#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/05/2230556.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230556_Fobs loop_ _publ_author_name 'Qiang, Hong' 'Zhang, Fan' _publ_section_title ; trans-Dichloridobis[(6-nicotinoyl-2-pyridyl-\kN^6^)(3-pyridyl-\kN)methanone]copper(II) ; _journal_coeditor_code ZQ2102 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m758 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 121.522 _cell_angle_gamma 90.000 _cell_length_a 18.7283 _cell_length_b 11.8971 _cell_length_c 16.6946 _exptl_crystal_F_000 1452.00 _reflns_d_resolution_high 0.7488 _[local]_cod_data_source_file zq2102Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' y in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 529.00 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 54065.39 52500.70 4536.26 o 4 0 0 85854.27 81748.62 3979.17 o 6 0 0 45365.85 45917.21 966.18 o 8 0 0 356.94 420.82 10.41 o 10 0 0 6.99 8.58 5.12 o 12 0 0 1941.34 2041.70 59.72 o 14 0 0 2475.40 2437.73 51.14 o 16 0 0 292.10 278.37 17.15 o 18 0 0 1124.07 1122.21 47.76 o 20 0 0 1136.19 1259.41 54.77 o 1 1 0 21490.06 21038.66 475.44 o 3 1 0 48467.64 51037.60 474.36 o 5 1 0 31739.57 32971.76 336.22 o 7 1 0 3329.79 3669.68 40.66 o 9 1 0 169.19 188.02 4.91 o 11 1 0 52.89 45.83 3.83 o 13 1 0 1919.61 1866.21 33.69 o 15 1 0 529.97 493.34 28.15 o 17 1 0 366.01 345.97 24.06 o 19 1 0 0.07 -6.07 13.83 o 21 1 0 2.57 -10.62 10.62 o 0 2 0 55093.38 55456.08 854.61 o 2 2 0 1126.07 1082.29 12.21 o 4 2 0 3726.43 3442.22 34.23 o 6 2 0 5186.08 5081.57 54.40 o 8 2 0 960.00 668.08 9.74 o 10 2 0 8791.94 9107.16 88.28 o 12 2 0 28.29 28.19 6.14 o 14 2 0 2637.01 2445.03 42.53 o 16 2 0 211.81 212.72 12.97 o 18 2 0 27.73 24.16 8.91 o 20 2 0 71.72 99.01 15.06 o 1 3 0 622.53 670.88 10.74 o 3 3 0 2411.12 2704.58 32.66 o 5 3 0 22763.19 24377.04 225.39 o 7 3 0 209.70 282.73 8.00 o 9 3 0 62.88 77.84 4.03 o 11 3 0 98.17 101.82 5.85 o 13 3 0 0.29 -0.37 6.48 o 15 3 0 834.20 850.20 22.43 o 17 3 0 17.12 16.49 7.97 o 19 3 0 115.50 92.55 11.47 o 0 4 0 3469.29 3737.00 108.33 o 2 4 0 2928.32 2678.52 42.95 o 4 4 0 34925.66 36977.29 340.35 o 6 4 0 819.95 545.19 14.47 o 8 4 0 16740.99 17757.73 166.83 o 10 4 0 16260.95 16232.85 153.97 o 12 4 0 1055.49 1035.88 22.72 o 14 4 0 822.47 821.26 21.56 o 16 4 0 35.36 34.80 8.90 o 18 4 0 15.29 16.32 9.08 o 20 4 0 9.65 -1.29 11.68 o 1 5 0 114.89 120.79 3.93 o 3 5 0 