#------------------------------------------------------------------------------ #$Date: 2011-08-08 08:56:15 +0300 (Mon, 08 Aug 2011) $ #$Revision: 23417 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2230610.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230610_Fobs loop_ _publ_author_name 'Gubina, Kateryna' 'Shatrava, Iuliia' 'Ovchynnikov, Vladimir' 'Amirkhanov, Vladimir' _publ_section_title ; 2-Ureido-1,3-thiazol-3-ium dihydrogen phosphate ; _journal_coeditor_code DN2693 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1607 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.231 _cell_angle_gamma 90.000 _cell_length_a 11.9038 _cell_length_b 9.7936 _cell_length_c 8.1914 _exptl_crystal_F_000 496.00 _reflns_d_resolution_high 0.7572 _[local]_cod_data_source_file dn2693Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' s1 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 148.44 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 408.19 431.27 1.95 o 2 0 0 22033.78 18278.54 69.92 o 3 0 0 7597.29 8241.69 31.91 o 4 0 0 1737.55 1893.57 8.38 o 5 0 0 1267.39 1536.38 7.73 o 6 0 0 290.68 327.40 3.50 o 7 0 0 778.49 976.50 6.76 o 8 0 0 301.19 337.74 4.15 o 9 0 0 89.05 92.80 2.85 o 10 0 0 145.87 153.12 3.74 o 11 0 0 23.76 23.85 1.38 o 12 0 0 2.36 3.99 2.77 o 13 0 0 314.80 323.25 6.27 o 14 0 0 43.46 40.78 1.87 o 15 0 0 7.30 10.50 1.47 o 1 1 0 0.04 5.37 0.41 o 2 1 0 1948.52 2318.16 8.87 o 3 1 0 2580.00 2889.52 11.40 o 4 1 0 73.90 102.73 1.95 o 5 1 0 897.72 1084.60 6.19 o 6 1 0 517.18 586.74 4.72 o 7 1 0 164.40 195.93 3.09 o 8 1 0 383.08 396.26 4.64 o 9 1 0 261.28 290.36 4.23 o 10 1 0 395.84 428.34 5.62 o 11 1 0 868.95 901.93 8.71 o 12 1 0 1008.02 1082.89 10.18 o 13 1 0 126.13 128.86 4.48 o 14 1 0 62.99 61.54 2.69 o 15 1 0 126.21 120.88 4.97 o 1 2 0 109.07 125.03 1.79 o 2 2 0 1891.83 2163.42 8.87 o 3 2 0 550.49 625.49 4.07 o 4 2 0 25.33 33.05 1.63 o 5 2 0 3.35 0.49 1.55 o 6 2 0 503.02 653.41 5.21 o 7 2 0 26.10 37.93 1.47 o 8 2 0 146.83 146.69 3.26 o 9 2 0 1218.47 1322.78 9.52 o 10 2 0 88.01 84.50 3.09 o 11 2 0 45.24 42.00 2.04 o 12 2 0 189.19 192.60 4.80 o 13 2 0 4.52 5.13 2.77 o 14 2 0 27.07 25.80 1.55 o 15 2 0 6.06 3.83 3.34 o 2 3 0 3.81 0.65 1.14 o 3 3 0 2076.33 2005.09 8.79 o 4 3 0 164.53 176.56 2.36 o 5 3 0 17.67 30.44 1.47 o 6 3 0 403.43 409.61 3.91 o 7 3 0 167.02 150.19 2.69 o 8 3 0 268.04 258.86 3.66 o 9 3 0 62.30 57.31 2.28 o 10 3 0 190.98 175.18 3.66 o 11 3 0 0.21 -0.73 2.04 o 12 3 0 39.20 31.26 1.38 o 13 3 0 17.97 12.70 1.22 o 14 3 0 19.12 20.92 1.38 o 15 3 0 1.89 -2.85 2.85 o 3 4 0 172.74 202.77 2.52 o 4 4 0 659.76 695.90 4.97 o 5 4 0 96.67 69.44 1.95 o 6 4 0 134.42 149.05 2.77 o 7 4 0 518.85 456.42 4.72 o 8 4 0 331.22 325.28 4.31 o 9 4 0 1310.59 1250.98 9.20 o 10 4 0 650.90 623.29 6.67 o 11 4 0 217.11 201.06 4.31 o 12 4 0 292.58 267.81 5.21 o 13 4 0 91.18 88.40 3.58 o 14 4 0 0.41 0.57 2.52 o 3 5 0 17.15 11.80 0.65 o 4 5 0 189.20 200.09 2.85 o 5 5 0 6.43 6.19 0.73 o 6 5 0 109.42 117.14 2.60 o 7 5 0 35.59 35.74 1.38 o 8 5 0 52.81 50.55 2.28 o 9 5 0 12.58 13.11 1.06 o 10 5 0 7.26 5.45 1.06 o 11 5 0 86.37 82.62 3.01 o 12 5 0 22.31 24.09 1.30 o 13 5 0 0.17 0.16 2.44 o 14 5 0 11.09 8.95 1.30 o 2 6 0 5.65 12.45 0.73 o 3 6 0 10.88 12.86 0.73 o 4 6 0 85.37 79.04 2.20 o 5 6 0 360.02 357.03 4.31 o 6 6 0 21.36 21.00 1.06 o 7 6 0 32.23 33.70 1.47 o 8 6 0 463.61 436.64 5.45 o 9 6 0 94.35 91.25 3.17 o 10 6 0 1.07 0.65 2.28 o 11 6 0 0.47 -0.65 2.28 o 12 6 0 44.02 43.39 1.79 o 13 6 0 8.81 10.75 1.30 o 4 7 0 500.62 482.88 4.97 o 5 7 0 18.09 13.11 0.98 o 6 7 0 5.85 8.30 0.98 o 7 7 0 674.93 645.11 6.51 o 8 7 0 32.96 35.17 1.63 o 9 7 0 146.15 135.86 3.66 o 10 7 0 32.06 30.85 1.30 o 11 7 0 24.54 19.78 1.30 o 12 7 0 7.22 4.64 2.69 o 13 7 0 0.21 4.80 2.44 o 3 8 0 75.17 67.89 2.60 o 4 8 0 6.72 8.14 0.90 o 5 8 0 476.15 442.01 5.37 o 6 8 0 8.55 8.06 0.98 o 7 8 0 56.02 52.18 1.95 o 8 8 0 573.12 547.43 6.67 o 9 8 0 504.82 484.02 6.59 o 10 8 0 128.30 120.72 3.99 o 11 8 0 121.22 132.60 4.23 o 12 8 0 169.02 169.89 5.05 o 4 9 0 1.38 0.49 2.04 o 5 9 0 89.23 94.83 3.09 o 6 9 0 192.63 190.15 4.23 o 7 9 0 14.42 15.79 1.22 o 8 9 0 272.83 283.20 5.29 o 10 9 0 78.64 76.11 3.83 o 11 9 0 91.89 102.65 4.15 o 5 10 0 7.88 9.36 1.22 o 6 10 0 173.06 165.90 4.40 o 7 10 0 0.05 2.52 2.44 o 8 10 0 26.53 29.71 1.55 o 9 10 0 14.03 16.44 1.47 o 3 11 0 1.66 4.40 2.52 o 6 11 0 161.84 169.15 4.56 o 7 11 0 111.94 114.94 4.31 o 8 11 0 159.48 175.83 5.29 o 1 12 0 0.09 2.60 3.17 o 3 12 0 0.31 -0.41 2.85 o 5 12 0 0.10 0.08 2.77 o -15 1 1 88.73 85.96 3.09 o -14 1 1 0.08 0.41 2.77 o -13 1 1 78.11 90.60 3.91 o -12 1 1 7.01 7.41 1.30 o -11 1 1 0.86 3.17 1.22 o -10 1 1 8.09 5.86 1.06 o -9 1 1 158.74 168.58 3.34 o -8 1 1 241.18 270.09 3.66 o -7 1 1 593.02 656.10 5.21 o -6 1 1 87.52 123.16 2.28 o -5 1 1 2787.93 2868.68 12.05 o -4 1 1 1223.48 1329.70 6.35 o -3 1 1 83.66 62.35 1.38 o -2 1 1 157.90 165.16 1.55 o -1 