#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:23:33 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181229 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/07/2230717.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230717_Fobs loop_ _publ_author_name 'Bentiss, Fouad' 'Capet, Fr\'ed\'eric' 'Lagren\'ee, Michel' 'Saadi, Mohamed' 'El Ammari, Lahcen' _publ_section_title ; trans-Diaquabis[2,5-bis(pyridin-2-yl)-1,3,4-thiadiazole]cobalt(II) bis(tetrafluoridoborate) ; _journal_coeditor_code IM2290 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m834 _journal_page_last m835 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.114 _cell_angle_gamma 90.000 _cell_length_a 10.8319 _cell_length_b 11.0623 _cell_length_c 13.2120 _exptl_crystal_F_000 754.00 _reflns_d_resolution_high 0.8107 _cod_data_source_file im2290Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CoBF4100K in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 283.85 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9107.08 9502.28 62.82 o 4 0 0 219.93 189.72 1.85 o 6 0 0 380.71 404.63 3.99 o 8 0 0 59.42 60.62 2.23 o 10 0 0 4881.15 4738.38 48.70 o 12 0 0 321.09 287.60 9.60 o 1 1 0 2569.67 2485.53 24.17 o 2 1 0 3834.21 4137.03 23.00 o 3 1 0 1715.51 1749.80 9.18 o 4 1 0 3396.55 3375.35 15.91 o 5 1 0 668.25 784.05 4.32 o 6 1 0 422.12 501.46 3.28 o 7 1 0 2189.06 2104.05 12.35 o 8 1 0 0.24 0.08 0.67 o 9 1 0 2883.77 2913.50 19.91 o 10 1 0 421.49 440.07 4.80 o 11 1 0 76.06 76.91 3.41 o 12 1 0 128.08 137.53 5.30 o 13 1 0 230.03 263.31 6.31 o 0 2 0 8085.58 8423.60 75.39 o 1 2 0 70.84 95.15 1.06 o 2 2 0 2626.18 2665.49 20.19 o 3 2 0 231.34 236.08 1.92 o 4 2 0 816.11 800.20 4.81 o 5 2 0 38.42 37.54 0.75 o 6 2 0 5422.61 5651.40 30.18 o 7 2 0 258.94 260.93 2.53 o 8 2 0 913.19 921.20 7.00 o 9 2 0 788.25 777.97 6.54 o 10 2 0 8.23 12.36 1.41 o 11 2 0 411.02 395.67 5.96 o 12 2 0 70.81 75.60 3.30 o 1 3 0 7218.03 7505.27 44.44 o 2 3 0 1613.86 1693.35 12.01 o 3 3 0 2265.23 2580.06 17.05 o 4 3 0 79.71 112.76 1.45 o 5 3 0 6528.22 6838.04 37.11 o 6 3 0 2432.65 2506.27 15.25 o 7 3 0 154.05 180.29 2.51 o 8 3 0 271.13 268.73 2.95 o 9 3 0 59.56 58.96 1.77 o 10 3 0 1895.73 1837.58 16.24 o 11 3 0 889.42 863.20 9.48 o 12 3 0 9.99 4.32 1.52 o 0 4 0 4773.18 4754.26 37.42 o 1 4 0 65.92 88.13 1.10 o 2 4 0 4716.13 4609.90 31.88 o 3 4 0 516.30 511.68 4.10 o 4 4 0 2871.48 2925.77 18.04 o 5 4 0 122.97 118.49 1.52 o 6 4 