#------------------------------------------------------------------------------ #$Date: 2011-10-06 14:27:20 +0300 (Thu, 06 Oct 2011) $ #$Revision: 27511 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/10/2231034.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231034_Fobs loop_ _publ_author_name 'Betz, Richard' 'Gerber, Thomas' 'Hosten, Eric' _publ_section_title ; (3-Aminophenyl)methanol ; _journal_coeditor_code BX2363 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2118 _journal_volume 67 _journal_year 2011 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 4.7977 _cell_length_b 6.2954 _cell_length_c 21.6341 _exptl_crystal_F_000 264.00 _reflns_d_resolution_high 0.7571 _[local]_cod_data_source_file bx2363Isup3.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ba273_s in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 65.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 20.94 26.18 0.39 o 4 0 0 678.37 668.04 8.43 o 6 0 0 0.10 0.40 0.30 o 1 1 0 3108.43 2749.79 20.07 o 2 1 0 343.23 362.24 2.63 o 3 1 0 340.37 345.38 2.74 o 4 1 0 9.08 8.84 0.25 o 5 1 0 4.62 6.13 0.43 o 6 1 0 51.66 50.99 0.81 o 0 2 0 237.28 229.68 2.70 o 1 2 0 99.75 84.12 0.64 o 2 2 0 8.96 9.06 0.26 o 3 2 0 67.71 67.64 0.66 o 4 2 0 0.66 0.95 0.14 o 5 2 0 20.37 19.59 0.44 o 6 2 0 0.00 -0.21 0.21 o 1 3 0 64.06 74.10 0.71 o 2 3 0 6.74 7.23 0.20 o 3 3 0 34.26 34.53 0.46 o 4 3 0 4.71 4.48 0.28 o 5 3 0 5.51 5.22 0.65 o 0 4 0 288.22 279.81 3.86 o 1 4 0 30.18 31.60 0.39 o 2 4 0 0.04 0.14 0.11 o 3 4 0 16.39 22.63 0.47 o 4 4 0 37.01 36.98 0.65 o 5 4 0 9.85 10.55 0.45 o 1 5 0 1.47 1.61 0.20 o 2 5 0 0.00 0.34 0.17 o 3 5 0 26.04 24.63 0.51 o 4 5 0 6.32 5.98 0.32 o 5 5 0 5.75 7.21 0.58 o 0 6 0 104.81 107.00 1.70 o 1 6 0 0.04 0.12 0.18 o 2 6 0 2.21 2.46 0.24 o 3 6 0 13.38 12.01 0.41 o 4 6 0 0.22 0.80 0.33 o 1 7 0 92.21 92.29 1.42 o 2 7 0 53.36 55.03 0.99 o 3 7 0 0.25 0.24 0.26 o 0 8 0 21.56 21.76 1.11 o 1 8 0 64.05 67.62 1.16 o 1 0 1 406.42 386.53 2.43 o 2 0 1 506.54 485.24 3.78 o 3 0 1 4.37 3.43 0.14 o 5 0 1 77.69 75.79 1.01 o 6 0 1 15.26 14.98 0.43 o 0 1 1 22.90 22.82 0.21 o 1 1 1 2816.31 2471.14 14.84 o 2 1 1 1250.42 1216.05 6.47 o 3 1 1 115.62 121.94 0.73 o 4 1 1 2.53 2.21 0.10 o 5 1 1 67.24 65.41 0.69 o 6 1 1 15.19 17.11 0.32 o 0 2 1 96.42 97.03 0.84 o 1 2 1 561.26 570.87 3.22 o 2 2 1 442.93 481.80 2.66 o 3 2 1 43.07 51.14 0.36 o 4 2 1 32.82 30.83 0.31 o 5 2 1 4.17 4.06 0.18 o 6 2 1 2.24 1.83 0.18 o 0 3 1 164.97 171.74 1.70 o 1 3 1 96.96 105.13 0.72 o 2 3 1 150.46 145.64 1.01 o 3 3 1 44.39 44.79 0.39 o 4 3 1 31.07 26.54 0.36 o 5 3 1 31.58 28.87 0.47 o 0 4 1 21.55 24.05 0.34 o 1 4 1 34.04 36.22 0.33 o 2 4 1 5.14 5.94 0.15 o 3 4 1 52.75 43.06 0.48 o 4 4 1 25.10 20.35 0.33 o 5 4 1 20.43 17.04 0.39 o 0 5 1 19.00 19.90 0.32 o 1 5 1 24.54 26.27 0.28 o 2 5 1 56.36 53.03 0.53 o 3 5 1 1.71 1.79 0.16 o 4 5 1 9.05 7.86 0.25 o 5 5 1 13.17 14.31 0.43 o 0 6 1 117.34 116.50 1.64 o 1 6 1 20.16 20.33 0.33 o 2 6 1 4.59 4.05 0.19 o 3 6 1 8.01 7.54 0.26 o 4 6 1 8.52 8.61 0.32 o 0 7 1 3.70 4.22 0.30 o 1 7 1 10.20 11.08 0.30 o 2 7 1 35.00 36.81 0.54 o 3 7 1 2.07 2.50 0.21 o 0 8 1 4.78 5.49 0.36 o 1 8 1 0.45 0.67 0.19 o 1 0 2 2001.48 