#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/06/2230600.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230600_Fobs loop_ _publ_author_name 'Du, Chao-Jun' 'Song, Xing-Hua' 'Wang, Li-Sheng' 'Du, Chao-Ling' _publ_section_title ; Diaquabis(5-carboxy-1H-imidazole-4-carboxylato-\k^2^N^3^,O^4^)iron(II) ; _journal_coeditor_code CV5111 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m997 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.733 _cell_angle_gamma 90.000 _cell_length_a 5.0676 _cell_length_b 22.7690 _cell_length_c 6.6725 _exptl_crystal_F_000 408.00 _reflns_d_resolution_high 0.8348 _[local]_cod_data_source_file cv5111Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 115.09 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1148.98 1049.75 14.09 o 2 0 0 159.54 157.53 9.09 o 3 0 0 157.33 152.92 10.11 o 4 0 0 3.28 4.34 5.57 o 1 1 0 85.86 93.63 3.26 o 2 1 0 302.55 315.58 17.74 o 3 1 0 270.20 282.75 9.13 o 4 1 0 30.29 27.48 5.01 o 5 1 0 7.12 4.44 7.32 o 1 2 0 2225.02 2101.76 15.13 o 2 2 0 4890.87 4782.52 32.40 o 3 2 0 651.63 653.63 13.31 o 4 2 0 139.16 136.01 8.29 o 5 2 0 155.62 159.39 15.23 o 1 3 0 705.51 713.56 9.25 o 2 3 0 63.32 56.88 3.85 o 3 3 0 702.19 728.20 14.19 o 4 3 0 934.54 920.23 18.42 o 5 3 0 1.88 -2.45 7.47 o 0 4 0 2255.58 2213.47 28.12 o 1 4 0 347.82 360.45 5.97 o 2 4 0 1663.29 1651.69 17.56 o 3 4 0 530.63 594.95 15.43 o 4 4 0 247.00 264.46 10.67 o 5 4 0 246.32 288.24 19.11 o 1 5 0 3483.32 3475.26 24.80 o 2 5 0 86.90 95.93 4.82 o 3 5 0 0.17 -0.32 2.50 o 4 5 0 61.10 51.90 9.03 o 5 5 0 29.05 44.92 10.19 o 0 6 0 351.43 348.38 11.80 o 1 6 0 2431.07 2388.02 20.23 o 2 6 0 1691.72 1703.65 18.05 o 3 6 0 39.70 38.16 4.45 o 4 6 0 41.84 40.00 9.17 o 5 6 0 170.49 207.14 17.91 o 1 7 0 203.93 224.72 6.15 o 2 7 0 33.53 39.99 3.55 o 3 7 0 396.57 383.89 12.61 o 4 7 0 148.02 157.21 14.60 o 5 7 0 0.01 -13.27 9.43 o 0 8 0 720.07 819.15 20.75 o 1 8 0 938.34 847.07 12.36 o 2 8 0 16.61 26.30 4.60 o 3 8 0 1022.65 985.87 16.55 o 4 8 0 990.83 1022.91 45.09 o 5 8 0 169.08 196.84 26.00 o 1 9 0 2315.97 2475.64 21.07 o 2 9 0 29.60 30.16 5.84 o 3 9 0 749.34 709.31 20.42 o 4 9 0 0.13 -1.18 8.86 o 5 9 0 17.96 26.02 15.61 o 0 10 0 5970.81 6346.83 75.70 o 1 10 0 224.96 234.01 6.66 o 2 10 0 1235.80 1248.56 19.08 o 3 10 0 1201.95 1249.18 45.19 o 4 10 0 46.16 83.85 15.61 o 5 10 0 140.63 145.35 24.30 o 1 11 0 0.12 0.24 1.84 o 2 11 0 175.13 