#------------------------------------------------------------------------------ #$Date: 2011-08-08 08:56:15 +0300 (Mon, 08 Aug 2011) $ #$Revision: 23417 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2230640.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230640_Fobs loop_ _publ_author_name 'Woli\'nska, Ewa' 'Karczmarzyk, Zbigniew' 'Rykowski, Andrzej' 'Wysocki, Waldemar' _publ_section_title ; 5,5',6,6'-Tetramethyl-3,3'-bi-1,2,4-triazine ; _journal_coeditor_code FY2014 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1613 _journal_volume 67 _journal_year 2011 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.1167 _cell_length_b 10.6662 _cell_length_c 12.7127 _exptl_crystal_F_000 456.00 _reflns_d_resolution_high 0.7822 _[local]_cod_data_source_file fy2014Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ew_1 in P b c a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 158.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 25177.38 28526.24 195.84 o 4 0 0 228.48 194.13 5.07 o 6 0 0 72.95 65.81 2.32 o 8 0 0 13.60 15.00 0.83 o 10 0 0 119.19 110.74 3.77 o 2 1 0 516.42 549.88 4.16 o 4 1 0 327.60 297.01 4.50 o 6 1 0 0.00 0.22 0.90 o 8 1 0 15.10 11.97 1.04 o 10 1 0 0.37 0.61 0.27 o 0 2 0 7557.85 5258.76 23.41 o 2 2 0 217.46 214.32 4.06 o 4 2 0 138.05 146.27 4.76 o 6 2 0 82.54 88.19 2.88 o 8 2 0 30.76 31.06 1.10 o 10 2 0 0.48 0.65 0.82 o 2 3 0 325.28 346.83 5.69 o 4 3 0 930.58 869.15 12.13 o 6 3 0 7.80 6.45 0.63 o 8 3 0 6.57 8.14 0.69 o 10 3 0 1.74 1.23 0.25 o 0 4 0 462.01 493.53 7.25 o 2 4 0 46.02 56.13 1.91 o 4 4 0 9.32 10.24 0.58 o 6 4 0 23.53 26.33 1.02 o 8 4 0 1.13 2.28 0.55 o 2 5 0 579.66 609.46 9.54 o 4 5 0 25.77 36.12 1.30 o 6 5 0 17.97 17.59 0.93 o 8 5 0 0.78 13.06 0.68 o 0 6 0 1685.56 1491.94 17.01 o 2 6 0 536.19 585.77 10.51 o 4 6 0 88.76 117.44 4.12 o 6 6 0 16.08 19.55 0.93 o 8 6 0 0.62 0.18 0.43 o 2 7 0 0.68 1.26 1.63 o 4 7 0 3.26 0.52 2.30 o 6 7 0 7.24 9.32 0.78 o 8 7 0 0.88 1.31 0.39 o 0 8 0 794.11 786.66 14.85 o 2 8 0 464.99 515.10 12.23 o 4 8 0 96.10 107.83 3.53 o 6 8 0 22.26 28.89 1.04 o 8 