1 1 209.10 215.27 19.11 o
8 -1 1 0.19 12.45 14.62 <
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-6 0 1 235.36 226.74 16.57 o
-5 0 1 175.41 155.28 11.53 o
-4 0 1 109.81 109.15 10.05 o
-3 0 1 764.55 707.98 10.98 o
-2 0 1 494.23 503.33 8.09 o
-1 0 1 1324.81 1332.72 9.95 o
1 0 1 341.89 356.58 6.76 o
2 0 1 239.60 222.03 4.88 o
3 0 1 13.42 11.73 3.71 o
4 0 1 2819.15 2907.81 20.11 o
5 0 1 3218.30 3137.06 26.90 o
6 0 1 26.78 22.76 8.99 <
7 0 1 49.82 41.23 11.93 o
8 0 1 5.78 21.03 17.74 <
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-3 1 1 1848.32 1900.45 16.32 o
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-1 1 1 252.62 242.15 5.91 o
0 1 1 627.23 704.57 7.14 o
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2 1 1 7073.09 6817.62 29.16 o
3 1 1 1642.97 1506.75 15.27 o
4 1 1 169.12 157.77 10.00 o
5 1 1 168.79 214.02 15.05 o
6 1 1 139.32 134.13 14.01 o
7 1 1 2.37 6.63 7.46 <
8 1 1 44.31 38.69 20.00 <
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-4 2 1 1998.50 2224.31 21.11 o
-3 2 1 360.80 389.95 10.85 o
-2 2 1 2250.21 2549.22 19.65 o
-1 2 1 43.88 56.78 5.18 o
0 2 1 3364.19 3233.47 14.43 o
1 2 1 2467.51 2659.31 9.29 o
2 2 1 0.40 6.33 3.19 <
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4 2 1 12.14 8.63 6.22 <
5 2 1 157.65 128.48 13.07 o
6 2 1 18.00 8.76 6.75 <
7 2 1 148.29 135.11 16.07 o
8 2 1 281.06 244.43 29.15 o
-7 3 1 102.62 90.78 19.12 o
-6 3 1 419.01 406.33 20.01 o
-5 3 1 14.56 14.51 9.47 <
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-3 3 1 24.33 22.34 6.68 o
-2 3 1 139.94 132.34 8.39 o
-1 3 1 1021.65 1147.66 12.59 o
0 3 1 45.44 57.17 5.33 o
1 3 1 2744.54 2323.37 11.10 o
2 3 1 90.30 89.72 5.31 o
3 3 1 21.59 25.45 6.73 o
4 3 1 145.22 148.70 11.78 o
5 3 1 94.05 104.64 13.54 o
6 3 1 345.19 336.52 17.45 o
7 3 1 59.04 51.16 12.89 o
8 3 1 20.04 6.02 16.87 <
-6 4 1 540.15 533.03 24.82 o
-5 4 1 4.77 7.19 7.87 <
-4 4 1 202.41 187.98 14.34 o
-3 4 1 397.21 383.00 11.88 o
-2 4 1 38.16 36.49 6.92 o
-1 4 1 815.51 788.44 10.55 o
0 4 1 7.41 8.91 4.44 <
1 4 1 0.83 2.88 2.55 <
2 4 1 242.74 246.40 8.07 o
3 4 1 20.65 22.88 6.37 o
4 4 1 898.59 962.55 17.93 o
5 4 1 463.57 529.34 17.06 o
6 4 1 252.17 248.15 17.27 o
7 4 1 69.90 54.20 16.51 o
-6 5 1 86.15 86.21 18.71 o
-5 5 1 442.31 423.71 18.58 o
-4 5 1 40.00 23.98 8.42 <
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-2 5 1 201.90 201.00 10.35 o
-1 5 1 767.01 773.96 12.26 o
