#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:24:51 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181232 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/10/2231030.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231030_Fobs loop_ _publ_author_name 'Kubono, Koji' 'Synmyouzu, Teruo' 'Goto, Kenta' 'Tsujioka, Tsuyoshi' 'Tani, Keita' _publ_section_title ; 1,2-Bis[5-(9-ethyl-9H-carbazol-3-yl)-2-methylthiophen-3-yl]-3,3,4,4,5,5-hexafluorocyclopentene ; _journal_coeditor_code BV2188 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2194 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.798 _cell_angle_gamma 90.000 _cell_length_a 14.6687 _cell_length_b 17.0977 _cell_length_c 14.0017 _exptl_crystal_F_000 1560.00 _reflns_d_resolution_high 0.8300 _cod_data_source_file bv2188Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 3CZ-DAE_9' _shelx_refln_list_code 4 _shelx_f_calc_maximum 308.85 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6813.18 7756.01 143.11 o 2 0 0 600.14 602.95 6.55 o 3 0 0 29096.49 36080.24 986.50 o 4 0 0 7572.58 8302.44 129.78 o 5 0 0 3528.71 4016.82 53.33 o 6 0 0 1365.77 1713.93 22.52 o 7 0 0 3188.25 3066.48 39.53 o 8 0 0 5485.61 4559.55 80.07 o 9 0 0 9279.58 7859.92 172.02 o 10 0 0 609.35 495.03 28.75 o 11 0 0 390.59 334.82 37.22 o 12 0 0 897.33 889.62 51.11 o 13 0 0 567.79 544.83 34.36 o 14 0 0 2195.77 2046.43 83.40 o 15 0 0 442.43 492.73 29.13 o 16 0 0 2.02 -4.87 10.62 o 17 0 0 243.02 227.49 61.57 o 1 1 0 1144.76 1233.48 11.99 o 2 1 0 6177.72 7348.57 81.06 o 3 1 0 9823.70 10507.05 195.70 o 4 1 0 10106.32 10943.43 135.91 o 5 1 0 207.96 218.27 6.85 o 6 1 0 2325.91 2052.78 17.77 o 7 1 0 820.08 790.51 8.89 o 8 1 0 4662.90 4085.85 44.25 o 9 1 0 56.77 103.27 4.22 o 10 1 0 479.53 397.93 18.53 o 11 1 0 3150.25 3257.35 92.28 o 12 1 0 2.54 15.95 9.47 o 13 1 0 718.93 683.48 34.42 o 14 1 0 2.00 23.32 11.19 o 15 1 0 9.70 4.28 9.02 o 16 1 0 7.73 5.41 7.87 o 17 1 0 378.67 343.81 15.08 o 0 2 0 8021.74 9132.49 146.81 o 1 2 0 17701.53 21301.37 302.69 o 2 2 0 6381.37 7212.33 76.36 o 3 2 0 6056.71 6819.92 71.69 o 4 2 0 692.31 620.51 7.67 o 5 2 0 698.35 870.26 10.04 o 6 2 0 2366.72 2586.74 30.40 o 7 2 0 418.02 345.12 4.87 o 8 2 0 1231.68 1310.80 14.41 o 9 2 0 1.38 19.37 3.71 o 10 2 0 583.39 525.16 17.30 o 11 2 0 20.33 16.04 10.33 o 12 2 0 296.50 247.80 17.37 o 13 2 0 377.00 423.82 21.24 o 14 2 0 64.29 76.65 12.94 o 15 2 0 10.50 15.35 11.91 o 16 2 0 1.36 1.51 7.43 o 17 2 0 275.88 269.96 13.36 o 1 3 0 226.76 267.18 4.27 o 2 3 0 17256.38 19466.70 282.23 o 3 3 0 1561.31 1868.65 19.80 o 4 3 0 640.29 586.21 7.69 o 5 3 0 1584.53 1477.04 16.72 o 6 3 0 62.58 60.88 3.52 o 7 3 0 1833.52 1852.85 20.37 o 8 3 0 170.15 137.19 3.82 o 9 3 0 97.41 57.13 4.36 o 10 3 0 121.20 166.79 11.99 o 11 3 0 3750.16 3594.37 88.61 o 12 3 0 1426.73 1541.57 49.78 o 13 3 0 1115.71 963.21 38.52 o 14 3 0 192.09 266.24 18.03 o 15 3 0 2.75 0.48 7.97 o 16 3 0 573.73 650.84 24.86 o 17 3 0 280.82 303.71 