8 0 40.67 37.41 1.25 o 4 9 0 223.18 288.59 9.29 o 6 9 0 0.14 -1.41 1.34 o 0 10 0 1.03 0.72 0.67 o 2 10 0 0.34 1.17 0.71 o 4 10 0 0.04 -1.54 1.81 o 6 10 0 1.12 0.70 1.33 o 2 11 0 28.93 32.63 1.08 o 4 11 0 12.89 12.34 0.67 o 6 11 0 1.74 1.09 0.25 o 0 12 0 5.99 6.97 0.64 o 4 12 0 4.47 4.08 0.41 o 2 13 0 0.19 0.51 0.95 o 1 1 1 2234.25 2239.51 10.46 o 2 1 1 1062.35 1147.39 11.78 o 3 1 1 2.88 2.50 0.19 o 4 1 1 145.85 124.36 2.07 o 5 1 1 154.33 157.07 4.78 o 6 1 1 5.50 6.10 0.30 o 7 1 1 12.09 12.18 0.40 o 8 1 1 35.68 37.69 0.74 o 9 1 1 11.03 12.06 0.33 o 10 1 1 3.14 2.75 0.16 o 0 2 1 208.51 160.51 58.61 o 1 2 1 40.65 37.43 9.39 o 2 2 1 692.31 669.95 24.55 o 3 2 1 62.17 72.29 1.76 o 4 2 1 519.06 521.43 20.92 o 5 2 1 5.22 4.82 0.42 o 6 2 1 168.91 185.91 4.34 o 7 2 1 42.66 42.87 3.71 o 8 2 1 6.33 6.29 0.68 o 9 2 1 12.10 13.64 0.95 o 10 2 1 6.08 5.44 0.37 o 1 3 1 114.45 97.04 21.08 o 2 3 1 671.84 623.46 86.15 o 3 3 1 307.88 299.21 4.37 o 4 3 1 1.50 2.14 0.29 o 5 3 1 361.21 427.91 6.86 o 6 3 1 0.64 1.19 0.79 o 7 3 1 68.70 74.77 3.63 o 8 3 1 22.48 24.37 1.47 o 9 3 1 1.94 1.03 0.30 o 10 3 1 0.91 0.90 0.49 o 0 4 1 339.96 315.19 117.19 o 1 4 1 40.10 37.25 6.79 o 2 4 1 68.40 64.48 9.91 o 3 4 1 110.00 114.60 4.66 o 4 4 1 0.12 0.92 0.40 o 5 4 1 26.29 32.40 0.74 o 6 4 1 1.30 0.91 1.17 o 7 4 1 1.62 2.08 0.40 o 8 4 1 0.53 0.34 0.48 o 9 4 1 0.03 0.71 0.33 o 1 5 1 1009.42 1170.87 200.24 o 2 5 1 108.75 88.27 20.59 o 3 5 1 197.80 215.03 6.20 o 4 5 1 39.32 43.19 3.49 o 5 5 1 12.74 13.87 0.83 o 6 5 1 1.76 1.70 0.45 o 7 5 1 3.79 13.40 6.69 o 8 5 1 4.67 4.87 0.44 o 9 5 1 2.50 2.76 0.26 o 0 6 1 66.75 61.14 18.51 o 1 6 1 206.28 243.39 42.11 o 2 6 1 127.58 92.75 45.23 o 3 6 1 395.85 435.40 70.28 o 4 6 1 108.71 122.34 2.96 o 5 6 1 26.85 35.94 0.85 o 6 6 1 38.24 42.49 2.10 o 7 6 1 13.85 16.13 0.59 o 8 6 1 7.68 8.43 0.41 o 9 6 1 6.71 6.99 0.26 o 1 7 1 234.29 269.96 46.60 o 2 7 1 198.39 144.16 66.69 o 3 7 1 70.66 66.33 19.46 o 4 7 1 1.23 1.55 1.44 o 5 7 1 9.93 10.21 1.54 o 6 7 1 2.67 2.30 0.64 o 7 7 1 0.00 0.86 1.25 o 8 7 1 33.79 36.59 0.86 o 0 8 1 85.47 89.45 