#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:23:13 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181228 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/06/2230689.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230689_Fobs loop_ _publ_author_name 'Caracelli, Ignez' 'Coelho, Daniel C. S.' 'Olivato, Paulo R.' 'Rodrigues, Alessandro' 'Tiekink, Edward R. T.' _publ_section_title ; (5R)-3-(2-Chloroacetyl)-4-methyl-5-phenyl-1,3,4-oxadiazinan-2-one ; _journal_coeditor_code HG5045 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1571 _journal_page_last o1572 _journal_volume 67 _journal_year 2011 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.4862 _cell_length_b 9.6237 _cell_length_c 13.2433 _exptl_crystal_F_000 560.00 _reflns_d_resolution_high 0.8110 _cod_data_source_file hg5045Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' s97 in P 21 21 21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 109.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 849.58 767.54 12.01 o 4 0 0 132.06 103.12 2.48 o 6 0 0 1978.53 1859.98 16.23 o 8 0 0 199.96 185.40 4.81 o 10 0 0 1041.17 1036.26 16.80 o 1 1 0 3769.87 3589.28 37.23 o 2 1 0 1065.79 1080.90 10.68 o 3 1 0 219.37 184.65 2.37 o 4 1 0 440.82 435.39 4.10 o 5 1 0 1590.80 1580.18 9.62 o 6 1 0 741.21 782.03 5.54 o 7 1 0 46.07 46.07 1.21 o 8 1 0 179.92 179.78 2.88 o 9 1 0 306.07 294.77 4.13 o 10 1 0 21.47 25.58 1.51 o 11 1 0 223.16 230.40 4.08 o 0 2 0 2050.55 2037.27 23.73 o 1 2 0 431.81 449.63 4.76 o 2 2 0 31.47 24.26 0.67 o 3 2 0 1676.74 1715.07 10.33 o 4 2 0 480.61 444.16 3.24 o 5 2 0 17.54 10.08 0.53 o 6 2 0 139.66 148.95 1.97 o 7 2 0 200.03 212.49 2.51 o 8 2 0 151.08 144.33 2.53 o 9 2 0 181.12 167.62 3.20 o 10 2 0 309.34 310.73 4.54 o 11 2 0 83.63 94.50 2.73 o 1 3 0 4615.57 4595.56 25.89 o 2 3 0 5275.41 5336.66 28.88 o 3 3 0 454.54 407.92 3.13 o 4 3 0 149.99 163.17 1.63 o 5 3 0 699.79 683.25 4.48 o 6 3 0 189.85 189.12 2.31 o 7 3 0 405.55 392.75 3.66 o 8 3 0 0.61 2.01 0.62 o 9 3 0 89.66 92.77 2.46 o 10 3 0 63.34 65.25 2.60 o 11 3 0 411.79 443.60 7.55 o 0 4 0 840.39 776.31 7.35 o 1 4 0 1315.05 1315.71 7.87 o 2 4 0 6.27 8.49 0.35 o 3 4 0 93.90 81.86 1.15 o 4 4 0 431.39 431.78 3.34 o 5 4 0 15.06 13.87 0.59 o 6 4 0 739.66 727.45 5.31 o 7 4 0 82.10 82.78 1.79 o 8 4 0 22.53 18.75 1.19 o 9 4 0 89.78 76.25 2.23 o 10 4 0 211.49 207.34 6.10 o 11 4 0 1.95 1.50 1.19 o 1 5 0 424.93 457.26 3.32 o 2 5 0 287.81 306.92 2.33 o 3 5 0 53.94 55.23 0.97 o 4 5 0 3.70 1.90 0.32 o 5 5 