#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:23:13 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181228 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/06/2230606.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230606_Fobs loop_ _publ_author_name 'Wang, Jun' 'Lu, Lu' 'Wei-Ping, Wu' 'He, Xi-Yang' 'Tao, Wang' _publ_section_title ; Tris(1,10-phenanthroline)cadmium 3,3'-dicarboxy-4,4'-diazenediyldibenzoate--4,4'-diazenediyldiphthalic acid--methanol (1/0.5/1) ; _journal_coeditor_code DN2688 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m867 _journal_page_last m868 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 79.022 _cell_angle_beta 73.492 _cell_angle_gamma 64.439 _cell_length_a 13.6902 _cell_length_b 13.7659 _cell_length_c 16.9518 _exptl_crystal_F_000 1242.00 _reflns_d_resolution_high 0.8346 _cod_data_source_file dn2688Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' aa_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 408.52 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 22725.74 21792.86 147.23 o 3 0 0 2537.22 3417.54 58.33 o 4 0 0 972.71 944.62 9.67 o 5 0 0 3097.72 3076.12 32.65 o 6 0 0 650.14 626.81 11.87 o 7 0 0 1.90 2.48 3.87 o 8 0 0 2177.53 2221.73 39.55 o 9 0 0 10.77 12.12 4.59 o 10 0 0 625.14 606.09 20.99 o 11 0 0 305.44 335.79 17.70 o 12 0 0 83.89 84.59 18.06 o 13 0 0 120.18 144.88 16.34 o 14 0 0 0.48 0.03 16.34 o -13 1 0 0.08 0.25 12.90 o -12 1 0 303.44 284.68 29.24 o -11 1 0 249.25 237.67 26.66 o -10 1 0 113.42 130.36 22.16 o -9 1 0 1638.82 1779.73 27.81 o -8 1 0 5.98 4.23 4.51 o -7 1 0 1735.75 1853.52 25.60 o -6 1 0 308.60 313.71 15.78 o -5 1 0 3629.12 3688.05 44.10 o -4 1 0 777.75 753.15 14.48 o -3 1 0 1231.09 1255.61 21.38 o -2 1 0 1283.25 898.79 7.27 o -1 1 0 11250.95 14504.73 300.94 o 3 1 0 27732.53 29332.67 598.44 o 4 1 0 278.83 360.50 8.51 o 5 1 0 662.32 726.44 11.70 o 6 1 0 1778.01 1791.57 41.76 o 7 1 0 177.91 164.73 7.88 o 8 1 0 1923.29 1922.73 27.57 o 9 1 0 274.21 296.66 10.38 o 10 1 0 21.78 21.36 7.51 o 11 1 0 1651.80 1506.47 34.27 o 12 1 0 98.93 107.98 12.73 o 13 1 0 68.10 51.99 12.90 o 14 1 0 123.15 119.73 18.91 o -13 2 0 5.90 5.35 9.37 o -12 2 0 31.63 29.04 9.37 o -11 2 0 530.84 502.68 21.31 o -10 2 0 338.56 303.02 13.24 o -9 2 0 227.72 226.85 20.47 o -8 2 0 2114.33 