0 326.32 318.33 2.93 o 7 4 0 342.72 359.27 3.40 o 8 4 0 5454.99 5462.09 33.19 o 9 4 0 532.25 491.11 5.16 o 10 4 0 38.47 27.82 1.59 o 11 4 0 2.18 1.32 1.19 o 12 4 0 477.17 506.98 7.26 o 1 5 0 5652.97 5454.95 32.41 o 2 5 0 657.68 732.31 5.28 o 3 5 0 282.44 252.02 2.85 o 4 5 0 3208.80 3412.46 24.10 o 5 5 0 1470.34 1437.79 10.67 o 6 5 0 31.63 33.64 0.98 o 7 5 0 59.10 58.36 1.49 o 8 5 0 254.20 217.37 2.93 o 9 5 0 54.67 49.09 1.57 o 10 5 0 1883.89 1925.08 19.62 o 11 5 0 379.51 368.46 5.19 o 12 5 0 21.40 11.19 1.81 o 0 6 0 4.09 10.28 1.21 o 1 6 0 749.18 845.84 5.98 o 2 6 0 18.82 30.01 1.03 o 3 6 0 2934.66 2941.14 20.26 o 4 6 0 379.11 314.34 4.47 o 5 6 0 0.69 0.69 0.69 o 6 6 0 1431.54 1390.76 13.15 o 7 6 0 1810.43 1790.19 13.23 o 8 6 0 56.08 60.79 1.86 o 9 6 0 11.73 9.70 0.92 o 10 6 0 588.08 604.43 7.18 o 11 6 0 148.37 161.36 3.21 o 1 7 0 134.12 137.98 2.46 o 2 7 0 19.74 21.32 0.97 o 3 7 0 1692.55 1634.51 11.94 o 4 7 0 35.96 37.58 1.01 o 5 7 0 416.06 415.42 6.34 o 6 7 0 233.06 234.40 3.36 o 7 7 0 3093.72 3170.59 24.47 o 8 7 0 49.99 41.68 2.66 o 9 7 0 780.10 790.37 9.02 o 10 7 0 5.32 3.78 1.33 o 11 7 0 4.77 3.48 1.09 o 0 8 0 12888.96 13239.08 103.39 o 1 8 0 4.89 2.55 0.76 o 2 8 0 43.29 61.86 1.36 o 3 8 0 1448.15 1384.38 10.50 o 4 8 0 477.72 480.39 4.96 o 5 8 0 448.15 429.44 4.55 o 6 8 0 43.05 40.82 2.38 o 7 8 0 532.94 490.38 6.72 o 8 8 0 110.81 126.03 2.96 o 9 8 0 126.12 134.78 3.90 o 10 8 0 895.22 840.22 13.34 o 1 9 0 178.17 170.05 2.31 o 2 9 0 14.80 11.66 0.87 o 3 9 0 579.98 560.86 5.15 o 4 9 0 1225.20 1185.31 9.94 o 5 9 0 273.52 261.37 3.59 o 6 9 0 104.63 88.28 2.21 o 7 9 0 140.04 122.68 2.99 o 8 9 0 227.67 234.11 5.12 o 9 9 0 119.55 107.87 4.11 o 0 10 0 2440.98 2480.52 26.57 o 1 10 0 101.62 95.91 1.86 o 2 10 0 2280.41 2256.72 16.34 o 3 10 0 6.99 12.88 1.00 o 4 10 0 501.00 500.67 5.29 o 5 10 0 3.65 6.61 1.20 o 6 10 0 929.54 842.44 9.42 o 7 10 0 74.63 71.96 2.70 o 8 10 0 499.12 476.34 11.08 o 1 11 0 158.93 166.07 2.83 o 2 11 0 88.05 77.14 2.50 o 3 11 0 64.89 69.89 2.29 o 4 11 0 21.14 20.98 1.33 o 5 11 0 1198.82 1154.58 11.35 o 6 11 0 27.49 21.36 2.68 o 7 11 0 20.34 27.20 2.23 o 0 12 0 231.66 230.34 12.22 o 1 12 0 130.29 142.29 4.11 o 2 12 0 301.14 313.32 4.88 o 3 12 0 170.99 164.31 3.34 o 4 12 0 785.08 821.47 10.43 o 5 12 0 42.61 32.34 1.74 o 6 12 0 111.33 112.74 3.01 o 1 13 0 537.80 524.44 7.47 o 2 13 0 0.14 -2.09 1.39 o 3 13 0 371.69 354.18 5.73 o -13 0 1 1.30 5.86 2.77 o -11 