#------------------------------------------------------------------------------ #$Date: 2011-08-08 08:56:15 +0300 (Mon, 08 Aug 2011) $ #$Revision: 23417 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2230783.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230783_Fobs loop_ _publ_author_name 'Boer\'e, Ren\'e T.' 'Masuda, Jason D.' _publ_section_title ; Tricarbonyl[N,N',N''-tris(2,6-diisopropylphenyl)guanidine]molybdenum(0) ; _journal_coeditor_code LH5261 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m895 _journal_page_last m896 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 89.128 _cell_angle_beta 78.713 _cell_angle_gamma 67.240 _cell_length_a 10.6525 _cell_length_b 11.7642 _cell_length_c 16.5482 _exptl_crystal_F_000 760.00 _reflns_d_resolution_high 0.7727 _[local]_cod_data_source_file lh5261Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' DippGuan-Mo(CO)3 (RB10045) in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 211.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1106.70 1224.72 12.82 o 2 0 0 6117.99 6160.37 76.88 o 3 0 0 2343.89 2349.07 26.56 o 4 0 0 606.15 647.71 14.43 o 5 0 0 3294.08 3488.39 39.26 o 6 0 0 550.04 586.47 16.84 o 7 0 0 367.74 420.71 19.72 o 8 0 0 0.59 -1.31 8.16 o 9 0 0 71.74 93.74 16.98 o 10 0 0 366.25 381.32 31.75 o 11 0 0 14.58 18.66 14.67 o 12 0 0 104.30 107.84 22.30 o -12 1 0 1.27 17.88 17.12 o -11 1 0 86.14 101.83 21.18 o -10 1 0 9.84 11.25 13.81 o -9 1 0 785.19 677.32 34.44 o -8 1 0 14.26 21.62 10.08 o -7 1 0 61.56 61.30 11.45 o -6 1 0 1348.19 1318.77 25.36 o -5 1 0 50.34 52.47 6.83 o -4 1 0 806.61 712.79 15.80 o -3 1 0 1368.01 1441.98 24.47 o -2 1 0 4964.98 6426.49 100.58 o -1 1 0 2229.66 2122.91 30.62 o 0 1 0 3222.71 3396.21 130.54 o 1 1 0 32749.04 35154.89 407.68 o 2 1 0 3438.40 3586.43 41.75 o 3 1 0 7259.13 7114.10 76.74 o 4 1 0 556.48 605.94 13.02 o 5 1 0 4380.63 4346.31 64.90 o 6 1 0 1010.38 1145.05 31.55 o 7 1 0 1226.05 1248.38 24.50 o 8 1 0 18.04 8.77 8.28 o 9 1 0 256.55 285.48 26.14 o 10 1 0 5.13 -4.62 11.73 o 11 1 0 5.14 11.74 13.25 o 12 1 0 171.38 163.57 25.22 o -11 2 0 243.24 211.29 28.20 o -10 2 0 72.63 93.55 19.38 o -9 2 0 262.35 300.78 28.26 o -8 2 0 774.38 846.90 30.20 o -7 2 0 319.99 310.59 20.43 o -6 2 0 1981.02 1964.76 33.61 o -5 2 0 304.89 401.24 14.83 o -4 2 0 349.47 302.76 12.19 o -3 2 0 978.21 