168.88 7.29 o 3 11 0 0.63 -6.75 4.50 o 4 11 0 1.10 -2.60 8.40 o 5 11 0 10.08 -10.30 12.02 o 0 12 0 625.10 645.23 22.07 o 1 12 0 2067.11 2184.98 24.66 o 2 12 0 1148.84 1152.97 24.20 o 3 12 0 439.61 490.34 30.45 o 4 12 0 137.58 168.76 22.56 o 1 13 0 9.76 20.71 3.48 o 2 13 0 18.60 11.55 4.94 o 3 13 0 27.70 7.94 8.37 o 4 13 0 225.10 190.18 24.73 o 0 14 0 86.59 87.20 10.08 o 1 14 0 2.36 0.25 2.22 o 2 14 0 902.42 915.08 22.74 o 3 14 0 1109.61 1092.49 47.01 o 4 14 0 693.56 746.54 42.76 o 1 15 0 13.76 9.59 2.91 o 2 15 0 216.20 259.76 22.38 o 3 15 0 6.90 3.36 8.80 o 4 15 0 3.16 -3.05 8.26 o 0 16 0 6.04 1.49 4.33 o 1 16 0 821.24 837.27 17.44 o 2 16 0 285.06 298.24 24.33 o 3 16 0 36.75 45.43 14.70 o 4 16 0 339.00 336.46 31.39 o 1 17 0 246.95 247.55 13.87 o 2 17 0 389.22 406.33 28.23 o 3 17 0 91.68 121.74 20.54 o 4 17 0 0.45 -2.48 10.35 o 0 18 0 173.90 155.14 14.64 o 1 18 0 887.35 911.63 25.39 o 2 18 0 4.51 20.88 10.54 o 3 18 0 99.94 76.30 18.73 o 4 18 0 140.35 134.65 25.72 o 1 19 0 495.93 450.62 22.30 o 2 19 0 71.14 98.89 17.90 o 3 19 0 58.26 67.27 18.53 o 0 20 0 1.73 -2.66 4.90 o 1 20 0 320.60 320.03 24.84 o 2 20 0 333.60 360.63 28.80 o 3 20 0 499.07 430.31 34.83 o 1 21 0 1.46 -1.00 7.83 o 2 21 0 105.54 83.89 17.57 o 3 21 0 12.38 0.52 11.90 o 1 22 0 1067.75 995.60 43.08 o 2 22 0 6.13 1.85 9.49 o 3 22 0 207.49 224.09 29.49 o 1 23 0 61.62 64.17 14.77 o 2 23 0 38.66 32.87 13.68 o 0 24 0 241.11 217.02 24.62 o 1 24 0 333.60 297.79 26.31 o 2 24 0 281.09 321.43 29.97 o 1 25 0 176.58 185.64 23.02 o 2 25 0 14.14 27.34 13.68 o -5 1 1 265.82 294.95 18.27 o -4 1 1 57.97 65.08 5.93 o -3 1 1 604.63 561.33 11.78 o -2 1 1 28.87 33.84 3.49 o -1 1 1 8963.31 9131.00 113.52 o 0 1 1 2327.28 2250.48 13.95 o 1 1 1 6179.68 5965.42 33.29 o 2 1 1 3910.46 3756.84 29.74 o 3 1 1 35.83 32.33 4.44 o 4 1 1 1207.87 1214.24 25.96 o 5 1 1 25.48 19.38 9.18 o -5 2 1 89.37 92.22 12.18 o -4 2 1 39.00 35.88 5.02 o -3 2 1 124.31 134.83 6.53 o -2 2 1 1108.32 1152.10 15.34 o -1 2 1 209.41 169.85 6.26 o 0 2 1 5355.83 5284.35 26.90 o 1 2 1 6.01 2.52 3.17 o 2 2 1 785.86 949.32 14.11 o 3 2 1 60.78 56.43 5.25 o 4 2 1 45.62 42.82 7.57 o 5 2 1 31.16 17.81 13.46 o -5 3 1 528.97 539.86 23.05 o -4 3 1 53.08 44.52 8.19 o -3 3 1 1783.00 1748.88 23.53 o -2 3 1 381.22 294.67 7.59 o -1 3 1 2.59 6.79 2.08 o 0 3 1 1664.38 1893.09 16.76 o 1 3 1 484.93 476.58 7.43 o 2 3 1 4736.17 4716.65 41.93 o 3 3 1 911.77 908.89 