8881.48 9294.57 112.85 o 5 5 0 6825.70 7380.56 71.76 o 7 5 0 791.51 782.02 11.82 o 9 5 0 74.03 76.10 4.41 o 11 5 0 21.72 20.03 4.91 o 13 5 0 284.77 301.38 13.24 o 15 5 0 1.63 -5.42 6.12 o 17 5 0 158.44 163.16 17.00 o 19 5 0 3.38 14.63 18.57 o 0 6 0 8104.39 7462.89 94.03 o 2 6 0 2493.89 2214.42 34.33 o 4 6 0 10507.39 10425.79 115.70 o 6 6 0 1883.11 1652.28 30.10 o 8 6 0 524.34 538.10 10.07 o 10 6 0 1606.71 1550.45 20.71 o 12 6 0 880.65 882.11 20.42 o 14 6 0 735.45 751.91 27.16 o 16 6 0 506.40 454.49 40.46 o 18 6 0 604.92 619.61 45.10 o 1 7 0 568.33 668.11 10.86 o 3 7 0 1818.84 1861.35 25.28 o 5 7 0 1406.10 1403.01 21.04 o 7 7 0 776.45 801.60 19.45 o 9 7 0 89.95 103.23 6.50 o 11 7 0 16.26 12.02 5.74 o 13 7 0 118.34 93.00 13.02 o 15 7 0 78.62 91.76 13.64 o 17 7 0 61.43 54.08 34.96 o 19 7 0 0.06 0.09 12.61 o 0 8 0 18761.55 18076.10 274.63 o 2 8 0 11351.04 11665.22 167.38 o 4 8 0 5716.05 6040.72 69.52 o 6 8 0 3401.72 3252.55 42.49 o 8 8 0 274.34 285.63 9.62 o 10 8 0 112.07 136.55 7.78 o 12 8 0 34.80 53.27 16.35 o 14 8 0 375.96 350.21 21.22 o 16 8 0 327.83 357.97 22.70 o 18 8 0 270.18 313.43 23.72 o 1 9 0 56.47 50.94 5.61 o 3 9 0 73.88 86.23 7.81 o 5 9 0 1831.58 1728.00 26.15 o 7 9 0 967.75 937.39 18.02 o 9 9 0 502.76 487.01 14.43 o 11 9 0 7.26 9.68 8.76 o 13 9 0 555.89 651.10 27.39 o 15 9 0 28.87 1.86 17.24 o 17 9 0 18.30 14.36 13.77 o 0 10 0 3790.30 3810.33 70.95 o 2 10 0 4237.36 4060.54 60.28 o 4 10 0 4814.67 4882.26 70.36 o 6 10 0 4484.53 4464.13 65.70 o 8 10 0 4436.88 4490.69 57.03 o 10 10 0 1619.34 1610.12 27.55 o 12 10 0 828.19 805.80 22.49 o 14 10 0 544.25 536.18 25.90 o 16 10 0 172.67 172.52 19.81 o 1 11 0 222.63 223.82 11.61 o 3 11 0 68.06 28.76 6.61 o 5 11 0 78.49 86.77 10.72 o 7 11 0 947.37 982.59 23.95 o 9 11 0 161.23 156.12 11.84 o 11 11 0 48.96 52.73 11.35 o 13 11 0 3.42 2.65 18.57 o 15 11 0 43.62 42.82 20.65 o 0 12 0 154.90 158.46 13.73 o 2 12 0 372.64 364.40 14.70 o 4 12 0 1341.31 1330.97 41.50 o 6 12 0 792.87 874.88 23.01 o 8 12 0 919.04 939.85 24.61 o 10 12 0 1447.68 1603.19 35.08 o 12 12 0 108.28 119.79 14.66 o 1 13 0 0.08 -9.41 11.09 o 3 13 0 331.77 309.49 14.67 o 5 13 0 365.45 348.49 16.02 o 7 13 0 134.80 142.09 11.95 o 9 13 0 19.63 20.96 11.05 o 11 13 0 0.02 -9.70 9.70 o 0 14 0 2554.40 2473.25 77.35 o 2 14 0 1974.99 2053.32 45.04 o 4 14 0 2289.30 2274.41 44.22 o 6 14 0 386.71 401.29 17.51 o 8 14 0 418.36 428.80 29.24 o 10 14 0 110.51 90.84 