921.48 17.08 o -2 2 0 2551.30 2670.72 32.31 o -1 2 0 270.62 207.02 7.79 o 0 2 0 1022.50 1282.34 26.45 o 1 2 0 9765.66 9817.01 151.73 o 2 2 0 3211.98 3331.92 83.76 o 3 2 0 12680.79 13212.44 215.69 o 4 2 0 2025.18 2374.95 33.70 o 5 2 0 5500.63 5657.23 82.37 o 6 2 0 1610.64 1648.58 24.85 o 7 2 0 306.83 317.44 13.76 o 8 2 0 612.39 626.89 23.52 o 9 2 0 152.85 154.58 20.20 o 10 2 0 97.56 109.96 19.05 o 11 2 0 52.74 38.75 15.37 o 12 2 0 35.21 36.69 16.69 o 13 2 0 5.14 -24.32 24.32 o -11 3 0 19.41 4.97 18.98 o -10 3 0 224.06 215.17 26.89 o -9 3 0 1.58 3.38 12.63 o -8 3 0 417.12 428.29 24.19 o -7 3 0 107.78 136.08 16.00 o -6 3 0 1930.51 1965.22 34.10 o -5 3 0 831.07 766.07 20.81 o -4 3 0 5.65 -0.23 4.52 o -3 3 0 726.98 626.33 15.82 o -2 3 0 417.00 385.50 11.68 o -1 3 0 11.64 2.92 3.51 o 0 3 0 1477.72 1684.73 38.87 o 1 3 0 1637.51 1390.53 30.14 o 2 3 0 112.26 166.49 7.24 o 3 3 0 645.36 652.43 12.87 o 4 3 0 6567.82 7251.67 122.66 o 5 3 0 239.85 197.86 9.28 o 6 3 0 1965.25 2013.57 27.46 o 7 3 0 515.33 624.11 17.65 o 8 3 0 334.53 322.76 17.86 o 9 3 0 61.73 79.12 15.82 o 10 3 0 948.43 974.02 50.39 o 11 3 0 24.02 24.15 14.81 o 12 3 0 29.83 28.92 16.09 o 13 3 0 5.08 2.79 15.76 o -10 4 0 229.96 227.28 36.82 o -9 4 0 230.05 245.42 34.29 o -8 4 0 273.88 277.94 23.08 o -7 4 0 399.20 435.44 23.57 o -6 4 0 87.56 92.26 11.50 o -5 4 0 3417.65 3540.02 46.51 o -4 4 0 325.95 333.61 14.61 o -3 4 0 5024.96 5024.67 85.09 o -2 4 0 365.24 383.24 18.87 o -1 4 0 25.92 2.50 3.71 o 0 4 0 481.59 448.81 12.71 o 1 4 0 967.32 1309.92 33.35 o 2 4 0 234.08 152.13 7.57 o 3 4 0 318.19 325.80 10.18 o 4 4 0 223.32 411.47 12.62 o 5 4 0 2009.76 2302.21 29.15 o 6 4 0 2854.58 2972.02 65.46 o 7 4 0 769.90 782.39 19.56 o 8 4 0 1749.74 1800.96 36.70 o 9 4 0 2.58 9.25 11.32 o 10 4 0 498.94 448.75 28.69 o 11 4 0 416.13 433.91 31.32 o 12 4 0 28.95 24.51 15.19 o 13 4 0 51.87 43.82 19.24 o -9 5 0 73.73 91.54 25.79 o -8 5 0 7.22 10.65 12.59 o -7 5 0 401.94 387.45 29.45 o -6 5 0 0.46 -4.76 7.33 o -5 5 0 121.67 128.92 12.91 o -4 5 0 263.52 269.22 14.47 o -3 5 0 1619.42 1622.32 49.68 o -2 5 0 3103.09 3318.79 100.97 o -1 5 0 950.55 1032.45 23.63 o 0 5 0 761.52 1266.71 34.22 o 1 5 0 13.82 6.58 3.96 o 2 5 0 4614.97 4622.92 90.61 o 3 5 0 2825.33 3157.58 37.27 o 4 5 0 53.31 18.87 4.87 o 5 5 0 660.60 849.15 18.36 o 6 5 0 81.15 65.40 7.81 o 7 5 