0 175.96 179.27 2.16 o 6 5 0 306.07 311.21 3.17 o 7 5 0 365.97 362.92 3.83 o 8 5 0 12.26 17.51 1.17 o 9 5 0 10.22 7.13 1.06 o 10 5 0 25.51 23.33 2.57 o 0 6 0 0.52 0.75 0.39 o 1 6 0 126.98 160.33 1.68 o 2 6 0 4146.69 4172.57 23.51 o 3 6 0 54.90 69.31 1.20 o 4 6 0 672.35 632.46 4.75 o 5 6 0 0.92 1.40 0.42 o 6 6 0 543.90 496.62 4.71 o 7 6 0 19.30 23.52 1.21 o 8 6 0 691.66 626.83 6.77 o 9 6 0 2.84 2.67 0.94 o 10 6 0 24.01 26.06 2.24 o 1 7 0 287.28 270.32 2.55 o 2 7 0 99.80 102.93 1.77 o 3 7 0 306.75 293.94 3.17 o 4 7 0 35.49 38.07 1.22 o 5 7 0 603.76 606.47 5.57 o 6 7 0 25.68 25.65 1.18 o 7 7 0 112.84 133.86 2.73 o 8 7 0 181.24 191.22 3.64 o 9 7 0 57.64 73.52 2.89 o 0 8 0 524.41 513.62 6.73 o 1 8 0 41.86 46.49 1.25 o 2 8 0 43.79 38.42 1.28 o 3 8 0 18.68 22.64 1.08 o 4 8 0 117.62 114.54 2.24 o 5 8 0 17.97 19.22 1.51 o 6 8 0 16.66 19.21 1.20 o 7 8 0 20.79 13.67 1.25 o 8 8 0 16.95 12.57 1.40 o 1 9 0 494.71 493.04 5.14 o 2 9 0 564.60 542.03 5.27 o 3 9 0 534.65 515.99 4.97 o 4 9 0 202.10 205.43 3.82 o 5 9 0 495.59 496.73 5.57 o 6 9 0 92.37 103.10 2.47 o 7 9 0 27.48 28.71 1.74 o 0 10 0 152.92 155.72 4.21 o 1 10 0 160.90 160.99 2.95 o 2 10 0 891.05 858.81 7.90 o 3 10 0 55.86 56.12 2.01 o 4 10 0 243.85 250.73 3.87 o 5 10 0 8.76 9.59 1.05 o 6 10 0 3.91 4.78 0.94 o 1 11 0 202.03 211.46 3.69 o 2 11 0 0.38 0.90 0.76 o 3 11 0 18.69 19.43 1.34 o 4 11 0 34.97 30.93 1.68 o 1 0 1 1889.76 1876.22 12.91 o 2 0 1 5.24 7.19 0.43 o 3 0 1 360.04 355.51 2.89 o 4 0 1 324.36 309.94 2.77 o 5 0 1 57.75 62.63 1.20 o 6 0 1 5.32 5.67 0.44 o 7 0 1 36.13 41.23 1.05 o 8 0 1 108.72 111.67 1.94 o 9 0 1 317.32 318.87 4.08 o 10 0 1 4.62 7.61 1.13 o 11 0 1 65.49 76.12 2.88 o -11 1 1 187.68 200.30 5.30 o -10 1 1 32.14 30.91 1.64 o -9 1 1 17.54 19.41 1.27 o -8 1 1 547.70 568.85 5.77 o -7 1 1 947.35 930.43 7.36 o -6 1 1 157.96 146.11 1.77 o -5 1 1 781.77 777.76 6.15 o -4 1 1 920.50 881.42 6.48 o -3 1 1 1542.03 1518.34 11.19 o -2 1 1 10858.17 10207.59 131.85 o -1 1 1 360.93 396.74 3.82 o 0 1 1 117.14 116.62 1.49 o 1 1 1 380.73 410.85 3.92 o 2 1 1 10771.13 10370.89 92.41 o 3 1 1 1543.53 1528.39 9.68 o 4 1 1 910.50 880.20 6.17 o 5 1 1 770.69 780.27 5.85 o 6 1 1 165.25 153.77 2.15 o 7 1 1 952.77 949.08 7.48 o 8 1 1 556.44 558.38 5.42 o 9 1 1 16.46 19.82 1.25 o 10 1 1 29.05 27.21 1.55 o 11 1 1 188.54 198.61 3.78 o -11 2 1 228.03 237.58 4.39 o -10 2 1 36.48 34.44 1.81 o -9 2 1 633.53 637.89 6.88 o -8 2 1 7.24 7.37 1.15 o -7 2 1 96.33 97.97 1.80 o -6 2 1 484.67 501.59 4.04 o -5 2 1 206.91 