1863.79 15.00 o 2 0 2 12.15 13.71 0.18 o 3 0 2 24.66 29.02 0.32 o 4 0 2 43.98 44.68 0.54 o 5 0 2 8.34 9.38 0.33 o 6 0 2 12.38 10.99 0.38 o 0 1 2 702.88 682.16 5.46 o 1 1 2 4298.81 3569.81 33.80 o 2 1 2 115.46 117.99 0.66 o 3 1 2 332.83 337.56 1.89 o 4 1 2 17.23 17.76 0.22 o 5 1 2 8.37 9.01 0.23 o 6 1 2 4.01 4.69 0.21 o 0 2 2 14.47 17.37 0.20 o 1 2 2 1292.49 1250.99 6.64 o 2 2 2 774.76 793.72 4.50 o 3 2 2 308.94 305.96 1.84 o 4 2 2 12.87 12.01 0.20 o 5 2 2 30.75 29.74 0.39 o 6 2 2 2.41 2.15 0.18 o 0 3 2 339.81 326.20 3.13 o 1 3 2 61.37 59.45 0.46 o 2 3 2 179.61 189.08 1.26 o 3 3 2 6.83 7.77 0.17 o 4 3 2 102.36 104.68 0.96 o 5 3 2 2.76 3.69 0.21 o 0 4 2 27.15 27.10 0.37 o 1 4 2 26.70 26.54 0.27 o 2 4 2 34.94 35.31 0.35 o 3 4 2 15.55 14.36 0.25 o 4 4 2 14.87 12.66 0.27 o 5 4 2 1.22 1.51 0.19 o 0 5 2 0.00 0.21 0.15 o 1 5 2 53.88 49.14 0.44 o 2 5 2 41.04 34.91 0.40 o 3 5 2 22.80 21.39 0.34 o 4 5 2 5.47 5.78 0.29 o 5 5 2 10.92 13.51 0.43 o 0 6 2 117.37 116.70 1.82 o 1 6 2 30.43 33.44 0.44 o 2 6 2 5.31 5.07 0.21 o 3 6 2 41.13 42.71 0.55 o 4 6 2 29.81 30.00 0.50 o 0 7 2 96.65 100.91 1.50 o 1 7 2 82.02 81.37 0.91 o 2 7 2 18.73 19.23 0.38 o 3 7 2 9.78 11.10 0.33 o 0 8 2 9.97 9.88 0.59 o 1 8 2 1.44 1.06 0.22 o 1 0 3 4.56 4.79 0.10 o 2 0 3 611.51 597.72 4.48 o 3 0 3 73.94 67.82 0.61 o 4 0 3 160.69 152.12 1.47 o 5 0 3 4.17 4.92 0.28 o 6 0 3 3.08 2.78 0.26 o 0 1 3 0.07 2.17 0.84 o 1 1 3 227.53 230.52 1.12 o 2 1 3 200.24 203.80 1.08 o 3 1 3 41.08 43.16 0.32 o 4 1 3 45.90 45.03 0.38 o 5 1 3 14.83 15.29 0.30 o 6 1 3 21.58 21.31 0.36 o 0 2 3 3.69 3.64 0.17 o 1 2 3 469.22 467.36 2.47 o 2 2 3 643.81 670.63 3.69 o 3 2 3 288.38 281.48 1.64 o 4 2 3 22.59 21.23 0.25 o 5 2 3 23.94 25.48 0.36 o 6 2 3 12.56 11.99 0.29 o 0 3 3 100.91 102.23 1.05 o 1 3 3 526.50 545.78 3.34 o 2 3 3 67.41 70.27 0.50 o 3 3 3 89.46 87.32 0.65 o 4 3 3 18.93 18.17 0.28 o 5 3 3 8.21 8.03 0.26 o 0 4 3 211.16 227.07 2.24 o 1 4 3 68.30 65.54 0.52 o 2 4 3 73.83 70.09 0.55 o 3 4 3 14.01 12.67 0.28 o 4 4 3 10.58 8.46 0.24 o 5 4 3 9.73 10.58 0.33 o 0 5 3 81.34 83.04 0.90 o 1 5 3 66.54 63.50 0.58 o 2 5 3 1.32 0.56 0.12 o 3 5 3 64.67 57.92 0.62 o 4 5 3 7.86 8.70 0.27 o 5 5 3 1.99 2.04 0.38 o 0 6 3 44.08 44.05 0.69 o 1 6 3 213.92 206.66 2.04 o 2 6 3 22.04 20.10 0.35 o 3 6 3 15.62 18.26 0.35 o 4 6 3 7.15 8.58 0.32 o 0 7 3 87.23 84.88 1.31 o 1 7 3 4.18 4.38 0.22 o 2 7 3 16.49 17.75 0.37 o 3 7 3 22.85 25.64 0.46 o 0 8 3 0.31 0.22 0.34 o 1 8 3 3.50 4.12 0.27 o 1 0 4 149.84 164.34 1.06 o 2 0 4 52.66 52.43 0.47 o 3 0 4 91.55 101.99 0.87 o 4 0 4 57.13 57.12 0.65 o 5 0 4 14.09 16.58 0.41 o 6 0 4 9.26 8.77 0.36 o 0 1 4 2612.02 2244.70 25.97 o 1 1 4 268.60 280.47 1.35 o 2 1 4 60.80 63.45 0.37 o 3 1 4 215.13 211.98 1.25 o 4 1 4 39.67 38.09 0.38 o 5 1 4 6.65 6.14 0.21 o 6 1 4 33.58 35.70 0.47 o 0 2 4 542.90 530.38 5.07 o 1 2 4 57.24 56.81 0.34 o 2 2 4 191.42 198.24 1.13 o 3 2 4 69.87 73.41 0.49 o 4 2 4 5.23 5.92 0.16 o 5 2 4 2.61 3.31 0.17 o 6 2 4 0.60 0.87 0.17 o 0 3 4 837.49 808.21 6.87 o 1 3 4 108.87 115.61 0.70 o 2 3 4 26.56 25.74 0.22 o 3 3 4 44.65 43.79 0.38 o 4 3 4 126.71 126.33 1.04 o 5 3 4 10.42 10.07 0.27 o 0 4 4 156.97 163.22 1.58 o 1 4 4 116.22 109.60 0.77 