#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/06/2230666.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230666_Fobs loop_ _publ_author_name 'Danish, Muhammad' 'Tahir, M. Nawaz' 'Ghafoor, Sabiha' 'Ahmad, Nazir' 'Nisa, Mehwish' _publ_section_title ; catena-Poly[bis(\m~3~-2-methyl-3,5-dinitrobenzoato)disilver(I)] ; _journal_coeditor_code HB5898 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m938 _journal_page_last m939 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.493 _cell_angle_gamma 90.000 _cell_length_a 5.7073 _cell_length_b 11.9204 _cell_length_c 14.5117 _exptl_crystal_F_000 648.00 _reflns_d_resolution_high 0.7492 _[local]_cod_data_source_file hb5898Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' DANISHAG3N_0m in P2(1)/n collected on' _shelx_refln_list_code 4 _shelx_f_calc_maximum 200.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13460.60 12818.76 253.41 o 4 0 0 699.23 710.10 22.87 o 6 0 0 76.57 81.07 14.87 o 1 1 0 519.93 546.89 9.53 o 2 1 0 124.28 122.83 6.68 o 3 1 0 2700.83 2455.10 35.64 o 4 1 0 73.05 81.52 7.95 o 5 1 0 4314.53 4378.04 67.20 o 6 1 0 24.89 18.66 8.60 o 7 1 0 1213.74 1279.67 86.98 o 0 2 0 35165.92 34792.35 551.05 o 1 2 0 2.12 -2.13 2.13 o 2 2 0 9966.80 10080.12 117.88 o 3 2 0 1811.27 1998.06 34.37 o 4 2 0 1602.49 1616.75 35.58 o 5 2 0 171.09 157.57 19.77 o 6 2 0 174.26 167.12 17.00 o 7 2 0 129.26 124.63 24.77 o 1 3 0 5.09 2.77 2.62 o 2 3 0 5093.22 5679.23 70.17 o 3 3 0 354.14 281.11 13.03 o 4 3 0 1425.76 1373.57 33.36 o 5 3 0 3610.58 3686.38 87.51 o 6 3 0 455.38 497.07 50.13 o 7 3 0 443.76 467.98 45.07 o 0 4 0 33310.35 33589.28 474.07 o 1 4 0 11432.20 11648.60 122.03 o 2 4 0 10776.32 11324.73 166.07 o 3 4 0 2414.61 2488.97 40.21 o 4 4 0 791.67 740.55 29.21 o 5 4 0 32.15 15.61 14.56 o 6 4 0 3.36 -0.62 14.90 o 7 4 0 102.65 101.94 52.75 o 1 5 0 84.12 109.08 9.78 o 2 5 0 2232.28 2294.18 33.45 o 3 5 0 1802.61 1847.86 35.21 o 4 5 0 1239.86 1185.78 26.49 o 5 5 0 1412.32 1486.76 64.15 o 6 5 0 792.32 788.12 56.23 o 7 5 0 136.69 150.97 43.49 o 0 6 0 896.86 996.29 39.88 o 1 6 0 1343.60 1292.59 33.40 o 2 6 0 950.46 898.37 23.43 o 3 6 0 2626.31 2581.84 53.96 o 4 6 0 88.68 115.72 13.93 o 5 6 0 20.20 62.71 25.37 o 6 6 0 1.02 37.27 50.13 o 7 6 0 26.30 26.85 24.27 o 1 7 0 26.73 31.58 10.18 o 2 7 0 