224.28 2.17 o -4 2 1 1425.96 1427.36 8.38 o -3 2 1 8687.90 8726.76 50.80 o -2 2 1 1169.99 1175.64 7.71 o -1 2 1 671.75 674.30 5.18 o 0 2 1 7404.78 7433.99 61.66 o 1 2 1 720.95 722.13 7.27 o 2 2 1 1149.23 1156.36 7.80 o 3 2 1 8773.80 8874.25 47.19 o 4 2 1 1421.59 1425.49 8.75 o 5 2 1 188.52 203.98 2.15 o 6 2 1 493.53 510.65 4.12 o 7 2 1 91.84 94.50 1.72 o 8 2 1 8.09 9.12 0.92 o 9 2 1 642.48 630.96 6.56 o 10 2 1 37.36 37.76 1.86 o 11 2 1 235.56 231.96 4.32 o -11 3 1 387.62 386.96 6.76 o -10 3 1 308.68 302.98 5.35 o -9 3 1 68.92 68.74 2.20 o -8 3 1 238.51 232.86 3.46 o -7 3 1 13.70 11.66 0.86 o -6 3 1 187.34 191.14 2.08 o -5 3 1 151.19 166.00 1.80 o -4 3 1 1011.70 1104.52 6.73 o -3 3 1 2459.29 2618.25 13.83 o -2 3 1 682.65 722.45 4.32 o -1 3 1 2368.52 2375.34 12.75 o 0 3 1 124.20 128.06 1.28 o 1 3 1 2362.07 2375.71 15.10 o 2 3 1 669.37 721.79 4.90 o 3 3 1 2461.26 2629.00 14.92 o 4 3 1 998.15 1089.57 6.82 o 5 3 1 150.85 172.92 2.09 o 6 3 1 191.07 193.24 2.10 o 7 3 1 13.63 10.77 0.74 o 8 3 1 234.63 232.96 3.17 o 9 3 1 70.04 67.95 2.48 o 10 3 1 306.46 300.77 5.27 o 11 3 1 385.65 388.17 6.46 o -10 4 1 18.21 23.07 2.09 o -9 4 1 66.36 56.18 2.11 o -8 4 1 26.73 28.35 1.30 o -7 4 1 449.95 444.93 4.29 o -6 4 1 12.09 16.16 0.74 o -5 4 1 194.93 180.63 2.08 o -4 4 1 409.77 421.86 3.11 o -3 4 1 526.31 533.31 3.46 o -2 4 1 852.79 873.52 5.37 o -1 4 1 430.13 456.21 2.92 o 0 4 1 78.13 90.59 1.13 o 1 4 1 409.76 434.08 3.94 o 2 4 1 838.73 862.32 6.96 o 3 4 1 503.15 510.28 3.61 o 4 4 1 397.40 400.50 3.54 o 5 4 1 184.92 171.24 2.34 o 6 4 1 12.52 16.03 0.71 o 7 4 1 445.63 435.06 4.38 o 8 4 1 25.14 27.83 1.96 o 9 4 1 62.71 57.95 2.12 o 10 4 1 18.79 20.84 1.81 o -10 5 1 113.39 109.96 3.91 o -9 5 1 20.59 20.02 2.09 o -8 5 1 176.11 175.31 3.10 o -7 5 1 37.99 37.80 1.41 o -6 5 1 229.61 226.37 2.67 o -5 5 1 210.20 196.85 2.29 o -4 5 1 768.55 757.38 4.99 o -3 5 1 64.36 59.96 0.98 o -2 5 1 1612.89 1630.94 9.25 o -1 5 1 325.86 315.77 2.48 o 0 5 1 1202.68 1213.05 7.45 o 1 5 1 344.85 331.16 3.21 o 2 5 1 1645.22 1660.15 10.99 o 3 5 1 69.68 67.27 1.11 o 4 5 1 760.35 746.49 5.16 o 5 5 1 205.44 187.46 2.30 o 6 5 1 243.70 239.44 2.77 o 7 5 1 42.17 42.45 1.34 o 8 5 1 175.60 175.40 3.29 o 9 5 1 21.22 21.51 1.48 o 10 5 1 113.26 100.48 3.41 o -10 6 1 6.07 3.96 1.25 o -9 6 1 287.87 319.80 5.36 o -8 6 1 55.90 55.87 1.98 o -7 6 1 60.35 60.51 1.70 o -6 6 1 72.88 65.46 1.55 o -5 6 1 380.37 382.26 3.59 o -4 6 1 380.74 373.48 3.08 o -3 6 1 285.00 257.80 2.57 o -2 6 1 461.75 437.51 3.21 o -1 