#------------------------------------------------------------------------------ #$Date: 2011-10-06 14:27:20 +0300 (Thu, 06 Oct 2011) $ #$Revision: 27511 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/10/2231046.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231046_Fobs loop_ _publ_author_name 'Wang, Zhi-jian' 'Jia, Wei-min' 'Liu, Qing-lei' 'Wang, Wei' _publ_section_title ; 3-(4-Amino-3-ethyl-5-sulfanylidene-4,5-dihydro-1H-1,2,4-triazol-1-yl)-3-(2-chlorophenyl)-1-phenylpropan-1-one ; _journal_coeditor_code CV5121 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1922 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.606 _cell_angle_gamma 90.000 _cell_length_a 29.0226 _cell_length_b 7.5606 _cell_length_c 18.2861 _exptl_crystal_F_000 1616.00 _reflns_d_resolution_high 0.7623 _[local]_cod_data_source_file cv5121Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' shelx in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 363.85 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2723.76 2926.24 26.89 o 4 0 0 578.00 698.51 13.85 o 6 0 0 1249.64 1006.51 15.84 o 8 0 0 37812.86 40928.55 432.06 o 10 0 0 58553.76 64154.77 969.09 o 12 0 0 42.40 57.56 12.48 o 14 0 0 11662.05 12981.78 273.72 o 16 0 0 2452.82 2492.36 56.80 o 18 0 0 1837.63 1621.45 56.21 o 20 0 0 49.03 38.97 19.21 o 22 0 0 650.73 665.18 35.08 o 24 0 0 2977.64 3042.59 108.27 o 26 0 0 358.91 345.67 44.51 o 28 0 0 5265.88 5401.84 239.01 o 30 0 0 564.58 527.65 79.51 o 32 0 0 1050.40 971.53 114.42 o 34 0 0 926.03 934.80 98.16 o 1 1 0 2785.30 2917.83 20.34 o 3 1 0 14.79 33.25 3.64 o 5 1 0 61086.34 67415.88 1086.89 o 7 1 0 3033.53 3202.33 24.33 o 9 1 0 5747.68 5690.64 25.59 o 11 1 0 21410.43 23217.01 200.33 o 13 1 0 2907.52 2771.50 47.29 o 15 1 0 3182.25 3711.72 43.83 o 17 1 0 148.68 152.86 14.96 o 19 1 0 13337.27 13420.79 280.28 o 21 1 0 1289.45 1288.47 39.10 o 23 1 0 8389.77 8148.84 153.07 o 25 1 0 476.91 363.37 27.31 o 27 1 0 122.15 118.91 44.01 o 29 1 0 47.37 45.38 21.51 o 31 1 0 1.38 14.36 21.31 o 33 1 0 1198.94 1181.88 76.01 o 35 1 0 2.21 13.71 18.60 o 0 2 0 9295.65 9758.34 80.45 o 2 2 0 16550.63 17854.42 91.49 o 4 2 0 386.13 401.09 7.43 o 6 2 0 919.81 917.71 10.38 o 8 2 0 12523.01 13185.78 163.73 o 10 2 0 130.04 123.31 12.69 o 12 2 0 4749.65 4860.30 61.09 o 14 2 0 1099.68 1265.67 38.73 o 16 2 0 95.40 80.42 25.24 o 18 2 0 455.18 428.55 26.30 o 20 2 0 36.62 49.44 20.77 o 22 2 0 973.30 897.65 52.35 o 24 2 0 43.48 37.32 17.52 o 26 2 0 323.67 282.93 80.97 o 28 2 0 157.22 161.93 52.65 o 30 2 0 158.10 162.74 64.70 o 32 2 0 299.49 272.86 58.67 o 34 2 0 7.82 3.61 40.46 o 1 3 0 329.93 261.39 9.58 o 3 3 0 23208.38 26156.35 218.77 o 5 3 0 22263.63 23476.65 200.73 o 7 3 0 1030.57 876.62 21.85 o 9 3 0 607.63 508.71 12.78 o 11 3 0 4292.49 3954.60 60.81 o 13 3 0 1043.15 945.47 30.28 o 15 3 0 2121.38 2071.91 43.80 o 17 3 0 1434.42 1414.80 47.73 o 19 3 0 1811.35 1738.56 66.94 o 21 3 0 24.26 33.18 16.15 o 23 3 0 878.88 935.92 52.17 o 25 3 0 6396.22 6327.03 