o 2 4 4 110.37 105.24 0.73 o 3 4 4 28.99 28.05 0.35 o 4 4 4 33.66 29.48 0.43 o 5 4 4 21.50 21.14 0.42 o 0 5 4 454.66 447.89 4.41 o 1 5 4 227.66 219.86 1.96 o 2 5 4 32.29 28.90 0.36 o 3 5 4 103.25 95.91 0.91 o 4 5 4 32.19 33.36 0.48 o 0 6 4 25.97 26.93 0.50 o 1 6 4 91.30 90.51 0.93 o 2 6 4 12.71 11.31 0.28 o 3 6 4 16.84 17.73 0.34 o 4 6 4 9.36 10.71 0.33 o 0 7 4 16.44 17.35 0.48 o 1 7 4 9.20 9.24 0.28 o 2 7 4 24.09 24.58 0.43 o 3 7 4 3.72 3.82 0.25 o 0 8 4 1.11 0.48 0.34 o 1 8 4 6.58 6.46 0.32 o 1 0 5 1320.06 1253.69 8.83 o 2 0 5 362.56 362.97 2.70 o 3 0 5 14.07 11.57 0.21 o 4 0 5 25.94 26.63 0.42 o 5 0 5 232.78 230.81 2.63 o 6 0 5 2.98 3.98 0.28 o 0 1 5 218.60 196.82 1.39 o 1 1 5 708.77 713.75 3.99 o 2 1 5 462.99 473.15 2.51 o 3 1 5 21.34 21.68 0.20 o 4 1 5 50.84 49.04 0.41 o 5 1 5 23.04 21.95 0.33 o 6 1 5 52.62 52.34 0.59 o 0 2 5 465.40 456.16 3.44 o 1 2 5 207.99 209.09 1.21 o 2 2 5 186.88 191.57 1.14 o 3 2 5 22.91 26.53 0.24 o 4 2 5 29.49 30.24 0.31 o 5 2 5 42.01 39.85 0.44 o 6 2 5 6.40 6.40 0.25 o 0 3 5 196.32 236.04 2.40 o 1 3 5 2.13 1.54 0.07 o 2 3 5 46.77 40.89 0.30 o 3 3 5 12.94 14.15 0.28 o 4 3 5 17.27 15.67 0.28 o 5 3 5 2.85 3.28 0.18 o 0 4 5 22.86 21.71 0.32 o 1 4 5 58.41 63.15 0.48 o 2 4 5 645.53 637.39 3.81 o 3 4 5 12.95 15.97 0.25 o 4 4 5 11.93 11.74 0.29 o 5 4 5 0.98 1.46 0.20 o 0 5 5 3.26 4.02 0.18 o 1 5 5 188.21 183.36 1.97 o 2 5 5 30.65 26.40 0.34 o 3 5 5 5.81 6.90 0.23 o 4 5 5 0.27 0.53 0.17 o 0 6 5 140.38 138.39 1.70 o 1 6 5 63.18 60.54 0.61 o 2 6 5 23.26 20.96 0.35 o 3 6 5 4.47 6.54 0.25 o 4 6 5 11.92 14.86 0.37 o 0 7 5 3.34 5.13 0.43 o 1 7 5 20.41 19.14 0.40 o 2 7 5 6.68 7.22 0.27 o 3 7 5 17.78 21.35 0.45 o 0 8 5 0.10 -0.14 0.33 o 1 8 5 18.53 18.42 0.45 o 0 0 6 477.20 437.36 8.29 o 1 0 6 646.00 598.58 4.69 o 2 0 6 150.00 166.47 1.34 o 3 0 6 14.52 16.73 0.24 o 4 0 6 75.72 76.02 0.88 o 5 0 6 51.96 55.37 0.82 o 6 0 6 35.30 31.57 0.62 o 0 1 6 92.64 99.95 0.77 o 1 1 6 76.63 73.04 0.50 o 2 1 6 186.80 189.71 1.17 o 3 1 6 86.69 88.22 0.58 o 4 1 6 77.14 79.33 0.62 o 5 1 6 28.65 28.09 0.36 o 6 1 6 4.47 5.24 0.22 o 0 2 6 118.87 111.57 0.93 o 1 2 6 353.20 375.94 2.20 o 2 2 6 119.40 119.46 0.70 o 3 2 6 96.71 100.84 0.69 o 4 2 6 32.18 31.13 0.34 o 5 2 6 26.69 26.06 0.37 o 6 2 6 6.71 6.60 0.36 o 0 3 6 246.42 289.43 2.50 o 1 3 6 307.51 313.68 2.10 o 2 3 6 141.78 155.03 0.98 o 3 3 6 258.53 248.82 1.75 o 4 3 6 32.04 29.17 0.37 o 5 3 6 2.40 2.59 0.17 o 0 4 6 36.02 32.79 0.44 o 1 4 6 63.08 61.34 0.46 o 2 4 6 178.12 180.89 1.18 o 3 4 6 71.66 68.22 0.60 o 4 4 6 30.74 30.46 0.44 o 5 4 6 4.55 4.02 0.28 o 0 5 6 4.73 3.96 0.17 o 1 5 6 73.15 71.90 0.59 o 2 5 6 56.50 49.41 0.51 o 3 5 6 29.60 29.48 0.42 o 4 5 6 13.71 15.17 0.35 o 0 6 6 81.37 77.75 1.03 o 1 6 6 12.11 10.11 0.25 o 2 6 6 6.64 7.72 0.24 o 3 6 6 38.77 35.52 0.53 o 4 6 6 4.77 6.06 0.33 o 0 7 6 81.34 81.09 1.98 o 1 7 6 1.35 1.08 0.19 o 2 7 6 14.25 12.92 0.31 o 3 7 6 9.51 10.50 0.35 o 0 8 6 0.02 -0.31 0.31 o 1 8 6 2.28 2.89 0.52 o 1 0 7 0.77 0.59 0.07 o 2 0 7 178.06 192.55 1.54 o 3 0 7 0.89 1.21 0.09 o 4 0 7 63.25 64.05 0.78 o 5 0 7 3.45 3.95 0.38 o 6 0 7 34.33 32.87 0.63 o 0 1 7 150.23 142.10 1.09 o 1 1 7 128.65 139.10 0.92 o 2 1 7 173.09 186.92 