0 1 565.56 562.03 10.66 o -9 0 1 39.45 50.66 2.49 o -7 0 1 909.51 950.95 8.14 o -5 0 1 575.79 477.97 3.93 o -3 0 1 2208.14 2350.67 15.19 o 1 0 1 7110.04 6424.86 137.49 o 3 0 1 9950.35 10332.99 67.36 o 5 0 1 7094.35 7653.72 52.18 o 7 0 1 192.86 186.35 3.62 o 9 0 1 2250.26 2202.76 23.70 o 11 0 1 582.12 582.84 13.06 o -13 1 1 43.98 39.62 3.03 o -12 1 1 566.09 528.08 10.97 o -11 1 1 207.08 183.09 4.26 o -10 1 1 1005.07 990.90 8.37 o -9 1 1 1111.97 1104.52 8.12 o -8 1 1 5559.26 5597.41 32.98 o -7 1 1 225.30 210.47 2.14 o -6 1 1 1250.19 1218.73 6.99 o -5 1 1 520.02 497.81 3.17 o -4 1 1 2766.71 2908.08 15.44 o -3 1 1 613.91 634.79 3.83 o -2 1 1 1204.69 1105.03 6.16 o -1 1 1 2023.14 2209.27 16.42 o 0 1 1 1126.38 1049.07 27.68 o 1 1 1 3603.30 3479.42 25.62 o 2 1 1 1296.59 1435.37 8.01 o 3 1 1 2967.08 2989.64 14.79 o 4 1 1 43.66 35.97 0.64 o 5 1 1 82.88 73.75 0.97 o 6 1 1 1006.08 971.41 6.05 o 7 1 1 27.62 11.48 0.74 o 8 1 1 1026.21 1005.85 8.11 o 9 1 1 1.07 0.35 0.84 o 10 1 1 208.75 201.85 3.68 o 11 1 1 648.64 657.51 8.90 o 12 1 1 126.31 132.42 4.53 o -13 2 1 293.09 350.59 6.82 o -12 2 1 858.13 819.39 12.28 o -11 2 1 453.13 469.96 6.28 o -10 2 1 2.22 4.32 1.04 o -9 2 1 2078.32 2066.41 14.20 o -8 2 1 196.93 187.44 2.45 o -7 2 1 1148.86 1143.68 7.69 o -6 2 1 432.91 470.12 3.74 o -5 2 1 7.60 13.83 0.73 o -4 2 1 5235.76 5273.05 29.05 o -3 2 1 48.41 42.69 0.90 o -2 2 1 1650.67 1776.77 11.27 o -1 2 1 4496.88 4425.26 25.65 o 0 2 1 6452.39 6834.11 33.74 o 1 2 1 13.02 15.69 0.41 o 2 2 1 1012.70 1095.57 6.70 o 3 2 1 4307.60 4401.50 23.98 o 4 2 1 2463.06 2469.30 14.73 o 5 2 1 960.34 876.43 5.43 o 6 2 1 1732.24 1775.95 11.15 o 7 2 1 981.97 930.86 6.77 o 8 2 1 386.28 387.74 4.17 o 9 2 1 317.88 297.67 3.98 o 10 2 1 69.95 60.12 2.26 o 11 2 1 38.75 34.06 2.29 o 12 2 1 263.14 277.88 5.61 o -12 3 1 48.16 60.96 2.76 o -11 3 1 0.83 2.21 1.35 o -10 3 1 759.67 750.52 6.86 o -9 3 1 86.41 102.48 1.94 o -8 3 1 593.51 613.08 4.72 o -7 3 1 320.78 340.44 3.08 o -6 3 1 1229.51 1136.12 7.05 o -5 3 1 41.60 32.13 0.97 o -4 3 1 556.25 522.09 3.95 o -3 3 1 2685.81 2542.20 16.70 o -2 3 1 2992.03 2965.90 19.19 o -1 3 1 1342.06 1379.60 7.80 o 0 3 1 4145.53 4179.02 22.04 o 1 3 1 1148.72 1163.60 7.50 o 2 3 1 68.15 55.33 0.97 o 3 3 1 1109.21 1209.06 8.16 o 4 3 1 355.58 333.73 2.92 o 5 3 1 228.21 235.36 2.30 o 6 3 1 1107.54 1110.81 8.61 o 7 3 1 73.76 74.85 1.55 o 8 3 1 397.21 416.90 4.29 o 9 3 1 130.87 132.09 2.46 o 10 3 