14.93 o 1 15 0 6.48 9.50 12.60 o 3 15 0 137.85 192.14 14.70 o 5 15 0 107.55 104.51 14.54 o -21 1 1 124.05 132.83 16.21 o -19 1 1 581.18 591.22 25.26 o -17 1 1 1941.66 1832.75 36.24 o -15 1 1 4.63 4.41 5.60 o -13 1 1 1083.27 981.78 21.65 o -11 1 1 813.97 801.14 15.65 o -9 1 1 65.00 143.34 6.04 o -7 1 1 18822.55 19316.02 186.64 o -5 1 1 16903.36 17399.51 161.24 o -3 1 1 8268.40 8719.85 91.70 o -1 1 1 6144.52 6319.84 75.65 o 1 1 1 26434.61 28310.80 293.69 o 3 1 1 32197.29 32318.89 332.22 o 5 1 1 3800.50 3653.08 39.81 o 7 1 1 993.81 979.01 12.94 o 9 1 1 9.62 10.34 2.32 o 11 1 1 21.72 8.95 6.50 o 13 1 1 2851.22 2741.71 45.67 o 15 1 1 1566.62 1609.39 32.93 o 17 1 1 1122.63 1105.77 27.71 o 19 1 1 531.31 573.98 25.52 o -20 2 1 34.58 39.83 12.46 o -18 2 1 35.27 34.11 8.87 o -16 2 1 366.66 348.63 15.11 o -14 2 1 4041.82 3888.47 61.09 o -12 2 1 336.56 264.36 10.59 o -10 2 1 4429.15 4663.22 58.11 o -8 2 1 5.94 21.14 2.41 o -6 2 1 10548.41 10865.94 102.47 o -4 2 1 18446.12 20616.81 190.41 o -2 2 1 1442.42 1410.70 14.87 o 0 2 1 1811.65 2259.64 55.01 o 2 2 1 1981.18 2191.20 31.87 o 4 2 1 24703.76 25857.33 238.60 o 6 2 1 9842.80 10460.36 98.98 o 8 2 1 222.52 226.19 5.18 o 10 2 1 177.19 147.38 6.08 o 12 2 1 277.42 224.52 11.25 o 14 2 1 741.86 769.84 20.94 o 16 2 1 1.22 -6.67 6.67 o 18 2 1 69.86 77.50 10.71 o 20 2 1 11.40 -7.35 10.79 o -21 3 1 249.81 310.58 21.30 o -19 3 1 208.59 204.26 14.25 o -17 3 1 30.08 43.62 8.60 o -15 3 1 4976.72 4825.99 72.20 o -13 3 1 977.03 971.31 22.15 o -11 3 1 4033.96 3722.51 39.91 o -9 3 1 10822.25 11178.37 106.94 o -7 3 1 14225.62 15251.21 143.09 o -5 3 1 68.67 43.99 2.40 o -3 3 1 16.28 12.14 1.45 o -1 3 1 93.75 42.18 3.28 o 1 3 1 4737.04 5310.96 51.36 o 3 3 1 4732.78 4632.11 49.63 o 5 3 1 8799.32 8839.56 99.76 o 7 3 1 10882.08 10995.82 104.54 o 9 3 1 2890.42 2653.18 29.36 o 11 3 1 1986.89 2034.68 35.22 o 13 3 1 1419.51 1333.74 27.94 o 15 3 1 14.03 12.89 6.88 o 17 3 1 64.20 50.13 9.60 o 19 3 1 8.24 1.45 8.58 o -20 4 1 62.28 99.10 14.97 o -18 4 1 326.45 312.19 16.19 o -16 4 1 24.09 17.72 7.35 o -14 4 1 110.48 107.76 10.69 o -12 4 1 23.29 24.55 4.65 o -10 4 1 143.48 184.27 6.23 o -8 4 1 90.09 131.94 6.35 o -6 4 1 2545.32 3187.63 34.89 o -4 4 1 186.86 205.64 5.53 o -2 4 1 721.66 731.83 11.31 o 0 4 1 153.66 155.62 3.93 o 2 4 1 10.78 21.59 5.22 o 4 4 1 462.52 509.90 8.54 o 6 4 1 1789.55 2148.88 24.11 o 8 4 1 5.06 13.15 2.76 o 10 4 1 464.99 