19.41 o 1 8 1 174.70 187.35 30.96 o 2 8 1 30.84 34.00 1.17 o 3 8 1 367.70 347.69 52.31 o 4 8 1 54.28 66.40 9.80 o 5 8 1 26.55 31.86 1.19 o 6 8 1 33.62 41.61 1.50 o 7 8 1 21.90 27.20 1.11 o 8 8 1 10.02 10.18 0.63 o 1 9 1 379.63 415.14 68.20 o 2 9 1 2.84 1.07 0.80 o 3 9 1 54.22 63.72 19.84 o 4 9 1 14.17 18.27 2.57 o 5 9 1 0.07 0.06 0.63 o 6 9 1 0.92 0.36 1.07 o 7 9 1 0.79 0.72 0.34 o 0 10 1 1.52 1.60 0.65 o 1 10 1 0.53 -0.42 1.00 o 2 10 1 1.80 4.14 1.75 o 3 10 1 1.63 0.84 0.62 o 4 10 1 19.42 21.69 4.57 o 5 10 1 3.18 4.37 1.85 o 6 10 1 11.08 11.67 1.74 o 7 10 1 1.51 1.09 0.19 o 1 11 1 18.48 29.09 6.57 o 2 11 1 2.04 1.36 0.75 o 3 11 1 1.83 0.10 1.32 o 4 11 1 7.59 8.66 1.94 o 5 11 1 18.37 19.62 5.08 o 6 11 1 3.21 3.20 0.57 o 0 12 1 3.13 3.78 0.74 o 1 12 1 0.09 -0.17 1.39 o 2 12 1 5.90 2.11 0.64 o 3 12 1 0.26 -1.27 0.94 o 4 12 1 0.58 0.30 0.81 o 1 13 1 2.30 3.13 0.82 o 2 13 1 0.30 -0.75 0.70 o 3 13 1 0.83 0.77 0.50 o 0 0 2 6921.82 6675.89 65.13 o 1 0 2 3342.33 3954.13 71.59 o 2 0 2 12636.84 15112.96 132.27 o 3 0 2 4234.29 4421.05 24.08 o 4 0 2 38.96 67.14 2.26 o 5 0 2 302.36 331.26 8.15 o 6 0 2 9.50 13.46 0.75 o 7 0 2 46.05 51.80 1.89 o 8 0 2 23.13 29.03 1.04 o 9 0 2 23.36 24.97 0.89 o 10 0 2 2.96 3.46 0.33 o 1 1 2 8622.21 9630.47 510.31 o 2 1 2 5514.01 6299.94 94.09 o 3 1 2 461.59 519.97 5.27 o 4 1 2 243.13 202.75 6.04 o 5 1 2 7.23 9.34 0.43 o 6 1 2 43.05 38.65 0.95 o 7 1 2 0.65 0.02 1.23 o 8 1 2 21.14 26.32 0.74 o 9 1 2 39.76 41.50 1.47 o 10 1 2 3.66 3.10 0.22 o 0 2 2 50.34 52.54 1.99 o 1 2 2 19.12 16.77 1.36 o 2 2 2 1441.29 1478.06 12.24 o 3 2 2 5.04 7.24 0.45 o 4 2 2 69.86 61.91 2.10 o 5 2 2 18.12 19.74 0.76 o 6 2 2 100.11 118.91 3.80 o 7 2 2 1.18 1.48 0.57 o 8 2 2 3.70 3.08 0.59 o 9 2 2 0.44 0.00 1.30 o 10 2 2 8.03 5.42 0.32 o 1 3 2 1248.59 1204.28 492.10 o 2 3 2 1432.42 936.72 14.18 o 3 3 2 93.76 80.03 2.61 o 4 3 2 12.19 17.57 0.66 o 5 3 2 6.87 5.96 0.59 o 6 3 2 20.99 21.33 0.92 o 7 3 2 0.19 -0.82 1.72 o 8 3 2 7.62 9.95 0.69 o 9 3 2 0.57 0.30 1.22 o 10 3 2 0.95 0.57 0.21 o 0 4 2 112.47 73.09 2.76 o 1 4 2 48.54 40.39 22.02 o 