6 1 603.84 599.88 4.16 o 0 6 1 968.32 949.48 6.04 o 1 6 1 623.49 619.34 5.25 o 2 6 1 454.08 433.03 3.92 o 3 6 1 291.95 271.16 2.59 o 4 6 1 386.74 377.52 3.37 o 5 6 1 374.77 371.91 3.71 o 6 6 1 72.10 65.73 1.42 o 7 6 1 64.07 64.23 1.65 o 8 6 1 54.75 59.72 2.09 o 9 6 1 283.34 311.46 4.94 o 10 6 1 5.90 6.74 1.27 o -9 7 1 122.23 117.50 3.60 o -8 7 1 72.44 67.62 2.46 o -7 7 1 138.49 143.30 2.85 o -6 7 1 223.25 205.66 2.97 o -5 7 1 87.49 84.98 1.83 o -4 7 1 447.89 445.17 4.46 o -3 7 1 465.38 449.42 4.18 o -2 7 1 125.11 133.01 1.83 o -1 7 1 20.09 23.38 0.74 o 0 7 1 1.03 3.15 0.38 o 1 7 1 18.41 21.16 0.80 o 2 7 1 132.62 138.96 2.09 o 3 7 1 466.47 454.84 4.67 o 4 7 1 447.07 439.63 4.70 o 5 7 1 90.74 91.05 1.79 o 6 7 1 224.52 210.19 2.95 o 7 7 1 135.26 138.94 3.16 o 8 7 1 69.38 66.90 2.23 o 9 7 1 123.51 123.38 3.34 o -8 8 1 320.04 317.85 5.75 o -7 8 1 188.21 202.55 3.76 o -6 8 1 80.24 79.83 2.09 o -5 8 1 225.96 217.77 3.27 o -4 8 1 13.10 13.55 0.94 o -3 8 1 70.42 72.69 1.72 o -2 8 1 1899.39 1883.85 12.40 o -1 8 1 1870.08 1837.73 12.10 o 0 8 1 44.72 35.75 1.13 o 1 8 1 1896.93 1891.15 11.77 o 2 8 1 1893.19 1867.03 11.89 o 3 8 1 82.39 85.37 2.16 o 4 8 1 15.59 15.97 0.99 o 5 8 1 226.75 222.41 4.06 o 6 8 1 78.42 76.42 2.01 o 7 8 1 182.19 190.14 5.24 o 8 8 1 324.16 319.19 5.27 o -7 9 1 154.53 157.17 3.68 o -6 9 1 30.26 32.46 1.56 o -5 9 1 37.03 38.95 1.61 o -4 9 1 241.43 240.96 3.33 o -3 9 1 72.30 69.53 1.80 o -2 9 1 635.30 653.18 7.21 o -1 9 1 26.58 26.62 1.30 o 0 9 1 188.83 175.98 2.64 o 1 9 1 26.99 25.53 1.11 o 2 9 1 611.88 621.89 5.60 o 3 9 1 77.97 75.30 1.79 o 4 9 1 242.77 244.88 3.52 o 5 9 1 36.08 38.57 1.58 o 6 9 1 29.21 31.34 1.54 o 7 9 1 149.87 153.73 3.19 o -6 10 1 106.20 110.78 3.01 o -5 10 1 19.53 17.15 1.25 o -4 10 1 7.11 3.71 0.84 o -3 10 1 16.62 16.55 1.24 o -2 10 1 98.38 99.31 2.40 o -1 10 1 61.89 63.56 1.98 o 0 10 1 91.16 85.48 2.13 o 1 10 1 60.95 61.50 2.29 o 2 10 1 99.52 98.80 2.40 o 3 10 1 16.22 14.30 1.09 o 4 10 1 7.15 2.97 0.72 o 5 10 1 19.66 15.55 1.34 o 6 10 1 105.07 111.37 2.71 o -4 11 1 160.53 166.61 3.54 o -3 11 1 22.30 22.80 1.70 o -2 11 1 84.11 89.60 2.48 o -1 11 1 224.94 237.16 4.83 o 0 11 1 402.06 398.23 5.27 o 1 11 1 214.93 214.66 5.01 o 2 11 1 82.42 90.18 2.37 o 3 11 1 20.31 23.28 1.41 o 4 11 1 170.08 183.31 3.30 o 0 0 2 12094.87 10693.13 244.19 o 1 0 2 1129.63 1132.16 10.96 o 2 0 2 53.33 43.70 0.79 o 3 0 2 1675.80 1627.97 9.28 o 4 0 2 41.02 46.14 0.86 o 5 0 2 82.17 55.07 1.31 o 6 0 2 590.72 592.75 4.69 o 7 0 2 890.79 892.86 