898.60 948.11 59.06 o 3 7 0 45.60 60.10 14.05 o 4 7 0 1335.04 1298.75 161.47 o 5 7 0 115.34 125.20 26.90 o 6 7 0 817.84 832.12 63.45 o 0 8 0 722.27 728.15 40.44 o 1 8 0 3800.58 3771.39 147.21 o 2 8 0 20.93 18.75 9.62 o 3 8 0 1634.33 1639.61 87.88 o 4 8 0 18.87 3.78 15.82 o 5 8 0 89.92 73.31 28.59 o 6 8 0 7.99 -9.25 20.64 o 1 9 0 0.17 -7.68 7.68 o 2 9 0 1027.76 1069.37 56.31 o 3 9 0 75.94 65.21 55.57 o 4 9 0 1042.83 1039.21 107.51 o 5 9 0 5.29 31.62 22.59 o 6 9 0 313.25 364.72 102.08 o 0 10 0 35.30 53.90 16.97 o 1 10 0 35.81 43.62 11.26 o 2 10 0 136.94 139.43 19.36 o 3 10 0 441.78 419.89 45.33 o 4 10 0 91.19 60.16 23.96 o 5 10 0 15.30 26.64 23.17 o 1 11 0 65.05 57.52 12.09 o 2 11 0 59.58 66.57 27.03 o 3 11 0 134.81 154.25 31.59 o 4 11 0 260.84 279.77 84.36 o 5 11 0 40.00 82.20 29.99 o 0 12 0 1795.25 1886.83 81.07 o 1 12 0 162.61 202.88 43.18 o 2 12 0 68.85 40.20 18.62 o 3 12 0 54.22 52.00 26.04 o 4 12 0 16.32 29.58 24.27 o 1 13 0 0.02 10.87 12.25 o 2 13 0 146.60 100.31 27.89 o 3 13 0 7.89 -12.40 19.07 o 4 13 0 78.97 71.75 30.84 o 0 14 0 107.84 134.71 31.35 o 1 14 0 16.60 10.30 22.25 o 2 14 0 49.58 29.44 23.91 o 3 14 0 17.98 37.48 26.50 o 1 15 0 0.04 -2.62 18.79 o 2 15 0 9.16 22.60 22.14 o -5 0 1 6169.63 6055.76 134.87 o -3 0 1 1561.47 1509.88 46.91 o -1 0 1 810.68 846.05 20.94 o 1 0 1 12254.84 12259.52 151.22 o 3 0 1 11361.15 11500.97 166.64 o 5 0 1 8114.96 7965.15 146.60 o -7 1 1 48.13 53.15 30.20 o -6 1 1 58.81 47.91 9.17 o -5 1 1 42.63 32.88 6.97 o -4 1 1 4207.85 4262.04 81.19 o -3 1 1 139.75 162.28 8.90 o -2 1 1 21242.26 21385.14 292.55 o -1 1 1 93.47 72.20 3.88 o 0 1 1 17419.09 16469.68 613.72 o 1 1 1 6314.01 6591.34 62.31 o 2 1 1 8234.48 8158.07 89.28 o 3 1 1 126.87 132.25 9.63 o 4 1 1 2.57 0.48 4.25 o 5 1 1 356.74 404.98 16.59 o 6 1 1 6.84 20.75 8.34 o 7 1 1 8.46 32.62 29.80 o -7 2 1 1727.97 1672.50 70.74 o -6 2 1 585.93 607.89 48.34 o -5 2 1 3315.38 3348.11 89.49 o -4 2 1 188.71 195.96 12.37 o -3 2 1 54.07 45.34 5.76 o -2 2 1 0.25 -2.07 3.67 o -1 2 1 973.26 978.81 15.25 o 0 2 1 539.55 534.76 8.48 o 1 2 1 907.84 952.86 13.37 o 2 2 1 1121.07 1085.23 19.44 o 3 2 1 11848.70 12380.34 161.48 o 4 2 1 1583.63 1640.57 37.38 o 5 2 1 4116.84 4017.88 87.01 o 6 2 1 100.07 117.13 15.78 o 7 2 1 875.93 1008.87 58.34 o -7 3 1 22.02 29.04 21.95 o -6 3 1 55.69 