491.30 11.33 o 12 4 1 991.64 919.79 25.28 o 14 4 1 1.20 4.09 6.76 o 16 4 1 196.78 194.02 13.07 o 18 4 1 3.08 -16.08 16.08 o 20 4 1 9.24 -18.95 18.95 o -19 5 1 13.34 27.75 12.46 o -17 5 1 223.15 273.02 19.74 o -15 5 1 2079.75 2016.78 38.07 o -13 5 1 4091.71 4012.43 60.84 o -11 5 1 7242.47 7132.42 72.18 o -9 5 1 14797.28 15912.95 151.06 o -7 5 1 10695.36 10592.67 101.70 o -5 5 1 3080.52 3139.09 32.99 o -3 5 1 342.54 536.47 11.15 o -1 5 1 13140.60 13423.71 116.05 o 1 5 1 2868.07 3655.72 41.82 o 3 5 1 93.73 158.61 7.91 o 5 5 1 3926.48 3630.72 37.81 o 7 5 1 742.29 632.01 10.43 o 9 5 1 926.14 868.03 14.63 o 11 5 1 554.29 522.21 15.72 o 13 5 1 142.00 186.54 11.30 o 15 5 1 6.36 -2.59 9.08 o 17 5 1 17.23 -6.78 10.43 o 19 5 1 54.31 89.56 16.37 o -20 6 1 14.06 29.34 14.04 o -18 6 1 10.76 5.97 11.15 o -16 6 1 11.97 23.88 10.70 o -14 6 1 391.74 418.63 30.79 o -12 6 1 4.47 5.52 5.34 o -10 6 1 5546.15 5508.13 57.31 o -8 6 1 3291.87 3213.35 35.30 o -6 6 1 4456.51 4518.88 46.52 o -4 6 1 3666.54 3941.01 46.18 o -2 6 1 7117.04 9006.78 87.71 o 0 6 1 2583.42 2540.34 28.24 o 2 6 1 3.97 1.60 4.68 o 4 6 1 1401.18 1433.32 24.13 o 6 6 1 525.56 484.60 11.45 o 8 6 1 626.60 670.93 11.98 o 10 6 1 707.72 631.39 16.56 o 12 6 1 615.39 612.05 23.91 o 14 6 1 25.42 31.82 12.03 o 16 6 1 2.55 -2.85 10.50 o 18 6 1 90.12 113.95 16.78 o -19 7 1 317.90 404.43 26.04 o -17 7 1 269.95 297.14 21.26 o -15 7 1 127.74 125.81 19.52 o -13 7 1 44.45 33.36 7.08 o -11 7 1 3256.05 3157.34 41.66 o -9 7 1 423.10 402.69 10.82 o -7 7 1 1751.74 1595.47 23.74 o -5 7 1 12426.49 11763.02 127.05 o -3 7 1 13033.70 12894.30 124.43 o -1 7 1 14804.23 14844.54 129.11 o 1 7 1 8790.97 8715.66 94.97 o 3 7 1 2920.93 2855.40 35.87 o 5 7 1 422.83 495.22 11.17 o 7 7 1 1029.94 959.36 16.98 o 9 7 1 3908.35 3652.51 47.66 o 11 7 1 36.78 17.15 6.86 o 13 7 1 1071.40 1046.03 33.51 o 15 7 1 716.17 763.36 30.08 o 17 7 1 522.50 577.68 28.56 o -18 8 1 21.67 7.00 13.21 o -16 8 1 14.78 25.29 12.25 o -14 8 1 15.09 -5.54 9.50 o -12 8 1 43.22 47.84 8.06 o -10 8 1 31.58 27.66 5.23 o -8 8 1 443.25 445.47 11.53 o -6 8 1 404.26 365.83 10.26 o -4 8 1 723.21 742.04 19.98 o -2 8 1 21.67 20.01 3.43 o 0 8 1 19.94 10.36 3.16 o 2 8 1 902.83 974.28 16.36 o 4 8 1 915.27 874.14 15.92 o 6 8 1 712.97 681.96 14.27 o 8 8 1 196.35 171.28 10.61 o 10 8 1 882.83 797.24 20.22 o 12 8 1 648.75 597.13 24.89 o 14 8 1 127.04 111.70 14.96 o 16 8 1 0.08 -0.23 11.34 o -17 9 1 