1 1 0.07 -0.57 0.73 o 0 1 1 6.36 4.97 0.41 o 1 1 1 546.80 665.38 3.42 o 2 1 1 359.47 410.92 2.85 o 3 1 1 1104.98 1431.04 6.92 o 4 1 1 133.30 114.13 2.20 o 5 1 1 545.18 648.77 4.88 o 6 1 1 1757.37 1991.01 10.26 o 7 1 1 72.18 84.09 2.52 o 8 1 1 689.93 777.88 6.67 o 9 1 1 16.66 20.92 1.06 o 10 1 1 73.07 83.11 3.01 o 11 1 1 11.17 11.88 1.22 o 12 1 1 1.13 4.15 2.36 o 13 1 1 2.71 4.97 2.69 o 14 1 1 13.00 16.28 1.47 o 15 1 1 0.33 5.05 2.77 o -15 2 1 73.08 79.37 2.93 o -14 2 1 9.50 10.91 1.47 o -13 2 1 0.00 0.49 2.60 o -12 2 1 48.79 54.78 2.20 o -11 2 1 0.00 0.49 2.28 o -10 2 1 50.08 49.90 1.87 o -9 2 1 326.15 347.67 4.64 o -8 2 1 151.01 159.87 3.09 o -7 2 1 75.57 87.02 2.28 o -6 2 1 3353.28 3780.14 16.28 o -5 2 1 1304.48 1255.95 6.76 o -4 2 1 935.97 949.15 5.21 o -3 2 1 183.59 155.40 1.95 o -2 2 1 507.44 404.24 2.69 o -1 2 1 3148.66 2924.69 11.80 o 0 2 1 95.59 142.86 1.63 o 1 2 1 838.82 1100.23 5.29 o 2 2 1 11635.33 11998.72 45.26 o 3 2 1 2226.04 2485.52 10.66 o 4 2 1 5415.88 6454.52 26.54 o 5 2 1 105.19 98.09 2.28 o 6 2 1 1934.57 2202.00 11.23 o 7 2 1 1782.58 1904.48 10.75 o 8 2 1 48.24 51.85 1.79 o 9 2 1 500.21 516.66 6.02 o 10 2 1 43.50 46.64 1.95 o 11 2 1 219.25 227.44 4.56 o 12 2 1 1.88 3.83 2.36 o 13 2 1 9.42 10.66 1.38 o 14 2 1 0.12 1.71 2.69 o 15 2 1 1.91 -0.73 3.17 o -15 3 1 116.75 112.01 4.40 o -14 3 1 14.95 15.63 1.30 o -13 3 1 42.19 45.99 1.95 o -12 3 1 4.26 3.17 1.06 o -11 3 1 1.13 1.30 2.12 o -10 3 1 13.34 13.35 0.90 o -9 3 1 249.55 232.97 3.74 o -8 3 1 17.19 18.07 0.90 o -7 3 1 1128.25 1064.82 6.92 o -6 3 1 312.45 273.35 3.17 o -5 3 1 2213.91 2143.88 9.93 o -4 3 1 25.25 48.35 1.47 o -3 3 1 0.20 2.44 0.57 o -2 3 1 0.72 2.93 0.49 o -1 3 1 18.49 15.47 0.81 o 0 3 1 399.42 379.33 2.77 o 1 3 1 1273.39 1272.07 6.11 o 2 3 1 864.75 831.60 4.72 o 3 3 1 4744.87 4423.38 17.01 o 4 3 1 4.70 6.02 0.65 o 5 3 1 1934.02 1908.71 9.44 o 6 3 1 1458.63 1361.28 8.06 o 7 3 1 363.77 376.48 4.07 o 8 3 1 559.08 524.07 5.21 o 9 3 1 6.20 3.26 1.95 o 10 3 1 51.07 55.52 2.60 o 11 3 1 19.36 16.28 1.14 o 12 3 1 4.78 3.91 1.14 o 13 3 1 17.36 15.14 1.22 o 14 3 1 25.68 25.97 1.47 o -14 4 1 86.82 89.70 3.99 o -13 4 1 4.88 3.74 2.52 o -12 4 1 199.83 189.91 4.48 o -11 4 1 0.06 -0.73 2.28 o -10 4 1 523.37 510.55 5.94 o -9 4 1 65.99 64.14 2.52 o -8 4 1 1198.82 1143.86 8.06 o -7 4 1 941.01 914.63 6.67 o -6 4 1 1155.87 1059.04 6.84 o -5 4 1 1028.50 952.89 6.02 o -4 4 1 3.13 -0.41 1.22 o -3 4 1 296.94 300.37 2.85 o -2 4 