0 5 1 837.53 768.21 14.89 o
1 5 1 1721.67 1903.22 19.33 o
2 5 1 388.01 376.70 8.90 o
3 5 1 2202.03 2490.34 18.46 o
4 5 1 328.88 335.50 12.58 o
5 5 1 17.41 20.19 9.82 <
6 5 1 27.84 13.35 12.00 <
7 5 1 290.95 264.32 24.23 o
-5 6 1 1.03 2.47 12.70 <
-4 6 1 784.44 798.62 30.06 o
-3 6 1 602.30 632.65 28.64 o
-2 6 1 326.16 271.92 20.76 o
-1 6 1 572.53 494.35 18.80 o
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1 6 1 2225.37 2562.07 27.66 o
2 6 1 170.46 143.58 11.46 o
3 6 1 144.95 150.13 14.70 o
4 6 1 1.36 12.58 8.28 <
5 6 1 153.32 110.66 27.44 o
6 6 1 1.77 2.41 14.57 <
-4 7 1 133.44 149.30 26.04 o
-3 7 1 0.25 5.46 12.94 <
-2 7 1 73.58 64.03 15.14 o
-1 7 1 74.46 44.17 11.09 o
0 7 1 9.39 5.07 6.09 <
1 7 1 1223.62 1247.45 22.59 o
2 7 1 286.46 300.72 16.39 o
3 7 1 0.28 4.94 7.28 <
4 7 1 62.83 52.04 16.77 o
5 7 1 7.74 6.71 16.24 <
-3 8 1 1.45 6.66 12.59 <
-2 8 1 0.31 8.82 10.20 <
-1 8 1 513.23 567.51 28.92 o
0 8 1 12.87 13.34 10.88 <
1 8 1 1.01 3.58 10.38 <
2 8 1 42.60 61.46 16.05 o
3 8 1 48.20 49.65 15.14 o
4 8 1 43.26 42.34 16.58 <
-1 9 1 51.97 31.77 13.52 <
0 9 1 301.61 330.29 31.41 o
1 9 1 50.07 45.76 25.97 <
2 9 1 17.11 26.56 20.81 <
-2 -8 2 61.33 70.31 21.90 o
-1 -8 2 3.86 11.04 9.95 <
0 -8 2 72.75 74.58 19.11 o
1 -8 2 110.03 127.21 23.15 o
2 -8 2 108.57 100.95 19.62 o
-4 -7 2 0.82 10.81 16.62 <
-3 -7 2 176.07 181.35 30.76 o
-2 -7 2 94.83 102.90 21.79 o
-1 -7 2 1.63 4.38 6.85 <
0 -7 2 376.90 455.86 18.79 o
1 -7 2 151.39 133.53 14.34 o
2 -7 2 311.08 314.96 18.16 o
3 -7 2 28.73 25.96 14.75 <
4 -7 2 64.78 58.07 19.31 o
-5 -6 2 16.08 7.50 21.45 <
-4 -6 2 0.78 6.01 9.56 <
-3 -6 2 1.80 9.23 9.24 <
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-1 -6 2 34.62 44.63 12.11 o
0 -6 2 304.97 312.21 15.32 o
1 -6 2 159.60 145.72 11.62 o
2 -6 2 12.55 21.58 11.79 <
3 -6 2 219.24 207.55 17.29 o
4 -6 2 0.62 15.39 12.85 <
5 -6 2 164.60 145.15 25.08 o
-6 -5 2 15.41 11.44 17.41 <
-5 -5 2 15.40 6.91 15.95 <
-4 -5 2 408.74 408.68 25.63 o
-3 -5 2 0.30 12.21 11.81 <
-2 -5 2 2.61 11.17 12.59 <
-1 -5 2 462.24 484.25 17.20 o
0 -5 2 20.44 19.40 7.14 <
1 -5 2 16.05 13.24 6.88 <
2 -5 2 192.16 176.17 11.12 o
3 -5 2 859.64 747.22 18.49 o
4 -5 2 1050.04 1113.08 29.16 o
5 -5 2 27.20 27.97 11.72 <
6 -5 2 32.92 19.55 21.52 <
-6 -4 2 19.35 24.55 14.61 <
-5 -4 2 18.91 16.21 10.72 <
-4 -4 2 94.12 90.48 12.62 o
-3 -4 2 1708.91 2016.73 25.84 o
-2 -4 2 2.57 1.98 3.67 <
-1 -4 2 67.50 60.51 7.08 o