12.72 o 0 4 0 85114.08 99876.20 4948.33 o 1 4 0 23126.79 28042.87 483.82 o 2 4 0 961.12 1069.51 12.95 o 3 4 0 599.63 715.05 8.35 o 4 4 0 702.44 594.77 8.04 o 5 4 0 3651.98 3696.13 41.26 o 6 4 0 127.39 72.22 3.40 o 7 4 0 3411.10 3583.98 41.78 o 8 4 0 6.63 40.91 2.83 o 9 4 0 40.92 35.31 3.76 o 10 4 0 45.45 77.03 10.28 o 11 4 0 573.14 623.74 23.16 o 12 4 0 19.54 18.86 9.73 o 13 4 0 2316.45 2448.95 69.95 o 14 4 0 535.52 596.02 23.84 o 15 4 0 19.75 1.68 8.37 o 16 4 0 208.16 218.06 13.65 o 17 4 0 559.34 568.76 16.81 o 1 5 0 21904.78 23762.26 389.21 o 2 5 0 183.46 342.50 4.88 o 3 5 0 2168.16 1813.52 28.90 o 4 5 0 660.32 789.56 11.36 o 5 5 0 368.67 426.23 6.95 o 6 5 0 3712.07 3774.05 47.04 o 7 5 0 234.54 222.54 5.91 o 8 5 0 2184.10 2023.78 27.00 o 9 5 0 207.99 212.08 7.14 o 10 5 0 1077.07 1049.24 30.48 o 11 5 0 28.30 26.79 8.54 o 12 5 0 159.88 180.43 12.94 o 13 5 0 228.16 264.63 17.82 o 14 5 0 16.46 15.07 9.14 o 15 5 0 89.58 106.46 11.99 o 16 5 0 58.29 75.44 8.89 o 17 5 0 1.43 0.25 5.25 o 0 6 0 17437.07 17700.62 394.86 o 1 6 0 902.34 1345.08 17.83 o 2 6 0 397.26 230.04 6.86 o 3 6 0 5018.64 4534.82 49.39 o 4 6 0 5449.91 5451.21 62.25 o 5 6 0 3511.70 3637.96 43.09 o 6 6 0 273.92 213.48 5.09 o 7 6 0 6036.80 5732.14 75.78 o 8 6 0 179.42 219.54 9.65 o 9 6 0 773.12 901.24 19.43 o 10 6 0 41.73 43.06 6.87 o 11 6 0 0.27 -5.42 9.19 o 12 6 0 1675.73 1724.49 45.62 o 13 6 0 558.84 494.12 27.31 o 14 6 0 779.47 692.87 24.69 o 15 6 0 1218.65 1241.67 39.11 o 16 6 0 8.43 4.11 7.17 o 1 7 0 191.84 67.59 2.81 o 2 7 0 26.95 3.67 1.99 o 3 7 0 206.08 273.72 5.42 o 4 7 0 2635.59 2477.54 36.81 o 5 7 0 5732.18 5535.84 79.43 o 6 7 0 7.58 8.92 2.84 o 7 7 0 806.95 663.78 12.74 o 8 7 0 147.23 164.33 9.35 o 9 7 0 1225.62 1213.32 35.96 o 10 7 0 419.39 414.92 13.46 o 11 7 0 32.70 86.40 11.57 o 12 7 0 163.47 183.17 12.98 o 13 7 0 578.66 588.74 21.12 o 14 7 0 10.99 0.82 6.19 o 15 7 0 284.23 292.21 16.48 o 16 7 0 191.33 193.69 9.90 o 0 8 0 5169.01 5635.61 100.21 o 1 8 0 202.23 273.86 4.85 o 2 8 0 2448.75 2901.25 27.41 o 3 8 0 799.74 758.17 12.32 o 4 8 0 112.77 119.24 4.16 o 5 8 0 1.02 10.86 2.70 o 6 8 0 366.00 279.32 7.68 o 7 8 0 1040.98 932.23 21.38 o 8 8 0 342.42 420.68 13.43 o 9 8 0 93.49 70.77 10.91 o 10 8 0 101.79 122.76 8.85 o 11 8 0 327.55 306.39 13.68 o 12 8 0 2402.92 2278.59 62.68 o 13 8 0 243.48 262.99 14.10 o 14 8 0 153.35 178.09 11.26 o 15 8 0 230.82 213.14 13.61 o 16 8 0 72.50 54.19 8.65 o 1 9 0 3564.52 3467.06 34.77 o 2 9 0 474.55 658.59 7.79 o 3 9 0 396.71 571.25 7.78 o 4 9 0 864.47 757.26 10.49 o 5 9 0 1430.72 1331.62 21.82 o 6 9 0 1671.82 1488.17 28.21 o 7 9 0 174.06 111.35 5.78 o 8 9 0 3350.37 3375.13 67.93 o 9 9 0 592.27 642.65 20.32 o 10 9 0 2393.63 2423.57 51.72 o 11 9 0 329.83 318.30 13.80 o 12 9 0 121.63 125.66 13.05 o 13 9 0 267.07 287.07 14.52 o 14 9 0 149.54 132.42 9.61 o 15 9 0 66.36 73.84 10.29 o 0 10 0 211.83 167.72 5.31 o 1 10 0 2193.86 2592.96 26.36 o 2 10 0 790.61 845.02 10.61 o 3 10 0 307.74 234.75 7.44 o 4 