#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:23:49 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181230 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/08/2230803.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230803_Fobs loop_ _publ_author_name 'Doboszewski, Bogdan' 'McGarrah, James' 'Nazarenko, Alexander Y.' 'da Paixao Soares, Fabio' _publ_section_title ; Dimethyl hydrazine-1,2-dicarboxylate--triphenylphosphine oxide (1/1) ; _journal_coeditor_code MW2011 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1565 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.090 _cell_angle_gamma 90.000 _cell_length_a 26.4938 _cell_length_b 8.5545 _cell_length_c 20.4426 _exptl_crystal_F_000 1792.00 _reflns_d_resolution_high 0.8392 _cod_data_source_file mw2011Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bd111 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 576.04 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 159.97 234.95 16.09 o 6 0 0 38546.27 34946.44 168.47 o 8 0 0 78379.01 79036.24 551.90 o 10 0 0 120.64 186.74 22.03 o 12 0 0 1721.05 1598.23 123.69 o 14 0 0 16622.80 17407.56 293.75 o 16 0 0 40.41 -11.67 27.26 o 18 0 0 4172.70 4213.89 129.67 o 20 0 0 2948.73 3144.19 122.27 o 22 0 0 426.52 420.87 64.39 o 24 0 0 619.86 527.21 74.12 o 26 0 0 121.77 90.83 51.73 o 28 0 0 502.94 394.76 87.70 o 1 1 0 40402.60 36803.57 272.34 o 3 1 0 1409.26 1370.87 18.53 o 5 1 0 10702.32 10392.80 99.53 o 7 1 0 6686.67 6909.19 84.73 o 9 1 0 306.80 243.57 16.19 o 11 1 0 62.43 80.41 16.24 o 13 1 0 1908.20 1723.26 49.40 o 15 1 0 6465.58 6698.67 104.42 o 17 1 0 2231.67 2364.03 69.57 o 19 1 0 6862.01 6591.65 118.44 o 21 1 0 236.65 265.62 38.53 o 23 1 0 56.12 34.62 29.34 o 25 1 0 237.22 236.02 42.23 o 27 1 0 1245.56 1265.95 77.79 o 29 1 0 35.37 61.76 47.22 o 0 2 0 68421.06 64672.70 280.50 o 2 2 0 47427.62 45045.27 107.40 o 4 2 0 8455.29 8114.91 49.09 o 6 2 0 5907.08 6143.96 53.63 o 8 2 0 7388.49 7427.67 70.61 o 10 2 0 2133.75 2529.56 49.94 o 12 2 0 9841.79 10337.54 126.41 o 14 2 0 131.65 175.24 26.14 o 16 2 0 436.15 376.17 37.06 o 18 2 0 2165.13 2420.86 79.66 o 20 2 0 1758.90 1854.45 76.10 o 22 2 0 380.21 350.01 44.87 o 24 2 0 364.09 306.13 43.70 o 26 2 0 0.40 30.60 32.81 o 28 2 0 7.80 32.71 41.00 o 1 3 0 378.17 458.50 16.38 o 3 3 0 25211.46 26358.58 94.59 o 5 3 0 1580.66 1557.47 27.51 o 7 3 0 2016.35 1836.68 38.39 o 9 3 0 8898.22 8997.63 101.53 o 11 3 0 103.52 85.43 20.41 o 13 3 0 1549.65 1629.83 54.54 o 15 