0 -4 2 511.19 467.08 7.83 o
1 -4 2 850.86 852.00 9.30 o
2 -4 2 2455.78 2443.18 14.06 o
3 -4 2 206.20 198.85 9.72 o
4 -4 2 130.82 125.30 11.35 o
5 -4 2 38.52 35.85 8.66 o
6 -4 2 108.05 113.13 16.14 o
7 -4 2 116.13 125.66 26.87 o
-7 -3 2 121.65 102.82 22.58 o
-6 -3 2 58.75 40.49 13.99 <
-5 -3 2 1310.18 1417.24 25.65 o
-4 -3 2 72.22 50.02 11.81 o
-3 -3 2 1.67 5.74 5.42 <
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-1 -3 2 1134.00 1031.91 12.63 o
0 -3 2 3245.00 2986.10 15.40 o
1 -3 2 56.30 60.89 5.19 o
2 -3 2 3342.78 3088.67 12.59 o
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4 -3 2 312.58 297.69 13.05 o
5 -3 2 17.39 17.98 7.47 <
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7 -3 2 703.63 783.47 23.97 o
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-5 -2 2 624.56 714.61 24.11 o
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-3 -2 2 378.63 375.84 14.13 o
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-1 -2 2 979.30 945.56 11.30 o
0 -2 2 5411.54 5223.10 18.54 o
1 -2 2 1460.36 1558.58 9.90 o
2 -2 2 176.73 155.56 4.35 o
3 -2 2 1019.12 1016.99 10.66 o
4 -2 2 5.16 6.44 5.75 <
5 -2 2 1077.48 1152.48 17.94 o
6 -2 2 167.74 138.85 15.77 o
7 -2 2 4.40 10.59 8.83 <
8 -2 2 30.58 30.96 12.56 <
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-6 -1 2 98.20 107.87 17.00 o
-5 -1 2 104.90 94.88 11.88 o
-4 -1 2 293.77 277.19 12.70 o
-3 -1 2 400.30 381.43 10.98 o
-2 -1 2 127.64 109.01 8.16 o
-1 -1 2 187.04 153.40 6.46 o
0 -1 2 60.25 72.15 4.86 o
1 -1 2 2412.94 2492.14 18.40 o
2 -1 2 4605.24 5023.40 21.83 o
3 -1 2 31.52 27.23 5.35 o
4 -1 2 3441.85 3757.71 28.77 o
5 -1 2 798.39 830.31 19.61 o
6 -1 2 70.91 59.87 13.10 o
7 -1 2 455.70 440.03 19.56 o
8 -1 2 186.49 161.05 18.34 o
-7 0 2 77.84 76.07 23.32 o
-6 0 2 265.78 250.45 16.98 o
-5 0 2 2.75 6.88 6.96 <
-4 0 2 17.75 13.52 6.31 <
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-2 0 2 1089.94 1134.98 12.71 o
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1 0 2 8.10 7.52 3.73 <
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5 1 9 7.67 9.31 18.28 <
0 2 9 12.95 17.53 16.51 <
1 2 9 24.08 23.55 13.84 <
2 2 9 30.57 39.22 16.86 <
3 2 9 7.04 5.64 11.67 <
4 2 9 89.49 69.04 19.10 o
5 2 9 145.14 149.06 28.18 o
1 3 9 59.19 45.73 22.65 <
2 3 9 73.30 62.36 19.50 o
3 3 9 107.90 83.39 18.62 o
4 3 9 46.57 31.33 14.97 <
2 4 9 77.07 54.82 24.81 <
3 4 9 830.06 840.36 36.94 o
4 4 9 12.78 9.22 13.06 <