10 0 685.29 606.95 9.24 o 5 10 0 774.23 583.67 10.60 o 6 10 0 394.87 469.10 12.11 o 7 10 0 13.30 15.67 5.28 o 8 10 0 196.89 184.63 11.49 o 9 10 0 627.93 682.93 19.99 o 10 10 0 1256.87 1229.18 35.90 o 11 10 0 77.55 88.96 8.96 o 12 10 0 130.51 144.81 11.31 o 13 10 0 511.72 444.81 21.28 o 14 10 0 136.03 129.25 9.10 o 15 10 0 0.70 12.67 5.66 o 1 11 0 64.31 67.90 3.65 o 2 11 0 50.50 47.73 3.41 o 3 11 0 5.49 15.23 3.29 o 4 11 0 331.52 341.79 14.13 o 5 11 0 872.29 779.71 19.33 o 6 11 0 281.58 322.87 11.99 o 7 11 0 496.43 516.27 16.58 o 8 11 0 395.81 387.63 14.49 o 9 11 0 139.21 129.41 11.17 o 10 11 0 209.00 199.25 11.66 o 11 11 0 103.46 127.54 11.45 o 12 11 0 335.71 305.81 13.65 o 13 11 0 486.90 465.85 17.53 o 14 11 0 401.43 357.46 18.90 o 0 12 0 301.68 171.21 7.38 o 1 12 0 23.39 35.12 4.57 o 2 12 0 1143.73 1166.04 45.66 o 3 12 0 2.89 4.58 5.55 o 4 12 0 315.10 383.48 14.10 o 5 12 0 417.81 396.96 15.41 o 6 12 0 20.09 61.43 14.69 o 7 12 0 496.07 576.76 34.03 o 8 12 0 1483.60 1496.59 37.66 o 9 12 0 338.56 334.52 16.74 o 10 12 0 185.51 194.35 11.98 o 11 12 0 980.74 998.50 24.75 o 12 12 0 1724.95 1648.80 43.97 o 13 12 0 43.51 38.91 5.72 o 14 12 0 15.56 23.16 6.46 o 1 13 0 1120.71 1109.87 25.44 o 2 13 0 0.98 1.04 6.69 o 3 13 0 136.53 139.46 10.44 o 4 13 0 1607.90 1607.22 38.64 o 5 13 0 796.25 828.88 25.96 o 6 13 0 551.36 519.71 19.11 o 7 13 0 282.61 399.48 24.07 o 8 13 0 509.44 517.46 25.38 o 9 13 0 9.99 41.66 11.03 o 10 13 0 31.16 26.22 9.46 o 11 13 0 73.88 82.29 9.75 o 12 13 0 323.31 304.35 12.17 o 13 13 0 16.34 16.59 7.48 o 0 14 0 697.41 627.25 29.35 o 1 14 0 851.13 750.06 20.65 o 2 14 0 729.21 764.97 23.22 o 3 14 0 86.22 104.11 11.76 o 4 14 0 331.11 420.29 20.45 o 5 14 0 612.40 587.13 21.22 o 6 14 0 0.21 2.89 7.06 o 7 14 0 656.92 684.60 29.43 o 8 14 0 67.17 70.96 12.70 o 9 14 0 15.90 33.28 9.17 o 10 14 0 42.93 40.21 8.94 o 11 14 0 15.91 10.21 6.77 o 12 14 0 241.59 211.32 17.16 o 1 15 0 1731.43 1649.97 44.85 o 2 15 0 408.49 492.00 21.59 o 3 15 0 3368.21 3438.73 92.03 o 4 15 0 1760.36 1785.13 47.42 o 5 15 0 291.31 271.93 14.94 o 6 15 0 507.67 536.22 19.72 o 7 15 0 11.87 29.71 11.21 o 8 15 0 7.94 8.62 8.55 o 9 15 0 182.63 174.54 13.34 o 10 15 0 17.98 29.04 10.77 o 11 15 0 160.05 154.26 13.31 o 12 15 0 72.77 59.25 11.55 o 0 16 0 2253.05 2175.43 69.26 o 1 16 0 211.39 201.61 13.05 o 2 16 0 122.20 140.98 12.42 o 3 16 0 345.89 334.74 18.16 o 4 16 0 841.90 806.58 24.10 o 5 16 0 1350.72 1396.04 37.79 o 6 16 0 30.70 53.62 8.87 o 7 16 0 198.48 229.14 15.35 o 8 16 0 171.62 178.45 17.63 o 9 16 0 42.99 46.67 9.53 o 10 16 0 3.93 9.73 5.74 o 11 16 0 52.63 31.74 9.56 o 1 17 0 808.65 810.70 27.96 o 2 17 0 24.89 27.73 8.95 o 3 17 0 537.48 540.37 21.76 o 4 17 0 227.54 238.42 12.46 o 5 17 0 40.14 47.71 9.45 o 6 17 0 326.76 269.73 15.92 o 7 17 0 47.59 41.02 8.37 o 8 17 0 655.17 678.03 25.82 o 9 17 0 14.38 3.95 5.56 o 0 18 0 27.87 17.87 11.81 o 1 18 0 48.50 58.71 8.87 o 2 18 0 26.42 46.35 8.19 o 3 18 0 260.75 259.90 15.91 o 4 18 