245.08 281.79 22.45 o -15 9 1 781.53 798.09 30.88 o -13 9 1 115.35 99.85 12.81 o -11 9 1 3408.24 3406.81 46.04 o -9 9 1 4056.47 4006.59 60.78 o -7 9 1 634.39 562.65 13.45 o -5 9 1 19081.25 18738.91 199.71 o -3 9 1 11642.80 11748.04 149.56 o -1 9 1 7182.78 7255.83 84.68 o 1 9 1 3406.79 3506.45 51.97 o 3 9 1 7336.71 7223.31 96.47 o 5 9 1 159.49 156.15 9.82 o 7 9 1 334.25 359.83 11.46 o 9 9 1 2773.05 2743.32 38.55 o 11 9 1 829.22 861.97 47.67 o 13 9 1 393.03 420.49 27.76 o 15 9 1 963.90 932.94 34.71 o -16 10 1 2.92 28.68 13.02 o -14 10 1 23.65 19.30 10.97 o -12 10 1 0.17 -7.05 7.05 o -10 10 1 771.02 747.57 17.29 o -8 10 1 1356.33 1236.73 26.57 o -6 10 1 471.70 397.39 14.44 o -4 10 1 2958.46 2789.56 45.21 o -2 10 1 46.50 46.76 5.90 o 0 10 1 860.41 839.16 17.88 o 2 10 1 4955.14 4600.13 66.56 o 4 10 1 276.56 252.15 15.03 o 6 10 1 279.79 280.11 13.27 o 8 10 1 1030.55 1003.14 27.00 o 10 10 1 2682.07 2546.24 54.35 o 12 10 1 369.70 361.91 21.45 o 14 10 1 133.23 119.48 22.74 o -15 11 1 762.42 730.58 50.79 o -13 11 1 715.25 818.46 29.74 o -11 11 1 1028.24 1039.44 25.49 o -9 11 1 814.92 841.24 22.26 o -7 11 1 9.52 6.91 6.57 o -5 11 1 11.60 20.55 6.51 o -3 11 1 247.32 228.63 12.01 o -1 11 1 9.67 0.22 4.95 o 1 11 1 333.22 326.96 13.05 o 3 11 1 736.18 858.29 21.68 o 5 11 1 4181.79 3949.60 61.36 o 7 11 1 1512.07 1630.18 32.78 o 9 11 1 1185.00 1265.02 28.41 o 11 11 1 512.08 537.75 23.40 o 13 11 1 15.77 43.58 22.17 o -14 12 1 4.04 39.79 22.36 o -12 12 1 241.83 258.56 39.70 o -10 12 1 2.21 -6.23 6.23 o -8 12 1 198.48 192.84 17.40 o -6 12 1 318.72 311.50 14.49 o -4 12 1 61.62 66.69 8.93 o -2 12 1 80.46 60.24 8.57 o 0 12 1 28.77 38.97 7.36 o 2 12 1 1.06 1.13 6.14 o 4 12 1 126.84 132.13 10.53 o 6 12 1 103.88 97.75 10.03 o 8 12 1 109.64 95.86 14.74 o 10 12 1 285.68 311.38 19.77 o 12 12 1 83.02 91.71 25.20 o -11 13 1 199.81 188.04 17.44 o -9 13 1 1301.50 1370.20 32.01 o -7 13 1 1142.91 1123.22 28.07 o -5 13 1 302.44 318.44 19.10 o -3 13 1 77.76 94.12 10.93 o -1 13 1 1414.91 1451.65 37.19 o 1 13 1 509.03 520.24 18.14 o 3 13 1 178.11 214.04 25.66 o 5 13 1 1688.29 1651.13 34.88 o 7 13 1 665.12 637.44 21.00 o 9 13 1 207.47 219.76 18.33 o 11 13 1 142.83 132.34 16.86 o -10 14 1 146.49 133.36 13.09 o -8 14 1 206.11 203.37 14.21 o -6 14 1 244.86 268.00 15.99 o -4 14 1 365.49 386.19 17.06 o -2 14 1 118.90 119.45 22.36 o 0 14 1 467.06 533.22 19.45 o 2 14 1 712.60 689.35 24.95 o 4 14 1 