#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/06/2230623.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230623_Fobs loop_ _publ_author_name 'Betz, Richard' 'Gerber, Thomas' 'Schalekamp, Henk' _publ_section_title ; 5-Aminopentan-1-ol ; _journal_coeditor_code EZ2250 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1841 _journal_volume 67 _journal_year 2011 _space_group_IT_number 56 _symmetry_space_group_name_Hall '-P 2ab 2ac' _symmetry_space_group_name_H-M 'P c c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.0973 _cell_length_b 17.4145 _cell_length_c 7.0564 _exptl_crystal_F_000 464.00 _reflns_d_resolution_high 0.7503 _[local]_cod_data_source_file ez2250Isup3.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ba221_s in Pccn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 71.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z' 'x+1/2, -y, -z+1/2' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z' '-x-1/2, y, z-1/2' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 870.27 985.72 13.62 o 10 0 0 544.84 494.55 15.36 o 12 0 0 458.41 437.54 10.71 o 1 1 0 443.30 406.17 8.53 o 3 1 0 383.52 417.95 2.75 o 5 1 0 137.08 155.13 1.06 o 7 1 0 327.11 365.03 6.27 o 9 1 0 85.43 88.36 1.76 o 11 1 0 15.44 17.70 0.82 o 13 1 0 45.52 47.79 1.36 o 0 2 0 32.09 34.81 0.53 o 2 2 0 1238.72 1211.14 8.36 o 4 2 0 237.22 227.68 2.83 o 6 2 0 260.52 282.82 2.79 o 8 2 0 528.36 551.45 5.82 o 10 2 0 177.59 166.48 2.74 o 12 2 0 57.43 48.78 0.90 o 1 3 0 7.23 7.73 0.10 o 3 3 0 12.37 15.94 0.23 o 5 3 0 127.25 142.64 1.07 o 7 3 0 161.11 168.63 2.66 o 9 3 0 52.51 46.70 0.73 o 11 3 0 25.23 26.85 0.75 o 13 3 0 80.61 84.30 1.62 o 0 4 0 917.77 871.89 4.20 o 2 4 0 296.06 271.33 2.30 o 4 4 0 437.02 450.39 3.85 o 6 4 0 116.27 112.22 0.90 o 8 4 0 199.32 212.13 1.56 o 10 4 0 0.65 0.54 0.34 o 12 4 0 0.10 0.15 0.21 o 1 5 0 123.62 116.39 2.14 o 3 5 0 512.03 569.61 4.56 o 5 5 0 18.79 18.48 0.51 o 7 5 0 42.32 39.40 0.65 o 9 5 0 92.74 85.03 1.43 o 11 5 0 0.81 0.81 0.28 o 13 5 0 25.07 27.29 0.79 o 2 6 0 581.17 561.32 4.36 o 4 6 0 448.03 483.75 5.84 o 6 6 0 680.38 630.30 11.46 o 8 6 0 8.14 7.62 0.38 o 10 6 0 1197.94 1191.22 21.47 o 12 6 0 0.00 0.23 0.22 o 1 7 0 956.21 1031.88 22.51 o 3 7 0 676.95 652.95 6.11 o 5 7 0 1074.02 1115.76 19.51 o 7 7 0 1256.86 1200.93 28.22 o 9 7 0 1853.79 1845.88 42.69 o 11 7 0 244.41 250.54 5.61 o 0 8 0 1175.56 1192.91 10.55 o 2 8 0 3433.74 3517.26 26.03 o 4 8 0 130.04 129.81 1.86 o 6 8 0 2132.85 2102.85 27.98 o 8 8 0 973.52 942.80 11.91 o 10 8 0 121.22 124.48 0.82 o 12 8 0 52.40 51.39 0.67 o 1 9 0 76.70 92.91 2.09 o 3 9 0 777.39 833.26 14.62 o 5 9 0 394.77 411.48 12.88 o 7 9 0 1.22 0.27 0.12 o 9 9 0 4.23 4.02 0.39 o 11 9 0 15.73 15.72 0.47 o 0 10 0 832.96 847.16 4.34 o 2 10 0 1054.50 1079.41 28.97 o 4 10 0 41.85 49.60 1.69 o 6 10 0 621.23 618.72 23.65 o 8 10 0 438.99 435.59 12.52 o 10 10 0 8.54 7.30 0.43 o 12 10 0 0.96 0.43 0.28 o 1 11 0 31.75 25.86 0.78 o 3 11 0 90.87 99.03 1.36 o 5 11 0 435.05 422.97 14.54 o 