0 122.64 142.43 11.19 o 8 5 0 261.42 230.29 16.44 o 9 5 0 867.09 777.77 33.27 o 10 5 0 3.79 7.92 11.16 o 11 5 0 435.36 414.45 31.97 o 12 5 0 5.37 13.71 13.65 o 13 5 0 16.46 10.35 16.18 o -9 6 0 358.14 361.00 60.56 o -8 6 0 9.46 -4.88 14.88 o -7 6 0 377.50 398.03 31.06 o -6 6 0 13.05 4.19 9.21 o -5 6 0 454.09 448.96 22.49 o -4 6 0 1751.37 1671.34 37.93 o -3 6 0 667.96 708.39 20.68 o -2 6 0 2884.21 3056.52 60.76 o -1 6 0 16.32 10.40 5.10 o 0 6 0 2414.64 2588.42 73.83 o 1 6 0 218.07 259.98 11.09 o 2 6 0 1732.22 1645.51 25.18 o 3 6 0 3535.50 3770.91 79.70 o 4 6 0 1936.95 2164.39 28.79 o 5 6 0 249.16 213.73 11.28 o 6 6 0 610.69 623.62 16.43 o 7 6 0 135.19 135.81 11.43 o 8 6 0 277.89 311.85 16.05 o 9 6 0 517.08 480.19 33.38 o 10 6 0 57.90 63.45 15.20 o 11 6 0 234.00 231.05 25.65 o 12 6 0 46.09 35.47 15.83 o 13 6 0 37.11 27.87 20.78 o -8 7 0 204.57 199.20 46.06 o -7 7 0 158.16 169.42 29.43 o -6 7 0 144.44 151.54 21.71 o -5 7 0 441.45 443.64 23.81 o -4 7 0 570.70 543.49 24.77 o -3 7 0 26.79 27.09 9.70 o -2 7 0 1297.56 1323.01 32.48 o -1 7 0 553.80 470.40 21.46 o 0 7 0 3527.41 3665.99 84.77 o 1 7 0 516.30 433.50 17.44 o 2 7 0 52.52 77.35 8.03 o 3 7 0 2207.35 2247.75 40.97 o 4 7 0 14.46 8.36 4.90 o 5 7 0 1202.58 1263.02 31.80 o 6 7 0 32.78 21.64 6.58 o 7 7 0 127.08 137.96 12.11 o 8 7 0 272.13 271.91 16.06 o 9 7 0 73.78 95.31 16.80 o 10 7 0 199.35 194.85 22.75 o 11 7 0 0.89 8.68 12.65 o 12 7 0 92.01 92.42 20.25 o 13 7 0 0.02 17.22 19.49 o -7 8 0 1.46 6.25 16.10 o -6 8 0 294.23 326.93 38.21 o -5 8 0 1.38 3.19 10.50 o -4 8 0 225.13 239.44 24.44 o -3 8 0 610.66 600.15 25.95 o -2 8 0 424.25 425.26 21.71 o -1 8 0 769.69 830.34 26.89 o 0 8 0 2223.81 2273.51 76.50 o 1 8 0 1276.48 1275.75 52.65 o 2 8 0 135.43 179.04 12.09 o 3 8 0 3199.83 3167.63 77.13 o 4 8 0 2.19 1.42 5.48 o 5 8 0 2016.18 2136.77 33.42 o 6 8 0 68.91 68.40 9.44 o 7 8 0 233.54 262.27 16.10 o 8 8 0 335.94 374.74 18.20 o 9 8 0 0.79 3.61 10.26 o 10 8 0 29.62 43.20 13.82 o 11 8 0 3.00 -5.81 11.70 o 12 8 0 30.95 35.70 20.17 o 13 8 0 16.08 7.36 18.93 o -6 9 0 721.70 734.66 50.98 o -5 9 0 12.05 13.49 12.40 o -4 9 0 123.83 116.82 19.55 o -3 9 0 546.01 559.87 31.63 o -2 9 0 1.64 6.46 9.73 o -1 9 0 436.40 414.40 25.72 o 0 9 0 4.08 7.00 8.12 o 1 9 0 922.58 974.89 29.23 o 2 9 0 27.81 17.98 8.07 o 3 9 0 177.08 173.08 15.28 o 4 9 0 2045.94 2161.45 