61.78 18.08 o -5 3 1 268.38 307.02 38.39 o -4 3 1 2047.50 2167.48 42.24 o -3 3 1 2431.65 2344.64 41.70 o -2 3 1 3256.14 3196.36 46.97 o -1 3 1 2187.79 2116.16 27.17 o 0 3 1 34882.78 36212.57 407.21 o 1 3 1 2702.95 2693.71 35.12 o 2 3 1 2601.48 2623.99 32.07 o 3 3 1 1478.64 1571.16 41.09 o 4 3 1 6.72 6.13 7.04 o 5 3 1 97.41 75.19 15.54 o 6 3 1 158.45 137.88 20.56 o 7 3 1 67.90 86.35 25.91 o -7 4 1 836.24 903.58 88.99 o -6 4 1 639.29 613.69 46.24 o -5 4 1 2063.14 2007.14 54.35 o -4 4 1 2136.82 2145.74 68.35 o -3 4 1 490.74 473.85 13.97 o -2 4 1 142.56 139.89 13.42 o -1 4 1 843.72 816.85 15.71 o 0 4 1 1469.19 1575.81 23.79 o 1 4 1 4555.55 4491.47 52.12 o 2 4 1 2873.46 2874.62 44.74 o 3 4 1 3965.13 4083.31 61.32 o 4 4 1 3347.26 3225.76 51.21 o 5 4 1 1419.55 1438.06 60.76 o 6 4 1 775.89 687.39 42.45 o 7 4 1 592.46 597.55 76.10 o -7 5 1 5.11 -13.29 31.01 o -6 5 1 21.02 38.88 18.28 o -5 5 1 340.83 325.83 35.84 o -4 5 1 237.56 263.72 20.40 o -3 5 1 2492.56 2412.56 47.78 o -2 5 1 3811.72 3680.71 62.64 o -1 5 1 9604.23 9857.13 153.93 o 0 5 1 10185.64 10247.72 160.98 o 1 5 1 1806.83 1747.15 28.51 o 2 5 1 792.84 742.64 13.92 o 3 5 1 1231.51 1266.09 33.03 o 4 5 1 3.01 8.47 6.85 o 5 5 1 25.41 18.56 16.05 o 6 5 1 13.75 27.80 22.35 o 7 5 1 269.63 252.64 65.63 o -7 6 1 197.76 276.63 60.00 o -6 6 1 598.00 678.92 72.28 o -5 6 1 283.41 328.39 36.13 o -4 6 1 830.23 839.78 30.61 o -3 6 1 9.35 6.14 9.19 o -2 6 1 129.63 142.60 9.38 o -1 6 1 5.86 1.14 6.57 o 0 6 1 1092.10 996.32 34.93 o 1 6 1 1.17 -2.31 5.18 o 2 6 1 1999.65 2119.13 35.43 o 3 6 1 354.59 321.74 18.96 o 4 6 1 3193.21 3154.19 64.89 o 5 6 1 298.01 322.23 29.97 o 6 6 1 881.47 889.25 63.35 o 7 6 1 99.67 100.80 30.14 o -6 7 1 0.88 20.74 21.07 o -5 7 1 440.01 368.58 40.40 o -4 7 1 75.10 54.20 21.05 o -3 7 1 1839.17 1743.02 61.05 o -2 7 1 734.93 726.85 25.51 o -1 7 1 7137.72 6875.30 141.18 o 0 7 1 1658.11 1618.69 39.77 o 1 7 1 678.82 638.89 43.34 o 2 7 1 8.09 8.89 6.47 o 3 7 1 564.83 531.22 25.93 o 4 7 1 25.91 16.00 16.63 o 5 7 1 0.95 13.57 18.76 o 6 7 1 13.19 21.00 21.55 o -6 8 1 319.22 380.82 51.34 o -5 8 1 18.34 4.53 19.36 o -4 8 1 1043.17 954.92 71.47 o -3 8 1 10.83 -10.42 10.42 o -2 8 1 418.93 384.95 25.03 o -1 8 1 153.61 129.86 14.63 o 0 8 1 1166.08 1193.83 37.89 o 1 8 1 89.44 97.74 15.40 o 2 8 1 1720.91 