0 66.35 56.56 9.07 o 5 18 0 61.96 56.84 7.91 o 6 18 0 136.63 103.50 9.21 o 7 18 0 33.88 48.90 7.00 o 8 18 0 78.61 72.92 10.03 o 1 19 0 42.60 34.80 8.95 o 2 19 0 7.30 0.67 5.97 o 3 19 0 3.00 1.09 6.65 o 4 19 0 2.21 6.23 6.67 o 5 19 0 152.29 136.09 16.45 o 6 19 0 71.97 67.60 9.24 o 0 20 0 1049.40 1101.33 39.67 o 1 20 0 151.33 145.88 12.17 o 2 20 0 129.52 111.79 8.12 o 3 20 0 0.03 -7.82 7.82 o 4 20 0 34.24 42.19 8.70 o -17 1 1 79.21 77.01 21.26 o -16 1 1 155.54 194.21 12.60 o -15 1 1 64.53 53.11 12.59 o -14 1 1 594.46 590.58 24.53 o -13 1 1 10.96 22.72 10.03 o -12 1 1 1554.18 1539.46 45.16 o -11 1 1 2857.83 2770.57 75.53 o -10 1 1 628.87 560.41 24.47 o -9 1 1 1617.18 1514.30 19.45 o -8 1 1 5987.58 5401.34 63.01 o -7 1 1 3415.09 3392.66 35.42 o -6 1 1 4453.30 4616.74 45.65 o -5 1 1 6698.99 7197.76 77.79 o -4 1 1 4910.16 4784.88 47.26 o -3 1 1 240.95 315.73 5.85 o -2 1 1 26999.63 33435.04 572.50 o -1 1 1 2025.91 2303.15 14.50 o 0 1 1 1265.65 1362.78 8.60 o 1 1 1 3337.59 3612.66 29.61 o 2 1 1 15578.31 18665.17 251.53 o 3 1 1 2223.86 2335.36 19.09 o 4 1 1 1884.19 2095.20 18.12 o 5 1 1 471.70 420.04 6.52 o 6 1 1 3668.55 3833.52 34.51 o 7 1 1 203.78 156.71 6.38 o 8 1 1 567.28 568.80 13.91 o 9 1 1 7.48 8.21 5.07 o 10 1 1 329.53 430.62 19.54 o 11 1 1 43.60 81.22 11.21 o 12 1 1 883.49 915.18 41.32 o 13 1 1 16.71 12.24 9.74 o 14 1 1 465.91 539.62 23.13 o 15 1 1 286.05 280.98 17.32 o 16 1 1 982.32 978.27 30.57 o 17 1 1 69.81 88.65 9.23 o -17 2 1 194.49 236.00 12.32 o -16 2 1 94.31 81.73 10.85 o -15 2 1 0.88 6.07 8.97 o -14 2 1 3425.23 3232.26 92.45 o -13 2 1 655.96 656.79 28.18 o -12 2 1 73.65 81.94 14.44 o -11 2 1 134.59 140.62 14.04 o -10 2 1 1.41 7.87 4.67 o -9 2 1 1266.07 1212.72 17.32 o -8 2 1 7699.35 7956.36 107.41 o -7 2 1 4309.14 4792.43 54.78 o -6 2 1 3454.57 3670.91 38.40 o -5 2 1 389.83 307.90 5.41 o -4 2 1 1016.59 1287.66 13.87 o -3 2 1 63563.09 75596.16 2024.02 o -2 2 1 6093.18 6618.14 73.44 o -1 2 1 2262.94 1938.46 13.23 o 0 2 1 1007.74 1085.77 11.13 o 1 2 1 924.23 1037.82 7.18 o 2 2 1 4551.83 5188.58 51.17 o 3 2 1 2370.14 2569.73 20.51 o 4 2 1 579.34 548.28 6.38 o 5 2 1 1735.48 1808.31 17.06 o 6 2 1 1878.03 1882.95 18.48 o 7 2 1 3517.41 4076.36 42.40 o 8 2 1 600.69 399.03 6.82 o 9 2 1 2182.81 2011.01 33.97 o 10 2 1 984.91 761.79 27.12 o 11 2 1 2.94 -0.79 9.66 o 12 2 1 4726.12 4677.73 134.64 o 13 2 1 184.83 161.38 15.68 o 14 2 1 128.70 180.28 14.54 o 15 2 1 92.57 105.44 12.43 o 16 2 1 191.14 195.08 14.34 o 17 2 1 118.40 109.97 19.82 o -17 3 1 39.90 44.89 7.88 o -16 3 1 5.24 6.31 7.78 o -15 3 1 18.12 4.66 8.34 o -14 3 1 289.63 302.49 17.30 o -13 3 1 158.79 157.75 14.03 o -12 3 1 265.33 256.63 17.36 o -11 3 1 149.71 241.27 13.05 o -10 3 1 2.14 5.14 4.46 o -9 3 1 160.25 170.89 6.38 o -8 3 1 189.71 283.21 5.79 o -7 3 1 45.44 124.47 4.51 o -6 3 1 40.93 30.62 3.27 o -5 3 1 198.38 160.51 3.68 o -4 3 1 490.78 605.69 7.68 o -3 3 1 646.12 950.11 8.32 o -2 3 1 10242.51 12718.46 153.86 o -1 3 1 4861.85 5052.38 