2 4 2 191.81 80.24 2.70 o 3 4 2 199.78 169.20 5.59 o 4 4 2 12.54 21.13 0.81 o 5 4 2 7.06 8.14 0.65 o 6 4 2 0.86 0.80 1.72 o 7 4 2 3.75 1.62 2.24 o 8 4 2 2.54 12.89 0.71 o 9 4 2 2.29 2.15 0.39 o 1 5 2 1725.43 1983.45 1046.25 o 2 5 2 1.61 -0.44 1.25 o 3 5 2 212.20 172.73 5.59 o 4 5 2 73.34 65.10 2.35 o 5 5 2 1.24 0.65 0.53 o 6 5 2 3.43 3.04 0.63 o 7 5 2 0.40 -0.26 2.06 o 8 5 2 0.04 0.78 1.37 o 9 5 2 2.29 2.20 0.36 o 0 6 2 25.00 13.13 0.91 o 1 6 2 23.53 31.57 15.61 o 2 6 2 103.12 24.77 2.03 o 3 6 2 43.62 33.04 1.34 o 4 6 2 19.70 20.96 0.98 o 5 6 2 16.76 20.08 1.00 o 6 6 2 0.97 -1.37 2.00 o 7 6 2 0.00 0.47 1.34 o 8 6 2 10.21 12.02 0.64 o 9 6 2 2.12 2.02 0.29 o 1 7 2 7.04 7.46 5.24 o 2 7 2 4.02 0.22 2.20 o 3 7 2 1.63 -1.47 1.47 o 4 7 2 0.78 0.54 2.06 o 5 7 2 1.61 1.81 0.59 o 6 7 2 4.34 6.74 0.73 o 7 7 2 10.80 9.85 0.71 o 8 7 2 2.13 2.06 0.40 o 0 8 2 4.57 1.67 0.70 o 1 8 2 58.63 64.61 34.12 o 2 8 2 22.91 -0.50 3.63 o 3 8 2 135.11 48.33 2.61 o 4 8 2 68.71 55.26 2.19 o 5 8 2 3.33 0.00 1.78 o 6 8 2 58.42 68.12 2.41 o 7 8 2 14.79 15.50 0.72 o 8 8 2 9.24 8.52 0.39 o 1 9 2 634.42 497.02 293.66 o 2 9 2 41.63 6.82 1.63 o 3 9 2 76.09 32.60 2.08 o 4 9 2 21.48 18.37 1.17 o 5 9 2 5.75 5.89 0.70 o 6 9 2 0.20 -0.16 1.51 o 7 9 2 0.05 -0.26 0.33 o 0 10 2 121.54 83.69 3.05 o 1 10 2 10.60 10.95 5.56 o 2 10 2 21.64 -1.28 3.95 o 3 10 2 32.08 9.96 1.38 o 4 10 2 0.57 -0.21 1.80 o 5 10 2 3.50 3.06 0.54 o 6 10 2 5.07 5.04 0.46 o 1 11 2 2.09 0.33 1.10 o 2 11 2 6.67 -1.25 2.19 o 4 11 2 8.46 1.18 1.78 o 5 11 2 1.02 0.00 1.22 o 1 12 2 1.14 1.21 0.37 o 2 12 2 0.09 0.28 1.46 o 3 12 2 2.69 0.91 1.48 o 4 12 2 1.91 -0.69 1.20 o 1 13 2 12.76 12.62 4.21 o 2 13 2 0.25 -0.81 0.95 o 1 1 3 2259.25 2203.93 180.96 o 2 1 3 922.43 944.74 31.81 o 3 1 3 1282.19 1233.36 13.84 o 4 1 3 392.79 346.16 5.25 o 5 1 3 496.54 538.66 11.94 o 6 1 3 10.24 11.54 0.51 o 7 1 3 105.71 102.36 5.02 o 8 1 3 31.22 33.50 0.81 o 9 1 3 5.51 5.62 0.36 o 10 1 3 3.97 4.80 1.11 o 0 2 3 396.01 383.53 5.35 o 1 2 3 556.41 569.84 4.83 o 2 2 3 32.40 33.33 1.16 o 3 2 3 922.17 887.18 10.85 o 4 2 3 363.59 355.67 