#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:24:07 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181231 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/09/2230907.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2230907_Fobs loop_ _publ_author_name 'Boeckmann, Jan' 'Reinert, Thorben' 'N\"ather, Christian' _publ_section_title ; Poly[bis(\m~2~-pyrimidine-\k^2^N:N')bis(selenocyanato-\kN)zinc] ; _journal_coeditor_code WM2498 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m948 _journal_volume 67 _journal_year 2011 _space_group_IT_number 64 _symmetry_space_group_name_Hall '-C 2ac 2' _symmetry_space_group_name_H-M 'C m c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.4025 _cell_length_b 16.7146 _cell_length_c 8.7886 _exptl_crystal_F_000 832.00 _reflns_d_resolution_high 0.8256 _cod_data_source_file wm2498Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Zn(SeCN)2(pyrimidine)2]n in Cmca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 267.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1, z+1/2' '-x+1/2, y+1, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x, y-1/2, -z-1/2' 'x, -y-1/2, z-1/2' '-x, y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, y, -z-1/2' 'x+1/2, -y, z-1/2' '-x+1/2, y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 71721.07 60046.78 119.01 o 8 0 0 22625.36 20570.39 2166.85 o 10 0 0 5458.12 5334.81 670.51 o 2 2 0 28.72 44.71 12.37 o 4 2 0 503.93 518.71 18.45 o 6 2 0 2211.28 2321.48 103.82 o 8 2 0 490.37 468.89 30.41 o 10 2 0 206.74 210.30 16.44 o 2 4 0 9492.10 8644.16 219.19 o 4 4 0 666.78 1071.74 221.62 o 6 4 0 5571.86 6284.17 222.01 o 8 4 0 68.47 87.27 9.96 o 10 4 0 150.98 117.95 13.69 o 4 6 0 49974.87 53701.11 1984.46 o 6 6 0 14587.85 14877.20 556.03 o 8 6 0 13756.55 14451.06 620.34 o 10 6 0 3511.64 3584.04 160.43 o 0 8 0 1150.81 1006.44 47.19 o 2 8 0 9681.00 10404.37 199.37 o 4 8 0 5049.32 5447.50 99.12 o 6 8 0 2188.54 2387.18 80.79 o 8 8 0 1740.62 1969.97 94.64 o 10 8 0 2249.10 2170.69 121.81 o 2 10 0 49.55 136.38 16.69 o 4 10 0 182.28 280.47 29.38 o 6 10 0 2092.39 2220.89 68.93 o 8 10 0 904.87 966.46 56.02 o 4 12 0 16819.97 17321.29 434.46 o 6 12 0 8932.87 9321.00 353.98 o 8 12 0 5435.44 5694.34 207.99 o 2 14 0 2131.22 2130.40 68.34 o 4 14 0 286.41 274.23 17.20 o 6 14 0 5826.15 5792.71 164.63 o 8 14 0 15.46 12.16 15.84 o 4 16 0 910.14 892.33 22.00 o 6 16 0 8.01 2.73 17.36 o 4 18 0 2702.13 3102.52 182.66 o 1 1 1 2919.32 2071.52 35.75 o 3 1 1 3381.19 3267.98 67.39 o 5 1 1 1611.41 1862.15 92.84 o 7 1 1 897.11 