1.18 o 3 1 7 31.59 29.00 0.25 o 4 1 7 97.31 94.94 0.72 o 5 1 7 59.02 57.31 0.58 o 6 1 7 5.32 5.56 0.22 o 0 2 7 589.38 626.27 4.88 o 1 2 7 312.27 346.48 2.18 o 2 2 7 101.85 106.53 0.67 o 3 2 7 99.14 97.67 0.70 o 4 2 7 101.29 98.53 0.84 o 5 2 7 19.65 18.84 0.32 o 0 3 7 40.66 42.34 0.44 o 1 3 7 438.96 468.87 3.10 o 2 3 7 1.67 1.85 0.09 o 3 3 7 511.47 500.58 3.58 o 4 3 7 2.38 3.30 0.16 o 5 3 7 5.39 4.97 0.21 o 0 4 7 107.73 119.14 1.18 o 1 4 7 58.61 57.38 0.46 o 2 4 7 103.26 100.28 0.76 o 3 4 7 6.02 6.16 0.22 o 4 4 7 58.37 54.16 0.64 o 5 4 7 6.97 7.63 0.29 o 0 5 7 48.18 48.98 0.69 o 1 5 7 101.59 96.78 0.78 o 2 5 7 25.15 23.32 0.32 o 3 5 7 21.21 21.10 0.35 o 4 5 7 37.08 35.96 0.54 o 0 6 7 64.19 62.41 0.89 o 1 6 7 6.89 6.78 0.27 o 2 6 7 18.47 16.63 0.32 o 3 6 7 4.63 4.42 0.23 o 4 6 7 36.87 39.04 0.59 o 0 7 7 28.35 25.83 0.89 o 1 7 7 2.79 3.24 0.27 o 2 7 7 44.94 45.87 0.61 o 3 7 7 21.76 24.14 1.33 o 0 8 7 0.08 -0.26 0.41 o 0 0 8 1133.83 1090.26 12.64 o 1 0 8 252.59 266.81 2.53 o 2 0 8 86.80 111.42 0.92 o 3 0 8 60.57 72.12 0.68 o 4 0 8 38.45 37.37 0.53 o 5 0 8 40.52 39.42 0.59 o 6 0 8 14.00 13.91 0.43 o 0 1 8 785.16 798.53 6.78 o 1 1 8 299.65 337.97 2.39 o 2 1 8 63.80 72.52 0.51 o 3 1 8 52.76 51.40 0.38 o 4 1 8 51.03 49.87 0.46 o 5 1 8 47.93 46.47 0.49 o 6 1 8 9.87 9.40 0.30 o 0 2 8 479.88 529.17 4.12 o 1 2 8 354.23 372.41 2.53 o 2 2 8 82.94 79.41 0.57 o 3 2 8 109.84 107.34 0.76 o 4 2 8 81.31 77.04 0.68 o 5 2 8 13.10 13.82 0.28 o 0 3 8 12.07 14.36 0.21 o 1 3 8 31.20 34.05 0.30 o 2 3 8 49.18 51.44 0.46 o 3 3 8 11.32 13.60 0.37 o 4 3 8 59.77 57.15 0.55 o 5 3 8 4.93 5.84 0.25 o 0 4 8 379.19 390.90 3.63 o 1 4 8 48.51 46.92 0.40 o 2 4 8 77.09 72.60 0.66 o 3 4 8 26.18 24.19 0.30 o 4 4 8 61.17 56.75 0.66 o 5 4 8 31.00 30.24 0.50 o 0 5 8 21.92 21.27 0.43 o 1 5 8 76.87 76.64 0.74 o 2 5 8 21.60 21.26 0.34 o 3 5 8 2.51 3.01 0.19 o 4 5 8 3.04 3.81 0.28 o 0 6 8 0.23 0.27 0.21 o 1 6 8 73.96 70.89 0.76 o 2 6 8 18.70 18.40 0.33 o 3 6 8 36.54 37.58 0.55 o 4 6 8 5.23 5.66 0.67 o 0 7 8 7.84 8.69 0.50 o 1 7 8 0.48 0.31 0.20 o 2 7 8 14.38 13.95 0.38 o 1 0 9 36.48 42.48 0.45 o 2 0 9 0.39 1.30 0.07 o 3 0 9 4.26 4.65 0.16 o 4 0 9 16.08 15.61 0.32 o 5 0 9 5.97 5.97 0.27 o 6 0 9 0.00 0.42 0.25 o 0 1 9 86.00 93.51 0.83 o 1 1 9 90.10 101.06 0.81 o 2 1 9 163.11 153.76 0.98 o 3 1 9 75.00 70.55 0.50 o 4 1 9 26.19 24.38 0.28 o 5 1 9 22.21 22.15 0.32 o 0 2 9 66.71 71.57 0.66 o 1 2 9 120.01 128.58 0.92 o 2 2 9 24.67 27.28 0.28 o 3 2 9 118.90 112.78 0.80 o 4 2 9 83.76 86.23 0.71 o 5 2 9 19.39 19.14 0.32 o 0 3 9 2.12 1.18 0.07 o 1 3 9 160.85 164.38 1.18 o 2 3 9 331.37 320.62 2.25 o 3 3 9 102.92 99.80 0.81 o 4 3 9 46.41 43.93 0.46 o 5 3 9 13.34 13.69 0.33 o 0 4 9 16.19 13.60 0.24 o 1 4 9 73.94 72.28 0.80 o 2 4 9 222.96 223.83 1.78 o 3 4 9 49.78 51.52 0.52 o 4 4 9 30.86 31.70 0.63 o 5 4 9 25.45 26.63 0.52 o 0 5 9 27.97 26.91 0.45 o 1 5 9 186.29 182.74 1.57 o 2 5 9 46.37 47.57 0.52 o 3 5 9 2.25 2.23 0.18 o 4 5 9 28.88 28.15 0.47 o 0 6 9 20.94 20.03 0.54 o 1 6 9 23.71 23.14 0.36 o 2 6 9 5.16 5.30 0.21 o 3 6 9 3.80 3.65 0.22 o 0 7 9 3.14 3.74 0.37 o 1 7 9 17.83 17.31 0.57 o 2 7 9 26.45 26.57 0.55 o 0 0 10 104.48 106.91 1.51 o 1 0 10 0.22 