3 0 13.32 23.96 19.68 o 17 3 0 89.77 56.38 23.97 o 19 3 0 2975.26 2855.14 83.03 o 21 3 0 291.01 233.92 37.97 o 23 3 0 154.34 129.41 35.54 o 25 3 0 34.19 45.27 33.64 o 27 3 0 11.88 6.67 38.18 o 0 4 0 646.15 874.62 39.70 o 2 4 0 4796.26 5020.16 61.57 o 4 4 0 1004.55 997.83 31.41 o 6 4 0 1717.31 1499.79 41.22 o 8 4 0 214.65 147.55 20.78 o 10 4 0 10126.49 10601.60 119.78 o 12 4 0 1504.96 1536.75 54.37 o 14 4 0 66.38 86.87 23.98 o 16 4 0 526.71 451.43 43.30 o 18 4 0 942.66 890.78 54.35 o 20 4 0 4.11 38.72 27.59 o 22 4 0 6.52 13.32 27.97 o 24 4 0 128.48 120.85 36.97 o 26 4 0 28.89 61.12 34.67 o 1 5 0 338.85 346.05 28.13 o 3 5 0 1272.12 1100.80 40.28 o 5 5 0 4360.51 4572.09 77.44 o 7 5 0 4310.68 4257.84 88.80 o 9 5 0 306.45 242.62 27.46 o 11 5 0 929.06 816.31 43.43 o 13 5 0 1689.15 1673.61 59.00 o 15 5 0 590.38 545.78 44.91 o 17 5 0 1657.61 1569.40 65.88 o 19 5 0 26.57 59.70 28.63 o 21 5 0 1419.38 1537.24 86.74 o 23 5 0 0.90 25.60 31.95 o 25 5 0 82.65 101.45 39.12 o 0 6 0 889.04 804.37 60.27 o 2 6 0 636.94 745.60 42.31 o 4 6 0 432.56 484.55 36.15 o 6 6 0 442.83 392.84 33.74 o 8 6 0 139.33 124.25 24.28 o 10 6 0 1484.31 1373.75 66.42 o 12 6 0 35.42 11.04 20.49 o 14 6 0 1851.35 1904.86 68.69 o 16 6 0 593.11 545.51 47.99 o 18 6 0 447.88 446.10 46.81 o 20 6 0 120.15 128.17 36.03 o 22 6 0 92.50 104.05 36.82 o 24 6 0 67.77 106.34 39.43 o 1 7 0 50.30 47.69 22.89 o 3 7 0 4079.08 4045.20 91.33 o 5 7 0 240.15 278.30 32.86 o 7 7 0 3.64 30.43 21.01 o 9 7 0 570.75 564.62 45.02 o 11 7 0 4630.10 4509.11 101.00 o 13 7 0 151.47 162.66 33.24 o 15 7 0 1256.76 1189.15 64.22 o 17 7 0 1973.60 2082.63 81.84 o 19 7 0 29.50 60.64 32.85 o 21 7 0 18.25 39.22 37.43 o 0 8 0 79.20 173.09 48.54 o 2 8 0 66.39 52.97 26.16 o 4 8 0 1120.63 1012.01 59.59 o 6 8 0 246.73 260.91 36.67 o 8 8 0 1.65 1.85 23.41 o 10 8 0 440.53 518.37 48.55 o 12 8 0 4.02 18.10 26.09 o 14 8 0 1223.78 1258.53 72.01 o 16 8 0 51.65 82.22 33.49 o 18 8 0 11.35 14.02 32.80 o 1 9 0 375.83 345.06 46.07 o 3 9 0 146.66 170.23 38.19 o 5 9 0 126.32 117.65 37.24 o 7 9 0 9.33 7.52 29.95 o 9 9 0 114.72 77.18 34.45 o 11 9 0 717.76 700.83 66.39 o 13 9 0 3.37 24.49 34.36 o 0 10 0 126.05 84.98 59.37 o 2 10 0 17.80 2.19 38.38 o 4 10 0 1033.02 993.59 90.98 o -29 1 1 700.54 636.98 69.55 o -27 1 1 976.75 955.56 69.69 o -25 1 1 78.87 71.47 33.47 o -23 1 1 99.85 79.22 30.39 o -21 1 1 2016.23 1960.35 72.72 o -19 1 1 4033.55 4246.05 96.48 o -17 1 1 166.66 116.56 25.75 o -15 1 1 11125.97 11065.46 132.12 o -13 1 1 