940.42 38.41 o 9 1 1 0.34 1.02 9.78 o 11 1 1 930.09 836.20 43.97 o 0 2 1 585.35 431.30 15.71 o 4 2 1 9502.38 9396.80 195.20 o 6 2 1 970.15 877.52 22.83 o 8 2 1 2581.42 2555.24 93.55 o 10 2 1 1777.53 1649.94 74.97 o 5 3 1 41966.91 39246.88 1023.29 o 7 3 1 21796.70 21559.57 722.68 o 9 3 1 10343.43 10196.40 370.17 o 11 3 1 3412.25 2939.52 165.31 o 0 4 1 2261.62 3266.66 733.22 o 2 4 1 390.33 373.71 25.63 o 4 4 1 44.24 116.82 9.96 o 6 4 1 1825.78 1868.83 59.62 o 8 4 1 10.91 7.58 11.66 o 10 4 1 1.72 28.38 9.44 o 1 5 1 102.69 87.77 11.32 o 3 5 1 1628.63 1709.66 32.48 o 5 5 1 217.03 215.75 13.26 o 7 5 1 481.35 486.03 16.68 o 9 5 1 919.80 946.93 36.02 o 0 6 1 9635.43 10067.04 135.41 o 2 6 1 170.58 200.33 11.08 o 4 6 1 3178.48 3502.77 61.75 o 6 6 1 131.00 129.35 8.55 o 8 6 1 1306.76 1405.79 50.02 o 10 6 1 4.00 0.24 12.53 o 1 7 1 3111.79 3176.56 60.42 o 3 7 1 1503.76 1609.80 28.16 o 5 7 1 621.09 729.36 17.01 o 7 7 1 190.79 226.36 11.86 o 9 7 1 8.51 30.17 10.50 o 0 8 1 696.47 947.40 27.13 o 2 8 1 2760.50 2960.57 28.14 o 4 8 1 129.78 166.90 21.20 o 6 8 1 105.18 333.36 78.23 o 8 8 1 31.60 34.85 11.63 o 10 8 1 147.50 132.45 12.18 o 3 9 1 49703.46 50714.84 136.49 o 5 9 1 20871.08 21673.52 307.57 o 7 9 1 11128.43 12037.44 267.64 o 9 9 1 7878.58 7580.51 215.83 o 0 10 1 30.88 58.85 22.78 o 2 10 1 275.66 301.46 11.75 o 4 10 1 362.43 344.30 10.25 o 6 10 1 5.38 9.67 8.66 o 8 10 1 34.12 77.90 17.97 o 1 11 1 3984.95 3963.42 61.68 o 3 11 1 8013.72 8460.97 119.22 o 5 11 1 1971.25 1992.04 34.18 o 7 11 1 1791.07 1848.60 47.39 o 9 11 1 2319.02 2284.02 59.19 o 0 12 1 367.89 384.81 25.15 o 2 12 1 12.86 24.68 12.90 o 4 12 1 1398.29 1443.65 29.12 o 6 12 1 2313.19 2492.22 47.31 o 8 12 1 964.59 967.17 24.34 o 1 13 1 899.00 840.45 21.84 o 3 13 1 1756.92 1789.16 32.21 o 5 13 1 161.03 181.28 11.00 o 7 13 1 28.07 26.68 10.01 o 0 14 1 1594.67 1468.82 74.43 o 2 14 1 353.64 380.04 16.96 o 4 14 1 121.25 140.38 11.77 o 6 14 1 802.39 803.92 21.57 o 8 14 1 2.54 18.26 11.21 o 1 15 1 12385.52 13729.11 256.79 o 3 15 1 5571.95 6491.34 108.15 o 5 15 1 7490.32 7730.01 142.91 o 7 15 1 3845.99 3742.42 132.58 o 2 16 1 23.38 36.31 19.87 o 4 16 1 115.43 120.24 13.16 o 6 16 1 263.07 252.18 11.75 o 3 17 1 1696.61 1603.69 68.01 o 5 17 1 1403.68 1315.03 37.15 o 4 18 1 197.47 154.00 20.79 o 0 0 2 19104.72 15960.14 432.07 o 4 0 2 23066.69 19028.00 462.97 o 6 0 2 26297.35 24086.26 1002.77 o 8 0 2 7138.14 6603.46 365.77 o 10 0 2 7191.63 6772.60 397.24 o 1 1 2 18827.78 14643.11 180.18 o 3 1 2 84.76 65.14 9.63 o 5 1 2 6734.54 6267.52 168.06 o 7 1 2 2329.26 