2038.86 36.33 o -7 2 0 46.04 46.07 6.71 o -6 2 0 3015.14 2923.99 37.42 o -5 2 0 1153.70 983.46 15.50 o -4 2 0 1465.88 1460.07 20.29 o -3 2 0 7893.11 7673.05 82.65 o -2 2 0 416.93 533.48 25.49 o -1 2 0 404.12 759.11 32.67 o 0 2 0 22.16 7.68 7.83 o 1 2 0 8034.66 7585.19 84.27 o 2 2 0 3039.95 4283.25 79.27 o 3 2 0 51.23 44.91 2.43 o 4 2 0 68.44 68.57 5.72 o 5 2 0 7200.19 7696.06 94.73 o 6 2 0 54.60 47.83 2.52 o 7 2 0 1718.36 1832.35 22.11 o 8 2 0 679.54 750.96 11.71 o 9 2 0 361.27 377.20 13.99 o 10 2 0 989.25 971.27 25.62 o 11 2 0 1.53 5.66 8.85 o 12 2 0 682.31 651.84 33.54 o 13 2 0 29.76 20.42 9.06 o 14 2 0 4.98 4.70 8.85 o 15 2 0 36.67 26.48 22.36 o -12 3 0 15.39 24.32 11.18 o -11 3 0 233.64 224.59 13.09 o -10 3 0 594.24 599.68 26.59 o -9 3 0 222.76 222.69 11.57 o -8 3 0 626.98 659.28 15.31 o -7 3 0 1228.77 1224.00 22.85 o -6 3 0 646.07 651.25 20.50 o -5 3 0 1006.50 861.41 14.13 o -4 3 0 39.83 50.63 4.07 o -3 3 0 1646.52 1630.92 20.62 o -2 3 0 1240.80 1335.20 22.28 o -1 3 0 4344.66 4757.77 53.18 o 0 3 0 56180.23 56941.86 641.73 o 1 3 0 19739.94 20172.95 339.63 o 2 3 0 98.54 135.20 6.45 o 3 3 0 500.07 426.26 8.60 o 4 3 0 1080.70 1231.52 19.82 o 5 3 0 5140.83 5284.43 63.59 o 6 3 0 3963.60 3810.00 79.10 o 7 3 0 1397.89 1589.25 21.58 o 8 3 0 2820.20 2734.44 27.10 o 9 3 0 109.85 121.82 8.32 o 10 3 0 974.03 990.39 25.36 o 11 3 0 562.64 550.50 27.51 o 12 3 0 57.85 50.75 20.64 o 13 3 0 75.05 78.26 18.06 o 14 3 0 27.07 24.01 9.23 o 15 3 0 14.58 9.48 10.40 o -12 4 0 161.75 178.70 30.95 o -11 4 0 147.25 154.36 11.91 o -10 4 0 445.65 443.81 19.58 o -9 4 0 651.64 587.37 16.68 o -8 4 0 57.83 47.76 7.66 o -7 4 0 1669.23 1705.84 28.63 o -6 4 0 904.61 908.00 34.80 o -5 4 0 0.24 3.81 3.84 o -4 4 0 2161.94 2106.14 28.63 o -3 4 0 7415.80 7685.57 76.31 o -2 4 0 4479.21 4704.57 50.16 o -1 4 0 381.90 284.35 7.81 o 0 4 0 7423.39 8450.83 133.78 o 1 4 0 18666.65 19931.37 198.76 o 2 4 0 2175.85 2369.24 24.34 o 3 4 0 611.75 635.83 12.00 o 4 4 0 163.18 143.22 5.72 o 5 4 0 2387.72 2372.27 31.80 o 6 4 0 3610.95 3593.45 75.67 o 7 4 0 360.79 331.41 10.75 o 8 4 0 1525.84 1477.38 38.69 o 9 4 0 780.87 805.19 22.28 o 10 4 0 0.56 0.00 4.76 o 11 4 0 996.46 900.13 21.11 o 12 4 0 105.85 102.62 9.96 o 13 4 0 106.53 109.04 11.94 o 14 4 0 107.02 129.14 17.19 o 15 4 0 15.16 15.03 10.40 o -11 5 0 96.77 