1.07 0.08 o 2 0 10 433.01 461.52 3.62 o 3 0 10 16.89 16.66 0.25 o 4 0 10 8.25 7.19 0.25 o 5 0 10 1.68 1.62 0.20 o 0 1 10 100.98 107.18 0.95 o 1 1 10 376.80 414.96 3.00 o 2 1 10 26.69 29.84 0.26 o 3 1 10 10.24 10.12 0.19 o 4 1 10 77.73 77.35 0.61 o 5 1 10 41.54 40.99 0.45 o 0 2 10 230.66 258.89 2.23 o 1 2 10 190.41 184.25 1.45 o 2 2 10 8.03 7.95 0.15 o 3 2 10 267.39 256.70 1.70 o 4 2 10 49.09 50.74 0.47 o 5 2 10 10.19 10.41 0.25 o 0 3 10 88.40 94.85 0.82 o 1 3 10 5.89 4.52 0.24 o 2 3 10 6.61 7.07 0.36 o 3 3 10 50.14 48.85 0.47 o 4 3 10 18.66 19.49 0.32 o 5 3 10 6.07 6.63 0.27 o 0 4 10 95.98 99.85 1.01 o 1 4 10 157.87 152.62 1.48 o 2 4 10 11.97 12.08 0.34 o 3 4 10 110.32 110.10 0.99 o 4 4 10 18.32 17.80 0.35 o 5 4 10 8.81 12.40 0.34 o 0 5 10 190.62 177.59 2.07 o 1 5 10 11.77 12.85 0.24 o 2 5 10 8.39 7.91 0.22 o 3 5 10 21.61 20.86 0.38 o 4 5 10 63.48 68.82 0.89 o 0 6 10 11.05 10.18 0.41 o 1 6 10 12.58 12.07 0.31 o 2 6 10 56.75 58.15 0.83 o 3 6 10 6.23 6.46 0.27 o 0 7 10 44.27 40.49 1.05 o 1 7 10 16.43 16.30 0.41 o 2 7 10 1.18 1.23 0.21 o 1 0 11 9.82 12.40 0.20 o 2 0 11 67.64 70.72 0.67 o 3 0 11 28.56 31.08 0.39 o 4 0 11 2.97 2.63 0.19 o 5 0 11 5.23 4.66 0.30 o 0 1 11 0.59 0.67 0.07 o 1 1 11 17.53 16.19 0.35 o 2 1 11 41.05 41.16 0.35 o 3 1 11 6.34 6.72 0.14 o 4 1 11 28.08 27.13 0.30 o 5 1 11 12.22 14.05 0.27 o 0 2 11 277.62 321.67 2.76 o 1 2 11 189.35 210.65 1.65 o 2 2 11 1.78 1.90 0.09 o 3 2 11 196.79 192.38 1.40 o 4 2 11 74.67 76.08 0.64 o 5 2 11 34.03 32.09 0.49 o 0 3 11 164.38 177.95 1.63 o 1 3 11 4.77 3.97 0.12 o 2 3 11 400.72 389.37 3.19 o 3 3 11 131.30 129.99 1.21 o 4 3 11 80.98 77.02 0.81 o 5 3 11 4.29 4.76 0.24 o 0 4 11 1.18 0.63 0.09 o 1 4 11 13.07 13.23 0.21 o 2 4 11 75.80 72.28 0.73 o 3 4 11 64.03 65.81 0.68 o 4 4 11 45.72 44.32 0.64 o 0 5 11 92.09 93.11 1.48 o 1 5 11 18.08 16.72 0.26 o 2 5 11 0.04 0.03 0.11 o 3 5 11 19.11 19.86 0.39 o 4 5 11 30.77 32.01 0.53 o 0 6 11 4.63 5.05 0.34 o 1 6 11 47.55 46.21 0.63 o 2 6 11 6.92 7.18 0.28 o 3 6 11 30.85 33.47 0.53 o 0 7 11 1.88 3.05 0.36 o 1 7 11 6.73 7.80 0.34 o 2 7 11 0.06 0.19 0.20 o 0 0 12 148.65 154.99 2.42 o 1 0 12 352.69 386.87 3.67 o 2 0 12 6.84 5.78 0.18 o 3 0 12 20.27 21.28 0.32 o 4 0 12 12.96 11.89 0.30 o 5 0 12 38.46 35.70 0.56 o 0 1 12 577.47 615.11 8.21 o 1 1 12 261.98 280.00 2.34 o 2 1 12 72.99 82.04 0.65 o 3 1 12 0.43 0.72 0.09 o 4 1 12 32.38 32.98 0.35 o 5 1 12 71.59 72.17 0.76 o 0 2 12 0.27 0.10 0.06 o 1 2 12 38.08 40.99 0.40 o 2 2 12 33.00 29.88 0.39 o 3 2 12 18.42 19.47 0.49 o 4 2 12 100.49 98.25 0.83 o 5 2 12 7.87 8.54 0.29 o 0 3 12 102.88 98.68 0.91 o 1 3 12 39.98 39.53 0.40 o 2 3 12 532.82 536.13 4.63 o 3 3 12 24.12 24.32 0.43 o 4 3 12 12.68 13.15 0.26 o 5 3 12 2.61 3.05 0.26 o 0 4 12 143.56 128.77 2.48 o 1 4 12 149.59 143.49 1.24 o 2 4 12 2.24 2.43 0.25 o 3 4 12 65.16 65.02 0.83 o 4 4 12 8.97 10.53 0.30 o 0 5 12 0.71 0.76 0.21 o 1 5 12 20.82 19.81 0.29 o 2 5 12 14.11 13.60 0.27 o 3 5 12 38.07 37.78 0.56 o 4 5 12 0.02 0.80 0.31 o 0 6 12 7.59 7.40 0.38 o 1 6 12 14.40 12.22 0.32 o 2 6 12 15.20 16.99 0.46 o 3 6 12 12.66 14.04 0.34 o 0 7 12 0.08 0.15 0.25 o 1 7 12 33.53 38.33 1.29 o 2 7 12 9.82 10.33 0.36 o 1 0 13 27.80 31.16 