44.99 o 0 3 1 9633.60 11366.53 134.46 o 1 3 1 2068.69 2255.29 20.50 o 2 3 1 3.62 5.59 1.67 o 3 3 1 618.18 611.99 6.49 o 4 3 1 580.21 607.66 7.65 o 5 3 1 3955.60 4091.62 47.95 o 6 3 1 234.90 277.04 5.33 o 7 3 1 231.70 349.12 5.30 o 8 3 1 4.05 27.21 3.42 o 9 3 1 263.44 211.02 9.29 o 10 3 1 1334.66 1346.94 35.39 o 11 3 1 3067.14 3130.07 84.71 o 12 3 1 2.64 9.23 9.43 o 13 3 1 403.56 365.44 23.22 o 14 3 1 883.86 858.98 32.49 o 15 3 1 1.97 -8.72 8.72 o 16 3 1 1293.69 1283.76 39.82 o 17 3 1 236.93 241.47 11.06 o -17 4 1 1.70 -0.24 6.52 o -16 4 1 20.74 45.90 8.51 o -15 4 1 56.25 92.77 12.14 o -14 4 1 1100.02 1228.24 40.47 o -13 4 1 6.18 4.23 9.24 o -12 4 1 824.24 786.43 25.90 o -11 4 1 572.15 556.49 17.83 o -10 4 1 87.10 66.98 6.93 o -9 4 1 4811.42 4594.40 58.76 o -8 4 1 3610.21 3206.27 37.53 o -7 4 1 184.10 254.44 5.77 o -6 4 1 4799.57 5220.31 62.95 o -5 4 1 564.74 486.40 7.87 o -4 4 1 329.51 239.31 6.89 o -3 4 1 2663.95 2750.27 23.35 o -2 4 1 17759.88 18948.40 271.28 o -1 4 1 65.62 62.07 3.68 o 0 4 1 56759.13 67477.91 1772.58 o 1 4 1 10.08 10.29 2.42 o 2 4 1 362.63 392.39 7.94 o 3 4 1 722.76 615.45 7.66 o 4 4 1 328.17 532.37 7.78 o 5 4 1 226.59 231.52 4.94 o 6 4 1 97.36 63.89 4.91 o 7 4 1 8052.14 8090.75 113.59 o 8 4 1 187.76 181.58 5.81 o 9 4 1 26.22 19.76 4.52 o 10 4 1 1103.88 1169.19 35.98 o 11 4 1 5.27 11.22 8.38 o 12 4 1 179.99 169.90 16.20 o 13 4 1 201.11 221.86 16.23 o 14 4 1 14.14 35.96 9.83 o 15 4 1 23.27 19.34 9.77 o 16 4 1 12.97 13.85 7.18 o 17 4 1 135.39 129.50 8.26 o -17 5 1 13.48 3.19 5.84 o -16 5 1 37.48 55.50 8.78 o -15 5 1 578.52 670.93 24.56 o -14 5 1 8.92 18.10 9.87 o -13 5 1 47.41 83.08 11.89 o -12 5 1 1871.21 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14725.61 17032.96 231.79 o -1 4 2 15219.12 18428.06 262.84 o 0 4 2 10080.60 11460.27 138.91 o 1 4 2 7760.07 8204.63 98.24 o 2 4 2 5.43 17.58 1.88 o 3 4 2 646.44 588.21 7.84 o 4 4 2 128.86 129.29 3.36 o 5 4 2 902.91 1012.46 12.03 o 6 4 2 1793.95 1774.83 20.49 o 7 4 2 27.21 29.72 3.46 o 8 4 2 7621.99 7027.09 118.53 o 9 4 2 511.02 512.79 18.19 o 10 4 2 6827.37 6875.96 192.05 o 11 4 2 572.19 554.75 22.76 o 12 4 2 534.19 553.41 31.10 o 13 4 2 290.83 315.14 17.65 o 14 4 2 54.27 77.97 10.95 o 15 4 2 387.72 390.15 20.11 o 16 4 2 0.09 4.86 6.29 o -17 5 2 5.56 10.33 7.87 o -16 5 2 103.82 123.32 10.92 o -15 5 2 204.50 191.21 13.68 o -14 5 2 659.89 700.73 25.78 o -13 5 2 150.40 136.32 13.05 o -12 5 2 20.95 32.78 7.63 o -11 5 2 436.46 428.00 15.25 o -10 5 2 308.96 305.15 9.20 o -9 5 2 1.15 5.23 3.45 o -8 5 2 5781.10 5823.70 76.62 o -7 5 2 517.47 581.87 8.66 o -6 5 2 4509.55 4515.12 53.37 o -5 5 2 257.04 211.81 6.18 o -4 5 2 372.62 288.12 6.02 o -3 5 2 6872.38 7341.47 86.79 o -2 5 2 567.51 589.72 7.98 o -1 5 2 4546.24 5047.88 50.62 o 0 5 2 1920.85 1955.63 17.21 o 1 5 2 2932.47 3303.49 30.21 o 2 5 2 10.84 18.98 2.14 o 3 5 2 2805.70 2974.61 30.50 o 4 5 2 4709.69 5218.79 60.66 o 5 5 2 115.04 116.89 4.35 o 6 5 2 236.31 184.76 4.92 o 7 5 2 