105.69 18.91 o -10 5 0 118.38 110.34 15.26 o -9 5 0 162.03 183.70 11.29 o -8 5 0 129.20 146.12 10.21 o -7 5 0 5.60 6.46 5.57 o -6 5 0 863.12 826.71 16.08 o -5 5 0 260.11 274.53 12.46 o -4 5 0 999.80 906.76 16.98 o -3 5 0 2935.76 3040.44 35.77 o -2 5 0 6045.35 6284.39 61.27 o -1 5 0 6590.03 6797.81 63.30 o 0 5 0 16061.50 17527.68 467.24 o 1 5 0 3551.08 3839.58 40.03 o 2 5 0 6175.25 6286.30 62.34 o 3 5 0 246.31 237.37 8.13 o 4 5 0 2418.69 2504.20 40.66 o 5 5 0 2745.79 2491.95 38.84 o 6 5 0 226.46 225.91 10.75 o 7 5 0 154.57 121.21 7.00 o 8 5 0 1282.48 1215.49 35.25 o 9 5 0 469.19 457.70 16.11 o 10 5 0 582.06 603.96 19.82 o 11 5 0 0.22 0.02 5.17 o 12 5 0 1040.91 961.33 51.77 o 13 5 0 176.66 189.29 12.79 o 14 5 0 87.63 80.12 11.94 o 15 5 0 43.70 61.40 12.73 o -11 6 0 20.28 21.96 13.99 o -10 6 0 167.76 191.40 18.12 o -9 6 0 109.50 96.04 15.26 o -8 6 0 4.62 9.16 11.13 o -7 6 0 245.91 240.56 23.21 o -6 6 0 9.42 8.09 7.14 o -5 6 0 609.25 627.74 15.28 o -4 6 0 1993.23 1831.14 26.17 o -3 6 0 39.38 44.22 5.28 o -2 6 0 2851.66 2849.06 40.05 o -1 6 0 744.54 715.06 40.69 o 0 6 0 2878.01 3317.42 61.08 o 1 6 0 11926.15 12294.35 111.06 o 2 6 0 1665.81 1781.27 26.03 o 3 6 0 848.56 808.69 11.76 o 4 6 0 131.25 157.37 9.83 o 5 6 0 2.28 1.78 2.20 o 6 6 0 400.34 348.02 24.07 o 7 6 0 128.66 117.70 7.83 o 8 6 0 1136.52 1125.89 23.95 o 9 6 0 155.01 154.07 11.13 o 10 6 0 323.09 326.72 14.87 o 11 6 0 191.58 203.18 12.73 o 12 6 0 0.22 0.30 8.60 o 13 6 0 292.09 277.02 14.29 o 14 6 0 26.80 31.85 7.92 o 15 6 0 40.22 18.18 10.40 o -10 7 0 15.75 8.74 12.73 o -9 7 0 121.83 134.10 16.51 o -8 7 0 222.84 252.44 19.00 o -7 7 0 112.47 93.99 22.36 o -6 7 0 106.49 109.89 13.63 o -5 7 0 0.26 0.01 9.06 o -4 7 0 592.03 571.30 24.94 o -3 7 0 397.75 374.23 22.36 o -2 7 0 1061.90 1001.13 14.53 o -1 7 0 836.63 739.02 21.63 o 0 7 0 3235.31 3387.42 63.22 o 1 7 0 9945.06 10001.97 89.47 o 2 7 0 2560.32 2468.83 30.64 o 3 7 0 111.79 123.51 5.28 o 4 7 0 4145.79 3991.85 43.88 o 5 7 0 13.60 2.67 2.64 o 6 7 0 5092.32 5174.05 51.60 o 7 7 0 3198.72 3271.61 49.58 o 8 7 0 130.65 135.59 9.50 o 9 7 0 1553.13 1465.50 30.98 o 10 7 0 44.64 70.92 8.60 o 11 7 0 704.50 624.13 20.25 o 12 7 0 387.22 437.88 19.38 o 13 7 0 27.42 23.32 7.56 o 14 7 0 118.14 138.26 11.16 o 15 7 0 24.71 34.63 9.02 o -9 8 0 15.74 22.66 13.21 