1760.35 51.87 o 3 8 1 4.84 -5.32 9.34 o 4 8 1 1526.76 1633.40 74.45 o 5 8 1 16.98 38.36 22.53 o 6 8 1 659.95 658.44 59.51 o -6 9 1 27.33 87.01 29.18 o -5 9 1 80.97 76.97 25.50 o -4 9 1 5.54 8.24 18.06 o -3 9 1 587.09 550.49 49.14 o -2 9 1 694.18 697.25 34.95 o -1 9 1 2160.51 2201.51 52.61 o 0 9 1 88.75 147.59 26.85 o 1 9 1 1838.69 1828.48 49.63 o 2 9 1 0.11 9.42 10.31 o 3 9 1 321.34 236.82 33.83 o 4 9 1 21.55 -16.82 23.76 o 5 9 1 57.72 61.68 24.88 o 6 9 1 5.75 -1.02 23.45 o -5 10 1 12.71 -13.32 21.10 o -4 10 1 92.24 98.22 26.36 o -3 10 1 16.99 15.52 18.12 o -2 10 1 101.69 76.80 20.15 o -1 10 1 16.44 11.71 12.21 o 0 10 1 453.09 463.59 24.32 o 1 10 1 491.62 515.37 29.74 o 2 10 1 370.05 356.33 28.66 o 3 10 1 229.25 172.37 31.22 o 4 10 1 507.52 495.94 92.01 o 5 10 1 51.08 39.54 29.39 o -5 11 1 81.92 72.77 30.03 o -4 11 1 38.16 83.83 28.47 o -3 11 1 250.73 277.99 39.13 o -2 11 1 140.54 123.56 19.63 o -1 11 1 197.93 209.32 19.48 o 0 11 1 10.78 21.40 11.24 o 1 11 1 717.89 702.19 34.28 o 2 11 1 68.77 74.05 16.87 o 3 11 1 55.64 38.00 21.96 o 4 11 1 6.51 -1.21 26.37 o 5 11 1 144.22 110.46 33.18 o -4 12 1 121.74 162.27 44.29 o -3 12 1 32.24 33.90 29.80 o -2 12 1 2.15 6.88 20.29 o -1 12 1 5.03 16.57 9.37 o 0 12 1 91.97 109.95 14.96 o 1 12 1 320.16 344.57 27.07 o 2 12 1 162.98 155.41 25.07 o 3 12 1 70.58 65.70 27.99 o 4 12 1 119.30 158.41 49.93 o -4 13 1 21.10 52.39 28.24 o -3 13 1 47.77 52.56 26.82 o -2 13 1 61.06 44.77 19.89 o -1 13 1 153.64 170.76 19.46 o 0 13 1 27.33 46.52 12.98 o 1 13 1 26.01 50.49 14.24 o 2 13 1 20.79 17.64 16.58 o 3 13 1 19.22 -8.36 34.83 o 4 13 1 20.06 42.75 28.87 o -3 14 1 7.43 20.27 20.75 o -2 14 1 0.08 -1.01 17.34 o -1 14 1 5.96 0.91 18.39 o 0 14 1 3.14 -7.19 12.24 o 1 14 1 25.91 38.42 26.04 o 2 14 1 4.18 -0.14 22.12 o 3 14 1 187.83 264.17 42.95 o -2 15 1 17.76 19.39 21.02 o -1 15 1 3.22 -2.73 19.11 o 0 15 1 41.40 21.69 17.19 o 1 15 1 0.01 -0.74 18.57 o 2 15 1 19.82 17.61 36.44 o -6 0 2 608.91 732.04 47.11 o -4 0 2 10294.05 10393.25 213.53 o -2 0 2 26453.33 27027.92 438.58 o 0 0 2 9383.31 9594.87 154.67 o 2 0 2 1753.23 1685.24 32.21 o 4 0 2 411.23 418.92 21.18 o 6 0 2 3123.56 3209.26 76.46 o -7 1 2 1601.97 1449.59 91.81 o -6 1 2 0.27 17.01 9.33 o -5 1 2 1974.08 1856.83 36.76 o -4 1 2 435.57 424.80 13.47 o -3 1 2 581.45 605.79 13.57 