1 352.91 395.78 3.17 o -1 4 1 1926.86 2151.94 9.28 o 0 4 1 2.29 5.29 0.57 o 1 4 1 11.77 19.86 0.90 o 2 4 1 0.05 -0.57 1.22 o 3 4 1 114.50 127.72 2.28 o 4 4 1 2146.46 2352.68 11.07 o 5 4 1 96.93 85.96 2.12 o 6 4 1 650.28 621.50 5.29 o 7 4 1 298.36 307.62 3.91 o 8 4 1 149.78 150.27 3.17 o 9 4 1 108.14 110.38 3.09 o 10 4 1 25.62 23.61 1.22 o 11 4 1 218.49 196.91 4.40 o 12 4 1 10.39 9.61 1.22 o 13 4 1 219.47 196.67 4.97 o 14 4 1 6.70 9.77 1.30 o -14 5 1 44.20 44.53 1.79 o -13 5 1 36.83 34.11 1.79 o -12 5 1 0.40 2.36 2.12 o -11 5 1 0.02 -0.90 2.04 o -10 5 1 14.57 12.21 1.14 o -9 5 1 11.82 14.25 0.98 o -8 5 1 693.47 619.63 5.94 o -7 5 1 30.82 30.44 1.47 o -6 5 1 2997.78 2833.52 13.76 o -5 5 1 160.94 138.79 2.69 o -4 5 1 3768.33 3693.12 15.79 o -3 5 1 516.19 502.25 4.15 o -2 5 1 1090.51 1114.39 6.35 o -1 5 1 253.23 236.72 2.77 o 0 5 1 970.47 972.59 5.78 o 1 5 1 392.05 389.83 3.58 o 2 5 1 785.92 759.15 5.21 o 3 5 1 2720.78 2685.69 12.37 o 4 5 1 855.01 843.40 6.02 o 5 5 1 1551.53 1567.15 9.12 o 6 5 1 250.27 238.59 3.58 o 7 5 1 319.64 295.57 4.15 o 8 5 1 197.64 175.75 3.42 o 9 5 1 17.57 14.25 1.06 o 10 5 1 24.71 18.56 1.22 o 11 5 1 1.09 2.85 2.20 o 12 5 1 16.45 16.12 1.38 o 13 5 1 21.20 22.96 1.47 o 14 5 1 12.57 12.37 1.47 o -13 6 1 0.34 -1.22 2.36 o -12 6 1 117.71 105.09 3.99 o -11 6 1 1.11 2.85 1.06 o -10 6 1 568.33 506.08 6.35 o -9 6 1 2.39 3.34 2.04 o -8 6 1 2336.63 2173.19 12.86 o -7 6 1 693.03 658.87 6.19 o -6 6 1 4312.64 3933.09 18.07 o -5 6 1 653.19 624.27 5.54 o -4 6 1 817.45 748.98 5.78 o -3 6 1 61.98 56.57 1.95 o -2 6 1 380.30 376.32 3.74 o -1 6 1 1488.74 1597.43 8.55 o 0 6 1 96.28 86.20 2.12 o 1 6 1 274.00 270.91 3.26 o 2 6 1 427.85 507.70 4.56 o 3 6 1 453.93 454.39 4.40 o 4 6 1 205.58 173.96 3.01 o 5 6 1 660.84 612.30 5.62 o 6 6 1 191.44 176.32 3.50 o 7 6 1 1890.85 1725.64 11.07 o 8 6 1 281.61 267.32 4.56 o 9 6 1 910.78 836.08 8.14 o 10 6 1 17.87 16.69 1.30 o 11 6 1 547.72 511.61 7.16 o 12 6 1 0.20 -2.69 2.69 o 13 6 1 242.07 220.52 5.70 o -13 7 1 7.30 4.15 2.93 o -12 7 1 5.69 1.71 2.60 o -11 7 1 14.72 10.75 1.22 o -10 7 1 27.63 28.49 1.30 o -9 7 1 78.85 72.53 3.01 o -8 7 1 216.16 207.25 3.91 o -7 7 1 1.21 0.98 2.12 o -6 7 1 1243.00 1234.05 8.79 o -5 7 1 90.96 89.22 2.60 o -4 7 1 1572.50 1552.42 9.52 o -3 7 1 87.71 83.11 2.44 o -2 7 1 359.92 392.76 4.31 o -1 7 1 9.59 5.86 0.81 o 0 7 1 105.82 111.11 2.52 o 1 7 1 104.39 103.54 2.44 o 2 7 1 125.93 108.92 2.60 o 3 7 1 618.55 604.98 5.45 