40.43 o 5 9 0 299.09 331.75 16.11 o 6 9 0 1323.69 1448.97 33.82 o 7 9 0 16.43 6.68 7.41 o 8 9 0 89.97 123.40 15.04 o 9 9 0 14.69 31.12 12.69 o 10 9 0 76.97 81.86 17.66 o 11 9 0 3.88 3.61 12.21 o 12 9 0 136.88 131.47 27.94 o 13 9 0 2.28 -12.57 15.08 o -5 10 0 702.71 773.09 44.94 o -4 10 0 14.09 9.07 11.95 o -3 10 0 570.58 578.25 33.36 o -2 10 0 409.45 391.46 28.72 o -1 10 0 982.92 966.88 39.80 o 0 10 0 522.96 575.04 30.94 o 1 10 0 150.90 133.50 18.13 o 2 10 0 214.57 206.66 21.57 o 3 10 0 6.24 7.05 8.16 o 4 10 0 667.22 684.93 27.30 o 5 10 0 16.22 26.81 9.48 o 6 10 0 1010.04 963.07 30.95 o 7 10 0 24.76 30.12 9.09 o 8 10 0 195.14 208.85 16.69 o 9 10 0 207.57 235.63 24.37 o 10 10 0 2.48 -1.41 11.94 o 11 10 0 129.13 135.14 26.89 o 12 10 0 9.12 8.46 17.17 o -4 11 0 8.77 22.82 14.75 o -3 11 0 211.45 218.48 26.58 o -2 11 0 302.33 293.64 29.08 o -1 11 0 26.04 25.80 13.06 o 0 11 0 1159.23 1093.31 43.03 o 1 11 0 26.86 20.74 11.24 o 2 11 0 382.41 388.86 27.45 o 3 11 0 2.05 7.71 9.64 o 4 11 0 125.28 127.32 18.39 o 5 11 0 523.97 528.94 28.95 o 6 11 0 198.62 183.48 21.23 o 7 11 0 145.86 157.03 17.00 o 8 11 0 35.04 52.93 14.21 o 9 11 0 99.02 86.37 21.19 o 10 11 0 0.24 -14.50 14.50 o 11 11 0 23.12 27.74 18.31 o 12 11 0 17.13 26.72 18.83 o -3 12 0 258.68 288.30 31.62 o -2 12 0 378.92 334.59 35.82 o -1 12 0 10.99 14.60 12.78 o 0 12 0 418.22 420.88 33.09 o 1 12 0 124.54 136.70 21.59 o 2 12 0 766.81 802.79 37.72 o 3 12 0 302.28 309.74 28.28 o 4 12 0 291.06 296.76 27.56 o 5 12 0 73.01 99.22 17.49 o 6 12 0 52.13 44.15 16.25 o 7 12 0 212.08 236.97 24.87 o 8 12 0 7.05 5.75 13.55 o 11 12 0 83.41 115.73 35.77 o -1 13 0 96.02 90.12 20.75 o 0 13 0 366.72 405.56 36.17 o 1 13 0 182.49 181.04 24.22 o 2 13 0 134.84 118.93 20.65 o 3 13 0 551.08 523.39 32.93 o 4 13 0 32.73 13.19 12.57 o 5 13 0 81.38 120.48 20.19 o 6 13 0 9.36 4.13 12.14 o 7 13 0 1.44 -10.94 10.94 o 8 13 0 114.47 82.53 31.80 o 0 14 0 47.39 72.59 28.06 o 1 14 0 204.56 208.08 27.75 o 2 14 0 7.86 -0.31 13.12 o 3 14 0 551.88 581.77 36.75 o 4 14 0 149.93 130.25 21.91 o 5 14 0 378.10 346.00 37.58 o 6 14 0 58.55 82.84 18.36 o 7 14 0 100.50 70.41 17.90 o 8 14 0 28.00 9.12 23.38 o 4 15 0 64.44 70.11 19.56 o 5 15 0 9.58 15.73 14.76 o 6 15 0 154.61 161.70 24.92 o 7 15 0 31.03 24.60 19.86 o -7 -15 1 9.20 9.36 18.76 o -6 -15 1 173.30 176.13 26.49 o -5 -15 1 30.84 