16.52 o 4 3 1 180.43 191.15 12.16 o 5 3 1 26.07 22.00 14.84 o -5 4 1 416.31 389.19 30.65 o -4 4 1 12.78 13.17 6.02 o -3 4 1 817.03 801.64 15.56 o -2 4 1 100.14 99.87 4.65 o -1 4 1 4097.19 3924.25 34.62 o 0 4 1 43.92 32.88 2.38 o 1 4 1 1176.11 1222.55 11.91 o 2 4 1 424.41 469.46 9.95 o 3 4 1 12.09 8.61 3.37 o 4 4 1 255.56 255.89 13.74 o 5 4 1 10.05 19.13 13.86 o -5 5 1 165.08 212.42 24.44 o -4 5 1 712.69 713.44 30.48 o -3 5 1 1241.53 1151.58 18.50 o -2 5 1 249.54 288.08 7.29 o -1 5 1 1158.09 1179.47 17.60 o 0 5 1 846.79 891.89 9.32 o 1 5 1 2611.10 2510.46 45.09 o 2 5 1 1419.30 1380.23 16.90 o 3 5 1 135.89 150.42 11.01 o 4 5 1 32.35 39.90 7.42 o 5 5 1 49.62 84.21 13.62 o -5 6 1 106.46 122.98 20.77 o -4 6 1 52.98 60.63 8.56 o -3 6 1 126.55 122.10 6.94 o -2 6 1 464.41 525.29 9.58 o -1 6 1 2506.02 2588.66 39.76 o 0 6 1 241.68 245.66 5.20 o 1 6 1 599.61 664.16 12.91 o 2 6 1 146.24 156.11 6.20 o 3 6 1 117.65 107.80 8.54 o 4 6 1 43.81 36.27 12.55 o 5 6 1 81.17 83.36 14.23 o -5 7 1 129.52 138.80 22.01 o -4 7 1 188.90 205.07 22.08 o -3 7 1 1268.60 1250.50 26.53 o -2 7 1 2108.74 2125.56 20.77 o -1 7 1 88.01 88.94 5.82 o 0 7 1 5539.56 5313.53 35.83 o 1 7 1 262.90 306.73 9.20 o 2 7 1 180.63 154.68 6.06 o 3 7 1 831.85 825.47 20.21 o 4 7 1 218.45 237.63 13.80 o 5 7 1 163.39 185.80 18.86 o -5 8 1 5.51 19.58 11.30 o -4 8 1 20.34 18.36 5.94 o -3 8 1 90.81 103.34 15.73 o -2 8 1 351.00 349.27 8.14 o -1 8 1 8.05 18.24 3.43 o 0 8 1 122.73 124.17 5.09 o 1 8 1 1632.62 1636.96 22.02 o 2 8 1 312.16 313.54 11.71 o 3 8 1 15.81 15.62 5.05 o 4 8 1 53.78 67.61 12.24 o -5 9 1 53.48 59.61 17.76 o -4 9 1 543.46 557.17 32.99 o -3 9 1 315.17 312.63 23.94 o -2 9 1 1028.71 1083.99 14.99 o -1 9 1 3225.06 3240.84 57.40 o 0 9 1 650.98 610.94 11.20 o 1 9 1 1739.71 1602.54 22.48 o 2 9 1 534.44 529.55 15.55 o 3 9 1 132.84 135.69 9.90 o 4 9 1 669.45 662.50 27.95 o -5 10 1 22.41 22.31 12.13 o -4 10 1 144.74 112.45 18.18 o -3 10 1 6.87 4.73 4.58 o -2 10 1 300.13 315.76 8.46 o -1 10 1 1320.60 1428.90 32.42 o 0 10 1 736.59 784.35 13.46 o 1 10 1 502.71 485.77 15.49 o 2 10 1 287.75 277.26 11.35 o 3 10 1 545.43 538.16 17.22 o 4 10 1 2.75 -0.33 7.45 o -5 11 1 73.74 51.97 15.72 o -4 11 1 1.09 -6.05 6.48 o -3 11 1 166.23 184.75 11.71 o -2 11 1 3342.07 3312.68 30.28 o -1 11 1 4411.81 4510.75 46.95 o 0 11 1 366.65 364.35 9.79 o 1 11 1 1591.87 1606.66 18.17 o 2 11 1 1250.10 1196.69 22.85 o 3 11 1 