o -8 8 0 107.42 113.24 15.26 o -7 8 0 114.03 107.88 17.19 o -6 8 0 162.05 178.56 16.51 o -5 8 0 326.07 313.10 19.78 o -4 8 0 207.44 226.52 32.67 o -3 8 0 1834.85 1897.26 39.17 o -2 8 0 45.22 50.51 25.79 o -1 8 0 1141.20 1098.50 29.63 o 0 8 0 9.11 8.55 6.08 o 1 8 0 2810.98 3155.97 45.78 o 2 8 0 1751.16 1637.46 23.64 o 3 8 0 496.28 484.62 10.06 o 4 8 0 163.97 154.85 6.38 o 5 8 0 3622.18 3709.54 39.47 o 6 8 0 726.92 862.13 14.95 o 7 8 0 1342.53 1360.90 27.51 o 8 8 0 219.55 206.42 11.13 o 9 8 0 388.90 352.84 15.26 o 10 8 0 510.24 506.82 17.35 o 11 8 0 28.87 31.00 8.26 o 12 8 0 1044.79 948.06 40.42 o 13 8 0 560.94 519.40 35.25 o 14 8 0 9.76 3.25 6.38 o 15 8 0 122.65 115.39 16.87 o -8 9 0 9.84 0.23 11.45 o -7 9 0 106.08 109.31 16.11 o -6 9 0 64.68 82.09 13.63 o -5 9 0 86.98 85.30 12.38 o -4 9 0 261.20 298.69 42.99 o -3 9 0 538.78 527.36 22.28 o -2 9 0 1354.91 1249.51 32.56 o -1 9 0 57.82 67.03 10.31 o 0 9 0 1802.71 1748.12 34.26 o 1 9 0 516.72 477.63 18.58 o 2 9 0 46.29 46.35 10.31 o 3 9 0 858.38 726.58 19.00 o 4 9 0 77.94 84.21 7.33 o 5 9 0 650.94 650.76 12.58 o 6 9 0 1065.72 943.46 16.43 o 7 9 0 65.16 72.98 13.76 o 8 9 0 2191.50 2177.70 42.99 o 9 9 0 418.80 413.32 15.26 o 10 9 0 21.41 20.60 7.00 o 11 9 0 14.01 12.03 7.29 o 12 9 0 20.64 33.79 8.59 o 13 9 0 71.12 47.18 10.15 o 14 9 0 79.50 65.71 11.45 o 15 9 0 3.83 0.04 6.48 o -7 10 0 49.77 41.92 13.63 o -6 10 0 67.54 85.57 14.44 o -5 10 0 7.27 14.59 11.13 o -4 10 0 30.48 40.55 11.98 o -3 10 0 534.80 495.09 22.28 o -2 10 0 11.71 26.52 10.95 o -1 10 0 795.29 847.52 27.18 o 0 10 0 270.44 268.56 16.11 o 1 10 0 859.65 888.61 30.09 o 2 10 0 351.66 355.93 16.89 o 3 10 0 81.20 114.14 30.09 o 4 10 0 777.86 768.60 21.48 o 5 10 0 98.56 97.63 12.04 o 6 10 0 1428.87 1337.71 31.82 o 7 10 0 754.74 820.88 20.03 o 8 10 0 59.73 62.15 7.51 o 9 10 0 759.79 728.29 40.42 o 10 10 0 134.50 138.27 11.45 o 11 10 0 111.77 90.44 10.15 o 12 10 0 101.29 133.19 12.38 o 13 10 0 2.15 0.04 7.29 o 14 10 0 15.91 13.26 8.59 o 15 10 0 57.23 60.16 11.72 o -6 11 0 14.24 2.49 11.98 o -5 11 0 68.44 88.60 15.48 o -4 11 0 10.37 10.79 21.49 o -3 11 0 436.98 452.80 23.50 o -2 11 0 690.07 767.77 27.65 o -1 11 0 193.05 193.78 20.64 o 0 11 0 702.00 680.52 31.82 o 1 11 0 1783.19 1578.93 36.72 o 2 11 0 1498.17 1426.17 34.26 o 3 11 0 472.37 463.13 18.58 o 4 