936.68 1045.11 14.35 o 8 5 2 534.28 419.15 10.50 o 9 5 2 118.44 119.87 7.84 o 10 5 2 17.18 20.25 9.99 o 11 5 2 171.07 179.64 14.15 o 12 5 2 566.49 539.19 24.83 o 13 5 2 5.03 9.81 8.93 o 14 5 2 51.41 74.16 10.98 o 15 5 2 124.87 129.59 13.55 o 16 5 2 488.48 442.22 22.28 o -16 6 2 392.15 399.50 18.77 o -15 6 2 183.55 202.27 12.20 o -14 6 2 891.37 964.87 32.78 o -13 6 2 1.02 8.29 8.07 o -12 6 2 925.12 986.32 26.52 o -11 6 2 382.54 418.85 16.09 o -10 6 2 611.33 540.91 18.34 o -9 6 2 575.90 579.23 12.78 o -8 6 2 8107.35 8083.36 118.43 o -7 6 2 2025.02 1889.50 22.25 o -6 6 2 58.32 98.98 4.24 o -5 6 2 664.78 694.53 15.06 o -4 6 2 7704.85 7521.87 82.94 o -3 6 2 333.64 469.94 6.17 o -2 6 2 9996.30 11213.93 141.67 o -1 6 2 256.81 337.06 6.43 o 0 6 2 1426.42 1348.02 12.59 o 1 6 2 1.30 4.86 1.96 o 2 6 2 14305.88 14616.86 204.00 o 3 6 2 1711.05 1774.66 17.13 o 4 6 2 13.96 3.90 1.84 o 5 6 2 150.56 35.46 2.76 o 6 6 2 1978.25 1753.09 27.09 o 7 6 2 155.07 81.53 4.28 o 8 6 2 987.55 1001.89 32.00 o 9 6 2 1269.32 1413.96 34.27 o 10 6 2 250.07 206.96 12.24 o 11 6 2 651.17 750.20 30.15 o 12 6 2 1202.09 1268.32 36.29 o 13 6 2 583.86 663.40 27.90 o 14 6 2 258.46 286.33 15.44 o 15 6 2 56.09 56.53 9.24 o 16 6 2 15.78 20.45 9.18 o -16 7 2 212.91 164.08 12.24 o -15 7 2 212.06 235.07 12.24 o -14 7 2 1035.30 986.09 26.49 o -13 7 2 80.08 101.09 11.07 o -12 7 2 62.37 81.96 9.70 o -11 7 2 15.18 29.44 8.00 o -10 7 2 182.03 164.15 8.05 o -9 7 2 1299.88 1352.36 38.79 o -8 7 2 16.49 13.53 4.02 o -7 7 2 2143.35 1764.32 21.95 o -6 7 2 3511.86 3066.10 35.88 o -5 7 2 964.94 984.77 11.85 o -4 7 2 807.40 595.14 7.91 o -3 7 2 6.16 2.41 2.20 o -2 7 2 1272.67 1295.82 13.87 o -1 7 2 13269.56 13467.83 189.28 o 0 7 2 3506.61 3664.19 36.91 o 1 7 2 244.67 231.43 4.80 o 2 7 2 1936.51 1901.68 21.61 o 3 7 2 18.77 29.42 4.75 o 4 7 2 3576.95 3129.28 36.56 o 5 7 2 169.96 115.59 5.81 o 6 7 2 2130.09 1905.72 25.50 o 7 7 2 468.79 449.91 10.26 o 8 7 2 1029.96 1051.42 35.40 o 9 7 2 142.29 185.01 11.14 o 10 7 2 63.95 86.06 9.61 o 11 7 2 174.07 163.51 13.94 o 12 7 2 841.71 869.81 27.90 o 13 7 2 286.90 300.69 15.05 o 14 7 2 46.71 32.34 10.92 o 15 7 2 0.78 13.85 7.34 o 16 7 2 0.40 -0.42 7.04 o -16 8 2 42.66 20.98 13.63 o -15 8 2 5.64 4.29 4.85 o -14 8 2 98.89 98.82 8.85 o -13 8 2 308.76 295.50 15.13 o -12 8 2 451.88 468.13 17.91 o -11 8 2 1374.90 1450.30 37.39 o -10 8 2 41.81 60.82 8.08 o -9 8 2 106.82 124.95 8.46 o -8 8 2 147.04 124.75 8.41 o -7 8 2 175.42 210.48 8.99 o -6 8 2 167.27 174.47 6.97 o -5 8 2 11.05 2.67 2.59 o -4 8 2 1567.31 1298.99 14.85 o -3 8 2 6503.08 6174.10 73.75 o -2 8 2 4236.18 3698.01 39.67 o -1 8 2 180.12 143.87 5.43 o 0 8 2 3009.06 3406.90 33.65 o 1 8 2 714.15 782.80 8.33 o 2 8 2 511.61 475.40 6.38 o 3 8 2 620.45 578.67 7.78 o 4 8 2 2064.97 2013.74 22.75 o 5 8 2 199.01 137.19 4.19 o 6 8 2 425.30 313.45 8.06 o 7 8 2 249.13 272.44 11.29 o 8 8 2 370.34 350.97 14.21 o 9 8 2 94.31 81.26 9.42 o 10 8 2 473.61 526.09 18.53 o 11 8 2 4.94 5.12 6.47 