7 11 0 21.90 21.35 0.40 o 9 11 0 20.32 22.74 0.66 o 11 11 0 3.47 2.48 0.28 o 0 12 0 214.88 212.62 1.31 o 2 12 0 362.94 356.40 9.25 o 4 12 0 18.13 23.54 0.96 o 6 12 0 283.71 256.68 7.95 o 8 12 0 146.17 148.98 4.81 o 10 12 0 3.45 3.24 0.28 o 1 13 0 2182.14 1989.17 13.05 o 3 13 0 868.88 767.82 14.67 o 5 13 0 754.71 674.67 28.44 o 7 13 0 167.16 135.90 5.14 o 9 13 0 20.52 16.95 0.78 o 11 13 0 115.52 123.31 4.40 o 0 14 0 202.47 199.60 1.44 o 2 14 0 76.07 84.31 2.92 o 4 14 0 42.18 38.42 1.14 o 6 14 0 166.17 167.69 3.13 o 8 14 0 7.17 7.94 0.40 o 10 14 0 63.41 67.26 2.13 o 1 15 0 1118.69 1007.66 11.08 o 3 15 0 603.66 543.80 13.70 o 5 15 0 331.77 295.32 7.81 o 7 15 0 101.59 76.62 3.12 o 9 15 0 0.03 0.20 0.26 o 0 16 0 81.30 73.62 1.01 o 2 16 0 104.40 101.13 1.80 o 4 16 0 11.95 13.67 0.49 o 6 16 0 69.38 58.58 0.99 o 8 16 0 108.49 114.78 3.47 o 1 17 0 86.92 85.39 0.78 o 3 17 0 2.98 2.50 0.28 o 5 17 0 238.08 230.20 7.29 o 7 17 0 49.49 45.92 1.48 o 9 17 0 12.14 12.01 0.92 o 0 18 0 225.17 210.06 1.68 o 2 18 0 169.54 166.19 2.80 o 4 18 0 4.67 6.37 0.46 o 6 18 0 127.95 120.95 2.81 o 8 18 0 154.39 162.77 5.22 o 1 19 0 21.30 23.06 0.54 o 3 19 0 19.39 17.01 0.95 o 5 19 0 170.91 170.68 5.47 o 7 19 0 0.87 -0.46 0.50 o 0 20 0 420.69 423.38 2.51 o 2 20 0 429.91 443.31 3.38 o 4 20 0 3.80 2.23 0.33 o 6 20 0 813.82 853.12 17.96 o 1 21 0 249.43 259.06 2.67 o 3 21 0 35.05 34.99 1.18 o 5 21 0 190.92 205.66 4.46 o 0 22 0 2.95 3.39 0.52 o 2 22 0 35.77 36.63 0.72 o 4 22 0 0.54 -0.37 0.37 o 1 23 0 0.49 0.89 0.35 o 1 1 1 188.76 173.69 1.49 o 3 1 1 1364.42 1373.29 5.05 o 4 1 1 13.11 15.70 0.29 o 5 1 1 57.07 56.32 0.31 o 6 1 1 1741.24 2045.43 14.52 o 7 1 1 485.76 506.98 5.22 o 8 1 1 18.27 24.40 0.54 o 9 1 1 30.37 26.67 0.25 o 10 1 1 49.12 29.57 0.44 o 11 1 1 59.53 62.05 0.82 o 12 1 1 22.82 19.19 0.35 o 13 1 1 24.05 23.67 0.52 o 1 2 1 1728.27 1703.15 35.99 o 2 2 1 1563.94 1510.38 8.42 o 3 2 1 331.18 321.77 1.55 o 4 2 1 5.33 4.92 0.16 o 5 2 1 104.60 127.17 0.72 o 6 2 1 83.46 97.20 0.67 o 7 2 1 338.10 352.99 2.77 o 8 2 1 1.13 0.78 0.08 o 9 2 1 193.57 180.21 1.71 o 10 2 1 12.08 8.92 0.21 o 11 2 1 43.16 38.11 0.71 o 12 2 1 10.10 9.96 0.38 o 13 2 1 23.38 24.76 0.40 o 1 3 1 13.59 14.23 0.19 o 2 3 1 157.33 141.77 0.87 o 3 3 1 457.25 438.65 2.66 o 4 3 1 1098.01 1151.95 6.08 o 5 3 1 20.82 25.14 0.16 o 6 3 1 676.13 723.91 5.91 o 7 3 1 230.17 238.05 2.14 o 8 3 1 0.98 0.15 0.10 o 9 3 1 7.26 6.36 0.20 o 10 3 1 18.67 20.24 0.34 o 11 3 1 11.20 12.05 0.29 o 12 3 1 0.59 0.15 0.14 o 13 3 1 0.21 0.04 0.19 o 2 4 1 325.56 319.06 2.91 o 3 4 1 699.51 722.52 5.17 o 4 4 1 28.93 25.06 0.16 o 5 4 1 323.24 342.28 2.13 o 6 4 1 31.16 32.63 0.26 o 7 4 1 810.99 814.07 7.80 o 8 4 1 6.95 5.38 0.27 o 9 4 1 241.84 228.71 1.96 o 10 4 1 2.11 1.14 0.11 o 11 4 1 12.43 9.77 0.24 o 12 4 1 13.43 13.26 0.41 o 13 4 1 3.73 3.00 0.22 o 1 5 1 149.20 138.11 1.33 o 2 5 1 545.01 541.90 5.22 o 3 5 1 488.49 499.70 4.43 o 4 5 1 1499.38 1547.35 10.92 o 5 5 1 97.94 98.75 0.76 o 6 5 1 195.19 210.20 1.75 o 7 5 1 