6.88 o 8 0 2 94.44 97.21 2.47 o 9 0 2 963.97 992.18 8.04 o 10 0 2 8.90 6.85 1.15 o 11 0 2 0.28 1.23 1.00 o -11 1 2 25.16 26.40 1.78 o -10 1 2 96.13 96.14 2.88 o -9 1 2 562.22 550.65 6.26 o -8 1 2 101.57 102.87 2.08 o -7 1 2 34.45 35.65 1.19 o -6 1 2 292.03 317.58 3.03 o -5 1 2 221.19 217.20 2.14 o -4 1 2 1882.10 1936.13 11.78 o -3 1 2 654.67 638.46 4.16 o -2 1 2 6228.94 6163.28 35.77 o -1 1 2 7136.13 6820.64 48.39 o 0 1 2 134.31 144.55 1.76 o 1 1 2 7097.66 6742.92 102.40 o 2 1 2 6223.24 6150.30 59.81 o 3 1 2 646.85 632.45 5.31 o 4 1 2 1861.09 1923.35 11.49 o 5 1 2 226.19 223.61 2.44 o 6 1 2 305.37 328.43 3.39 o 7 1 2 36.57 38.26 1.38 o 8 1 2 98.12 94.47 2.09 o 9 1 2 567.86 557.92 5.75 o 10 1 2 93.66 92.28 2.51 o 11 1 2 24.91 26.65 1.80 o -11 2 2 66.69 62.68 2.67 o -10 2 2 23.53 27.15 1.78 o -9 2 2 179.47 181.58 3.53 o -8 2 2 81.10 72.13 1.88 o -7 2 2 366.55 360.09 3.49 o -6 2 2 221.16 230.72 2.78 o -5 2 2 536.59 531.14 4.00 o -4 2 2 401.84 394.75 3.03 o -3 2 2 1024.35 1046.26 6.74 o -2 2 2 30.27 21.67 0.78 o -1 2 2 1900.02 1947.55 13.68 o 0 2 2 44.57 46.95 1.41 o 1 2 2 1911.61 1974.69 13.86 o 2 2 2 32.54 23.71 0.55 o 3 2 2 1019.78 1046.52 6.79 o 4 2 2 404.75 394.53 3.18 o 5 2 2 530.82 523.98 4.11 o 6 2 2 224.48 237.21 2.60 o 7 2 2 371.17 362.11 3.68 o 8 2 2 80.36 70.91 1.78 o 9 2 2 177.09 184.46 3.18 o 10 2 2 24.12 27.59 1.66 o 11 2 2 67.43 66.86 2.71 o -11 3 2 51.51 46.46 2.51 o -10 3 2 81.34 84.11 3.36 o -9 3 2 315.20 311.50 5.90 o -8 3 2 100.79 106.60 2.12 o -7 3 2 1.41 2.25 0.50 o -6 3 2 195.74 201.41 2.28 o -5 3 2 922.75 943.52 6.20 o -4 3 2 354.12 339.40 2.90 o -3 3 2 64.21 69.72 0.91 o -2 3 2 1178.89 1170.16 6.74 o -1 3 2 1069.47 1064.13 6.33 o 0 3 2 573.42 586.51 4.24 o 1 3 2 1049.57 1053.06 7.37 o 2 3 2 1167.21 1152.90 7.45 o 3 3 2 56.95 62.88 0.99 o 4 3 2 356.65 348.55 2.98 o 5 3 2 914.88 933.76 6.24 o 6 3 2 211.76 213.87 2.37 o 7 3 2 1.58 2.70 0.49 o 8 3 2 99.84 101.54 2.69 o 9 3 2 321.85 319.94 4.58 o 10 3 2 77.73 82.92 2.70 o 11 3 2 49.46 42.06 2.77 o -10 4 2 113.75 120.53 5.01 o -9 4 2 328.66 316.57 5.62 o -8 4 2 121.77 119.68 2.39 o -7 4 2 19.14 21.80 1.01 o -6 4 2 296.82 289.49 2.86 o -5 4 2 416.31 408.92 3.21 o -4 4 2 164.59 182.73 1.89 o -3 4 2 1002.00 1031.90 5.64 o -2 4 2 1703.73 1722.25 10.15 o -1 4 2 1339.57 1275.17 7.73 o 0 4 2 1107.25 1080.94 6.75 o 1 4 2 1350.37 1290.92 8.25 o 2 4 2 1685.56 1711.94 11.20 o 3 4 2 1024.57 1049.05 6.56 o 4 4 2 173.17 191.54 2.02 o 5 4 2 397.53 385.34 3.28 o 6 4 2 292.88 285.83 3.01 