24.73 16.42 o -4 -15 1 62.58 31.80 16.47 o -9 -14 1 14.88 22.21 23.85 o -8 -14 1 37.55 37.73 19.94 o -7 -14 1 30.81 19.40 21.51 o -6 -14 1 243.08 285.08 29.72 o -5 -14 1 16.70 10.38 12.40 o -4 -14 1 106.49 147.08 22.81 o -3 -14 1 8.57 15.19 13.18 o -2 -14 1 42.95 48.77 16.99 o -1 -14 1 490.27 502.74 37.50 o 0 -14 1 100.25 105.46 26.61 o -9 -13 1 0.02 -1.10 14.87 o -8 -13 1 218.74 249.24 33.11 o -7 -13 1 2.86 -3.46 11.08 o -6 -13 1 13.40 22.43 13.36 o -5 -13 1 427.72 445.49 30.24 o -4 -13 1 208.09 228.16 26.38 o -3 -13 1 211.98 215.12 25.57 o -2 -13 1 3.09 -9.77 9.77 o -1 -13 1 120.85 141.08 22.40 o 0 -13 1 375.14 362.69 33.76 o 1 -13 1 478.53 463.94 36.70 o 2 -13 1 75.21 99.35 26.45 o -11 -12 1 2.78 -9.82 19.64 o -10 -12 1 46.87 66.46 22.53 o -9 -12 1 65.80 66.75 16.13 o -8 -12 1 184.78 176.95 27.85 o -7 -12 1 46.00 49.55 15.03 o -6 -12 1 2.12 -1.37 10.14 o -5 -12 1 216.72 285.07 26.94 o -4 -12 1 104.20 80.34 16.48 o -3 -12 1 831.36 833.46 38.24 o -2 -12 1 155.35 150.37 21.44 o -1 -12 1 250.93 257.54 26.92 o 0 -12 1 319.30 309.30 30.08 o 1 -12 1 90.54 79.98 19.17 o 2 -12 1 452.40 455.76 35.24 o 3 -12 1 46.90 37.67 17.08 o -12 -11 1 30.94 33.46 21.37 o -11 -11 1 18.78 31.56 24.55 o -10 -11 1 22.70 28.90 14.38 o -9 -11 1 11.84 14.12 12.57 o -8 -11 1 77.62 68.48 15.58 o -7 -11 1 687.14 670.97 27.94 o -6 -11 1 83.55 64.86 12.87 o -5 -11 1 92.08 113.93 14.85 o -4 -11 1 58.69 50.54 13.63 o -3 -11 1 0.49 -3.90 8.89 o -2 -11 1 368.84 361.32 26.34 o -1 -11 1 0.12 -1.71 9.01 o 0 -11 1 116.30 146.06 23.79 o 1 -11 1 0.21 15.63 11.68 o 2 -11 1 772.52 719.80 37.57 o 3 -11 1 161.87 135.22 22.52 o 4 -11 1 219.93 209.96 26.63 o -12 -10 1 30.08 44.86 22.03 o -11 -10 1 226.71 212.94 25.84 o -10 -10 1 0.00 3.06 11.82 o -9 -10 1 139.66 160.14 21.35 o -8 -10 1 15.09 8.22 9.47 o -7 -10 1 58.12 85.36 13.15 o -6 -10 1 168.55 160.79 16.31 o -5 -10 1 471.99 485.92 22.60 o -4 -10 1 694.52 730.46 26.67 o -3 -10 1 1913.69 1744.74 39.47 o -2 -10 1 215.01 229.51 18.73 o -1 -10 1 54.63 49.69 11.42 o 0 -10 1 466.96 496.13 29.09 o 1 -10 1 13.73 12.51 10.10 o 2 -10 1 465.43 447.78 29.25 o 3 -10 1 165.47 190.53 23.39 o 4 -10 1 95.41 90.54 18.67 o 5 -10 1 259.88 262.34 37.52 o -12 -9 1 11.36 6.61 15.14 o -11 -9 1 68.12 68.20 17.44 o -10 -9 1 104.61 88.56 17.75 o -9 -9 1 61.29 56.29 15.56 o -8 -9 1 22.18 27.55 10.29 o -7 -9 1 5.10 -2.72 5.99 o -6 -9 1 533.43 561.90 30.71 o -5 -9 1 27.32 38.46 8.50 o -4 -9 1 271.59 294.47 17.72 o -3 -9 1 600.25 575.90 22.69 o -2 -9 1 1130.37 1117.58 42.21 o -1 -9 1 146.42 164.31 15.73 o 0 -9 1 740.16 737.17 26.85 o 1 -9 1 304.53 321.74 20.59 o 2 -9 1 30.31 32.86 10.19 o 3 -9 1 567.77 564.00 31.08 o 4 -9 1 57.93 57.12 15.49 o 5 -9 1 232.24 271.67 27.84 o 6 -9 1 32.72 30.78 19.88 o -13 -8 1 0.93 -20.93 26.54 o -12 -8 1 289.74 250.41 28.55 o -11 -8 1 55.78 68.27 17.67 o -10 -8 1 164.71 164.73 21.73 o -9 -8 1 26.13 23.88 12.14 o -8 -8 1 348.83 343.88 20.40 o -7 -8 1 0.85 4.32 6.73 o -6 -8 1 1531.27 1545.66 29.92 o -5 -8 1 124.15 134.00 11.49 o -4 -8 1 590.26 654.05 20.00 o -3 -8 1 309.57 295.94 13.77 o -2 -8 1 601.91 625.33 30.51 o -1 -8 1 175.08 170.12 14.67 o 0 -8 1 536.11 573.21 22.39 o 1 -8 1 1260.55 1201.45 32.36 o 2 -8 1 192.21 203.83 17.95 o 3 -8 1 680.69 673.74 27.08 o 4 -8 1 24.81 23.16 10.46 o 5 -8 1 322.89 351.07 24.30 o 6 -8 1 130.09 140.76 27.28 o 7 -8 1 101.28 110.25 26.99 o -13 -7 1 0.56 5.87 15.04 o -12 -7 1 86.86 87.08 19.49 o -11 -7 1 4.46 6.36 12.64 o -10 -7 1 18.31 30.97 13.68 o -9 -7 1 3.39 1.83 9.89 o -8 -7 1 251.46 259.76 18.78 o -7 -7 1 602.33 559.58 19.28 o -6 -7 1 493.77 552.75 16.57 o -5 -7 1 524.38 470.00 16.26 o -4 -7 1 290.88 304.97 15.42 o -3 -7 1 2003.30 2054.57 43.76 o -2 -7 1 1246.77 1450.94 29.01 o -1 -7 1 5776.32 5810.69 135.76 o 0 -7 1 136.03 151.04 13.26 o 1 -7 1 4523.30 4742.70 147.18 o 2 -7 1 723.64 788.72 26.17 o 3 -7 1 410.67 376.81 20.34 o 4 -7 1 555.12 575.61 25.04 o 5 -7 1 32.19 33.53 12.49 o 6 -7 1 329.59 336.19 29.63 o 7 -7 1 15.14 13.14 13.09 o 8 -7 1 149.50 120.38 27.36 o -13 -6 1 26.11 33.17 17.80 o -12 -6 1 115.04 136.22 22.45 o -11 -6 1 13.91 16.68 13.65 o -10 -6 1 0.40 2.81 10.69 o -9 -6 1 411.57 455.92 27.73 o -8 -6 1 696.57 711.44 28.93 o -7 -6 1 800.70 822.26 21.62 o -6 -6 1 4.95 12.09 5.87 o -5 -6 1 3793.87 3770.24 39.68 o -4 -6 1 1632.18 1791.59 26.52 o -3 -6 1 704.26 664.89 16.24 o -2 -6 1 123.85 114.60 8.34 o -1 -6 1 3704.23 3906.02 111.76 o 0 -6 1 2390.74 2386.96 48.79 o 1 -6 1 318.59 281.10 11.75 o 2 -6 1 1811.47 1897.24 32.35 o 3 -6 1 228.44 252.65 16.94 o 4 -6 1 4357.25 4430.70 62.24 o 5 -6 1 10.15 5.78 8.11 o 6 -6 1 488.41 516.20 30.43 o 7 -6 1 0.21 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