244.84 258.53 12.75 o 4 11 1 211.74 212.40 19.36 o -5 12 1 54.79 61.69 16.75 o -4 12 1 67.38 62.61 16.82 o -3 12 1 114.45 113.78 9.93 o -2 12 1 279.69 270.94 12.31 o -1 12 1 18.71 29.19 4.95 o 0 12 1 980.03 1098.32 17.61 o 1 12 1 43.00 38.81 6.22 o 2 12 1 728.16 698.46 21.23 o 3 12 1 48.09 60.00 10.98 o 4 12 1 1.85 3.91 10.46 o -5 13 1 72.88 81.73 20.15 o -4 13 1 342.33 349.15 28.91 o -3 13 1 1130.75 1185.79 46.20 o -2 13 1 831.87 778.69 20.63 o -1 13 1 826.70 835.72 19.88 o 0 13 1 1370.44 1260.20 19.72 o 1 13 1 861.94 871.67 22.43 o 2 13 1 359.09 360.31 16.22 o 4 13 1 150.71 145.45 24.41 o -5 14 1 2.56 8.54 10.52 o -4 14 1 110.00 114.39 20.73 o -3 14 1 363.90 357.48 27.20 o -2 14 1 277.19 294.50 13.44 o -1 14 1 497.83 518.93 16.25 o 0 14 1 229.58 244.52 9.48 o 1 14 1 5.08 9.45 5.42 o 2 14 1 101.45 106.92 19.20 o 3 14 1 170.61 186.14 22.46 o 4 14 1 16.93 20.59 11.30 o -4 15 1 283.61 298.83 30.10 o -3 15 1 672.96 729.20 38.28 o -2 15 1 243.05 229.94 21.74 o -1 15 1 1002.97 996.86 23.06 o 0 15 1 371.22 354.28 11.56 o 1 15 1 283.92 254.89 13.26 o 2 15 1 82.99 93.55 13.78 o 3 15 1 538.38 645.84 38.58 o 4 15 1 136.57 149.82 25.25 o -4 16 1 60.11 48.50 16.87 o -3 16 1 15.05 21.65 11.80 o -2 16 1 71.98 53.55 7.72 o -1 16 1 17.81 24.99 4.47 o 0 16 1 75.71 77.65 6.57 o 1 16 1 458.93 449.55 18.12 o 2 16 1 7.68 7.24 5.86 o 3 16 1 152.86 192.15 24.84 o 4 16 1 0.04 3.87 11.37 o -4 17 1 212.86 221.38 28.47 o -3 17 1 307.93 319.60 27.65 o -2 17 1 714.17 757.76 35.58 o -1 17 1 71.43 72.31 6.49 o 0 17 1 1870.58 1941.78 28.41 o 1 17 1 65.58 56.03 16.21 o 2 17 1 20.91 10.10 6.29 o 3 17 1 137.69 156.68 23.89 o -4 18 1 171.94 182.31 26.78 o -3 18 1 29.86 12.23 10.90 o -2 18 1 19.78 34.65 11.17 o -1 18 1 94.65 110.53 9.78 o 0 18 1 176.32 156.91 12.18 o 1 18 1 108.63 98.16 10.21 o 2 18 1 192.28 189.94 23.97 o 3 18 1 184.30 206.10 27.02 o -4 19 1 240.92 247.08 30.54 o -3 19 1 27.75 44.55 15.10 o -2 19 1 1821.78 1754.75 56.07 o -1 19 1 855.92 877.09 24.41 o 0 19 1 29.96 26.34 7.19 o 1 19 1 121.91 145.54 18.28 o 2 19 1 80.18 84.89 18.73 o 3 19 1 253.76 286.70 31.23 o -4 20 1 10.99 1.62 13.44 o -3 20 1 185.61 195.39 25.55 o -2 20 1 231.98 217.87 22.56 o -1 20 1 0.07 4.20 4.52 o 0 20 1 175.19 187.91 25.94 o 1 20 1 3.69 -0.88 7.93 o 2 20 1 0.47 2.38 10.43 o 3 20 1 0.59 5.48 12.24 o -3 21 1 1.82 -0.72 10.31 o -2 21 1 309.14 332.63 27.38 o -1 21 1 3.35 3.83 7.10 o 0 21 1 717.75 