7.83 o 5 2 3 8.18 8.10 0.61 o 6 2 3 108.22 109.05 4.17 o 7 2 3 72.68 80.65 2.86 o 8 2 3 0.06 0.24 1.77 o 9 2 3 24.56 21.95 0.81 o 10 2 3 2.61 2.24 0.24 o 1 3 3 180.48 203.40 3.18 o 2 3 3 74.73 82.26 2.86 o 3 3 3 4.13 4.14 0.43 o 4 3 3 157.33 156.50 5.13 o 5 3 3 0.65 0.00 1.55 o 6 3 3 14.41 15.88 0.85 o 7 3 3 0.54 -0.81 1.87 o 8 3 3 4.85 6.60 0.63 o 9 3 3 8.08 6.56 0.49 o 0 4 3 2713.17 3051.62 20.35 o 1 4 3 45.77 53.03 1.26 o 2 4 3 317.39 331.13 6.81 o 3 4 3 58.31 55.67 2.00 o 4 4 3 35.98 44.71 1.63 o 5 4 3 0.48 0.00 1.72 o 6 4 3 0.93 -0.53 1.92 o 7 4 3 4.33 4.19 0.63 o 8 4 3 0.27 0.41 1.26 o 9 4 3 0.00 -0.59 0.99 o 1 5 3 700.99 901.43 20.53 o 2 5 3 142.52 158.97 5.26 o 3 5 3 70.98 69.18 2.35 o 4 5 3 2.05 0.88 0.49 o 5 5 3 0.01 0.25 1.82 o 6 5 3 18.45 18.36 0.92 o 7 5 3 0.34 0.98 1.31 o 8 5 3 1.21 1.51 0.46 o 9 5 3 7.25 8.26 0.42 o 0 6 3 204.30 202.33 6.11 o 1 6 3 4.01 3.19 1.20 o 2 6 3 7.03 5.93 0.59 o 3 6 3 29.43 36.05 1.19 o 4 6 3 95.85 96.54 3.19 o 5 6 3 17.44 21.18 0.97 o 6 6 3 58.44 63.83 2.09 o 7 6 3 19.09 20.26 0.83 o 8 6 3 0.51 0.83 0.39 o 9 6 3 4.13 2.87 0.27 o 1 7 3 74.60 94.53 2.24 o 2 7 3 1.69 -0.45 1.85 o 3 7 3 203.28 223.19 7.62 o 4 7 3 30.71 42.87 1.35 o 5 7 3 439.99 455.13 11.81 o 6 7 3 58.22 62.86 2.01 o 7 7 3 134.51 148.82 4.91 o 8 7 3 20.57 20.59 0.77 o 0 8 3 0.01 1.22 1.88 o 1 8 3 15.21 16.03 0.63 o 2 8 3 9.04 14.46 0.88 o 3 8 3 61.26 72.48 2.43 o 4 8 3 80.46 91.39 2.86 o 5 8 3 12.92 16.97 0.89 o 6 8 3 78.49 96.74 3.14 o 7 8 3 4.58 4.86 0.48 o 8 8 3 3.19 3.26 0.28 o 1 9 3 323.11 437.12 8.08 o 2 9 3 21.73 30.14 1.15 o 3 9 3 56.74 72.94 2.64 o 4 9 3 0.03 -1.22 1.77 o 5 9 3 0.95 1.68 0.53 o 6 9 3 10.18 11.23 0.63 o 7 9 3 0.37 0.17 1.00 o 0 10 3 73.54 126.60 4.34 o 1 10 3 19.17 23.10 0.72 o 2 10 3 0.00 -2.23 2.11 o 3 10 3 58.89 70.65 2.58 o 4 10 3 4.87 5.59 0.61 o 5 10 3 2.38 3.79 0.50 o 6 10 3 1.66 1.83 0.37 o 1 11 3 0.12 0.49 0.40 o 2 11 3 8.83 9.36 0.74 o 3 11 3 2.16 3.88 0.54 o 4 11 3 0.01 -0.68 1.44 o 5 11 3 3.18 4.12 0.39 o 0 12 3 10.67 12.93 0.67 o 1 12 3 1.26 2.20 0.79 o 2 12 3 0.03 -0.64 1.48 o 3 