2203.25 81.62 o 9 1 2 13.56 8.36 11.02 o 11 1 2 652.68 542.51 27.66 o 0 2 2 60.95 79.21 9.45 o 2 2 2 1262.17 1030.19 20.19 o 4 2 2 624.70 610.94 15.52 o 6 2 2 585.16 576.48 20.19 o 8 2 2 466.08 442.43 21.43 o 10 2 2 745.41 640.77 25.46 o 1 3 2 873.38 773.54 10.84 o 3 3 2 8524.08 8822.23 123.64 o 5 3 2 559.50 583.36 17.75 o 7 3 2 84.73 80.64 8.79 o 9 3 2 994.73 1024.78 38.12 o 11 3 2 133.14 108.14 12.23 o 0 4 2 16.32 59.62 17.44 o 2 4 2 1651.73 1500.50 20.47 o 4 4 2 6.34 13.89 9.53 o 6 4 2 1728.66 1864.65 44.23 o 8 4 2 115.58 113.11 10.07 o 10 4 2 1025.84 939.10 40.70 o 1 5 2 11888.39 11512.42 177.79 o 3 5 2 10642.77 10441.13 162.40 o 5 5 2 4851.82 4976.44 110.97 o 7 5 2 1734.50 1757.11 45.69 o 9 5 2 1217.34 1142.26 36.60 o 4 6 2 27927.87 26943.80 450.11 o 6 6 2 27411.36 28132.71 594.62 o 8 6 2 8044.09 8439.72 250.20 o 10 6 2 6023.52 5876.19 216.61 o 1 7 2 10301.19 11090.50 237.74 o 3 7 2 3071.64 3035.53 53.20 o 5 7 2 3869.92 3814.11 83.81 o 7 7 2 1970.85 1842.08 53.92 o 9 7 2 302.04 312.44 15.83 o 0 8 2 3286.42 3554.01 64.83 o 2 8 2 654.31 620.10 17.82 o 4 8 2 1877.12 1954.56 37.93 o 6 8 2 855.72 890.90 21.61 o 8 8 2 870.48 947.57 28.41 o 10 8 2 180.63 214.14 11.05 o 1 9 2 3229.43 3558.81 69.68 o 3 9 2 767.59 754.70 12.01 o 5 9 2 1917.32 1941.19 30.83 o 7 9 2 570.42 609.51 18.16 o 9 9 2 73.74 70.62 11.67 o 0 10 2 951.53 929.81 24.07 o 2 10 2 1274.70 1410.37 17.31 o 4 10 2 1172.10 1121.88 15.98 o 6 10 2 8.41 18.75 11.43 o 8 10 2 137.29 150.17 9.48 o 1 11 2 8321.94 8183.83 272.18 o 3 11 2 669.39 700.27 11.34 o 5 11 2 4172.09 4128.49 75.90 o 7 11 2 1807.32 1813.27 35.53 o 9 11 2 10.61 19.53 11.42 o 0 12 2 24121.96 23358.76 185.76 o 2 12 2 19581.88 20763.32 567.14 o 4 12 2 14906.99 15211.91 268.52 o 6 12 2 9288.40 9536.04 199.95 o 8 12 2 5178.98 5364.33 111.90 o 1 13 2 24.03 38.65 13.88 o 3 13 2 2737.00 2813.97 45.42 o 5 13 2 128.25 143.60 10.40 o 7 13 2 14.42 28.37 10.24 o 0 14 2 5053.46 4645.04 203.35 o 2 14 2 2569.68 2499.57 61.48 o 4 14 2 5378.63 5597.21 140.00 o 6 14 2 705.24 703.19 15.64 o 1 15 2 458.17 465.13 18.13 o 3 15 2 242.80 263.46 15.12 o 5 15 2 282.29 270.05 10.72 o 7 15 2 61.15 54.27 11.19 o 0 16 2 1148.03 1134.72 30.67 o 2 16 2 480.82 529.91 28.30 o 4 16 2 331.94 305.86 12.92 o 6 16 2 203.16 196.56 11.82 o 1 17 2 564.32 666.61 21.32 o 3 17 2 1389.95 1366.41 82.44 o 5 17 2 169.21 202.78 12.29 o 0 18 2 5403.50 5742.66 494.97 o 2 18 2 2412.84 2652.69 119.34 o 4 18 2 3891.26 3743.89 311.94 o 3 19 2 219.74 231.17 20.31 o 1 1 3 1887.47 2084.00 14.20 o 3 1 3 7284.94 7044.59 