0.66 o 2 0 13 268.37 276.53 2.82 o 3 0 13 54.76 53.80 0.66 o 4 0 13 5.12 4.75 0.24 o 5 0 13 17.89 17.35 0.39 o 0 1 13 482.12 491.34 6.24 o 1 1 13 12.57 10.30 0.37 o 2 1 13 32.31 33.22 0.32 o 3 1 13 22.97 23.43 0.26 o 4 1 13 21.87 21.37 0.27 o 5 1 13 24.67 26.26 0.40 o 0 2 13 169.66 174.52 1.66 o 1 2 13 386.63 387.29 2.63 o 2 2 13 31.47 30.17 0.33 o 3 2 13 70.89 66.88 0.67 o 4 2 13 13.46 14.13 0.24 o 5 2 13 24.64 25.33 0.46 o 0 3 13 9.55 10.62 0.20 o 1 3 13 39.95 44.83 0.44 o 2 3 13 37.62 37.34 0.46 o 3 3 13 39.28 39.32 0.58 o 4 3 13 0.99 1.15 0.20 o 5 3 13 14.80 15.27 0.42 o 0 4 13 27.40 31.85 0.55 o 1 4 13 140.30 145.89 1.26 o 2 4 13 46.69 44.06 0.68 o 3 4 13 12.57 12.88 0.33 o 4 4 13 19.71 19.41 0.66 o 0 5 13 38.60 34.62 0.71 o 1 5 13 24.65 25.27 0.33 o 2 5 13 25.76 24.42 0.36 o 3 5 13 7.18 8.15 0.33 o 4 5 13 25.61 26.69 0.57 o 0 6 13 2.24 2.49 0.27 o 1 6 13 14.83 14.60 0.36 o 2 6 13 11.52 9.80 0.35 o 3 6 13 11.21 12.91 0.33 o 0 7 13 0.27 0.21 0.48 o 1 7 13 0.38 0.97 0.22 o 0 0 14 367.23 339.61 7.63 o 1 0 14 4.08 4.06 0.18 o 2 0 14 57.06 62.66 1.44 o 3 0 14 32.49 33.41 0.53 o 4 0 14 61.42 59.78 0.84 o 5 0 14 1.60 1.75 0.23 o 0 1 14 24.70 23.18 0.84 o 1 1 14 136.00 131.20 1.15 o 2 1 14 26.46 27.32 0.30 o 3 1 14 148.42 140.91 1.11 o 4 1 14 63.48 61.89 0.57 o 5 1 14 13.43 15.36 0.31 o 0 2 14 3.22 2.52 0.23 o 1 2 14 106.89 115.67 0.90 o 2 2 14 64.00 64.44 0.57 o 3 2 14 18.51 17.65 0.28 o 4 2 14 6.90 7.41 0.28 o 5 2 14 9.21 8.93 0.30 o 0 3 14 95.33 94.01 0.95 o 1 3 14 231.05 222.45 1.76 o 2 3 14 8.02 8.92 0.33 o 3 3 14 96.24 95.96 1.12 o 4 3 14 2.39 2.30 0.20 o 5 3 14 2.03 2.94 0.31 o 0 4 14 99.38 94.38 2.19 o 1 4 14 204.78 191.06 1.78 o 2 4 14 74.97 74.29 0.92 o 3 4 14 38.76 37.45 0.58 o 4 4 14 28.04 29.17 0.59 o 0 5 14 192.28 166.20 2.45 o 1 5 14 51.34 53.07 0.66 o 2 5 14 16.06 16.63 0.41 o 3 5 14 15.42 16.22 0.43 o 4 5 14 8.79 8.95 0.50 o 0 6 14 18.87 20.65 0.70 o 1 6 14 6.22 6.18 0.27 o 2 6 14 14.75 17.15 0.45 o 3 6 14 4.20 4.87 0.67 o 0 7 14 3.18 3.84 0.40 o 1 7 14 13.30 14.45 0.50 o 1 0 15 277.17 284.85 4.24 o 2 0 15 55.73 54.08 1.03 o 3 0 15 53.78 43.62 0.83 o 4 0 15 3.26 2.73 0.24 o 5 0 15 0.80 0.91 0.24 o 0 1 15 19.82 19.79 0.42 o 1 1 15 0.66 1.34 0.10 o 2 1 15 45.00 39.50 0.40 o 3 1 15 26.57 28.38 0.35 o 4 1 15 0.58 0.68 0.15 o 5 1 15 34.57 35.07 0.56 o 0 2 15 3.46 2.40 0.12 o 1 2 15 173.06 168.30 1.90 o 2 2 15 9.62 10.46 0.29 o 3 2 15 36.14 34.66 0.44 o 4 2 15 52.72 51.32 0.72 o 5 2 15 19.12 20.72 0.45 o 0 3 15 26.76 26.34 0.40 o 1 3 15 14.97 14.36 0.56 o 2 3 15 157.84 154.66 1.70 o 3 3 15 25.68 25.60 0.45 o 4 3 15 0.27 0.20 0.18 o 0 4 15 20.06 16.57 0.39 o 1 4 15 9.09 11.47 0.24 o 2 4 15 7.64 8.10 0.28 o 3 4 15 2.89 2.90 0.21 o 4 4 15 10.36 10.99 0.40 o 0 5 15 147.05 152.08 2.26 o 1 5 15 48.53 44.79 0.58 o 2 5 15 0.87 0.72 0.19 o 3 5 15 26.21 27.84 0.56 o 0 6 15 44.40 42.09 1.00 o 1 6 15 7.33 6.50 0.29 o 2 6 15 31.80 33.30 0.65 o 0 7 15 1.09 1.18 0.37 o 0 0 16 50.89 56.48 1.39 o 1 0 16 0.13 0.76 0.14 o 2 0 16 1.99 1.28 0.29 o 3 0 16 9.03 7.20 0.27 o 4 0 16 9.17 8.75 0.66 o 5 0 16 12.78 11.82 0.43 o 0 1 16 229.18 212.13 2.53 o 1 1 16 17.21 17.77 0.27 o 2 1 16 125.26 115.99 1.17 o 3 1 16 