12 3 6.46 9.87 0.50 o 4 12 3 1.65 0.59 0.98 o 1 13 3 9.22 13.47 0.33 o 2 13 3 3.19 4.95 0.30 o 0 0 4 81.63 69.15 2.41 o 1 0 4 4.51 4.37 0.28 o 2 0 4 1149.50 1091.47 10.89 o 3 0 4 195.62 176.61 4.88 o 4 0 4 111.42 98.04 3.18 o 5 0 4 37.13 47.95 1.53 o 6 0 4 57.21 66.35 2.22 o 7 0 4 11.09 10.80 0.76 o 8 0 4 14.64 14.11 0.79 o 9 0 4 1.13 1.00 0.39 o 10 0 4 6.71 4.01 0.26 o 1 1 4 14.88 15.54 1.63 o 2 1 4 3191.74 3002.30 152.89 o 3 1 4 114.96 90.82 2.16 o 4 1 4 2549.20 2648.96 78.94 o 5 1 4 80.86 105.55 2.37 o 6 1 4 9.61 9.52 0.67 o 7 1 4 56.14 59.54 1.44 o 8 1 4 32.22 39.65 2.88 o 9 1 4 2.77 3.00 0.32 o 10 1 4 1.35 1.28 0.14 o 0 2 4 2861.41 3118.01 18.61 o 1 2 4 116.48 109.37 5.79 o 2 2 4 124.94 146.97 4.20 o 3 2 4 8.98 10.03 0.51 o 4 2 4 129.53 142.83 4.78 o 5 2 4 2.96 3.10 0.52 o 6 2 4 83.72 83.10 2.73 o 7 2 4 30.57 31.75 1.11 o 8 2 4 60.11 56.12 2.05 o 9 2 4 8.53 9.53 0.54 o 1 3 4 0.19 2.30 0.66 o 2 3 4 117.40 116.96 3.90 o 3 3 4 22.49 22.59 0.80 o 4 3 4 104.69 118.60 3.89 o 5 3 4 7.75 8.83 0.67 o 6 3 4 0.01 1.05 1.31 o 7 3 4 3.28 4.12 0.62 o 8 3 4 12.58 12.04 0.69 o 9 3 4 3.57 3.37 0.40 o 0 4 4 430.45 386.33 8.04 o 1 4 4 154.63 165.01 28.81 o 2 4 4 4.36 5.29 0.53 o 3 4 4 105.94 94.42 3.36 o 4 4 4 3.38 2.83 0.52 o 5 4 4 14.82 13.82 0.77 o 6 4 4 2.56 -0.80 2.02 o 7 4 4 5.94 7.16 0.69 o 8 4 4 10.33 12.96 0.67 o 9 4 4 6.56 6.12 0.42 o 1 5 4 616.82 651.54 7.47 o 2 5 4 10.63 14.60 0.66 o 3 5 4 41.92 61.68 2.09 o 4 5 4 121.93 117.51 4.02 o 5 5 4 14.43 13.20 0.82 o 6 5 4 0.24 0.40 0.53 o 7 5 4 0.05 0.71 1.58 o 8 5 4 1.61 1.89 0.45 o 9 5 4 1.85 1.94 0.29 o 0 6 4 40.65 41.09 1.49 o 1 6 4 2.64 4.84 0.81 o 2 6 4 36.06 43.60 1.38 o 3 6 4 0.01 -2.04 1.71 o 4 6 4 17.63 18.75 0.93 o 5 6 4 8.57 8.35 0.75 o 6 6 4 49.09 50.64 1.69 o 7 6 4 7.33 7.98 0.62 o 8 6 4 3.20 2.38 0.40 o 1 7 4 12.38 15.56 0.63 o 2 7 4 0.22 1.06 0.56 o 3 7 4 14.79 18.59 0.92 o 4 7 4 29.11 40.13 1.26 o 5 7 4 63.75 74.91 2.46 o 6 7 4 9.56 10.36 0.79 o 7 7 4 8.60 10.08 0.64 o 8 7 4 0.72 0.38 0.31 o 0 8 4 419.53 435.88 11.12 o 1 8 4 0.11 0.12 1.32 o 2 8 4 78.89 86.51 2.50 o 