11 0 21.52 19.45 8.26 o 5 11 0 513.59 528.38 19.00 o 6 11 0 57.67 69.03 15.48 o 7 11 0 59.60 53.40 13.76 o 8 11 0 61.29 30.84 13.76 o 9 11 0 57.17 57.24 8.59 o 10 11 0 490.36 530.32 19.38 o 11 11 0 22.90 30.81 8.59 o 12 11 0 123.89 143.93 20.64 o 13 11 0 129.03 153.34 16.34 o 14 11 0 6.81 0.04 10.31 o -4 12 0 39.28 33.49 22.36 o -3 12 0 22.26 12.73 11.50 o -2 12 0 176.58 191.78 17.35 o -1 12 0 113.12 112.57 17.19 o 0 12 0 40.77 49.82 11.98 o 1 12 0 149.17 154.47 17.19 o 2 12 0 186.10 165.88 14.44 o 3 12 0 69.39 67.59 10.75 o 4 12 0 99.49 114.78 13.21 o 5 12 0 60.12 52.63 9.86 o 6 12 0 536.12 506.43 32.67 o 7 12 0 166.51 220.76 24.07 o 8 12 0 28.01 35.72 13.76 o 9 12 0 651.62 733.60 37.83 o 10 12 0 5.66 2.90 13.76 o 11 12 0 95.12 89.51 18.91 o 12 12 0 0.32 5.46 7.51 o 13 12 0 103.47 100.83 11.72 o 14 12 0 119.53 111.03 13.99 o -3 13 0 95.94 84.15 14.87 o -2 13 0 0.56 1.78 10.28 o -1 13 0 100.03 114.54 15.67 o 0 13 0 74.90 88.09 17.19 o 1 13 0 86.04 81.20 12.38 o 2 13 0 245.33 253.74 31.82 o 3 13 0 33.50 52.48 11.98 o 4 13 0 0.85 0.17 8.26 o 5 13 0 416.01 477.08 32.67 o 6 13 0 0.13 5.55 13.76 o 7 13 0 248.78 269.81 27.51 o 8 13 0 21.22 0.17 13.76 o 9 13 0 213.58 228.40 25.79 o 10 13 0 251.98 262.77 27.51 o 11 13 0 2.81 17.33 15.48 o 12 13 0 87.97 103.51 22.36 o 13 13 0 0.61 0.01 15.48 o -1 14 0 1.74 8.43 10.75 o 0 14 0 10.22 18.55 11.98 o 1 14 0 33.46 18.08 11.50 o 2 14 0 204.93 147.53 16.11 o 3 14 0 485.40 468.47 22.72 o 4 14 0 15.73 18.19 10.75 o 5 14 0 161.54 185.46 25.79 o 6 14 0 112.81 100.44 22.36 o 7 14 0 148.69 135.02 22.36 o 8 14 0 276.91 295.93 29.24 o 9 14 0 7.21 6.77 15.48 o 10 14 0 69.03 71.62 20.64 o 11 14 0 61.95 61.30 18.91 o 12 14 0 0.65 0.07 13.76 o 1 15 0 3.64 0.01 10.95 o 2 15 0 66.39 43.69 13.21 o 3 15 0 193.52 186.96 17.76 o 4 15 0 91.63 99.25 22.36 o 5 15 0 3.03 0.20 13.76 o 6 15 0 63.36 86.27 22.36 o 7 15 0 30.94 53.24 18.91 o 8 15 0 28.57 37.98 17.19 o 9 15 0 15.12 14.94 17.19 o 10 15 0 5.63 9.86 17.19 o 11 15 0 14.16 0.04 17.19 o 5 16 0 41.07 48.87 20.64 o 6 16 0 5.78 0.02 17.19 o 7 16 0 74.65 65.15 22.36 o 8 16 0 20.17 32.77 18.91 o -6 -16 1 7.10 3.97 17.19 o -10 -15 1 89.52 124.47 24.07 o -9 -15 1 0.38 0.06 17.19 o -8 -15 1 79.94 78.23 20.64 o -7 -15 1 90.89 92.56 22.36 o -6 -15 1 69.43 80.39 20.64 o -5 -15 1 26.61 34.60 