145.28 o 5 1 3 330.50 367.02 9.81 o 7 1 3 12.25 10.68 8.88 o 9 1 3 2295.91 2221.08 81.86 o 0 2 3 12650.19 12404.98 331.43 o 2 2 3 13787.99 12901.31 209.28 o 4 2 3 16987.00 16015.88 241.87 o 6 2 3 1261.30 1123.00 21.28 o 8 2 3 3854.51 3770.07 115.83 o 10 2 3 265.81 257.37 18.36 o 3 3 3 32615.75 29393.66 571.56 o 5 3 3 26182.66 24729.62 467.07 o 7 3 3 11839.17 11434.25 263.03 o 9 3 3 4873.41 4711.07 152.47 o 0 4 3 18138.00 19169.73 517.78 o 2 4 3 7173.44 6507.19 97.39 o 4 4 3 8102.28 7688.29 137.06 o 6 4 3 3891.99 3831.82 94.93 o 8 4 3 1502.59 1411.03 38.63 o 10 4 3 316.32 291.71 16.89 o 1 5 3 8658.43 9094.40 111.70 o 3 5 3 1971.40 1848.28 32.25 o 5 5 3 4824.60 5064.27 106.06 o 7 5 3 2729.96 2739.75 71.28 o 9 5 3 724.25 663.16 19.95 o 0 6 3 93.45 120.29 14.71 o 2 6 3 1959.67 2019.80 35.83 o 4 6 3 99.88 125.14 10.18 o 6 6 3 711.24 683.13 19.75 o 8 6 3 72.73 65.69 9.37 o 10 6 3 104.92 117.42 14.36 o 1 7 3 336.97 396.09 10.33 o 3 7 3 62.00 116.69 21.22 o 5 7 3 246.41 257.75 10.14 o 7 7 3 611.76 1130.14 222.10 o 9 7 3 282.71 254.74 11.55 o 0 8 3 12487.93 12850.36 110.42 o 2 8 3 8901.07 8572.56 122.58 o 4 8 3 10453.30 10978.60 243.84 o 6 8 3 1938.69 1961.28 42.21 o 8 8 3 2842.85 2776.20 68.98 o 1 9 3 26216.65 27147.18 922.02 o 3 9 3 8847.49 8739.61 236.82 o 5 9 3 14629.69 15063.19 285.02 o 7 9 3 7707.99 8224.07 210.44 o 9 9 3 1403.76 1479.79 50.40 o 0 10 3 5150.90 5413.81 53.49 o 2 10 3 5952.85 6042.44 106.86 o 4 10 3 4060.36 4086.31 107.93 o 6 10 3 2266.15 2398.95 56.68 o 8 10 3 929.83 806.19 28.89 o 1 11 3 3937.77 3930.51 45.94 o 3 11 3 157.64 169.50 10.17 o 5 11 3 2903.79 3183.20 80.41 o 7 11 3 1370.47 1438.03 29.60 o 9 11 3 56.21 62.64 13.96 o 0 12 3 20.88 42.69 17.38 o 2 12 3 4762.98 4798.18 90.04 o 4 12 3 390.14 410.78 11.26 o 6 12 3 731.38 708.87 17.64 o 8 12 3 105.31 107.09 11.41 o 1 13 3 515.65 455.29 14.55 o 3 13 3 49.40 52.10 11.70 o 5 13 3 194.24 216.45 11.43 o 7 13 3 5.61 23.29 11.30 o 0 14 3 8425.15 8266.04 40.95 o 2 14 3 5133.61 5348.90 140.69 o 4 14 3 4381.04 4656.60 89.43 o 6 14 3 2893.83 2884.21 77.08 o 1 15 3 5632.31 5474.08 123.23 o 3 15 3 11516.77 12056.39 329.47 o 5 15 3 2960.28 2913.38 88.04 o 0 16 3 574.96 622.71 23.36 o 2 16 3 341.51 392.39 15.70 o 4 16 3 181.61 205.36 12.91 o 6 16 3 333.31 385.18 19.82 o 1 17 3 2994.74 2685.71 108.16 o 3 17 3 3174.48 3008.87 173.63 o 5 17 3 2032.64 1831.90 66.75 o 0 18 3 1207.71 1153.99 43.08 o 2 18 3 2162.82 1934.97 128.17 o 4 18 3 616.75 577.62 53.49 o 1 19 3 81.32 75.78 19.25 o 0 0 4 14066.75 12836.14 427.14 o 2 0 4 22029.79 19549.53 