343.22 345.33 3.02 o 8 5 1 28.38 24.96 0.41 o 9 5 1 0.33 0.27 0.13 o 10 5 1 1.85 1.10 0.17 o 11 5 1 30.46 31.67 0.43 o 12 5 1 2.26 1.54 0.18 o 13 5 1 0.06 -0.28 0.28 o 2 6 1 661.94 734.04 6.65 o 3 6 1 2070.32 2271.35 24.23 o 4 6 1 16.93 20.87 0.26 o 5 6 1 1334.89 1289.14 13.99 o 6 6 1 65.46 66.42 0.54 o 7 6 1 2614.19 2618.11 25.18 o 8 6 1 9.65 11.17 0.50 o 9 6 1 1.70 1.22 0.18 o 10 6 1 7.52 8.41 0.33 o 11 6 1 315.86 332.25 3.69 o 12 6 1 2.02 2.38 0.19 o 1 7 1 1284.77 1271.41 12.78 o 2 7 1 964.05 951.56 12.19 o 3 7 1 690.24 725.43 6.96 o 4 7 1 664.27 679.80 6.64 o 5 7 1 84.01 80.32 1.05 o 6 7 1 0.64 0.63 0.19 o 7 7 1 70.85 71.30 0.95 o 8 7 1 1629.57 1613.06 20.28 o 9 7 1 47.17 48.24 0.75 o 10 7 1 66.38 63.94 0.88 o 11 7 1 18.45 18.31 0.40 o 12 7 1 546.13 577.66 5.74 o 1 8 1 8.64 2.19 0.13 o 2 8 1 896.32 919.14 10.26 o 3 8 1 329.19 329.27 5.21 o 4 8 1 132.26 134.07 2.27 o 5 8 1 294.68 322.27 4.90 o 6 8 1 111.15 111.11 1.53 o 7 8 1 251.68 254.43 2.90 o 8 8 1 134.05 137.90 1.82 o 9 8 1 536.03 538.96 5.99 o 10 8 1 2.04 1.77 0.15 o 11 8 1 413.44 422.89 5.56 o 12 8 1 50.81 56.34 0.49 o 1 9 1 0.00 0.11 0.06 o 2 9 1 9.57 8.99 0.18 o 3 9 1 56.15 56.31 1.30 o 4 9 1 82.80 93.63 1.62 o 5 9 1 14.50 12.56 0.25 o 6 9 1 23.32 23.37 0.62 o 7 9 1 38.88 39.58 0.59 o 8 9 1 34.10 35.51 0.53 o 9 9 1 7.25 6.63 0.24 o 10 9 1 19.33 18.84 0.41 o 11 9 1 16.04 16.83 0.34 o 12 9 1 2.62 1.62 0.20 o 1 10 1 31.44 29.38 0.48 o 2 10 1 88.79 87.41 1.70 o 3 10 1 277.24 281.26 4.00 o 4 10 1 0.05 0.06 0.07 o 5 10 1 3.77 2.78 0.20 o 6 10 1 11.79 11.72 0.46 o 7 10 1 179.00 179.07 3.55 o 8 10 1 0.00 -0.12 0.12 o 9 10 1 20.07 17.78 0.34 o 10 10 1 0.06 -0.16 0.16 o 11 10 1 11.77 11.06 0.32 o 12 10 1 2.01 0.58 0.38 o 1 11 1 1.48 1.62 0.10 o 2 11 1 39.06 35.93 0.65 o 3 11 1 19.51 17.45 0.23 o 4 11 1 6.86 3.05 0.19 o 5 11 1 0.93 0.65 0.09 o 6 11 1 19.47 18.60 0.32 o 7 11 1 20.72 18.63 0.39 o 8 11 1 73.24 75.38 1.56 o 9 11 1 4.42 3.37 0.18 o 10 11 1 3.35 2.86 0.19 o 11 11 1 0.41 0.25 0.24 o 1 12 1 0.64 1.00 0.11 o 2 12 1 37.18 33.75 0.93 o 3 12 1 424.38 418.06 6.87 o 4 12 1 0.95 0.37 0.13 o 5 12 1 21.29 18.60 0.49 o 6 12 1 5.17 2.47 0.14 o 7 12 1 286.27 258.94 5.16 o 8 12 1 1.02 0.93 0.16 o 9 12 1 167.51 161.75 3.14 o 10 12 1 6.10 6.29 0.29 o 11 12 1 46.39 51.45 0.92 o 1 13 1 348.30 336.94 4.17 o 2 13 1 1.05 1.06 0.28 o 3 13 1 65.76 61.08 1.10 o 4 13 1 1.67 2.08 0.12 o 5 13 1 59.16 51.15 0.66 o 6 13 1 93.25 82.91 1.23 o 7 13 1 0.95 0.89 0.17 o 8 13 1 250.14 251.67 4.31 o 9 13 1 20.50 23.78 0.73 o 10 13 1 17.18 18.92 0.51 o 11 13 1 0.03 -0.30 0.31 o 1 14 1 4718.60 4288.85 25.15 o 2 14 1 207.66 203.55 5.20 o 3 14 1 566.75 492.88 8.33 o 4 14 1 175.08 190.41 3.45 o 5 14 1 826.86 704.49 11.27 o 6 14 1 64.73 61.67 0.81 o 7 14 1 9.90 12.67 0.31 o 8 14 1 235.08 242.91 4.92 o 9 14 1 216.66 251.44 4.90 o 10 14 1 14.32 13.97 0.36 o 1 15 1 103.04 118.59 0.71 o 2 15 1 158.03 153.03 1.73 o 3 15 1 15.79 14.40 0.24 o 4 15 1 160.36 168.08 2.66 o 5 15 1 11.28 10.52 0.33 o 6 15 1 34.01 