o 7 4 2 23.34 24.61 1.24 o 8 4 2 119.57 123.67 2.37 o 9 4 2 332.09 326.02 5.20 o 10 4 2 114.06 108.38 3.19 o -10 5 2 5.40 2.13 1.09 o -9 5 2 2.71 1.47 0.92 o -8 5 2 93.78 89.86 2.18 o -7 5 2 256.84 241.69 3.23 o -6 5 2 43.62 43.39 1.18 o -5 5 2 274.11 263.78 2.49 o -4 5 2 118.65 117.29 1.51 o -3 5 2 352.68 351.75 2.71 o -2 5 2 748.74 784.87 4.98 o -1 5 2 1462.54 1561.95 9.07 o 0 5 2 3995.99 4206.42 22.55 o 1 5 2 1460.35 1573.38 10.07 o 2 5 2 749.83 785.83 6.35 o 3 5 2 354.38 350.91 3.16 o 4 5 2 117.78 118.13 1.61 o 5 5 2 271.41 262.46 2.67 o 6 5 2 43.95 40.39 1.30 o 7 5 2 255.21 242.38 2.99 o 8 5 2 92.85 88.65 2.14 o 9 5 2 2.81 3.55 0.91 o 10 5 2 5.64 2.00 0.96 o -9 6 2 17.46 16.28 1.52 o -8 6 2 192.01 179.48 3.30 o -7 6 2 62.40 66.91 1.80 o -6 6 2 86.51 84.71 1.81 o -5 6 2 396.60 398.09 3.51 o -4 6 2 665.35 669.18 4.74 o -3 6 2 83.18 93.17 1.39 o -2 6 2 296.30 303.48 2.56 o -1 6 2 612.00 576.97 4.07 o 0 6 2 0.21 0.72 0.28 o 1 6 2 601.32 574.58 4.72 o 2 6 2 286.65 294.95 3.04 o 3 6 2 72.00 82.63 1.47 o 4 6 2 660.91 660.11 5.07 o 5 6 2 388.63 390.82 3.97 o 6 6 2 92.20 87.02 1.79 o 7 6 2 59.17 60.98 1.90 o 8 6 2 197.86 180.94 3.11 o 9 6 2 19.06 17.26 1.46 o -9 7 2 8.54 6.04 1.31 o -8 7 2 151.86 148.22 3.26 o -7 7 2 397.22 367.55 5.78 o -6 7 2 769.30 746.16 7.37 o -5 7 2 70.12 69.42 1.57 o -4 7 2 1169.79 1140.59 8.75 o -3 7 2 493.65 495.31 4.48 o -2 7 2 868.34 831.30 6.02 o -1 7 2 689.65 680.11 4.87 o 0 7 2 1443.68 1368.35 8.16 o 1 7 2 695.56 678.04 5.39 o 2 7 2 861.41 820.68 6.73 o 3 7 2 505.08 511.47 4.53 o 4 7 2 1172.33 1143.37 9.30 o 5 7 2 74.11 72.31 1.79 o 6 7 2 774.20 748.93 7.15 o 7 7 2 390.66 364.34 5.22 o 8 7 2 152.99 151.07 3.38 o 9 7 2 7.64 6.63 1.20 o -8 8 2 24.31 26.93 1.86 o -7 8 2 212.97 215.96 6.45 o -6 8 2 0.39 2.73 0.81 o -5 8 2 135.12 112.04 2.33 o -4 8 2 3.71 3.17 0.61 o -3 8 2 60.94 64.47 1.62 o -2 8 2 246.25 248.36 3.15 o -1 8 2 594.52 612.34 5.70 o 0 8 2 293.62 291.37 3.13 o 1 8 2 602.69 612.99 4.93 o 2 8 2 243.91 249.93 3.22 o 3 8 2 60.34 65.22 1.71 o 4 8 2 3.53 4.01 0.78 o 5 8 2 133.86 114.55 2.58 o 6 8 2 0.44 1.67 0.76 o 7 8 2 215.66 214.43 4.04 o 8 8 2 24.58 28.96 2.39 o -7 9 2 217.80 220.06 6.40 o -6 9 2 241.53 239.60 5.44 o -5 9 2 50.64 47.11 1.78 o -4 9 2 107.57 108.10 2.24 o -3 9 2 57.74 57.78 1.75 o -2 9 2 19.75 18.44 1.29 o -1 9 2 83.52 82.00 1.95 o 0 9 2 1037.37 1030.92 8.62 o 1 9 2 79.08 79.30 2.41 o 2 9 2 16.72 15.29 0.85 o 3 9 2 54.92 53.87 1.80 o 4 9 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