1.11 1.07 0.14 o 4 1 16 14.86 14.14 0.34 o 5 1 16 14.32 14.48 0.36 o 0 2 16 6.66 7.07 0.18 o 1 2 16 114.65 109.80 1.23 o 2 2 16 232.51 222.48 2.31 o 3 2 16 28.23 26.22 0.45 o 4 2 16 33.33 33.53 0.51 o 5 2 16 5.11 4.36 0.39 o 0 3 16 0.34 0.01 0.13 o 1 3 16 52.70 42.70 0.61 o 2 3 16 111.21 107.96 1.25 o 3 3 16 45.91 45.29 0.82 o 4 3 16 1.34 1.12 0.23 o 0 4 16 220.74 203.71 4.76 o 1 4 16 74.26 66.34 0.99 o 2 4 16 6.40 6.49 0.28 o 3 4 16 50.20 47.63 0.68 o 4 4 16 12.06 10.74 0.37 o 0 5 16 102.12 105.57 1.99 o 1 5 16 33.04 31.80 0.46 o 2 5 16 2.46 2.94 0.29 o 3 5 16 1.29 1.43 0.23 o 0 6 16 0.13 0.30 0.26 o 1 6 16 23.57 23.96 0.50 o 2 6 16 55.85 58.76 1.78 o 1 0 17 11.40 11.95 0.30 o 2 0 17 15.59 11.87 0.36 o 3 0 17 0.03 0.61 0.27 o 4 0 17 6.21 5.11 0.30 o 5 0 17 1.05 1.51 0.24 o 0 1 17 743.02 684.06 10.39 o 1 1 17 9.56 9.66 0.21 o 2 1 17 9.16 8.52 0.24 o 3 1 17 4.91 5.92 0.23 o 4 1 17 36.98 37.52 0.75 o 5 1 17 13.54 12.93 0.37 o 0 2 17 7.42 8.65 0.25 o 1 2 17 129.20 121.12 1.47 o 2 2 17 5.42 6.83 0.42 o 3 2 17 30.71 29.45 0.48 o 4 2 17 3.87 5.46 0.50 o 0 3 17 9.74 10.04 0.39 o 1 3 17 14.65 12.60 0.36 o 2 3 17 112.50 107.09 1.24 o 3 3 17 16.29 16.99 0.38 o 4 3 17 10.97 10.89 0.38 o 0 4 17 3.48 4.18 0.51 o 1 4 17 0.22 0.42 0.17 o 2 4 17 1.88 1.78 0.18 o 3 4 17 4.57 5.19 0.30 o 4 4 17 18.32 17.72 2.15 o 0 5 17 1.70 1.83 0.26 o 1 5 17 32.41 31.92 0.56 o 2 5 17 3.34 3.66 1.09 o 3 5 17 27.88 31.04 1.18 o 0 6 17 14.27 15.88 0.57 o 1 6 17 21.16 20.79 0.46 o 2 6 17 7.25 6.92 0.63 o 0 0 18 60.47 61.71 1.80 o 1 0 18 491.82 491.82 9.20 o 2 0 18 0.75 1.54 0.21 o 3 0 18 106.52 102.29 1.67 o 4 0 18 1.81 1.69 0.22 o 0 1 18 153.14 156.14 2.23 o 1 1 18 137.69 136.52 2.21 o 2 1 18 1.91 3.07 0.16 o 3 1 18 13.61 13.16 0.32 o 4 1 18 36.86 36.29 0.75 o 0 2 18 90.62 80.38 1.50 o 1 2 18 112.66 112.12 1.85 o 2 2 18 38.48 37.69 0.64 o 3 2 18 22.85 22.31 0.80 o 4 2 18 7.46 7.90 0.34 o 0 3 18 38.06 33.30 0.76 o 1 3 18 15.83 14.05 0.42 o 2 3 18 39.98 36.89 0.76 o 3 3 18 2.10 2.53 0.23 o 4 3 18 7.42 8.30 0.33 o 0 4 18 0.13 -0.16 0.30 o 1 4 18 6.83 5.91 0.34 o 2 4 18 7.86 7.21 0.38 o 3 4 18 0.09 1.05 0.51 o 0 5 18 16.38 12.38 0.48 o 1 5 18 21.30 21.19 0.57 o 2 5 18 2.32 2.67 0.29 o 3 5 18 2.96 3.03 0.38 o 0 6 18 34.64 32.05 0.85 o 1 6 18 39.69 40.53 0.69 o 1 0 19 333.80 338.57 8.25 o 2 0 19 95.81 95.15 4.35 o 3 0 19 118.43 111.70 1.90 o 4 0 19 0.06 0.23 0.19 o 0 1 19 116.57 120.15 4.64 o 1 1 19 108.66 103.94 2.19 o 2 1 19 32.93 32.60 0.69 o 3 1 19 41.40 39.87 0.61 o 4 1 19 25.47 27.51 0.65 o 0 2 19 1.33 1.70 0.22 o 1 2 19 45.51 45.88 0.82 o 2 2 19 25.68 24.84 0.58 o 3 2 19 23.41 22.58 0.62 o 4 2 19 10.20 12.06 0.47 o 0 3 19 0.56 0.39 0.24 o 1 3 19 13.61 14.65 0.43 o 2 3 19 12.07 10.57 0.41 o 3 3 19 4.38 5.52 0.35 o 4 3 19 26.33 28.15 0.59 o 0 4 19 14.20 11.95 0.44 o 1 4 19 13.57 12.04 0.42 o 2 4 19 4.67 5.98 0.34 o 3 4 19 17.49 17.94 0.45 o 0 5 19 0.36 0.52 0.23 o 1 5 19 5.76 7.34 0.38 o 2 5 19 3.53 3.42 0.38 o 0 6 19 0.48 0.24 0.26 o 1 6 19 14.91 16.76 0.78 o 0 0 20 202.72 196.33 9.80 o 1 0 20 61.04 71.37 5.23 o 2 0 20 16.44 21.96 1.17 o 3 0 20 8.35 8.47 0.52 o 4 0 20 0.03 0.01 0.25 o 0 1 20 172.99 167.83 3.26 o 1 1 20 13.05 