1 1590.95 1562.47 14.79 o 11 3 1 11.83 13.78 1.63 o 12 3 1 6.16 3.30 1.66 o -12 4 1 0.85 1.91 1.52 o -11 4 1 65.43 60.77 2.20 o -10 4 1 7.05 2.27 1.03 o -9 4 1 193.61 207.70 2.77 o -8 4 1 26.92 33.85 1.17 o -7 4 1 5817.93 6004.20 34.06 o -6 4 1 10.17 3.81 0.55 o -5 4 1 413.50 401.83 3.32 o -4 4 1 1333.64 1316.80 8.71 o -3 4 1 17003.10 18356.10 120.87 o -2 4 1 1393.11 1389.09 9.38 o -1 4 1 26.89 30.96 0.53 o 0 4 1 1699.61 1746.98 10.06 o 1 4 1 12.21 7.34 0.39 o 2 4 1 64.99 60.78 1.05 o 3 4 1 3735.04 3771.00 24.15 o 4 4 1 444.86 432.49 4.63 o 5 4 1 2.04 1.73 0.78 o 6 4 1 1236.39 1211.84 11.33 o 7 4 1 3282.12 3140.51 22.05 o 8 4 1 115.75 114.90 2.10 o 9 4 1 222.86 208.57 3.25 o 10 4 1 229.56 245.36 4.06 o 11 4 1 185.94 190.41 3.82 o 12 4 1 54.26 47.51 2.56 o -12 5 1 268.03 265.56 4.77 o -11 5 1 637.46 686.82 7.40 o -10 5 1 239.78 239.25 3.66 o -9 5 1 575.76 586.17 5.46 o -8 5 1 10.71 9.08 0.79 o -7 5 1 6.28 2.80 0.69 o -6 5 1 511.50 526.74 4.46 o -5 5 1 21.93 37.77 1.36 o -4 5 1 870.90 942.44 7.05 o -3 5 1 327.55 305.86 3.00 o -2 5 1 4809.72 5035.70 29.04 o -1 5 1 63.54 40.10 0.71 o 0 5 1 4208.33 4079.33 22.78 o 1 5 1 1842.64 1765.48 10.06 o 2 5 1 934.62 996.43 6.70 o 3 5 1 4513.26 5076.19 49.25 o 4 5 1 1427.34 1395.74 11.02 o 5 5 1 43.18 53.07 1.62 o 6 5 1 546.65 535.56 4.99 o 7 5 1 491.39 504.09 5.13 o 8 5 1 415.45 397.32 4.18 o 9 5 1 6.88 4.69 0.98 o 10 5 1 1333.18 1333.41 11.83 o 11 5 1 1070.10 1073.07 10.58 o 12 5 1 302.12 290.51 5.42 o -11 6 1 488.06 451.64 5.73 o -10 6 1 23.65 27.04 1.56 o -9 6 1 981.74 909.87 7.00 o -8 6 1 472.67 485.47 4.56 o -7 6 1 133.85 148.15 2.21 o -6 6 1 8.38 7.14 0.70 o -5 6 1 3565.25 3541.73 26.31 o -4 6 1 2366.86 2137.69 15.04 o -3 6 1 196.53 279.52 3.02 o -2 6 1 937.09 1047.60 7.20 o -1 6 1 3084.49 3200.28 19.38 o 0 6 1 3049.37 3098.38 18.19 o 1 6 1 5079.45 5488.42 32.79 o 2 6 1 551.26 613.46 4.84 o 3 6 1 22.35 20.00 0.89 o 4 6 1 254.23 275.49 3.58 o 5 6 1 716.17 696.82 7.05 o 6 6 1 1491.32 1489.53 13.96 o 7 6 1 5.40 5.21 1.05 o 8 6 1 51.91 48.44 1.34 o 9 6 1 99.21 98.98 2.37 o 10 6 1 350.23 318.71 4.15 o 11 6 1 210.72 214.33 3.56 o -11 7 1 19.83 14.38 1.40 o -10 7 1 1.72 3.59 1.09 o -9 7 1 689.99 691.02 8.54 o -8 7 1 2188.03 2225.06 15.61 o -7 7 1 67.71 53.69 1.42 o -6 7 1 248.73 219.02 2.64 o -5 7 1 2.71 5.54 0.76 o -4 7 1 6.45 7.71 0.78 o -3 7 1 290.07 299.17 3.29 o -2 7 1 1103.55 1136.91 8.25 o -1 7 1 1013.92 1022.07 7.50 o 0 7 1 383.85 