o 12 8 2 176.24 223.42 16.66 o 13 8 2 0.19 19.32 10.06 o 14 8 2 12.24 17.29 8.45 o 15 8 2 267.36 245.82 16.71 o -15 9 2 12.58 11.58 4.37 o -14 9 2 2.04 -5.82 5.82 o -13 9 2 346.69 425.22 17.45 o -12 9 2 0.48 8.05 6.47 o -11 9 2 490.08 512.26 16.62 o -10 9 2 906.34 939.17 23.33 o -9 9 2 821.07 783.58 20.65 o -8 9 2 1233.14 1272.63 31.43 o -7 9 2 16.35 34.57 5.40 o -6 9 2 468.68 529.18 9.94 o -5 9 2 720.38 659.68 12.67 o -4 9 2 2880.58 2689.31 30.96 o -3 9 2 456.53 683.60 9.35 o -2 9 2 0.04 10.72 2.44 o -1 9 2 7946.06 7730.69 93.18 o 0 9 2 4550.13 4812.11 52.84 o 1 9 2 2555.34 2442.47 25.08 o 2 9 2 1890.06 1803.15 20.73 o 3 9 2 4.66 7.34 2.93 o 4 9 2 888.26 765.52 11.69 o 5 9 2 649.29 588.67 14.49 o 6 9 2 359.62 334.03 13.89 o 7 9 2 4.06 5.29 6.13 o 8 9 2 7.33 11.66 8.11 o 9 9 2 256.14 288.40 16.30 o 10 9 2 0.53 0.99 8.47 o 11 9 2 1522.32 1431.20 38.84 o 12 9 2 97.07 139.28 15.46 o 13 9 2 110.41 201.09 35.99 o 14 9 2 9.82 6.43 7.69 o 15 9 2 3.18 1.96 7.93 o -15 10 2 151.09 149.99 10.19 o -14 10 2 651.92 594.63 17.20 o -13 10 2 115.68 96.31 12.95 o -12 10 2 2251.41 2135.82 46.31 o -11 10 2 147.12 160.09 10.07 o -10 10 2 51.90 57.87 7.73 o -9 10 2 42.01 52.66 9.11 o -8 10 2 15.08 21.18 7.22 o -7 10 2 60.96 80.94 8.26 o -6 10 2 28.61 54.98 8.70 o -5 10 2 1593.09 1706.41 37.70 o -4 10 2 2013.04 1861.25 29.62 o -3 10 2 643.06 591.28 9.45 o -2 10 2 138.30 84.93 4.98 o -1 10 2 2242.82 2527.89 28.13 o 0 10 2 3635.20 3972.98 46.88 o 1 10 2 673.00 590.39 13.24 o 2 10 2 2291.75 2176.59 27.65 o 3 10 2 1694.74 1752.13 23.56 o 4 10 2 1.67 8.81 4.50 o 5 10 2 799.22 700.44 28.08 o 6 10 2 872.18 1118.62 29.80 o 7 10 2 214.52 239.75 18.83 o 8 10 2 288.06 325.27 15.24 o 9 10 2 7.38 5.13 8.47 o 10 10 2 69.91 122.49 12.77 o 11 10 2 170.32 142.02 11.72 o 12 10 2 519.62 480.60 38.63 o 13 10 2 379.49 395.22 17.57 o 14 10 2 24.59 23.60 7.99 o 15 10 2 163.99 173.01 12.73 o -14 11 2 157.28 121.46 11.09 o -13 11 2 140.83 138.42 10.67 o -12 11 2 110.09 100.03 9.19 o -11 11 2 128.92 133.82 18.57 o -10 11 2 5.46 2.66 7.20 o -9 11 2 132.78 144.11 11.19 o -8 11 2 147.67 137.95 10.07 o -7 11 2 824.21 806.60 22.39 o -6 11 2 12.96 31.79 7.19 o -5 11 2 79.29 104.43 8.93 o -4 11 2 183.67 152.91 8.42 o -3 11 2 186.81 159.67 7.00 o -2 11 2 47.52 46.78 4.68 o -1 11 2 545.53 669.98 11.91 o 0 11 2 125.32 122.51 5.69 o 1 11 2 3723.60 3434.78 44.61 o 2 11 2 50.14 65.85 5.06 o 3 11 2 42.56 72.71 5.96 o 4 11 2 1623.53 1641.90 33.34 o 5 11 2 157.09 202.95 12.09 o 6 11 2 868.55 898.21 27.49 o 7 11 2 197.01 168.48 12.70 o 8 11 2 34.87 61.52 9.26 o 9 11 2 342.93 334.23 14.69 o 10 11 2 96.52 86.57 12.57 o 11 11 2 186.68 183.21 13.67 o 12 11 2 304.97 267.82 12.61 o 13 11 2 88.54 73.97 10.41 o 14 11 2 11.00 9.65 5.86 o -14 12 2 263.26 222.38 16.69 o -13 12 2 676.29 567.62 28.62 o -12 12 2 117.89 113.35 9.66 o -11 12 2 26.83 31.04 7.34 o -10 12 2 30.05 52.25 8.61 o -9 12 2 29.54 30.45 9.18 o -8 12 2 38.30 54.14 8.26 o -7 12 2 95.35 82.90 9.01 o -6 12 2 