33.26 0.42 o 7 15 1 0.66 0.57 0.18 o 8 15 1 0.64 0.78 0.19 o 9 15 1 18.05 18.44 0.40 o 10 15 1 2.76 2.58 0.21 o 1 16 1 36.80 41.44 0.41 o 2 16 1 0.55 0.61 0.17 o 3 16 1 65.89 63.60 0.89 o 4 16 1 1.05 0.94 0.19 o 5 16 1 0.54 0.34 0.19 o 6 16 1 0.03 -0.03 0.19 o 7 16 1 51.33 47.63 0.86 o 8 16 1 0.39 0.49 0.20 o 9 16 1 61.43 61.54 1.51 o 1 17 1 0.19 0.24 0.18 o 2 17 1 4.59 3.21 0.21 o 3 17 1 1.94 1.47 0.19 o 4 17 1 3.72 1.90 0.20 o 5 17 1 0.26 0.23 0.19 o 6 17 1 15.31 15.64 0.37 o 7 17 1 0.87 0.71 0.19 o 8 17 1 30.97 33.60 0.44 o 9 17 1 0.86 0.52 0.46 o 1 18 1 23.46 21.50 0.38 o 2 18 1 7.87 7.96 0.32 o 3 18 1 53.41 50.84 0.49 o 4 18 1 0.42 0.37 0.19 o 5 18 1 23.10 20.72 0.44 o 6 18 1 2.15 1.88 0.22 o 7 18 1 22.72 23.40 0.76 o 8 18 1 0.72 0.59 0.22 o 1 19 1 8.61 8.95 0.34 o 2 19 1 15.54 16.93 0.37 o 3 19 1 4.97 4.09 0.47 o 4 19 1 81.95 86.59 1.57 o 5 19 1 0.12 0.00 0.21 o 6 19 1 1.19 0.96 0.23 o 7 19 1 0.91 0.58 0.22 o 1 20 1 220.81 225.85 1.19 o 2 20 1 57.48 61.80 0.57 o 3 20 1 134.69 134.30 1.50 o 4 20 1 58.07 60.63 1.10 o 5 20 1 1.98 1.16 0.23 o 6 20 1 23.18 26.39 0.48 o 1 21 1 90.66 95.75 0.67 o 2 21 1 7.56 7.19 0.37 o 3 21 1 39.03 39.52 0.83 o 4 21 1 262.15 284.56 3.08 o 5 21 1 13.52 13.51 0.56 o 1 22 1 64.33 65.74 0.61 o 2 22 1 22.55 23.38 0.47 o 3 22 1 167.74 185.96 0.94 o 2 0 2 2680.93 2672.14 46.90 o 3 0 2 17.26 17.98 1.34 o 4 0 2 1668.90 1919.24 13.47 o 5 0 2 1988.39 2122.59 16.14 o 6 0 2 1020.44 1049.27 9.03 o 7 0 2 317.04 295.55 3.16 o 8 0 2 162.28 108.59 2.39 o 9 0 2 984.70 1012.42 16.20 o 10 0 2 75.07 57.52 1.09 o 11 0 2 165.22 159.74 2.79 o 12 0 2 211.00 193.84 4.05 o 13 0 2 97.77 108.21 2.23 o 1 1 2 20.81 18.05 0.22 o 2 1 2 264.08 247.18 1.95 o 3 1 2 590.57 600.91 2.53 o 4 1 2 523.81 598.19 2.58 o 5 1 2 1083.37 1116.40 6.89 o 6 1 2 115.77 127.56 0.85 o 7 1 2 104.17 116.43 1.05 o 8 1 2 70.67 57.18 0.60 o 9 1 2 23.03 25.87 0.50 o 10 1 2 50.68 44.32 0.45 o 11 1 2 0.03 0.25 0.13 o 12 1 2 70.83 71.17 0.76 o 13 1 2 11.98 12.74 0.35 o 0 2 2 1.14 1.77 0.28 o 1 2 2 62.65 64.89 0.49 o 2 2 2 445.75 430.42 2.64 o 3 2 2 1.09 0.75 0.05 o 4 2 2 160.44 187.25 1.03 o 5 2 2 37.81 37.98 0.30 o 6 2 2 62.29 61.16 0.73 o 7 2 2 0.57 1.04 0.07 o 8 2 2 256.04 284.06 3.13 o 9 2 2 0.10 0.55 0.33 o 10 2 2 144.10 140.97 2.17 o 11 2 2 21.96 19.78 0.39 o 12 2 2 80.35 69.00 0.80 o 13 2 2 1.15 1.07 0.22 o 0 3 2 13.76 9.50 0.20 o 1 3 2 119.49 125.98 0.99 o 2 3 2 58.75 53.36 0.44 o 3 3 2 75.99 76.75 0.42 o 4 3 2 0.01 1.47 0.34 o 5 3 2 59.58 59.41 0.57 o 6 3 2 22.98 24.42 0.17 o 7 3 2 126.53 126.57 1.33 o 8 3 2 25.81 28.94 0.34 o 9 3 2 46.03 42.17 0.61 o 10 3 2 12.52 10.88 0.26 o 11 3 2 53.01 54.95 0.77 o 12 3 2 5.24 2.94 0.18 o 13 3 2 74.47 77.87 1.14 o 0 4 2 118.64 137.38 1.86 o 1 4 2 169.83 164.65 1.33 o 2 4 2 73.85 66.79 0.43 o 3 4 2 114.85 117.88 0.72 o 4 4 2 122.30 136.63 0.95 o 5 4 2 43.94 44.24 0.43 o 6 4 2 16.30 13.98 0.15 o 7 4 2 17.42 16.77 0.16 o 8 4 2 91.96 98.73 1.27 o 9 4 2 0.10 0.26 0.24 o 10 4 2 3.09 2.36 0.16 o 11 4 2 0.12 -0.13 