668.89 o 4 0 4 36723.12 36535.15 1440.61 o 6 0 4 593.03 582.05 25.23 o 8 0 4 14248.87 13856.46 538.56 o 10 0 4 1759.68 1728.04 115.94 o 1 1 4 19496.49 19092.70 241.52 o 3 1 4 22012.41 20799.79 442.86 o 5 1 4 7100.48 6848.64 177.41 o 7 1 4 3871.65 3509.33 105.03 o 9 1 4 2592.58 2381.63 77.85 o 0 2 4 882.92 785.45 38.19 o 2 2 4 3153.40 3131.15 25.55 o 4 2 4 3637.01 3700.09 84.39 o 6 2 4 427.20 395.61 14.56 o 8 2 4 1791.74 1747.31 56.66 o 10 2 4 753.30 673.41 33.00 o 1 3 4 123.17 181.04 30.51 o 3 3 4 2970.54 3055.55 45.98 o 5 3 4 32.49 163.01 55.65 o 7 3 4 26.82 26.72 9.85 o 9 3 4 426.59 388.15 18.74 o 0 4 4 7284.89 7656.62 176.74 o 2 4 4 10.69 46.39 8.55 o 4 4 4 1390.46 1402.92 25.03 o 6 4 4 1180.36 1181.69 30.23 o 8 4 4 441.67 395.27 15.75 o 10 4 4 160.03 115.32 11.27 o 1 5 4 21280.64 22174.59 314.46 o 3 5 4 12655.20 12626.35 151.87 o 5 5 4 8371.24 8389.79 181.06 o 7 5 4 4528.85 4749.26 158.42 o 9 5 4 1268.16 1152.65 35.30 o 0 6 4 33155.96 34165.25 471.10 o 2 6 4 14224.98 13490.20 136.58 o 4 6 4 18058.25 18739.71 422.27 o 6 6 4 7215.04 7700.81 186.02 o 8 6 4 6562.95 6641.93 178.78 o 10 6 4 1226.07 1181.23 59.27 o 1 7 4 8472.71 8766.01 107.29 o 3 7 4 7778.32 7981.06 99.16 o 5 7 4 3545.73 3444.77 64.94 o 7 7 4 1823.97 1965.18 63.94 o 9 7 4 1076.63 1026.48 41.54 o 0 8 4 7601.95 7758.50 35.08 o 2 8 4 6189.58 6530.81 71.55 o 4 8 4 2827.20 2916.77 52.15 o 6 8 4 5259.82 5580.55 118.37 o 8 8 4 1487.78 1471.26 39.64 o 1 9 4 1133.78 1164.46 26.04 o 3 9 4 1450.32 1431.49 27.01 o 5 9 4 443.10 434.73 8.28 o 7 9 4 268.09 295.54 9.48 o 9 9 4 156.70 170.70 11.67 o 0 10 4 2483.60 2569.26 22.05 o 2 10 4 403.50 365.55 9.71 o 4 10 4 0.16 19.00 8.52 o 6 10 4 1145.41 1107.35 37.23 o 8 10 4 2.88 11.75 10.24 o 1 11 4 9334.72 9254.00 91.28 o 3 11 4 11654.90 11708.87 186.76 o 5 11 4 4041.00 4307.25 135.21 o 7 11 4 2161.14 2172.70 55.71 o 0 12 4 4903.99 4588.72 111.46 o 2 12 4 3470.10 3325.77 54.02 o 4 12 4 2486.53 2628.53 37.84 o 6 12 4 2383.44 2461.57 77.46 o 8 12 4 714.10 723.67 22.47 o 1 13 4 3844.27 3936.94 44.61 o 3 13 4 787.05 850.87 18.99 o 5 13 4 2091.80 2066.79 41.19 o 7 13 4 1045.51 994.04 31.77 o 0 14 4 232.72 230.69 20.92 o 2 14 4 6836.35 6668.26 201.11 o 4 14 4 1990.34 2027.20 43.17 o 6 14 4 914.57 908.15 29.98 o 1 15 4 2375.52 2318.34 41.04 o 3 15 4 2077.24 1888.98 40.19 o 5 15 4 1188.96 1181.12 32.72 o 0 16 4 107.68 144.93 19.34 o 2 16 4 816.39 778.61 24.76 o 4 16 4 878.70 860.96 26.83 o 1 17 4 3625.48 3502.84 104.28 o 3 17 4 2114.25 2091.08 125.33 o 0 18 4 1200.21 1099.30 25.51 o 2 18 4 2581.13 