o 4 7 1 77.19 72.69 2.60 o 5 7 1 674.55 617.19 6.02 o 6 7 1 127.80 131.95 3.17 o 7 7 1 116.74 107.37 3.17 o 8 7 1 73.63 75.79 3.09 o 9 7 1 8.96 8.14 1.22 o 10 7 1 8.78 8.14 1.22 o 11 7 1 11.41 11.72 1.30 o 12 7 1 64.87 61.87 2.52 o -12 8 1 1.17 2.44 2.60 o -11 8 1 0.24 0.00 2.52 o -10 8 1 15.54 13.51 1.22 o -9 8 1 21.23 21.16 1.22 o -8 8 1 19.95 19.21 1.22 o -7 8 1 52.46 51.53 1.95 o -6 8 1 81.99 86.12 3.01 o -5 8 1 289.64 294.43 4.40 o -4 8 1 108.83 109.24 3.01 o -3 8 1 179.41 198.78 3.50 o -2 8 1 96.75 105.17 2.77 o -1 8 1 745.86 771.45 6.51 o 0 8 1 54.36 70.33 2.44 o 1 8 1 212.12 234.27 3.74 o 2 8 1 1046.30 986.35 7.73 o 3 8 1 275.73 288.24 4.31 o 4 8 1 610.29 552.56 5.86 o 5 8 1 51.94 48.84 1.79 o 6 8 1 279.13 272.45 4.56 o 7 8 1 55.54 55.35 1.95 o 8 8 1 9.68 9.69 1.14 o 9 8 1 18.52 22.14 1.30 o 10 8 1 6.04 7.08 1.30 o 11 8 1 0.39 -0.65 2.69 o -11 9 1 20.41 14.57 1.38 o -10 9 1 0.32 -1.06 2.44 o -9 9 1 109.74 100.94 3.66 o -8 9 1 11.12 11.23 1.22 o -7 9 1 126.35 116.08 3.66 o -6 9 1 0.13 -0.16 2.20 o -5 9 1 103.97 107.53 3.26 o -4 9 1 1.12 0.41 1.95 o -3 9 1 42.39 46.15 1.79 o -2 9 1 67.15 58.28 2.52 o -1 9 1 4.89 9.77 0.90 o 0 9 1 44.46 47.70 1.79 o 1 9 1 17.49 18.32 1.06 o 2 9 1 0.95 2.60 2.12 o 3 9 1 10.73 8.47 1.06 o 4 9 1 119.80 118.11 3.42 o 5 9 1 77.45 67.97 2.93 o 6 9 1 101.52 94.59 3.50 o 7 9 1 11.37 9.04 1.22 o 8 9 1 89.50 83.11 3.58 o 9 9 1 0.36 0.41 2.60 o 10 9 1 78.34 76.92 3.74 o -9 10 1 0.22 -2.85 2.85 o -8 10 1 170.96 189.67 4.88 o -7 10 1 0.11 0.73 2.44 o -6 10 1 175.98 182.10 4.40 o -5 10 1 9.76 10.26 1.14 o -4 10 1 34.97 32.80 1.55 o -3 10 1 105.89 121.04 3.74 o -2 10 1 35.18 39.97 1.87 o -1 10 1 496.87 555.89 6.27 o 0 10 1 44.78 61.62 3.01 o 1 10 1 147.42 170.70 3.99 o 2 10 1 597.56 595.86 6.84 o 3 10 1 111.10 133.34 3.66 o 4 10 1 326.17 302.00 5.29 o 5 10 1 42.31 44.69 2.12 o 6 10 1 17.83 16.69 1.30 o 7 10 1 85.85 97.28 3.74 o 8 10 1 6.45 6.92 1.38 o 9 10 1 92.42 96.30 4.23 o -8 11 1 0.50 -2.85 2.85 o -7 11 1 7.50 8.38 1.38 o -6 11 1 30.97 36.14 2.04 o -5 11 1 0.05 0.90 2.44 o -4 11 1 3.99 7.49 1.22 o -3 11 1 0.01 2.12 2.28 o -2 11 1 15.37 14.98 1.22 o -1 11 1 47.79 49.41 2.12 o 0 11 1 9.11 10.66 1.22 o 1 11 1 20.83 22.14 1.38 o 2 11 1 33.40 25.23 1.38 o 3 11 1 2.79 0.57 2.69 o 4 11 1 0.32 -1.71 2.60 o 5 11 1 1.94 3.74 2.60 o 6 11 1 0.32 4.64 2.60 o 7 11 1 1.78 1.87 2.85 o -5 12 1 34.41 36.31 1.87 o -4 12 1 0.07 -0.98 2.60 o -3 12 1 26.09 22.47 1.55 o -2 12 1 