0.13 o 12 4 2 0.12 -0.17 0.17 o 0 5 2 0.01 3.55 1.47 o 1 5 2 156.39 156.26 1.20 o 2 5 2 72.16 67.57 0.50 o 3 5 2 153.93 172.63 1.08 o 4 5 2 5.36 5.48 0.11 o 5 5 2 319.81 329.82 3.13 o 6 5 2 72.10 69.40 0.50 o 7 5 2 40.34 37.93 0.38 o 8 5 2 0.92 0.43 0.09 o 9 5 2 240.25 243.91 3.52 o 10 5 2 46.96 47.01 0.39 o 11 5 2 15.63 15.63 0.36 o 12 5 2 0.51 0.17 0.16 o 0 6 2 33.12 29.92 0.30 o 1 6 2 1822.30 1933.61 30.55 o 2 6 2 67.15 67.76 0.62 o 3 6 2 21.60 25.61 0.34 o 4 6 2 148.43 142.19 1.17 o 5 6 2 983.63 997.09 10.54 o 6 6 2 128.67 123.42 1.46 o 7 6 2 75.56 76.37 0.69 o 8 6 2 65.06 62.63 0.88 o 9 6 2 416.58 430.00 5.14 o 10 6 2 381.13 370.04 4.07 o 11 6 2 102.37 104.59 0.96 o 12 6 2 13.13 13.98 0.35 o 0 7 2 5151.31 5090.12 13.08 o 1 7 2 52.46 68.71 0.87 o 2 7 2 0.09 1.11 0.11 o 3 7 2 206.51 209.56 1.76 o 4 7 2 899.89 931.48 8.64 o 5 7 2 42.71 45.74 0.49 o 6 7 2 3.72 3.11 0.27 o 7 7 2 620.11 643.94 6.43 o 8 7 2 2.24 2.11 0.12 o 9 7 2 646.27 638.83 8.48 o 10 7 2 195.00 196.90 2.32 o 11 7 2 91.40 100.03 1.03 o 12 7 2 53.78 56.71 0.97 o 0 8 2 435.57 483.63 6.92 o 1 8 2 349.68 358.18 4.13 o 2 8 2 1627.13 1668.03 21.17 o 3 8 2 279.98 268.30 4.44 o 4 8 2 96.95 99.08 0.87 o 5 8 2 35.85 35.06 0.40 o 6 8 2 1013.91 1005.36 14.07 o 7 8 2 50.08 47.78 0.64 o 8 8 2 536.84 543.61 8.62 o 9 8 2 20.19 20.71 0.40 o 10 8 2 66.46 67.99 1.01 o 11 8 2 34.19 35.49 0.84 o 12 8 2 14.67 16.52 0.38 o 0 9 2 43.18 45.31 0.72 o 1 9 2 442.52 485.34 6.18 o 2 9 2 427.23 456.91 7.24 o 3 9 2 1059.14 1095.00 21.67 o 4 9 2 26.91 25.76 0.32 o 5 9 2 171.23 169.07 2.24 o 6 9 2 388.59 389.83 5.84 o 7 9 2 0.14 -0.11 0.11 o 8 9 2 137.96 139.73 2.09 o 9 9 2 1.26 1.17 0.29 o 10 9 2 28.34 29.90 0.43 o 11 9 2 6.25 4.98 0.35 o 12 9 2 3.59 2.84 0.26 o 0 10 2 949.85 940.54 9.60 o 1 10 2 54.83 55.18 1.15 o 2 10 2 384.33 412.79 6.67 o 3 10 2 0.00 0.10 0.09 o 4 10 2 0.44 0.01 0.08 o 5 10 2 67.22 64.09 0.95 o 6 10 2 161.09 150.21 2.07 o 7 10 2 0.58 0.22 0.13 o 8 10 2 178.67 180.20 3.15 o 9 10 2 6.82 6.93 0.24 o 10 10 2 47.95 48.83 0.85 o 11 10 2 19.53 20.82 0.58 o 0 11 2 4.86 6.93 0.32 o 1 11 2 63.44 63.03 0.76 o 2 11 2 124.76 127.62 1.79 o 3 11 2 249.95 256.15 4.99 o 4 11 2 31.72 34.77 0.56 o 5 11 2 154.93 162.62 2.61 o 6 11 2 143.89 137.76 2.16 o 7 11 2 16.96 16.88 0.49 o 8 11 2 91.75 94.56 1.78 o 9 11 2 4.27 3.70 0.19 o 10 11 2 3.48 2.74 0.19 o 11 11 2 6.37 5.43 0.32 o 0 12 2 772.32 724.83 3.94 o 1 12 2 326.45 307.96 5.03 o 2 12 2 82.88 83.40 1.45 o 3 12 2 123.24 113.86 1.70 o 4 12 2 37.95 29.91 0.70 o 5 12 2 74.84 64.98 1.26 o 6 12 2 14.93 11.05 0.30 o 7 12 2 9.72 7.38 0.29 o 8 12 2 36.54 38.23 0.81 o 9 12 2 0.10 0.15 0.16 o 10 12 2 97.08 102.60 2.08 o 11 12 2 38.70 40.36 0.73 o 0 13 2 522.21 475.59 6.16 o 1 13 2 657.33 596.25 11.50 o 2 13 2 95.50 105.54 1.58 o 3 13 2 404.71 358.56 5.40 o 4 13 2 240.26 221.05 3.35 o 5 13 2 148.29 130.18 2.35 o 6 13 2 255.70 275.06 4.23 o 7 13 2 168.53 146.17 3.61 o 8 13 2 57.68 53.66 1.38 o 9 13 2 9.22 11.17 0.32 o 10 13 2 159.64 168.15 3.02 