11933.30 12281.87 194.62 o -11 1 1 592.58 549.17 28.34 o -9 1 1 12168.12 12442.14 140.93 o -7 1 1 41681.27 41169.23 259.70 o -5 1 1 4667.00 4476.00 36.68 o -3 1 1 1524.47 1416.03 17.83 o -1 1 1 20373.80 19499.15 106.17 o 1 1 1 26.56 27.41 3.69 o 3 1 1 4959.15 4641.29 31.86 o 5 1 1 829.66 832.61 18.69 o 7 1 1 3603.85 3522.15 48.45 o 9 1 1 7098.48 7748.22 90.76 o 11 1 1 25.22 26.92 14.06 o 13 1 1 3067.38 3308.94 71.09 o 15 1 1 355.92 272.80 28.67 o 17 1 1 412.48 294.79 33.45 o 19 1 1 1370.83 1484.85 62.50 o 21 1 1 1403.87 1379.09 65.34 o 23 1 1 1791.95 1695.82 74.74 o 25 1 1 355.99 395.39 48.46 o 27 1 1 531.67 546.26 68.24 o 29 1 1 5.59 24.22 44.26 o -28 2 1 411.02 413.82 54.85 o -26 2 1 368.22 285.38 47.96 o -24 2 1 443.10 506.72 55.24 o -22 2 1 0.71 0.48 25.09 o -20 2 1 164.72 137.68 31.62 o -18 2 1 2191.81 2148.04 69.66 o -16 2 1 322.01 348.27 34.01 o -14 2 1 2493.08 2790.77 68.54 o -12 2 1 381.98 389.83 32.76 o -10 2 1 1653.03 1808.83 44.01 o -8 2 1 4592.14 4259.82 49.40 o -6 2 1 269.42 288.44 14.52 o -4 2 1 18.16 22.12 6.80 o -2 2 1 25496.25 24801.82 136.66 o 0 2 1 4408.80 4169.55 41.63 o 2 2 1 3114.67 2826.71 27.98 o 4 2 1 30044.57 29383.67 146.58 o 6 2 1 157.07 137.59 11.78 o 8 2 1 12395.71 13435.62 190.42 o 10 2 1 54.19 112.76 18.17 o 12 2 1 372.05 312.46 26.47 o 14 2 1 192.10 138.20 24.71 o 16 2 1 369.77 368.23 35.11 o 18 2 1 19.02 30.02 23.54 o 20 2 1 19.39 12.11 24.75 o 22 2 1 2969.12 3235.23 104.77 o 24 2 1 5.20 36.87 31.47 o 26 2 1 221.31 208.86 46.15 o 28 2 1 69.53 56.49 45.21 o -27 3 1 59.45 49.66 35.64 o -25 3 1 2501.83 2567.34 93.56 o -23 3 1 270.53 214.89 38.88 o -21 3 1 4921.87 5081.61 112.78 o -19 3 1 1563.57 1624.67 65.05 o -17 3 1 1946.29 1936.85 65.36 o -15 3 1 130.32 117.81 24.86 o -13 3 1 4077.68 4315.85 83.67 o -11 3 1 2250.42 2003.59 55.15 o -9 3 1 6.76 8.36 14.74 o -7 3 1 11328.65 11716.00 92.87 o -5 3 1 844.97 700.68 20.97 o -3 3 1 6380.72 6084.91 52.45 o -1 3 1 3422.49 3560.42 33.35 o 1 3 1 4763.22 4670.86 38.46 o 3 3 1 1706.05 1562.63 25.65 o 5 3 1 259.41 224.10 15.60 o 7 3 1 47.55 109.16 15.68 o 9 3 1 0.86 6.86 13.53 o 11 3 1 6092.95 6326.80 93.39 o 13 3 1 7952.92 7700.58 119.77 o 15 3 1 1484.63 1464.65 55.30 o 17 3 1 4.33 5.94 21.32 o 19 3 1 4664.97 4811.38 104.84 o 21 3 1 78.56 54.02 29.24 o 23 3 1 31.32 24.28 29.51 o 25 3 1 547.00 581.75 57.58 o 27 3 1 86.33 86.39 46.03 o -26 4 1 83.88 68.20 36.78 o -24 4 1 1853.14 1854.00 80.92 o -22 4 1 1895.77 1909.53 76.66 o -20 4 1 259.59 205.28 35.79 o -18 4 1 33.11 29.90 24.05 o -16 4 1 2523.85 2515.36 80.11 o -14 4 1 8939.80 9176.82 126.53 o -12 4 1 3463.12 3554.81 76.68 o -10 4 1 161.20 124.37 21.72 o -8 4 1 18641.68 19281.51 149.99 o -6 4 1 4378.02 4608.40 80.40 o -4 4 1 5693.60 5722.22 68.97 o -2 4 1 3928.29 4389.64 54.54 o 0 4 1 3098.54 3364.54 49.43 o 2 4 1 5891.48 5983.78 79.50 o 4 4 1 4593.21 4375.23 66.52 o 6 4 1 24458.01 25610.62 154.11 o 8 4 1 2.78 -2.87 14.19 o 10 4 1 115.29 251.41 27.33 o 12 4 1 655.02 658.70 40.43 o 14 4 1 1094.88 1106.12 51.76 o 16 4 1 1868.54 1856.72 64.62 o 18 4 1 2108.66 2075.87 72.71 o 20 4 1 3288.58 3469.41 94.41 o 22 4 1 78.04 82.67 33.82 o 24 4 1 3.84 -8.01 31.94 o 26 4 1 391.61 462.74 62.50 o -25 5 1 665.31 681.70 61.62 o -23 5 1 400.99 408.70 48.62 o -21 5 1 291.54 277.36 40.34 o -19 5 1 12.20 20.06 24.65 o -17 5 1 494.97 479.24 44.36 o -15 5 1 795.76 739.40 47.98 o -13 5 1 3748.96 3821.69 84.26 o -11 5 1 735.52 795.04 54.69 o -9 5 1 972.76 1145.96 46.63 o -7 5 1 4069.25 4071.88 92.29 o -5 5 1 2534.11 2597.01 59.02 o -3 5 1 1610.08 1645.08 47.27 o -1 5 1 92.48 82.61 17.05 o 1 5 1 2959.86 3036.67 60.03 o 3 5 1 412.44 596.78 30.56 o 5 5 1 5719.88 6175.27 89.24 o 7 5 1 128.85 100.03 19.87 o 9 5 1 1395.45 1515.73 51.59 o 11 5 1 1282.98 1326.89 51.73 o 13 5 1 710.11 654.39 44.34 o 15 5 1 48.49 50.72 24.91 o 17 5 1 619.68 556.97 47.77 o 19 5 1 2983.56 2953.97 87.78 o 21 5 1 392.11 398.53 46.48 o 23 5 1 339.15 303.28 46.39 o 25 5 1 482.13 524.76 64.37 o -24 6 1 0.14 42.72 35.67 o -22 6 1 52.79 81.47 35.19 o -20 6 1 756.84 663.52 60.92 o -18 6 1 633.20 651.21 54.94 o -16 6 1 285.29 215.70 35.81 o -14 6 1 3.97 20.05 22.96 o -12 6 1 243.35 186.88 30.04 o -10 6 1 181.34 130.70 26.17 o -8 6 1 65.44 113.18 23.63 o -6 6 1 500.55 448.35 35.13 o -4 6 1 4262.31 4422.13 99.00 o -2 6 1 625.13 676.51 40.71 o 0 6 1 739.93 777.68 41.59 o 2 6 1 435.45 326.68 33.06 o 4 6 1 4.11 21.92 16.41 o 6 6 1 5.97 21.16 23.79 o 8 6 1 270.28 333.54 33.46 o 10 6 1 47.37 22.97 19.57 o 12 6 1 68.44 52.19 22.82 o 14 6 1 393.50 365.29 39.64 o 16 6 1 2.19 -1.80 24.04 o 18 6 1 15.92 28.58 26.96 o 20 6 1 11.24 7.72 28.51 o 22 6 1 146.63 115.67 38.91 o -21 7 1 10.17 25.01 35.39 o -19 7 1 4.55 7.87 32.16 o -17 7 1 165.17 158.36 38.15 o -15 7 1 1041.24 973.76 60.60 o -13 7 1 135.11 138.30 32.91 o -11 7 1 384.25 333.55 38.19 o -9 7 1 0.62 -1.99 20.82 o -7 7 1 23.01 7.73 19.91 o -5 7 1 504.00 375.96 36.41 o -3 7 1 664.01 588.68 44.30 o -1 7 1 42.89 61.94 23.71 o 1 7 1 1382.17 