3 8 4 3.29 3.20 1.79 o 4 8 4 35.71 47.42 1.61 o 5 8 4 0.10 -0.95 1.69 o 6 8 4 26.68 32.73 1.01 o 7 8 4 1.04 1.26 0.39 o 8 8 4 0.24 0.02 0.19 o 1 9 4 43.69 54.11 1.47 o 2 9 4 36.67 47.03 1.62 o 3 9 4 19.74 28.69 1.09 o 4 9 4 21.06 26.66 0.98 o 5 9 4 10.96 13.34 0.71 o 6 9 4 1.03 -0.27 1.32 o 7 9 4 1.23 0.56 0.94 o 0 10 4 287.57 299.09 9.28 o 1 10 4 3.88 5.64 0.67 o 2 10 4 121.92 133.62 4.23 o 3 10 4 14.90 19.35 0.88 o 4 10 4 0.90 0.69 0.51 o 5 10 4 2.59 3.75 0.48 o 6 10 4 4.43 4.83 0.37 o 1 11 4 6.01 6.67 0.58 o 2 11 4 6.99 10.00 0.67 o 3 11 4 4.68 5.87 0.55 o 4 11 4 0.45 0.40 0.38 o 5 11 4 3.41 4.16 0.34 o 0 12 4 0.04 0.40 0.43 o 1 12 4 1.25 1.42 0.57 o 2 12 4 2.64 2.50 0.43 o 3 12 4 3.56 5.26 0.41 o 4 12 4 0.23 0.20 0.25 o 1 13 4 5.31 7.31 0.23 o 1 1 5 309.23 241.11 20.96 o 2 1 5 1.45 0.33 0.81 o 3 1 5 443.21 452.18 6.52 o 4 1 5 0.05 -2.06 1.03 o 5 1 5 380.67 385.93 10.52 o 6 1 5 26.94 26.12 0.72 o 7 1 5 95.75 107.58 2.45 o 8 1 5 10.11 9.60 0.48 o 9 1 5 5.84 6.04 0.33 o 0 2 5 193.18 186.47 4.65 o 1 2 5 290.52 266.15 4.04 o 2 2 5 45.54 47.74 1.63 o 3 2 5 364.23 340.47 7.56 o 4 2 5 461.26 480.96 10.08 o 5 2 5 0.60 0.95 0.52 o 6 2 5 262.55 251.05 8.53 o 7 2 5 51.63 55.99 2.08 o 8 2 5 11.73 10.62 0.70 o 9 2 5 21.85 19.74 0.66 o 1 3 5 43.76 40.58 0.70 o 2 3 5 17.35 12.30 0.57 o 3 3 5 3.91 5.11 0.48 o 4 3 5 1.18 1.03 1.70 o 5 3 5 1.21 0.78 0.54 o 6 3 5 46.03 47.37 1.74 o 7 3 5 0.56 1.88 0.56 o 8 3 5 3.40 2.26 0.52 o 9 3 5 1.67 2.28 0.34 o 0 4 5 1573.94 1437.37 17.27 o 1 4 5 63.55 83.12 7.70 o 2 4 5 1284.85 1179.63 16.96 o 3 4 5 155.76 166.58 5.66 o 4 4 5 30.48 29.30 1.09 o 5 4 5 27.65 25.70 1.12 o 6 4 5 0.97 1.74 0.58 o 7 4 5 3.77 0.49 1.92 o 8 4 5 28.41 27.01 1.10 o 9 4 5 3.22 3.99 0.34 o 1 5 5 72.09 76.59 12.21 o 2 5 5 0.41 0.77 1.82 o 3 5 5 1.21 1.30 1.61 o 4 5 5 63.91 54.54 2.04 o 5 5 5 2.35 2.54 0.61 o 6 5 5 15.95 14.33 0.89 o 7 5 5 1.17 1.09 0.52 o 8 5 5 0.75 0.14 1.19 o 9 5 5 2.33 1.83 0.26 o 0 6 5 24.16 23.45 1.08 o 1 6 5 41.60 42.50 13.72 o 2 6 5 1.12 0.67 1.71 o 3 6 5 67.77 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20.30 