o 0 14 2 84.78 89.26 2.43 o 1 14 2 9.15 11.88 0.64 o 2 14 2 32.37 33.84 0.33 o 3 14 2 12.66 12.62 0.31 o 4 14 2 21.60 20.50 0.30 o 5 14 2 0.40 0.15 0.14 o 6 14 2 81.19 84.38 1.24 o 7 14 2 2.32 1.21 0.18 o 8 14 2 2.84 3.10 0.20 o 9 14 2 1.08 0.89 0.18 o 10 14 2 43.45 48.58 0.80 o 0 15 2 47.02 39.43 0.57 o 1 15 2 313.28 281.50 5.87 o 2 15 2 141.75 150.50 2.07 o 3 15 2 222.22 195.84 1.46 o 4 15 2 63.87 61.67 1.09 o 5 15 2 73.68 61.03 0.86 o 6 15 2 358.53 371.25 5.39 o 7 15 2 90.38 79.05 1.31 o 8 15 2 68.50 67.80 1.22 o 9 15 2 13.81 16.36 0.42 o 0 16 2 191.82 185.80 1.47 o 1 16 2 118.93 109.56 0.79 o 2 16 2 12.17 10.68 0.31 o 3 16 2 66.48 59.42 0.49 o 4 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o 0 21 2 314.63 338.79 1.65 o 1 21 2 62.39 64.26 0.59 o 2 21 2 1.29 1.91 0.29 o 3 21 2 11.81 12.18 0.41 o 4 21 2 110.86 117.41 1.18 o 0 22 2 44.86 48.04 0.78 o 1 22 2 93.90 100.87 0.72 o 2 22 2 6.57 5.37 0.31 o 3 22 2 16.78 18.50 0.54 o 1 1 3 38.09 46.98 0.56 o 2 1 3 542.61 645.00 6.87 o 3 1 3 1176.13 1205.29 12.09 o 4 1 3 80.35 86.29 0.52 o 5 1 3 133.27 119.58 0.87 o 6 1 3 156.35 198.41 1.45 o 7 1 3 841.86 871.89 7.14 o 8 1 3 243.75 256.14 3.26 o 9 1 3 58.20 55.80 0.66 o 10 1 3 26.93 18.02 0.27 o 11 1 3 126.65 141.73 1.28 o 12 1 3 37.35 45.33 0.70 o 1 2 3 1116.72 1175.39 7.48 o 2 2 3 603.79 661.70 3.55 o 3 2 3 328.01 343.41 1.89 o 4 2 3 0.33 0.87 0.10 o 5 2 3 2.46 0.85 0.05 o 6 2 3 63.71 73.92 0.57 o 7 2 3 90.53 95.36 0.80 o 8 2 3 39.49 44.87 0.66 o 9 2 3 294.75 284.01 3.28 o 10 2 3 56.63 51.67 0.64 o 11 2 3 217.71 220.87 2.23 o 12 2 3 0.05 0.51 0.18 o 1 3 3 242.97 234.34 1.19 o 2 3 3 684.26 683.19 4.09 o 3 3 3 213.15 211.86 1.55 o 4 3 3 412.29 396.15 5.62 o 5 3 3 35.66 40.38 0.33 o 6 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9 6 3 0.93 0.39 0.14 o 10 6 3 31.29 29.59 0.31 o 11 6 3 109.40 113.92 1.22 o 12 6 3 13.73 13.97 0.34 o 1 7 3 1357.29 1329.01 7.99 o 2 7 3 14.99 16.31 0.15 o 3 7 3 476.77 464.24 3.98 o 4 7 3 6.25 7.89 0.13 o 5 7 3 96.22 91.55 1.09 o 6 7 3 150.88 146.38 2.10 o 7 7 3 28.47 28.16 0.63 o 8 7 3 209.63 200.47 2.69 o 9 7 3 172.00 170.99 2.69 o 10 7 3 7.31 6.11 0.41 o 11 7 3 29.92 29.71 0.71 o 12 7 3 112.51 118.93 1.74 o 1 8 3 310.67 314.94 2.19 o 2 8 3 532.28 539.85 3.64 o 3 8 3 256.73 269.24 2.40 o 4 8 3 175.84 171.33 1.67 o 5 8 3 160.35 173.15 1.93 o 6 8 3 58.34 59.06 0.85 o 7 8 3 18.36 18.48 0.24 o 8 8 3 268.05 261.64 3.34 o 9 8 3 63.06 70.23 1.33 o 10 8 3 0.68 0.30 0.14 o 11 8 3 84.34 84.60 1.34 o 1 9 3 55.53 54.20 0.50 o 2 9 3 218.32 212.36 2.31 o 3 9 3 1.74 1.40 0.08 o 4 9 3 189.48 191.65 1.99 o 5 9 3 54.00 53.17 0.64 o 6 9 3 108.01 107.80 1.85 o 7 9 3 20.87 17.17 0.27 o 8 9 3 132.90 136.91 1.80 o 9 9 3 5.90 6.73 0.23 o 10 9 3 14.14 14.38 0.30 o 11 9 3 30.74 27.74 0.42 o 1 10 3 6.26 6.41 0.17 o 2 10 3 33.33 37.54 0.49 o 3 10 3 24.47 27.85 0.28 o 4 10 3 1.47 1.52 0.10 o 5 10 3 11.02 10.24 0.27 o 6 10 3 12.77 11.70 0.32 o 7 10 3 14.25 13.24 0.26 o 8 10 3 8.25 7.89 0.26 o 9 10 3 10.78 9.62 0.26 