18.91 o -4 -15 1 0.07 0.06 15.48 o -3 -15 1 61.10 86.35 14.44 o -2 -15 1 240.16 216.07 18.58 o -1 -15 1 44.27 33.92 13.38 o -12 -14 1 30.70 39.23 20.64 o -11 -14 1 1.20 0.01 13.76 o -10 -14 1 34.00 55.92 20.64 o -9 -14 1 61.83 47.07 18.91 o -8 -14 1 0.08 6.61 15.48 o -7 -14 1 15.88 23.16 17.19 o -6 -14 1 114.44 162.14 24.07 o -5 -14 1 149.59 188.55 25.79 o -4 -14 1 181.36 173.74 16.11 o -3 -14 1 11.92 21.37 10.75 o -2 -14 1 98.99 96.31 13.63 o -1 -14 1 143.84 150.91 18.91 o 0 -14 1 9.89 7.65 12.90 o 1 -14 1 55.33 50.48 13.63 o -13 -13 1 48.97 23.74 18.91 o -12 -13 1 0.49 0.01 13.76 o -11 -13 1 125.18 132.60 22.36 o -10 -13 1 0.86 0.00 13.76 o -9 -13 1 161.48 189.12 24.07 o -8 -13 1 276.19 284.00 29.24 o -7 -13 1 44.39 45.51 17.19 o -6 -13 1 247.43 249.21 25.79 o -5 -13 1 529.47 527.61 34.39 o -4 -13 1 95.54 85.63 12.38 o -3 -13 1 473.27 494.17 38.69 o -2 -13 1 0.19 27.16 11.50 o -1 -13 1 315.01 269.25 18.58 o 0 -13 1 183.06 171.61 24.07 o 1 -13 1 35.64 19.96 17.19 o 2 -13 1 119.05 177.88 24.94 o 3 -13 1 12.34 17.78 13.21 o -13 -12 1 128.07 129.90 26.66 o -12 -12 1 137.44 125.72 24.07 o -11 -12 1 2.69 0.01 13.76 o -10 -12 1 137.04 153.86 22.36 o -9 -12 1 58.25 65.33 17.19 o -8 -12 1 323.10 296.61 27.51 o -7 -12 1 284.39 293.47 25.79 o -6 -12 1 17.18 8.95 13.76 o -5 -12 1 581.10 618.59 36.12 o -4 -12 1 64.00 36.51 10.28 o -3 -12 1 1516.69 1497.52 35.48 o -2 -12 1 437.30 392.32 19.82 o -1 -12 1 368.05 332.20 36.97 o 0 -12 1 2.39 0.28 18.06 o 1 -12 1 1.54 0.20 8.26 o 2 -12 1 83.94 115.86 14.44 o 3 -12 1 43.52 36.93 12.73 o 4 -12 1 7.24 0.04 20.64 o -14 -11 1 61.56 43.71 14.61 o -13 -11 1 1.56 0.02 12.90 o -12 -11 1 292.58 297.72 19.78 o -11 -11 1 103.99 100.21 11.18 o -10 -11 1 21.83 20.77 18.06 o -9 -11 1 394.15 386.16 29.24 o -8 -11 1 81.86 67.55 15.48 o -7 -11 1 151.65 165.28 18.91 o -6 -11 1 349.65 315.47 25.79 o -5 -11 1 68.56 61.62 9.50 o -4 -11 1 1221.58 1239.13 28.50 o -3 -11 1 41.72 49.85 9.50 o -2 -11 1 1124.60 1131.17 30.11 o -1 -11 1 271.06 234.46 16.89 o 0 -11 1 2.86 0.30 8.51 o 1 -11 1 837.38 807.57 27.18 o 2 -11 1 762.83 735.77 44.71 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19 17.59 24.17 8.51 o 2 1 19 209.51 198.85 13.94 o 3 1 19 245.64 302.15 16.38 o 4 1 19 10.52 6.37 7.29 o 5 1 19 225.77 220.64 13.94 o 6 1 19 56.99 60.64 10.28 