768.34 26.16 o 1 21 1 1295.84 1254.08 33.30 o 2 21 1 242.77 335.70 31.80 o 3 21 1 227.71 248.10 31.43 o -3 22 1 4.84 8.64 11.93 o -2 22 1 21.30 16.99 10.56 o 0 22 1 80.82 100.84 11.71 o 1 22 1 239.77 241.46 19.89 o 2 22 1 12.16 16.03 12.89 o -3 23 1 16.32 19.03 14.15 o -2 23 1 247.69 240.18 25.33 o 0 23 1 438.72 449.41 21.56 o 1 23 1 524.37 505.28 32.85 o 2 23 1 215.59 221.36 28.84 o -2 24 1 0.06 6.32 10.24 o 0 24 1 15.28 48.34 13.56 o 1 24 1 1.82 12.44 11.73 o 2 24 1 45.60 67.63 20.63 o -2 25 1 124.36 113.94 19.84 o -1 25 1 130.77 93.92 20.39 o 0 25 1 178.43 162.25 23.81 o 1 25 1 203.95 207.22 26.16 o -1 26 1 2.06 -2.52 11.11 o 0 26 1 45.97 60.11 17.31 o 1 26 1 75.24 101.06 20.81 o -5 0 2 6.93 1.29 9.99 o -4 0 2 1332.28 1428.05 46.45 o -3 0 2 3610.87 3525.24 65.75 o -2 0 2 57.47 51.37 7.65 o -1 0 2 3024.68 3115.79 30.64 o 0 0 2 838.40 811.85 14.47 o 1 0 2 3719.24 3671.00 38.25 o 2 0 2 854.43 832.16 30.92 o 3 0 2 2935.79 2768.36 43.92 o 4 0 2 422.16 380.22 29.35 o -5 1 2 0.14 -4.13 6.12 o -4 1 2 262.58 257.84 14.84 o -3 1 2 31.35 38.59 9.04 o -2 1 2 295.05 301.09 11.19 o -1 1 2 7288.16 7543.57 42.10 o 0 1 2 122.10 122.34 8.98 o 1 1 2 634.15 702.84 10.89 o 2 1 2 267.07 257.69 8.41 o 3 1 2 302.96 321.74 13.42 o 4 1 2 0.44 -0.51 6.63 o -5 2 2 3.18 -3.94 6.39 o -4 2 2 784.02 779.33 23.98 o -3 2 2 439.49 428.18 26.30 o -2 2 2 405.27 388.77 12.68 o -1 2 2 13246.47 13207.98 86.02 o 0 2 2 268.20 275.15 6.19 o 1 2 2 739.62 715.63 10.81 o 2 2 2 354.41 321.16 9.20 o 3 2 2 1174.97 1181.37 24.48 o 4 2 2 312.22 287.94 18.99 o -5 3 2 22.79 28.57 8.84 o -4 3 2 98.43 103.32 15.82 o -3 3 2 151.54 176.19 14.74 o -2 3 2 167.46 173.32 9.12 o -1 3 2 7142.21 7464.37 57.20 o 0 3 2 336.07 345.33 6.59 o 1 3 2 448.45 492.85 11.86 o 2 3 2 204.58 197.14 7.61 o 3 3 2 2.46 11.37 8.46 o 4 3 2 8.10 10.23 7.84 o -5 4 2 428.01 442.11 41.34 o -4 4 2 451.79 433.67 18.31 o -3 4 2 633.94 625.71 18.99 o -2 4 2 2272.24 2179.58 30.85 o -1 4 2 505.45 537.30 8.11 o 0 4 2 11.10 9.29 1.78 o 1 4 2 3772.21 3814.81 35.89 o 2 4 2 379.84 341.79 12.33 o 3 4 2 3.49 -0.44 5.52 o 4 4 2 171.78 177.47 16.03 o -5 5 2 0.00 10.36 10.28 o -4 5 2 42.80 39.91 8.32 o -3 5 2 828.24 844.07 22.25 o -2 5 2 161.90 164.07 8.89 o -1 5 2 71.91 71.63 3.50 o 0 5 2 1415.93 1356.17 13.17 o 1 5 2 23.69 25.75 7.86 o 2 5 2 332.60 326.86 16.72 o 3 5 2 119.10 102.83 10.63 o 4 5 2 8.94 5.29 5.86 o -5 6 2 898.15 930.70 30.24 