14.80 0.33 o 2 1 20 223.08 208.64 2.76 o 3 1 20 3.21 5.03 0.59 o 4 1 20 23.33 24.20 0.61 o 0 2 20 1.09 1.63 0.19 o 1 2 20 48.36 41.41 0.77 o 2 2 20 4.46 5.09 0.32 o 3 2 20 31.60 32.55 0.80 o 4 2 20 7.10 9.51 0.74 o 0 3 20 0.75 0.83 0.20 o 1 3 20 13.95 11.69 0.40 o 2 3 20 1.73 2.04 0.25 o 3 3 20 26.34 30.28 0.69 o 0 4 20 1.24 1.83 0.26 o 1 4 20 10.85 9.87 0.40 o 2 4 20 6.28 7.02 0.39 o 3 4 20 22.92 24.43 0.64 o 0 5 20 28.00 26.59 0.71 o 1 5 20 2.80 3.65 0.33 o 2 5 20 6.19 6.19 0.40 o 1 0 21 0.86 1.55 0.25 o 2 0 21 135.70 126.87 3.33 o 3 0 21 16.51 17.87 0.65 o 0 1 21 123.75 116.07 2.68 o 1 1 21 38.87 38.13 0.60 o 2 1 21 32.97 33.67 0.63 o 3 1 21 15.02 16.03 0.48 o 4 1 21 9.65 10.20 0.45 o 0 2 21 145.27 132.95 2.38 o 1 2 21 25.74 21.10 0.51 o 2 2 21 5.71 5.33 0.33 o 3 2 21 52.69 50.78 0.93 o 0 3 21 28.82 31.20 0.75 o 1 3 21 23.79 22.70 0.55 o 2 3 21 10.89 9.54 0.41 o 3 3 21 1.82 2.44 0.48 o 0 4 21 4.33 6.18 0.55 o 1 4 21 15.00 15.19 0.48 o 2 4 21 24.87 24.65 0.64 o 0 5 21 0.77 1.26 0.26 o 1 5 21 13.08 13.15 0.48 o 0 0 22 2.45 2.55 0.37 o 1 0 22 130.55 122.56 2.21 o 3 0 22 0.16 0.34 0.24 o 0 1 22 7.76 7.75 0.39 o 1 1 22 12.35 13.14 0.33 o 2 1 22 6.18 6.92 0.59 o 3 1 22 8.15 6.71 0.36 o 0 2 22 4.42 5.52 0.36 o 1 2 22 13.56 12.79 0.41 o 2 2 22 10.66 10.16 0.40 o 3 2 22 8.50 10.73 0.74 o 0 3 22 3.35 3.31 0.30 o 1 3 22 24.87 22.21 0.56 o 2 3 22 6.54 7.11 0.33 o 3 3 22 19.15 18.51 0.55 o 0 4 22 5.06 3.90 0.32 o 1 4 22 0.10 0.48 0.22 o 2 4 22 16.20 18.26 0.55 o 0 5 22 7.10 8.50 0.42 o 1 5 22 23.15 26.19 0.66 o 1 0 23 24.13 24.20 0.65 o 3 0 23 5.46 6.99 0.70 o 0 1 23 5.08 4.67 0.35 o 1 1 23 49.10 46.65 0.70 o 2 1 23 30.14 31.82 1.18 o 3 1 23 23.57 22.11 0.57 o 0 2 23 15.38 14.96 0.50 o 1 2 23 14.16 13.34 0.43 o 2 2 23 17.84 17.38 0.51 o 3 2 23 13.80 14.93 0.98 o 0 3 23 16.05 14.99 0.49 o 1 3 23 7.21 7.73 0.36 o 2 3 23 0.97 1.31 0.25 o 0 4 23 9.30 10.90 0.44 o 1 4 23 32.96 36.39 0.77 o 2 4 23 9.27 10.03 0.45 o 0 0 24 0.11 0.41 0.33 o 1 0 24 19.28 18.43 0.72 o 3 0 24 4.07 4.48 0.59 o 0 1 24 0.67 0.39 0.23 o 1 1 24 0.53 0.93 0.16 o 2 1 24 9.12 9.80 0.70 o 3 1 24 4.97 4.74 0.59 o 0 2 24 1.04 0.93 0.24 o 1 2 24 0.13 0.58 0.22 o 2 2 24 29.41 27.39 0.64 o 3 2 24 29.18 25.07 7.42 o 0 3 24 4.12 2.21 0.26 o 1 3 24 8.50 9.06 0.38 o 2 3 24 12.75 13.33 0.48 o 0 4 24 10.81 10.85 0.57 o 1 4 24 7.05 9.46 0.42 o 1 0 25 26.96 29.40 0.74 o 2 0 25 0.36 0.41 0.41 o 3 0 25 11.02 14.13 0.92 o 0 1 25 13.86 12.76 0.48 o 1 1 25 17.34 17.17 0.48 o 2 1 25 23.53 16.63 6.79 o 0 2 25 2.53 1.62 0.27 o 1 2 25 7.99 8.52 0.38 o 2 2 25 27.20 28.06 0.58 o 0 3 25 105.83 110.08 3.61 o 1 3 25 0.37 0.16 0.22 o 2 3 25 5.80 9.61 3.50 o 0 0 26 32.71 33.26 1.15 o 1 0 26 46.09 50.62 1.10 o 2 0 26 0.01 0.04 0.41 o 0 1 26 26.15 27.25 0.72 o 1 1 26 3.65 4.70 0.33 o 2 1 26 0.36 0.85 0.44 o 0 2 26 0.41 0.27 0.24 o 1 2 26 16.74 17.24 0.51 o 2 2 26 30.31 31.67 1.40 o 0 3 26 15.09 18.92 1.33 o 1 3 26 6.81 9.42 0.42 o 1 0 27 0.15 0.79 0.26 o 2 0 27 0.86 1.00 0.48 o 0 1 27 14.97 16.84 0.57 o 1 1 27 26.42 26.33 0.67 o 0 2 27 2.53 2.13 0.28 o 1 2 27 1.35 1.99 0.27 o 0 0 28 72.65 73.59 2.11 o 1 0 28 0.24 0.63 0.35 o 0 1 28 6.98 8.62 0.45 o 1 1 28 11.21 12.94 0.45 o