2189.84 76.83 o 1 1 5 2839.12 2835.03 22.21 o 3 1 5 3774.70 3628.97 63.54 o 5 1 5 1848.80 1917.24 56.93 o 7 1 5 1411.68 1478.02 47.53 o 9 1 5 1061.60 973.85 38.34 o 0 2 5 37101.14 37276.90 1178.18 o 2 2 5 14118.60 13388.15 137.09 o 4 2 5 6477.56 6458.65 169.54 o 6 2 5 17866.30 18110.00 498.03 o 8 2 5 571.98 565.20 22.03 o 1 3 5 10367.50 10201.56 208.16 o 3 3 5 7300.17 7361.10 158.26 o 5 3 5 5771.19 5890.12 152.99 o 7 3 5 3526.69 3876.47 122.20 o 9 3 5 1874.87 2033.55 66.83 o 0 4 5 9277.44 9108.20 196.06 o 2 4 5 21961.23 22210.88 243.02 o 4 4 5 12778.56 12594.70 296.28 o 6 4 5 3953.08 4164.87 125.44 o 8 4 5 2862.56 2869.40 95.63 o 1 5 5 6832.74 7098.71 161.30 o 3 5 5 5344.72 5395.30 84.58 o 5 5 5 4293.88 4588.19 102.40 o 7 5 5 2673.34 2876.63 94.52 o 9 5 5 1445.41 1400.65 54.61 o 0 6 5 3751.74 4122.40 102.34 o 2 6 5 608.38 579.20 11.41 o 4 6 5 3193.85 3385.19 44.05 o 6 6 5 114.47 150.04 9.68 o 8 6 5 888.28 898.49 22.46 o 1 7 5 1905.65 1956.61 41.20 o 3 7 5 1929.78 1957.63 25.79 o 5 7 5 1306.46 1332.26 32.51 o 7 7 5 988.93 1010.25 33.02 o 9 7 5 677.43 595.96 21.50 o 0 8 5 21850.74 21730.84 124.87 o 2 8 5 17548.74 18375.82 286.77 o 4 8 5 8788.42 9144.44 117.46 o 6 8 5 10940.57 11650.01 324.68 o 8 8 5 1273.97 1475.03 50.87 o 1 9 5 3702.92 3646.85 43.76 o 3 9 5 2623.41 2637.83 65.96 o 5 9 5 2230.29 2286.73 44.16 o 7 9 5 1414.74 1564.46 38.56 o 0 10 5 3724.33 3653.77 50.25 o 2 10 5 1966.86 1941.72 32.87 o 4 10 5 1519.83 1589.46 37.66 o 6 10 5 1032.35 1054.95 22.86 o 8 10 5 317.26 313.66 14.61 o 1 11 5 4030.08 3920.48 38.58 o 3 11 5 2837.76 3011.63 49.85 o 5 11 5 2709.04 2698.56 80.57 o 7 11 5 1626.19 1750.58 53.38 o 0 12 5 13565.67 13759.10 240.26 o 2 12 5 251.82 246.91 10.41 o 4 12 5 2135.60 2262.03 49.66 o 6 12 5 2581.38 2631.30 52.20 o 1 13 5 1116.23 1155.72 13.14 o 3 13 5 1167.91 1209.46 28.97 o 5 13 5 844.92 864.37 27.71 o 0 14 5 1815.16 1794.42 22.07 o 2 14 5 4529.91 4381.57 50.14 o 4 14 5 2612.40 2589.46 53.40 o 6 14 5 505.22 522.34 18.90 o 1 15 5 1121.46 1065.49 16.03 o 3 15 5 1296.75 1185.82 22.22 o 5 15 5 705.13 694.33 22.94 o 0 16 5 233.65 233.41 22.41 o 2 16 5 878.85 871.02 30.24 o 4 16 5 719.13 691.77 18.87 o 1 17 5 1394.61 1198.31 18.39 o 3 17 5 1200.31 998.37 29.76 o 0 0 6 3106.76 3067.95 60.38 o 2 0 6 2149.83 2114.19 65.07 o 4 0 6 16.28 23.78 9.99 o 6 0 6 7205.83 8169.21 388.41 o 8 0 6 62.53 53.85 15.71 o 1 1 6 16007.60 15879.27 232.25 o 3 1 6 20594.28 20111.42 237.88 o 5 1 6 6599.25 6952.47 180.41 o 7 1 6 3984.94 4273.48 141.46 o 9 1 6 3046.95 2930.70 138.01 o 0 2 6 9972.12 