1347.74 57.25 o 3 7 1 4705.43 4461.32 95.15 o 5 7 1 70.73 63.75 23.67 o 7 7 1 49.64 46.15 23.50 o 9 7 1 1317.77 1088.21 56.70 o 11 7 1 1616.44 1670.35 65.92 o 13 7 1 12.29 12.83 24.35 o 15 7 1 305.11 376.62 45.01 o 17 7 1 0.72 -5.05 27.12 o 19 7 1 66.00 49.66 35.36 o 21 7 1 11.53 4.11 32.65 o -18 8 1 254.75 281.44 47.89 o -16 8 1 253.91 241.85 44.37 o -14 8 1 344.18 345.04 45.29 o -12 8 1 12.42 0.45 25.58 o -10 8 1 68.63 66.49 28.67 o -8 8 1 30.57 11.35 24.85 o -6 8 1 25.59 25.91 27.50 o -4 8 1 2186.24 2191.42 78.35 o -2 8 1 13.22 18.46 26.28 o 0 8 1 6.20 -2.11 22.51 o 2 8 1 66.50 64.56 28.15 o 4 8 1 171.69 195.47 35.42 o 6 8 1 109.56 106.72 29.38 o 8 8 1 593.19 562.78 49.29 o 10 8 1 370.94 346.36 42.32 o 12 8 1 314.25 363.80 45.12 o 14 8 1 180.58 150.76 37.63 o 16 8 1 231.28 227.00 42.90 o -13 9 1 6.67 10.19 30.82 o -11 9 1 278.95 283.85 47.08 o -9 9 1 203.93 207.07 41.49 o -7 9 1 436.70 385.94 50.37 o -5 9 1 781.92 927.13 66.91 o -3 9 1 300.96 320.99 47.38 o -1 9 1 1069.31 1074.08 69.62 o 1 9 1 125.86 83.65 35.39 o 3 9 1 1154.00 1313.78 73.64 o 5 9 1 800.81 874.47 71.46 o 7 9 1 111.38 159.37 40.80 o 9 9 1 192.58 225.59 45.21 o 11 9 1 2.00 6.82 33.73 o 13 9 1 1091.25 1199.35 80.93 o -4 10 1 897.19 929.53 87.73 o -2 10 1 396.27 366.04 61.82 o 0 10 1 19.28 29.91 44.08 o 2 10 1 814.30 815.04 82.97 o 4 10 1 6.28 -1.08 39.27 o -30 0 2 497.99 578.29 90.14 o -28 0 2 262.74 262.92 66.73 o -26 0 2 695.45 829.42 89.20 o -24 0 2 576.14 523.45 72.51 o -22 0 2 1430.96 1438.44 97.70 o -20 0 2 2900.19 2987.29 140.87 o -18 0 2 7879.52 7331.51 165.71 o -16 0 2 3260.35 3441.85 141.87 o -14 0 2 4240.95 3834.85 105.86 o -12 0 2 11747.17 10966.47 186.38 o -10 0 2 32260.50 37211.09 765.96 o -8 0 2 15.23 44.95 14.09 o -6 0 2 331819.97 305635.50 787.11 o -4 0 2 10759.69 10989.48 83.45 o 2 0 2 4462.91 4171.19 50.44 o 4 0 2 101059.59 95108.63 886.19 o 6 0 2 89334.45 85270.05 856.05 o 8 0 2 15581.76 16260.06 279.87 o 10 0 2 198.04 142.69 24.38 o 12 0 2 16013.64 16916.54 332.95 o 14 0 2 0.35 -12.08 21.14 o 16 0 2 95.41 59.79 27.20 o 18 0 2 2461.42 2549.47 106.33 o 20 0 2 1098.40 1077.12 83.33 o 22 0 2 1844.37 1749.03 103.70 o 24 0 2 329.57 339.36 65.34 o 26 0 2 1482.89 1507.06 135.23 o 28 0 2 4.36 -47.26 49.83 o -29 1 2 892.74 1050.53 77.15 o -27 1 2 54.06 40.44 33.93 o -25 1 2 1912.49 1823.56 78.97 o -23 1 2 522.48 366.59 48.26 o -21 1 2 18075.71 17689.76 197.74 o -19 1 2 4086.78 4316.34 96.06 o -17 1 2 9779.93 9633.64 183.06 o -15 1 2 2794.83 