o 10 10 3 0.02 -0.11 0.19 o 11 10 3 0.14 -0.17 0.22 o 1 11 3 1.53 1.88 0.17 o 2 11 3 183.10 166.84 2.13 o 3 11 3 25.83 23.44 0.30 o 4 11 3 5.79 3.50 0.23 o 5 11 3 0.73 1.79 0.42 o 6 11 3 3.55 3.54 0.18 o 7 11 3 20.78 16.52 0.45 o 8 11 3 73.56 77.57 1.82 o 9 11 3 34.46 34.71 0.81 o 10 11 3 2.34 1.98 0.35 o 11 11 3 21.18 23.27 1.38 o 1 12 3 22.45 19.34 0.23 o 2 12 3 98.89 91.96 1.77 o 3 12 3 157.00 140.73 2.82 o 4 12 3 10.26 12.79 0.31 o 5 12 3 68.23 66.22 1.18 o 6 12 3 39.55 33.83 0.66 o 7 12 3 32.71 26.48 0.79 o 8 12 3 0.46 0.40 0.26 o 9 12 3 87.85 82.69 1.94 o 10 12 3 16.01 17.90 0.68 o 1 13 3 571.97 568.19 4.01 o 2 13 3 46.17 43.04 0.74 o 3 13 3 6.37 2.02 0.17 o 4 13 3 203.10 215.65 3.72 o 5 13 3 126.04 120.52 2.21 o 6 13 3 222.41 221.33 4.77 o 7 13 3 94.75 100.78 1.90 o 8 13 3 1.95 2.21 0.31 o 9 13 3 62.28 65.85 0.66 o 10 13 3 1.45 0.96 0.26 o 1 14 3 913.82 866.33 10.08 o 2 14 3 309.11 284.70 6.23 o 3 14 3 9.55 16.45 0.40 o 4 14 3 324.41 368.30 7.47 o 5 14 3 302.66 287.93 5.65 o 6 14 3 84.10 80.73 1.45 o 7 14 3 201.79 211.37 3.77 o 8 14 3 607.43 634.14 15.64 o 9 14 3 5.74 7.84 0.38 o 1 15 3 300.46 289.38 4.08 o 2 15 3 1.23 1.29 0.17 o 3 15 3 1.13 -0.05 0.16 o 4 15 3 457.19 475.85 6.05 o 5 15 3 65.00 57.51 0.89 o 6 15 3 143.14 141.51 1.62 o 7 15 3 58.58 64.10 0.56 o 8 15 3 139.84 153.44 2.70 o 9 15 3 33.87 38.94 0.56 o 1 16 3 1.95 3.08 0.27 o 2 16 3 0.72 0.02 0.18 o 3 16 3 41.80 39.45 0.42 o 4 16 3 26.55 26.59 0.38 o 5 16 3 9.32 9.66 0.34 o 6 16 3 3.41 2.31 0.22 o 7 16 3 11.85 9.98 0.36 o 8 16 3 14.55 15.90 0.57 o 1 17 3 0.75 0.28 0.14 o 2 17 3 19.84 17.83 0.36 o 3 17 3 6.98 5.00 0.37 o 4 17 3 1.64 0.86 0.19 o 5 17 3 3.45 2.38 0.21 o 6 17 3 8.13 8.98 0.36 o 7 17 3 1.72 0.77 0.22 o 8 17 3 34.59 39.57 0.71 o 1 18 3 6.77 6.66 0.33 o 2 18 3 21.25 20.17 0.42 o 3 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0.64 0.64 0.08 o 8 1 4 192.83 190.26 2.27 o 9 1 4 285.92 292.17 3.24 o 10 1 4 2.02 2.78 0.15 o 11 1 4 6.60 5.28 0.29 o 12 1 4 50.38 54.89 0.89 o 0 2 4 39.57 56.15 1.31 o 1 2 4 121.34 133.65 0.74 o 2 2 4 19.89 20.88 0.43 o 3 2 4 17.07 10.60 0.15 o 4 2 4 93.23 114.15 0.88 o 5 2 4 238.34 234.40 2.99 o 6 2 4 21.32 23.13 0.28 o 7 2 4 0.59 0.30 0.08 o 8 2 4 36.24 36.95 0.56 o 9 2 4 21.75 22.71 0.32 o 10 2 4 135.55 139.21 1.56 o 11 2 4 29.18 30.19 0.37 o 12 2 4 74.87 77.06 0.81 o 0 3 4 1.73 0.20 0.04 o 1 3 4 184.65 195.07 1.01 o 2 3 4 9.39 8.77 0.11 o 3 3 4 92.60 101.89 0.84 o 4 3 4 3.14 5.99 0.10 o 5 3 4 2.38 1.40 0.14 o 6 3 4 1.79 1.69 0.09 o 7 3 4 67.87 67.17 1.08 o 8 3 4 23.82 24.97 0.26 o 9 3 4 31.65 30.41 0.40 o 10 3 4 83.05 84.20 0.94 o 11 3 4 95.21 102.71 0.80 o 12 3 4 19.91 19.27 0.60 o 0 4 4 38.41 38.21 0.33 o 1 4 4 0.73 0.31 0.07 o 2 4 4 8.30 6.87 0.10 o 3 4 4 73.75 67.28 0.55 o 4 4 4 50.53 57.10 0.51 o 5 4 4 1.06 1.04 0.09 o 6 4 4 0.00 -0.06 0.07 o 7 4 4 56.59 54.53 0.81 o 8 4 4 22.83 26.08 0.21 o 9 4 4 27.95 24.99 0.40 o 10 4 4 1.48 1.40 0.14 o 11 4 4 7.69 8.47 0.33 o 0 5 4 466.09 443.54 4.47 o 1 5 4 267.60 