#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/05/2230537.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230537_Fobs loop_ _publ_author_name 'Yuan, Jing-Kun' 'Bai, Ying' 'Kou, Fan' 'Jia, Fei' 'Wu, Hui-Lu' _publ_section_title ; Bis[N,N-bis(1-allyl-1H-benzimidazol-2-ylmethyl-\kN^3^)benzylamine-\kN]cadmium dipicrate ; _journal_coeditor_code XU5213 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m800 _journal_page_last m801 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 90.595 _cell_angle_beta 110.890 _cell_angle_gamma 106.325 _cell_length_a 13.9030 _cell_length_b 14.1460 _cell_length_c 19.3300 _exptl_crystal_F_000 1508.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file xu5213Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 400.01 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 129.94 201.85 19.43 o 3 0 0 546.32 405.56 17.41 o 4 0 0 57.54 69.38 18.86 o 5 0 0 1782.82 1854.45 42.16 o 6 0 0 54.40 39.30 20.61 o 7 0 0 2372.76 2526.59 58.07 o 8 0 0 1474.18 1453.61 46.43 o 9 0 0 1121.76 1075.61 43.38 o 10 0 0 1345.44 1486.19 53.56 o 11 0 0 302.60 307.43 39.70 o 12 0 0 489.83 522.35 50.23 o 13 0 0 363.23 293.05 53.96 o -13 1 0 303.76 370.89 51.45 o -12 1 0 599.37 740.15 44.84 o -11 1 0 1106.72 1203.80 51.56 o -10 1 0 118.97 103.35 21.57 o -9 1 0 51.79 43.80 16.27 o -8 1 0 99.58 116.10 18.64 o -7 1 0 607.91 589.65 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2664.37 76.77 o -6 7 0 1502.98 1391.27 137.73 o -5 7 0 7351.86 7371.25 117.52 o -4 7 0 34.78 55.10 14.43 o -3 7 0 521.89 589.17 23.35 o -2 7 0 2354.35 2207.10 38.07 o -1 7 0 2363.84 2631.27 42.05 o 0 7 0 1556.69 1443.13 32.15 o 1 7 0 1040.68 1135.06 55.56 o 2 7 0 1907.28 1979.66 77.70 o 3 7 0 743.21 670.40 49.13 o 4 7 0 1398.05 1378.00 72.01 o 5 7 0 471.11 420.62 47.89 o 6 7 0 355.34 427.47 52.25 o 7 7 0 91.54 103.17 39.85 o 8 7 0 143.58 110.27 39.54 o 9 7 0 70.78 47.07 37.90 o 10 7 0 206.17 159.60 48.99 o 11 7 0 496.04 570.71 72.09 o -15 8 0 108.90 134.05 53.23 o -14 8 0 351.73 528.07 47.01 o -13 8 0 505.09 518.70 45.17 o -12 8 0 458.64 550.40 69.77 o -11 8 0 1232.30 1338.33 77.04 o -10 8 0 1.12 -24.35 20.20 o -9 8 0 1264.80 1279.16 53.45 o -8 8 0 277.66 251.32 27.68 o -7 8 0 1189.29 1244.03 49.07 o -6 8 0 20.73 37.69 16.09 o -5 8 0 423.78 501.58 30.80 o -4 8 0 1460.84 1425.98 30.07 o -3 8 0 3970.63 4014.36 57.38 o -2 8 0 301.31 264.83 17.57 o -1 8 0 1108.55 1048.65 39.84 o 0 8 0 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