o -2 1 2 543.77 527.57 14.20 o -1 1 2 617.52 643.34 12.51 o 0 1 2 9.26 10.45 1.90 o 1 1 2 4837.21 4963.04 44.44 o 2 1 2 1037.20 978.36 13.91 o 3 1 2 13451.93 13430.23 137.59 o 4 1 2 56.95 40.10 6.37 o 5 1 2 2003.19 1968.42 36.65 o 6 1 2 272.31 274.35 15.87 o 7 1 2 709.11 780.36 81.74 o -7 2 2 49.24 80.19 34.23 o -6 2 2 86.65 109.14 19.30 o -5 2 2 168.05 151.49 27.92 o -4 2 2 5085.13 5275.80 85.12 o -3 2 2 45.20 33.98 5.16 o -2 2 2 25742.35 26693.89 369.60 o -1 2 2 26539.43 27263.37 253.70 o 0 2 2 2864.96 2887.66 30.95 o 1 2 2 0.79 1.16 2.37 o 2 2 2 1336.02 1406.18 18.69 o 3 2 2 87.68 96.60 6.14 o 4 2 2 1176.32 1159.88 24.04 o 5 2 2 3.58 10.99 8.51 o 6 2 2 1172.43 1190.78 55.05 o 7 2 2 83.05 108.78 24.77 o -7 3 2 1078.24 1007.47 86.57 o -6 3 2 231.58 267.62 37.25 o -5 3 2 1180.55 1170.48 35.97 o -4 3 2 13.97 15.02 5.34 o -3 3 2 611.25 596.75 14.50 o -2 3 2 1075.38 1186.38 30.47 o -1 3 2 1053.26 1143.06 15.53 o 0 3 2 8730.87 8957.60 87.73 o 1 3 2 3644.26 3500.00 40.89 o 2 3 2 341.14 313.97 10.63 o 3 3 2 6079.42 6026.38 76.62 o 4 3 2 1953.34 1891.43 39.33 o 5 3 2 1714.06 1752.54 36.79 o 6 3 2 1038.11 1007.31 45.76 o 7 3 2 494.80 596.87 50.81 o -7 4 2 144.27 199.72 48.32 o -6 4 2 0.89 14.73 19.53 o -5 4 2 1384.77 1363.83 68.65 o -4 4 2 2637.02 2643.12 48.03 o -3 4 2 2780.48 2642.45 43.96 o -2 4 2 10493.23 10607.50 162.46 o -1 4 2 13210.91 13475.87 149.93 o 0 4 2 8087.23 8291.56 89.06 o 1 4 2 4013.92 4179.81 52.47 o 2 4 2 240.19 196.50 10.41 o 3 4 2 1.52 3.95 4.82 o 4 4 2 1099.80 1126.14 27.81 o 5 4 2 85.19 80.84 11.33 o 6 4 2 404.27 412.21 34.52 o 7 4 2 285.42 214.15 35.65 o -7 5 2 580.62 501.72 70.87 o -6 5 2 389.12 355.54 37.30 o -5 5 2 498.53 536.79 42.57 o -4 5 2 444.92 447.91 18.26 o -3 5 2 53.89 35.23 9.65 o -2 5 2 28.50 32.68 8.85 o -1 5 2 758.99 729.68 18.84 o 0 5 2 4299.98 4558.74 58.72 o 1 5 2 11.54 21.45 5.43 o 2 5 2 3549.29 3463.89 49.27 o 3 5 2 3001.67 3178.58 67.84 o 4 5 2 3967.56 4171.42 75.32 o 5 5 2 647.46 653.29 29.87 o 6 5 2 669.30 658.18 49.12 o 7 5 2 91.66 83.45 24.30 o -7 6 2 43.80 35.03 38.66 o -6 6 2 0.35 12.70 17.22 o -5 6 2 1434.00 1395.92 63.78 o -4 6 2 467.76 451.57 39.00 o -3 6 2 1919.46 1776.09 105.14 o -2 6 2 1577.46 1565.08 31.15 o -1 6 2 5339.22 5094.36 88.91 o 0 6 2 156.91 152.23 11.28 o 1 6 2 5375.32 5748.80 93.74 o 