o -4 6 2 1040.90 1048.61 33.52 o -3 6 2 315.93 304.81 14.58 o -2 6 2 728.07 668.92 17.22 o -1 6 2 1377.23 1349.81 14.73 o 0 6 2 3.01 2.67 1.40 o 1 6 2 457.47 415.67 11.83 o 2 6 2 733.25 712.50 17.62 o 3 6 2 138.52 141.60 14.07 o 4 6 2 369.62 370.41 17.14 o -5 7 2 1.20 5.52 7.03 o -4 7 2 173.55 166.72 13.07 o -3 7 2 394.30 392.74 15.74 o -2 7 2 64.39 60.24 6.23 o -1 7 2 17.14 23.77 2.60 o 0 7 2 530.56 549.57 8.26 o 1 7 2 98.13 107.71 6.92 o 2 7 2 214.33 183.56 13.51 o 3 7 2 272.79 254.31 13.01 o 4 7 2 51.44 60.07 17.18 o -5 8 2 2.86 -1.93 7.87 o -4 8 2 273.61 266.28 15.25 o -3 8 2 1592.75 1594.64 31.27 o -2 8 2 724.91 713.34 18.34 o -1 8 2 2899.91 2827.61 28.77 o 0 8 2 1227.58 1175.05 12.95 o 1 8 2 930.28 905.67 18.22 o 2 8 2 124.36 120.28 10.16 o 3 8 2 21.62 35.08 11.46 o 4 8 2 381.15 416.13 18.56 o -5 9 2 2.07 -11.09 7.39 o -4 9 2 5.78 2.29 5.01 o -3 9 2 4.77 0.82 3.91 o -2 9 2 137.46 123.50 8.63 o -1 9 2 319.82 339.24 10.00 o 0 9 2 391.17 399.56 7.78 o 1 9 2 467.74 489.43 15.87 o 2 9 2 90.80 95.88 7.12 o 3 9 2 83.18 86.09 10.41 o 4 9 2 41.00 62.29 9.62 o -5 10 2 40.31 29.02 13.46 o -4 10 2 3.86 10.15 10.30 o -3 10 2 333.54 334.12 15.26 o -2 10 2 1004.64 1025.85 22.98 o -1 10 2 702.74 694.06 14.48 o 0 10 2 3818.20 3689.80 32.06 o 1 10 2 384.81 368.65 14.15 o 2 10 2 894.26 920.39 21.59 o 3 10 2 873.05 847.02 23.10 o 4 10 2 27.67 24.60 10.28 o -5 11 2 13.20 10.36 9.72 o -4 11 2 57.34 56.36 12.45 o -3 11 2 2.02 6.06 4.56 o -2 11 2 152.38 149.45 11.09 o -1 11 2 426.07 434.28 13.04 o 0 11 2 45.61 45.95 3.59 o 1 11 2 703.91 650.53 16.67 o 2 11 2 143.32 118.43 9.16 o 3 11 2 141.06 134.37 11.13 o 4 11 2 56.22 75.39 14.02 o -5 12 2 27.85 47.46 15.24 o -4 12 2 231.37 211.28 15.24 o -3 12 2 118.74 114.04 10.29 o -2 12 2 108.77 86.85 8.22 o -1 12 2 1974.54 1939.81 26.43 o 0 12 2 761.93 729.31 13.60 o 1 12 2 1639.12 1554.37 26.40 o 2 12 2 817.18 789.56 20.66 o 3 12 2 444.48 450.38 17.83 o 4 12 2 34.09 41.50 13.20 o -5 13 2 105.19 123.15 22.28 o -4 13 2 0.20 4.65 9.31 o -3 13 2 99.75 94.25 15.22 o -2 13 2 7.05 16.66 4.97 o -1 13 2 504.00 512.23 15.70 o 0 13 2 97.86 125.44 10.31 o 1 13 2 9.93 13.57 4.51 o 2 13 2 0.05 -0.14 4.36 o 3 13 2 134.13 134.85 11.58 o 4 13 2 29.80 43.09 14.72 o -5 14 2 48.72 29.66 15.17 o -4 14 2 22.99 24.45 12.45 o -3 14 2 26.15 32.55 7.28 o -2 14 2 1415.67 1383.40 29.22 o -1 14 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