267.56 1.69 o 2 5 4 0.02 0.11 0.04 o 3 5 4 34.89 30.97 0.28 o 4 5 4 187.96 183.19 1.78 o 5 5 4 405.36 404.24 4.08 o 6 5 4 0.20 0.05 0.08 o 7 5 4 38.61 37.89 0.50 o 8 5 4 15.33 15.02 0.29 o 9 5 4 272.31 270.85 3.24 o 10 5 4 0.30 0.01 0.14 o 11 5 4 28.06 27.60 0.38 o 0 6 4 1082.48 1073.60 10.95 o 1 6 4 128.44 124.81 1.04 o 2 6 4 20.52 21.85 0.19 o 3 6 4 1.65 1.77 0.08 o 4 6 4 506.32 498.15 3.98 o 5 6 4 85.15 84.53 1.03 o 6 6 4 8.36 8.51 0.20 o 7 6 4 62.32 63.93 0.97 o 8 6 4 44.13 43.20 0.58 o 9 6 4 128.64 127.40 1.67 o 10 6 4 0.64 0.22 0.16 o 11 6 4 34.71 34.52 0.51 o 0 7 4 1262.15 1339.43 17.05 o 1 7 4 111.60 114.27 0.91 o 2 7 4 33.12 35.17 0.26 o 3 7 4 28.65 30.12 0.29 o 4 7 4 154.59 155.89 2.13 o 5 7 4 185.87 175.37 3.83 o 6 7 4 14.79 13.17 0.21 o 7 7 4 127.54 130.53 2.06 o 8 7 4 50.99 47.21 0.72 o 9 7 4 19.32 15.86 0.32 o 10 7 4 111.73 105.11 1.62 o 11 7 4 3.98 4.50 0.23 o 0 8 4 32.86 36.96 0.73 o 1 8 4 280.18 270.18 2.27 o 2 8 4 306.53 294.50 2.59 o 3 8 4 130.68 136.04 1.32 o 4 8 4 54.14 53.26 0.65 o 5 8 4 132.58 131.39 1.48 o 6 8 4 164.29 162.65 2.71 o 7 8 4 57.95 59.55 1.11 o 8 8 4 117.85 110.74 1.20 o 9 8 4 6.73 5.43 0.37 o 10 8 4 11.64 9.57 0.30 o 11 8 4 47.59 46.04 0.79 o 0 9 4 313.36 326.04 3.50 o 1 9 4 745.42 734.20 7.11 o 2 9 4 332.27 329.20 2.95 o 3 9 4 911.23 903.36 9.72 o 4 9 4 0.62 0.20 0.08 o 5 9 4 10.90 11.14 0.20 o 6 9 4 288.02 277.20 4.50 o 7 9 4 0.45 0.43 0.14 o 8 9 4 124.18 123.46 2.07 o 9 9 4 0.18 -0.13 0.13 o 10 9 4 1.28 0.45 0.16 o 0 10 4 348.38 360.92 4.45 o 1 10 4 70.15 67.16 0.64 o 2 10 4 26.23 26.92 0.47 o 3 10 4 123.70 122.85 1.50 o 4 10 4 10.89 10.22 0.30 o 5 10 4 8.97 7.87 0.22 o 6 10 4 0.41 0.63 0.12 o 7 10 4 0.49 0.26 0.12 o 8 10 4 10.61 9.22 0.38 o 9 10 4 0.89 0.44 0.19 o 10 10 4 66.22 64.02 0.88 o 0 11 4 317.69 301.93 2.78 o 1 11 4 131.74 121.48 1.20 o 2 11 4 48.86 49.35 0.72 o 3 11 4 273.86 268.79 3.72 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28.45 0.53 o 1 11 7 15.43 14.22 0.30 o 2 11 7 41.64 36.98 0.50 o 3 11 7 12.36 12.12 0.34 o 4 11 7 0.15 -0.14 0.16 o 5 11 7 100.60 104.21 1.83 o 6 11 7 0.38 1.16 0.26 o 1 12 7 8.48 7.79 0.31 o 2 12 7 9.34 10.80 0.35 o 3 12 7 34.80 39.98 0.61 o 4 12 7 61.15 65.30 1.39 o 5 12 7 75.84 78.45 0.70 o 1 13 7 12.33 12.52 0.56 o 2 13 7 48.67 54.54 0.48 o 3 13 7 106.59 113.78 0.75 o 4 13 7 60.45 63.43 1.36 o 1 14 7 4.64 3.80 0.37 o 2 14 7 1.00 0.11 0.55 o 3 14 7 1.18 0.81 0.39 o 1 15 7 1.72 1.73 0.37 o 0 0 8 34.89 31.12 0.92 o 1 0 8 6.69 7.12 1.13 o 2 0 8 0.03 0.31 0.32 o 3 0 8 82.83 86.25 3.27 o 4 0 8 10.39 11.95 0.86 o 5 0 8 82.64 81.81 1.38 o 6 0 8 4.77 4.71 0.55 o 7 0 8 3.49 2.17 0.49 o 0 1 8 0.86 0.66 0.32 o 1 1 8 74.07 69.91 0.61 o 2 1 8 60.22 62.78 0.60 o 3 1 8 122.89 118.12 1.31 o 4 1 8 24.15 20.58 0.72 o 5 1 8 0.50 1.35 0.31 o 6 1 8 89.40 94.52 1.01 o 7 1 8 2.09 0.78 0.36 o 0 2 8 25.22 22.07 0.63 o 1 2 8 99.09 92.36 0.67 o 2 2 8 26.06 26.68 0.47 o 3 2 8 207.21 201.39 3.07 o 4 2 8 10.48 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