2 6 2 84.99 90.95 9.34 o 3 6 2 55.27 57.91 8.03 o 4 6 2 348.23 358.96 25.48 o 5 6 2 94.43 95.56 15.65 o 6 6 2 70.33 108.74 37.49 o -6 7 2 349.99 401.76 45.30 o -5 7 2 189.05 167.90 29.61 o -4 7 2 122.64 84.06 22.12 o -3 7 2 14.70 20.05 10.93 o -2 7 2 297.05 288.26 17.78 o -1 7 2 244.81 264.16 24.88 o 0 7 2 3052.91 2955.18 53.85 o 1 7 2 138.36 142.30 14.26 o 2 7 2 2345.43 2351.83 46.30 o 3 7 2 380.22 376.03 21.35 o 4 7 2 3300.14 3191.56 90.15 o 5 7 2 101.43 119.50 17.92 o 6 7 2 507.41 578.71 52.28 o -6 8 2 2.74 6.06 21.46 o -5 8 2 930.49 977.62 67.74 o -4 8 2 28.69 32.66 18.89 o -3 8 2 1847.54 1731.01 147.98 o -2 8 2 6.99 3.01 6.06 o -1 8 2 3347.15 3345.08 67.26 o 0 8 2 220.29 207.05 14.98 o 1 8 2 2931.83 2974.38 64.95 o 2 8 2 8.50 8.89 9.05 o 3 8 2 9.16 4.27 8.26 o 4 8 2 2.72 -8.81 12.37 o 5 8 2 115.22 129.74 20.61 o 6 8 2 8.83 27.38 19.43 o -6 9 2 171.70 225.54 82.75 o -5 9 2 2.40 1.97 20.94 o -4 9 2 107.95 152.00 29.10 o -3 9 2 57.70 41.04 20.48 o -2 9 2 464.31 436.40 26.33 o -1 9 2 176.03 169.40 17.79 o 0 9 2 1191.31 1165.81 59.08 o 1 9 2 160.42 152.42 19.91 o 2 9 2 1410.00 1388.63 67.23 o 3 9 2 16.78 19.98 16.10 o 4 9 2 1382.68 1357.93 76.84 o 5 9 2 0.03 -0.52 18.65 o 6 9 2 351.79 290.36 61.13 o -5 10 2 161.99 138.87 34.11 o -4 10 2 84.74 54.87 24.36 o -3 10 2 198.28 171.28 32.04 o -2 10 2 117.90 118.52 11.43 o -1 10 2 2968.28 3101.07 80.15 o 0 10 2 16.92 16.82 9.24 o 1 10 2 168.76 158.40 18.66 o 2 10 2 172.88 173.46 25.93 o 3 10 2 3.21 -11.77 26.78 o 4 10 2 0.03 -7.79 21.14 o 5 10 2 8.07 42.17 26.02 o -5 11 2 5.72 16.51 25.34 o -4 11 2 35.53 41.40 26.19 o -3 11 2 3.70 -9.98 16.16 o -2 11 2 47.68 76.04 25.75 o -1 11 2 2.90 19.61 9.19 o 0 11 2 322.47 357.21 29.29 o 1 11 2 38.08 26.38 13.04 o 2 11 2 452.48 475.08 47.81 o 3 11 2 199.33 237.66 38.76 o 4 11 2 400.72 403.63 54.16 o 5 11 2 5.34 1.02 24.64 o -4 12 2 337.09 288.25 45.02 o -3 12 2 92.45 91.19 24.35 o -2 12 2 61.54 57.25 18.90 o -1 12 2 368.87 393.67 29.23 o 0 12 2 12.59 -10.41 10.41 o 1 12 2 200.43 191.88 21.89 o 2 12 2 51.62 2.57 24.36 o 3 12 2 4.82 16.97 23.63 o 4 12 2 6.29 1.91 20.81 o -4 13 2 8.77 17.90 26.44 o -3 13 2 25.63 36.88 18.99 o -2 13 2 3.48 -4.62 15.61 o -1 13 2 27.82 47.20 17.28 o 0 13 2 261.69 261.38 25.27 o 1 13 2 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