o 7 1 19 38.05 29.45 13.76 o 8 1 19 77.91 103.25 17.19 o -1 2 19 99.61 98.93 12.16 o 0 2 19 1.23 2.75 7.29 o 1 2 19 325.22 308.91 16.38 o 2 2 19 107.59 101.65 11.50 o 3 2 19 14.53 9.02 7.83 o 4 2 19 96.50 121.01 11.50 o 5 2 19 15.51 3.13 7.29 o 6 2 19 201.43 227.95 13.94 o 7 2 19 99.75 101.91 13.76 o 8 2 19 0.25 0.00 10.31 o 9 2 19 39.26 44.39 10.28 o 0 3 19 94.03 106.92 15.48 o 1 3 19 4.70 2.07 11.18 o 2 3 19 218.61 209.87 15.48 o 3 3 19 26.18 6.05 8.51 o 4 3 19 109.74 103.96 10.95 o 5 3 19 377.92 356.22 17.02 o 6 3 19 4.34 0.03 7.29 o 7 3 19 217.08 219.99 14.59 o 8 3 19 96.60 106.25 11.50 o 9 3 19 115.62 108.21 11.50 o 0 4 19 42.57 45.34 10.31 o 1 4 19 60.29 67.95 11.18 o 2 4 19 38.37 38.29 9.73 o 3 4 19 378.22 415.91 18.24 o 4 4 19 99.94 93.34 11.50 o 5 4 19 99.35 102.54 11.50 o 6 4 19 379.23 348.22 25.79 o 7 4 19 7.75 0.00 6.61 o 8 4 19 285.93 294.08 30.95 o 9 4 19 143.64 165.86 18.91 o 1 5 19 146.60 149.97 15.48 o 2 5 19 76.83 73.22 10.95 o 3 5 19 15.87 0.04 10.31 o 4 5 19 122.84 127.17 12.73 o 5 5 19 15.37 20.43 8.51 o 6 5 19 111.10 108.65 11.50 o 7 5 19 229.78 201.04 14.59 o 8 5 19 12.13 9.75 9.46 o 9 5 19 162.81 170.71 18.06 o 2 6 19 148.69 147.83 13.38 o 3 6 19 40.22 34.26 9.50 o 4 6 19 56.81 55.90 10.28 o 5 6 19 132.04 128.66 12.16 o 6 6 19 6.33 0.01 6.88 o 7 6 19 118.76 148.46 12.73 o 8 6 19 68.41 71.06 10.28 o 9 6 19 98.22 87.00 10.95 o 3 7 19 65.42 71.56 10.95 o 4 7 19 7.10 8.91 7.83 o 5 7 19 16.68 4.03 7.83 o 6 7 19 175.61 180.25 13.94 o 7 7 19 0.00 0.00 6.61 o 8 7 19 109.95 121.08 12.16 o 9 7 19 52.08 73.29 10.75 o 4 8 19 77.36 75.67 11.50 o 5 8 19 61.09 71.78 10.75 o 6 8 19 28.52 17.99 9.06 o 7 8 19 213.73 209.90 19.78 o 8 8 19 1.46 13.16 7.83 o 3 1 20 107.17 102.34 13.76 o 4 1 20 186.86 172.75 13.38 o 5 1 20 88.71 86.11 11.50 o 2 2 20 207.55 192.82 14.59 o 3 2 20 25.84 19.98 13.76 o 4 2 20 15.16 15.04 12.04 o 5 2 20 177.34 189.57 13.94 o 6 2 20 27.95 25.64 9.06 o 3 3 20 110.47 128.91 13.38 o 4 3 20 26.87 4.30 16.34 o 5 3 20 22.36 18.68 8.51 o 6 3 20 208.98 198.03 14.59 o 7 3 20 7.06 0.05 7.29 o 3 4 20 3.44 0.01 8.60 o 4 4 20 332.96 336.86 17.60 o 5 4 20 100.56 102.22 11.50 o 6 4 20 50.92 46.67 9.73 o 7 4 20 233.26 220.29 14.59 o 4 5 20 17.72 27.98 9.06 o 5 5 20 256.44 254.17 15.81 o 6 5 20 55.48 39.20 9.73 o 7 5 20 83.08 78.26 10.95 o