23.05 0.99 o 3 0 12 13.22 12.18 0.75 o 4 0 12 0.58 0.00 1.48 o 5 0 12 1.36 -0.18 1.31 o 6 0 12 11.00 10.63 0.51 o 1 1 12 4.24 3.94 0.32 o 2 1 12 0.59 0.58 0.51 o 3 1 12 41.81 37.88 0.94 o 4 1 12 13.95 12.69 0.52 o 5 1 12 15.65 15.80 1.31 o 6 1 12 2.93 4.03 0.28 o 0 2 12 182.17 170.61 5.54 o 1 2 12 49.95 48.48 1.94 o 2 2 12 24.10 22.55 0.95 o 3 2 12 26.34 24.64 0.95 o 4 2 12 6.23 6.49 0.60 o 5 2 12 0.42 0.53 0.41 o 6 2 12 3.03 2.68 0.37 o 1 3 12 51.64 52.30 3.48 o 2 3 12 4.62 4.37 0.59 o 3 3 12 0.02 -0.02 0.45 o 4 3 12 6.61 7.34 0.57 o 5 3 12 0.75 -0.14 1.13 o 6 3 12 0.09 -0.08 0.85 o 0 4 12 96.69 102.38 3.21 o 1 4 12 36.46 37.21 0.90 o 2 4 12 20.44 23.12 0.90 o 3 4 12 22.62 20.93 0.83 o 4 4 12 1.55 0.17 1.28 o 5 4 12 0.67 -1.33 1.14 o 6 4 12 0.10 -0.19 0.74 o 1 5 12 87.62 89.94 2.15 o 2 5 12 11.70 11.42 0.70 o 3 5 12 8.61 8.74 0.61 o 4 5 12 29.53 31.34 1.17 o 5 5 12 8.73 8.79 0.44 o 0 6 12 1.37 1.11 0.44 o 1 6 12 0.01 -0.26 0.88 o 2 6 12 1.54 1.48 0.44 o 3 6 12 6.66 8.06 0.50 o 4 6 12 0.39 0.00 0.94 o 5 6 12 0.01 -0.45 0.66 o 1 7 12 3.63 3.70 0.32 o 2 7 12 4.97 4.43 0.44 o 3 7 12 5.18 5.30 0.42 o 4 7 12 7.76 7.42 0.37 o 0 8 12 2.95 3.67 0.40 o 1 8 12 0.18 0.14 0.69 o 2 8 12 2.32 2.58 0.32 o 3 8 12 0.37 -0.65 0.69 o 1 9 12 6.72 5.20 0.37 o 1 1 13 34.29 31.55 1.24 o 2 1 13 11.07 9.38 0.51 o 3 1 13 2.98 2.62 0.43 o 4 1 13 1.88 1.72 1.10 o 5 1 13 3.50 4.16 0.29 o 6 1 13 0.00 0.42 0.49 o 0 2 13 8.12 7.02 0.62 o 1 2 13 0.30 -0.07 1.31 o 2 2 13 3.97 1.22 1.77 o 3 2 13 0.34 -1.44 1.50 o 4 2 13 19.70 21.22 0.75 o 5 2 13 2.20 0.20 0.99 o 6 2 13 10.99 8.99 0.39 o 1 3 13 1.07 1.99 0.83 o 2 3 13 1.62 0.76 1.48 o 3 3 13 8.85 9.61 0.58 o 4 3 13 2.88 2.96 0.39 o 5 3 13 3.17 3.77 0.33 o 0 4 13 196.30 188.85 6.38 o 1 4 13 34.13 34.25 0.82 o 2 4 13 152.40 162.52 5.47 o 3 4 13 68.51 68.56 2.34 o 4 4 13 9.92 11.02 0.49 o 5 4 13 12.35 12.70 0.44 o 1 5 13 17.88 17.05 0.60 o 2 5 13 2.83 2.46 0.43 o 3 5 13 3.39 3.13 0.40 o 4 5 13 14.71 12.47 0.51 o 0 6 13 0.10 -0.39 0.99 o 1 6 13 4.93 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