48.31 51.77 2.44 o -1 12 1 170.55 175.34 4.64 o 0 12 1 55.38 51.04 2.52 o 1 12 1 128.20 141.80 4.40 o 2 12 1 162.96 190.56 4.97 o 3 12 1 115.60 122.92 4.40 o 4 12 1 54.64 72.20 2.69 o 5 12 1 0.01 1.47 2.93 o -15 0 2 13.70 10.42 1.71 o -14 0 2 0.77 0.57 3.34 o -13 0 2 248.90 241.60 5.54 o -12 0 2 37.99 46.24 2.20 o -11 0 2 0.00 2.04 1.14 o -10 0 2 13.73 14.57 1.06 o -9 0 2 894.25 852.11 7.00 o -8 0 2 27.39 27.76 1.22 o -7 0 2 562.91 560.86 4.64 o -6 0 2 708.15 677.26 4.80 o -5 0 2 701.78 652.03 4.31 o -4 0 2 403.00 497.04 3.42 o -3 0 2 5119.03 4322.52 17.09 o -2 0 2 7492.85 6402.91 25.40 o -1 0 2 3605.11 3312.57 13.27 o 0 0 2 235.46 239.65 2.12 o 2 0 2 6823.57 6928.68 26.29 o 3 0 2 7328.59 7574.44 29.30 o 4 0 2 1061.02 1146.46 6.59 o 5 0 2 2227.02 2516.21 12.05 o 6 0 2 840.62 968.11 6.92 o 7 0 2 604.24 667.98 6.02 o 8 0 2 272.17 273.51 4.23 o 9 0 2 35.87 39.81 1.95 o 10 0 2 64.39 77.74 3.17 o 11 0 2 18.04 19.78 1.30 o 12 0 2 61.89 66.83 2.52 o 13 0 2 12.82 13.43 1.55 o 14 0 2 274.31 287.59 6.35 o -15 1 2 8.12 12.13 1.63 o -14 1 2 667.67 699.40 9.20 o -13 1 2 33.16 37.04 1.79 o -12 1 2 786.31 837.54 8.63 o -11 1 2 1704.27 1717.17 12.13 o -10 1 2 1647.91 1610.13 10.83 o -9 1 2 188.82 189.67 3.42 o -8 1 2 262.68 275.14 3.66 o -7 1 2 77.64 82.79 2.12 o -6 1 2 269.99 287.35 3.01 o -5 1 2 942.12 896.48 5.29 o -4 1 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78.39 1.95 o 4 2 2 28.57 28.17 1.22 o 5 2 2 13.43 16.44 0.90 o 6 2 2 591.88 640.80 5.70 o 7 2 2 352.53 410.51 4.88 o 8 2 2 135.66 146.03 3.50 o 9 2 2 56.16 52.67 2.12 o 10 2 2 488.09 489.71 6.43 o 11 2 2 21.40 23.77 1.38 o 12 2 2 11.09 5.05 2.85 o 13 2 2 40.68 38.99 1.71 o 14 2 2 13.69 14.82 1.47 o -15 3 2 30.06 26.13 1.55 o -14 3 2 0.82 -0.41 2.60 o -13 3 2 39.66 35.41 1.47 o -12 3 2 31.89 29.63 1.47 o -11 3 2 18.11 14.82 1.06 o -10 3 2 50.59 43.39 1.71 o -9 3 2 178.43 159.95 3.09 o -8 3 2 233.15 207.49 3.26 o -7 3 2 13.43 14.57 0.81 o -6 3 2 638.44 555.40 4.48 o -5 3 2 2077.54 2093.41 9.85 o -4 3 2 79.55 57.63 1.63 o -3 3 2 1012.21 1025.50 5.54 o -2 3 2 8743.25 8295.91 34.03 o 0 3 2 4064.32 3886.61 14.73 o 1 3 2 12.77 7.16 0.57 o 2 3 2 279.49 230.61 2.52 o 3 3 2 513.03 511.29 3.99 o 4 3 2 168.59 153.44 2.36 o 5 3 2 249.83 249.90 3.17 o 6 3 2 66.41 54.70 2.04 o 7 3 2 184.92 174.85 3.17 o 8 3 2 19.45 16.44 0.98 o 9 3 2 119.28 105.74 2.93 o 10 3 2 25.58 23.93 1.22 o 11 3 2 4.55 4.23 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