409.97 3.08 o 1 7 1 3.75 9.72 0.72 o 2 7 1 3384.68 3179.49 21.79 o 3 7 1 11.16 5.70 0.64 o 4 7 1 1848.29 1706.34 14.59 o 5 7 1 241.52 251.83 5.18 o 6 7 1 522.04 574.19 6.78 o 7 7 1 36.04 33.06 1.85 o 8 7 1 1541.77 1487.09 14.38 o 9 7 1 10.01 12.65 2.29 o 10 7 1 48.65 34.27 1.71 o 11 7 1 1.61 0.80 1.35 o -10 8 1 32.81 36.23 2.08 o -9 8 1 17.40 18.85 2.08 o -8 8 1 490.96 514.73 7.04 o -7 8 1 27.50 31.13 1.47 o -6 8 1 0.16 0.45 0.86 o -5 8 1 1957.37 1962.50 15.97 o -4 8 1 0.25 -0.22 0.86 o -3 8 1 1237.45 1285.61 9.41 o -2 8 1 1375.35 1324.04 9.59 o -1 8 1 3591.93 3541.74 22.53 o 0 8 1 128.90 133.84 2.02 o 1 8 1 5008.97 4951.17 32.01 o 2 8 1 559.10 560.56 5.41 o 3 8 1 16.85 26.47 1.59 o 4 8 1 13.07 11.58 0.73 o 5 8 1 1370.15 1348.75 13.84 o 6 8 1 364.92 354.58 6.67 o 7 8 1 251.04 233.61 5.19 o 8 8 1 312.59 286.22 6.35 o 9 8 1 887.06 873.23 16.79 o 10 8 1 64.70 61.91 4.12 o -9 9 1 39.36 48.67 3.85 o -8 9 1 477.08 485.08 8.13 o -7 9 1 0.81 0.85 1.14 o -6 9 1 1906.89 1855.39 17.03 o -5 9 1 503.71 439.78 4.99 o -4 9 1 1396.87 1390.24 10.67 o -3 9 1 579.99 555.93 4.92 o -2 9 1 308.81 343.48 3.56 o -1 9 1 320.96 330.18 3.40 o 0 9 1 55.92 70.26 1.38 o 1 9 1 412.06 380.47 3.93 o 2 9 1 671.25 693.77 5.80 o 3 9 1 1798.87 1748.65 13.07 o 4 9 1 879.06 903.14 7.92 o 5 9 1 163.89 154.87 2.67 o 6 9 1 447.22 416.23 8.35 o 7 9 1 26.02 34.15 3.06 o 8 9 1 99.24 88.23 4.69 o 9 9 1 231.03 242.12 5.64 o -9 10 1 23.33 11.47 2.21 o -8 10 1 1.67 -2.60 2.02 o -7 10 1 1775.57 1668.18 20.10 o -6 10 1 30.94 30.16 2.00 o -5 10 1 34.07 36.21 1.48 o -4 10 1 489.03 470.46 5.06 o -3 10 1 247.40 256.33 3.17 o -2 10 1 152.82 166.59 2.55 o -1 10 1 175.10 178.09 2.65 o 0 10 1 221.08 216.65 2.76 o 1 10 1 474.02 474.82 4.50 o 2 10 1 5.23 4.84 1.03 o 3 10 1 4417.60 4316.97 32.39 o 4 10 1 318.51 303.83 4.01 o 5 10 1 167.46 165.38 3.05 o 6 10 1 133.31 135.84 3.14 o 7 10 1 759.83 770.16 13.06 o 8 10 1 1.37 1.25 2.60 o -7 11 1 2.94 -0.88 1.65 o -6 11 1 1548.26 1509.41 15.40 o -5 11 1 51.61 40.89 1.70 o -4 11 1 1109.19 1079.17 14.04 o -3 11 1 54.57 49.03 2.03 o -2 11 1 30.12 37.54 1.93 o -1 11 1 0.01 -0.99 0.88 o 0 11 1 1315.43 1308.10 12.20 o 1 11 1 183.59 189.35 3.20 o 2 11 1 252.84 249.62 3.82 o 3 11 1 122.16 104.29 2.37 o 4 11 1 959.18 990.85 9.03 o 5 11 1 13.24 12.03 1.98 o 6 11 1 650.01 639.44 9.77 o 7 11 1 110.00 105.67 5.18 o -6 12 1 242.98 257.62 4.86 o -5 12 1 17.22 10.57 1.59 o -4 12 1 221.03 216.52 3.74 o -3 12 1 873.57 852.89 9.37 o -2 12 1 51.76 47.54 2.24 o -1 12 1 90.51 83.62 3.02 o 0 12 1 80.12 68.10 2.77 o 1 12 1 461.22 461.29 6.20 o 2 12 1 20.77 21.01 1.58 o 3 12 1 911.58 958.91 9.59 o 4 12 1 235.60 227.57 3.74 o 5 12 1 294.16 301.20 5.08 o 6 12 1 96.20 90.28 3.99 o -4 13 1 97.68 104.48 3.63 o -3 13 1 216.07 222.15 4.68 o -2 13 1 189.91 194.56 4.37 o -1 13 1 36.53 33.44 2.31 o 0 13 1 112.96 116.96 3.67 o 1 13 1 133.31 133.96 3.80 o 2 13 1 360.20 393.17 5.90 o 3 13 1 262.84 299.62 5.96 o -12 0 2 28.10 33.41 3.69 o -10 0 2 3918.42 3977.84 41.16 o -8 0 2 212.58 224.59 4.00 o -6 0 2 3.98 43.29 1.25 o -4 0 2 9127.82 9214.56 63.27 o -2 0 2 2867.65 2824.69 25.88 o 0 0 2 13494.31 13362.99 144.35 o 2 0 2 450.31 504.52 4.22 o 4 0 2 95.55 97.88 1.42 o 6 0 2 3123.11 3135.76 29.90 o 8 0 2 2015.33 2039.36 22.45 o 10 0 2 2406.02 2471.53 29.07 o 12 0 2 8.53 -0.53 2.77 o -13 1 2 553.50 549.75 8.75 o -12 1 2 0.03 0.14 1.58 o -11 1 2 16.73 15.39 1.55 o -10 1 2 0.21 1.01 0.90 o -9 1 2 146.37 155.64 2.48 o -8 1 2 11.49 17.37 1.05 o -7 1 2 677.11 696.81 5.09 o -6 1 2 595.02 735.57 4.86 o -5 1 2 427.80 492.28 3.32 o -4 1 2 3982.67 4322.25 21.74 o -3 1 2 4380.69 4428.57 23.12 o -2 1 2 11047.08 11174.37 63.40 o -1 1 2 11431.47 11785.68 68.94 o 0 1 2 62.89 68.76 0.94 o 1 1 2 7632.65 7978.06 41.10 o 2 1 2 774.57 816.63 4.51 o 3 1 2 2252.71 2108.31 10.97 o 4 1 2 32.17 26.59 0.60 o 5 1 2 2112.72 2186.97 11.37 o 6 1 2 1287.18 1275.42 7.75 o 7 1 2 1224.36 1215.04 8.27 o 8 1 2 2655.43 2701.74 18.40 o 9 1 2 424.39 403.50 4.03 o 10 1 2 635.21 666.59 8.16 o 11 1 2 390.00 379.50 6.44 o 12 1 2 41.69 37.34 2.59 o -13 2 2 50.67 68.26 4.07 o -12 2 2 387.42 353.06 6.36 o -11 2 2 118.37 115.09 3.02 o -10 2 2 29.55 29.38 1.47 o -9 2 2 3352.78 3326.69 21.11 o -8 2 2 32.02 23.70 0.99 o -7 2 2 197.18 196.85 1.95 o -6 2 2 147.17 155.59 1.63 o -5 2 2 961.09 949.11 5.57 o -4 2 2 2977.92 2993.71 16.02 o -3 2 2 351.19 407.41 2.66 o -2 2 2 8622.50 8835.17 58.96 o -1 2 2 17.89 5.47 0.43 o 0 2 2 337.42 291.50 1.87 o 1 2 2 9859.69 10135.31 54.91 o 2 2 2 195.56 161.56 1.26 o 3 2 2 2692.24 2744.83 15.24 o 4 2 2 194.77 183.36 1.74 o 5 2 2 4.25 10.65 0.53 o 6 2 2 1016.37 1068.34 7.67 o 7 2 2 647.28 636.91 5.20 o 8 2 2 822.25 805.03 7.14 o 9 2 2 1858.41 1881.26 15.44 o 10 2 2 13.41 13.94 1.57 o 11 2 2 14.98 13.73 1.92 o 12 2 2 344.03 350.43 6.34 o -13 3 2 2.21 4.30 1.86 o 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