2623.71 2751.73 64.41 o -5 12 2 133.00 123.62 9.21 o -4 12 2 714.82 714.37 20.96 o -3 12 2 376.12 378.39 16.00 o -2 12 2 1332.95 1249.69 23.46 o -1 12 2 3370.06 3589.64 57.93 o 0 12 2 584.71 749.34 17.85 o 1 12 2 1005.74 987.06 24.17 o 2 12 2 0.05 9.47 5.40 o 3 12 2 2.05 5.59 5.63 o 4 12 2 375.78 438.33 13.91 o 5 12 2 1272.22 1298.63 34.28 o 6 12 2 1907.43 1751.89 44.44 o 7 12 2 238.48 275.14 15.56 o 8 12 2 122.96 130.31 11.45 o 9 12 2 37.94 56.53 9.64 o 10 12 2 1330.56 1260.31 44.53 o 11 12 2 71.55 63.39 9.64 o 12 12 2 598.11 618.17 18.32 o 13 12 2 10.08 17.58 8.43 o -13 13 2 218.24 245.65 19.37 o -12 13 2 5.88 -5.67 5.83 o -11 13 2 115.38 126.21 14.87 o -10 13 2 45.69 46.22 10.33 o -9 13 2 269.05 260.13 16.65 o -8 13 2 358.84 332.09 13.68 o -7 13 2 10.80 14.01 7.59 o -6 13 2 184.82 188.31 11.00 o -5 13 2 89.24 133.04 10.00 o -4 13 2 53.16 48.65 8.60 o -3 13 2 24.67 7.86 6.19 o -2 13 2 9.83 4.18 5.66 o -1 13 2 1505.62 1556.85 33.45 o 0 13 2 104.35 99.87 8.51 o 1 13 2 0.53 -1.74 5.54 o 2 13 2 1884.48 1765.67 41.87 o 3 13 2 33.69 54.85 7.36 o 4 13 2 6.74 9.81 6.69 o 5 13 2 59.34 81.18 9.77 o 6 13 2 2100.42 2178.26 52.60 o 7 13 2 138.23 178.84 13.89 o 8 13 2 116.63 141.55 12.24 o 9 13 2 548.79 621.57 21.97 o 10 13 2 2.35 13.78 8.60 o 11 13 2 266.01 302.63 14.53 o 12 13 2 272.21 281.41 13.08 o 13 13 2 221.89 214.94 10.46 o -12 14 2 107.20 109.36 13.10 o -11 14 2 14.43 42.79 9.50 o -10 14 2 39.79 67.29 11.95 o -9 14 2 3.49 8.80 9.99 o -8 14 2 798.89 815.30 25.63 o -7 14 2 285.25 262.85 12.89 o -6 14 2 142.34 173.54 18.46 o -5 14 2 415.99 478.12 17.44 o -4 14 2 47.09 78.63 9.13 o -3 14 2 1713.05 1742.38 38.56 o -2 14 2 601.77 679.29 19.38 o -1 14 2 63.21 63.57 8.19 o 0 14 2 1483.12 1596.76 37.97 o 1 14 2 2402.78 2147.03 48.00 o 2 14 2 413.09 436.66 16.78 o 3 14 2 2464.60 2337.33 50.82 o 4 14 2 206.69 189.03 14.92 o 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o -8 16 2 100.27 131.82 12.01 o -7 16 2 339.94 355.68 17.14 o -6 16 2 59.66 75.02 11.37 o -5 16 2 2946.92 2933.70 67.43 o -4 16 2 483.03 425.37 17.29 o -3 16 2 1586.42 1508.79 46.47 o -2 16 2 185.17 211.18 14.13 o -1 16 2 3.29 5.16 7.97 o 0 16 2 435.09 423.08 15.10 o 1 16 2 32.50 38.39 9.25 o 2 16 2 1291.90 1309.44 37.55 o 3 16 2 324.94 329.11 21.53 o 4 16 2 561.22 540.60 22.70 o 5 16 2 161.76 175.31 13.52 o 6 16 2 11.18 9.85 8.75 o 7 16 2 117.71 137.66 11.75 o 8 16 2 90.46 103.42 11.12 o 9 16 2 499.20 488.87 18.38 o 10 16 2 1.75 1.20 7.75 o -9 17 2 9.47 -1.02 8.72 o -8 17 2 13.11 8.68 7.81 o -7 17 2 7.30 13.76 8.47 o -6 17 2 237.03 249.11 13.22 o -5 17 2 167.37 170.82 16.53 o -4 17 2 260.06 292.97 16.90 o -3 17 2 23.96 29.56 8.80 o -2 17 2 427.40 400.19 16.66 o -1 17 2 12.48 16.78 8.54 o 0 17 2 890.46 847.72 33.21 o 1 17 2 1012.48 957.40 28.43 o 2 17 2 337.98 330.14 16.77 o 3 17 2 83.54 96.40 10.72 o 4 17 2 174.03 199.71 22.61 o 5 17 2 82.80 83.67 11.47 o 6 17 2 6.44 10.07 8.79 o 7 17 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