350.56 380.97 17.32 o 6 14 1 35.80 22.42 8.65 o 8 14 1 16.18 2.59 8.74 o -7 15 1 125.36 119.58 19.29 o -5 15 1 810.43 771.05 24.80 o -3 15 1 803.59 817.56 29.08 o -1 15 1 1693.36 1646.03 70.32 o 1 15 1 416.74 397.61 18.50 o 3 15 1 15.46 -8.13 8.13 o 5 15 1 42.44 41.43 9.71 o -22 0 2 65.62 75.23 20.65 o -20 0 2 493.13 504.85 33.92 o -18 0 2 11.03 7.96 13.26 o -16 0 2 836.51 857.86 26.66 o -14 0 2 1256.60 1241.98 30.63 o -12 0 2 1253.21 1306.97 31.98 o -10 0 2 2469.70 2446.50 35.14 o -8 0 2 6457.65 5994.32 76.94 o -6 0 2 11452.00 11276.90 118.23 o -4 0 2 6251.65 6567.35 69.93 o -2 0 2 63328.66 61199.60 2951.64 o 0 0 2 16729.98 16635.76 244.78 o 2 0 2 6659.53 7243.20 201.44 o 6 0 2 15982.27 16961.82 358.51 o 8 0 2 13875.50 14152.62 304.45 o 10 0 2 3296.35 3329.47 85.54 o 12 0 2 6739.75 6309.62 150.90 o 14 0 2 1360.72 1326.63 48.33 o 16 0 2 15.64 14.11 9.64 o 18 0 2 1069.45 1162.55 50.98 o 20 0 2 0.92 7.96 17.24 o -21 1 2 0.99 -3.01 10.79 o -19 1 2 1.18 -8.05 8.58 o -17 1 2 15.98 12.52 7.21 o -15 1 2 668.19 637.79 15.39 o -13 1 2 301.61 301.93 6.88 o -11 1 2 2201.52 2180.52 21.15 o -9 1 2 2299.17 2353.65 28.18 o -7 1 2 7725.78 8477.96 80.82 o -5 1 2 659.26 675.16 13.09 o -3 1 2 11691.98 12707.85 122.32 o -1 1 2 6329.13 6260.40 90.88 o 1 1 2 10369.36 10808.56 111.49 o 3 1 2 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438.13 31.08 o -6 2 20 281.85 339.22 23.99 o -4 2 20 393.17 421.15 29.37 o -19 3 20 52.61 47.99 12.19 o -17 3 20 2.32 -7.69 10.22 o -15 3 20 207.93 219.95 18.16 o -13 3 20 79.00 78.12 12.78 o -11 3 20 218.13 186.18 23.78 o -9 3 20 0.26 -1.41 9.04 o -7 3 20 15.54 32.59 17.81 o -5 3 20 84.19 71.03 14.98 o -18 4 20 480.87 481.53 21.31 o -16 4 20 1064.16 1102.17 29.54 o -14 4 20 1123.26 1103.78 29.14 o -12 4 20 110.67 116.03 11.99 o -10 4 20 49.29 23.40 10.59 o -8 4 20 5.91 5.02 11.17 o -6 4 20 13.66 -4.11 11.68 o -17 5 20 19.25 13.92 9.25 o -15 5 20 28.21 27.52 9.84 o -13 5 20 14.83 3.92 8.81 o -11 5 20 88.62 66.89 10.49 o -9 5 20 190.58 162.56 13.15 o -7 5 20 1.00 16.68 18.76 o -16 6 20 311.27 340.76 18.70 o -14 6 20 492.95 471.76 34.37 o -12 6 20 232.34 255.00 16.19 o -10 6 20 374.91 366.85 17.81 o -8 6 20 517.48 509.09 31.93 o -11 7 20 0.47 -0.76 16.49 o -19 1 21 206.31 212.00 51.83 o -17 1 21 104.68 104.25 16.01 o -15 1 21 615.13 584.66 25.84 o -13 1 21 759.80 731.66 27.87 o -11 1 21 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