2515.95 65.76 o -13 1 2 1211.10 1022.02 42.44 o -11 1 2 1255.19 1300.74 33.55 o -9 1 2 32116.25 33756.63 324.92 o -7 1 2 486.30 576.26 18.72 o -5 1 2 2466.07 2431.95 27.83 o -3 1 2 1397.52 1319.43 15.79 o -1 1 2 2662.32 2818.72 27.64 o 1 1 2 10933.28 10559.46 55.18 o 3 1 2 69256.55 62996.59 438.88 o 5 1 2 234.62 318.29 13.54 o 7 1 2 0.76 13.95 8.38 o 9 1 2 1568.11 2081.73 40.14 o 11 1 2 3467.80 3786.08 62.94 o 13 1 2 360.21 298.98 24.47 o 15 1 2 3521.77 3535.45 66.49 o 17 1 2 164.53 137.86 29.10 o 19 1 2 7600.31 7759.27 127.97 o 21 1 2 1694.34 1614.82 68.60 o 23 1 2 74.65 50.21 31.31 o 25 1 2 81.55 67.34 38.83 o 27 1 2 689.40 575.02 72.11 o -30 2 2 56.94 27.47 71.19 o -28 2 2 17.73 7.77 35.11 o -26 2 2 285.63 363.26 48.79 o -24 2 2 1520.72 1407.01 72.40 o -22 2 2 481.54 480.87 46.31 o -20 2 2 1371.67 1357.84 61.44 o -18 2 2 3546.53 3446.03 84.85 o -16 2 2 2.53 -2.94 18.46 o -14 2 2 133.86 125.94 22.94 o -12 2 2 1263.73 1126.23 43.51 o -10 2 2 13.10 33.04 13.95 o -8 2 2 2821.84 3353.51 41.14 o -6 2 2 627.32 656.62 18.71 o -4 2 2 34331.52 33532.66 167.79 o -2 2 2 58426.54 56388.71 204.15 o 0 2 2 124.19 115.80 7.30 o 2 2 2 20885.93 20990.59 73.26 o 4 2 2 1596.85 1490.67 23.71 o 6 2 2 4272.44 4055.52 43.08 o 8 2 2 3431.26 3704.63 53.04 o 10 2 2 6859.74 7686.50 86.09 o 12 2 2 243.58 141.67 19.74 o 14 2 2 2470.33 2751.13 67.53 o 16 2 2 3.57 3.65 18.38 o 18 2 2 1340.60 1248.92 57.31 o 20 2 2 1623.38 1667.03 68.43 o 22 2 2 27.60 41.15 29.17 o 24 2 2 255.17 250.32 45.71 o 26 2 2 92.68 120.80 45.16 o 28 2 2 182.32 183.93 56.81 o -29 3 2 18.93 40.58 37.27 o -27 3 2 113.63 92.01 38.17 o -25 3 2 686.92 646.40 57.49 o -23 3 2 472.26 403.12 45.60 o -21 3 2 1710.07 1601.70 67.43 o -19 3 2 187.33 139.35 30.36 o -17 3 2 11.97 13.25 20.82 o -15 3 2 2347.26 2474.58 68.17 o -13 3 2 68.63 58.62 20.05 o -11 3 2 7203.68 7765.44 102.88 o -9 3 2 5961.34 5990.95 76.81 o -7 3 2 11418.47 11434.62 99.09 o -5 3 2 73.32 34.20 8.71 o -3 3 2 41253.24 41014.34 154.22 o -1 3 2 9746.18 10528.53 70.58 o 1 3 2 9744.95 10005.09 93.57 o 3 3 2 2778.34 2928.23 34.14 o 5 3 2 11.50 9.96 9.50 o 7 3 2 2128.90 2295.23 42.10 o 9 3 2 727.63 803.77 35.38 o 11 3 2 50.05 54.59 18.62 o 13 3 2 13.78 12.45 19.30 o 15 3 2 973.85 907.74 55.14 o 17 3 2 36.66 43.76 23.34 o 19 3 2 50.74 49.10 25.32 o 21 3 2 184.49 156.20 34.37 o 23 3 2 165.19 166.54 36.02 o 25 3 2 143.38 162.53 44.54 o 27 3 2 7.63 14.53 41.47 o -28 4 2 187.53 233.84 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