10277.43 161.27 o 2 2 6 6481.56 6504.28 47.75 o 4 2 6 3815.53 3820.73 59.98 o 6 2 6 5329.00 5623.51 173.65 o 8 2 6 1520.63 1457.39 47.39 o 1 3 6 613.83 642.69 15.92 o 3 3 6 4061.53 4041.85 40.79 o 5 3 6 203.66 236.13 14.04 o 7 3 6 215.39 267.24 10.53 o 9 3 6 919.91 892.54 51.38 o 0 4 6 2839.47 2791.62 48.75 o 2 4 6 9548.91 10205.02 161.78 o 4 4 6 3867.45 4076.62 77.91 o 6 4 6 2960.24 3046.06 59.57 o 8 4 6 2038.06 1972.26 62.71 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4823.34 59.45 o 3 1 8 957.42 953.79 12.04 o 5 1 8 2512.36 2574.53 51.88 o 7 1 8 926.79 1047.26 27.68 o 0 2 8 9926.31 10801.77 240.03 o 2 2 8 6381.59 6411.82 107.47 o 4 2 8 5710.87 5928.78 98.25 o 6 2 8 3856.86 4076.89 91.21 o 1 3 8 161.28 193.92 11.17 o 3 3 8 692.42 676.22 14.58 o 5 3 8 114.76 127.89 13.26 o 7 3 8 19.77 30.84 10.83 o 0 4 8 6892.86 7412.69 215.79 o 2 4 8 6041.83 5996.25 145.84 o 4 4 8 6213.85 6175.27 113.68 o 6 4 8 1708.86 1720.17 48.50 o 1 5 8 4421.38 4480.20 110.26 o 3 5 8 4138.53 4117.85 116.83 o 5 5 8 2273.19 2446.40 47.41 o 0 6 8 480.54 509.41 13.37 o 2 6 8 1533.14 1583.57 42.03 o 4 6 8 85.00 98.46 10.26 o 6 6 8 469.92 464.80 17.88 o 1 7 8 3579.70 3408.30 102.39 o 3 7 8 1878.35 1846.08 52.41 o 5 7 8 2037.54 2143.15 61.26 o 0 8 8 3684.90 3547.79 45.97 o 2 8 8 4881.56 4618.20 92.08 o 4 8 8 2972.18 3132.41 82.48 o 6 8 8 2495.74 2517.96 66.16 o 1 9 8 1625.12 1598.31 21.54 o 3 9 8 676.51 676.21 19.06 o 5 9 8 988.76 992.09 21.11 o 0 10 8 5988.14 5637.27 84.38 o 2 10 8 7550.15 7329.70 183.57 o 4 10 8 6439.65 6386.14 143.96 o 1 11 8 4471.23 4308.92 40.25 o 3 11 8 1189.56 1102.68 29.06 o 0 12 8 429.43 417.54 18.55 o 2 12 8 123.34 149.80 13.30 o 1 13 8 7.36 18.46 10.11 o 1 1 9 5697.41 5668.39 79.62 o 3 1 9 7325.33 7226.14 182.58 o 5 1 9 3144.53 3215.90 69.28 o 0 2 9 500.34 437.45 19.70 o 2 2 9 6217.45 6079.25 122.64 o 4 2 9 2493.58 2724.68 57.75 o 1 3 9 1211.00 1274.73 31.69 o 3 3 9 954.76 867.79 33.06 o 5 3 9 324.79 318.19 15.65 o 0 4 9 1206.67 1118.62 13.96 o 2 4 9 466.82 425.22 12.62 o 4 4 9 151.01 210.95 21.98 o 1 5 9 6068.81 5803.47 165.65 o 3 5 9 4500.15 4289.27 135.31 o 5 5 9 3827.00 3352.75 111.49 o 0 6 9 1591.81 1577.81 58.33 o 2 6 9 349.96 327.56 12.90 o 4 6 9 1079.63 1189.82 31.11 o 1 7 9 7824.73 8161.39 121.04 o 3 7 9 5954.62 5816.36 130.31 o 0 8 9 120.36 355.17 106.54 o 2 8 9 1611.67 1509.18 48.50 o 4 8 9 319.19 344.29 16.34 o 1 9 9 912.56 882.24 21.09 o 3 9 9 1419.52 1298.23 35.58 o 0 10 9 116.87 93.86 14.06 o 2 10 9 105.08 73.24 11.70 o 0 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