135.64 o 27 3 0 3.19 9.90 16.88 o 29 3 0 41.02 65.78 37.75 o 31 3 0 364.35 449.12 48.66 o 33 3 0 497.19 476.75 50.76 o 0 4 0 28071.54 31375.46 386.10 o 2 4 0 4990.30 5342.65 49.84 o 4 4 0 561.96 550.73 15.81 o 6 4 0 8011.34 7621.98 81.44 o 8 4 0 415.53 386.34 17.48 o 10 4 0 3303.83 3093.59 49.92 o 12 4 0 11.68 8.19 4.82 o 14 4 0 134.92 139.61 11.35 o 16 4 0 930.59 899.78 23.32 o 18 4 0 2669.67 2552.71 99.37 o 20 4 0 989.19 995.05 45.35 o 22 4 0 223.97 162.75 34.34 o 24 4 0 9319.67 9602.84 181.00 o 26 4 0 1508.75 1627.28 73.26 o 28 4 0 2669.57 2598.83 153.18 o 30 4 0 2829.96 2988.02 124.84 o 32 4 0 21.21 21.10 26.57 o 1 5 0 477.14 480.92 18.96 o 3 5 0 4595.44 4623.59 61.54 o 5 5 0 0.85 6.48 5.38 o 7 5 0 9089.16 8792.67 200.14 o 9 5 0 416.80 432.56 22.84 o 11 5 0 2182.31 2024.38 56.00 o 13 5 0 1807.99 1668.88 66.89 o 15 5 0 230.97 214.33 18.86 o 17 5 0 523.15 427.78 45.70 o 19 5 0 5352.17 5423.49 179.84 o 21 5 0 1677.05 1693.30 84.72 o 23 5 0 13.20 39.23 18.76 o 25 5 0 1348.64 1370.01 72.87 o 27 5 0 1059.59 1086.97 68.54 o 29 5 0 392.85 434.25 52.28 o 0 6 0 343.83 319.04 29.88 o 2 6 0 770.09 778.16 26.42 o 4 6 0 1047.43 1032.28 28.50 o 6 6 0 2627.07 2497.93 56.96 o 8 6 0 3379.34 3392.45 85.42 o 10 6 0 100.24 95.31 36.06 o 12 6 0 296.68 317.91 29.86 o 14 6 0 757.82 781.35 32.17 o 16 6 0 1904.08 1973.88 73.13 o 18 6 0 269.16 223.66 41.98 o 20 6 0 267.55 307.62 49.54 o 22 6 0 2109.74 2349.40 121.74 o 24 6 0 12.38 14.93 26.48 o 26 6 0 589.55 626.98 52.40 o 28 6 0 895.70 956.98 64.50 o 1 7 0 1441.28 1441.32 53.72 o 3 7 0 139.21 119.15 29.43 o 5 7 0 346.93 400.89 41.99 o 7 7 0 116.70 71.74 29.90 o 9 7 0 0.25 10.34 8.75 o 11 7 0 610.88 559.99 42.84 o 13 7 0 374.04 357.77 52.43 o 15 7 0 13.09 18.52 23.36 o 17 7 0 619.19 658.72 56.36 o 19 7 0 514.28 589.55 64.64 o 21 7 0 207.44 183.25 81.96 o 23 7 0 411.86 403.33 80.67 o 25 7 0 1600.09 1791.28 129.69 o 0 8 0 3803.90 3371.40 227.46 o 2 8 0 274.59 271.68 75.75 o 4 8 0 484.45 386.52 39.13 o 6 8 0 720.55 752.54 53.71 o 8 8 0 377.06 437.06 46.94 o 10 8 0 1840.99 1806.37 102.73 o 12 8 0 360.59 345.85 47.95 o 14 8 0 187.64 155.45 88.46 o 16 8 0 123.84 98.02 80.64 o 18 8 0 231.27 299.64 106.21 o 20 8 0 193.29 127.42 107.55 o 1 9 0 303.16 214.09 176.35 o 3 9 0 3681.59 4094.55 193.89 o 5 9 0 698.26 540.45 66.78 o 7 9 0 1944.13 2037.04 186.90 o 9 9 0 342.25 300.59 61.66 o 11 9 0 296.77 236.94 96.56 o 13 9 0 26.35 14.51 33.28 o 15 9 0 205.66 180.96 92.63 o -35 1 1 2513.50 2606.38 133.12 o -33 1 1 197.23 178.85 88.34 o -31 1 1 1442.43 1474.05 73.78 o -29 1 1 271.88 272.32 44.69 o -27 1 1 372.94 322.10 41.50 o -25 1 1 5187.56 4918.21 314.19 o -23 1 1 2073.83 2129.33 78.49 o -21 1 1 27.63 42.92 13.87 o -19 1 1 1321.10 1309.53 35.90 o -17 1 1 2929.83 2827.51 41.53 o -15 1 1 5480.94 5868.47 56.89 o -13 1 1 38.41 128.25 8.69 o -11 1 1 1921.26 1537.76 24.57 o -9 1 1 15794.84 17515.62 163.44 o -7 1 1 42902.53 45995.32 741.53 o -5 1 1 39061.02 43072.10 312.73 o -3 1 1 3888.29 3937.47 37.68 o -1 1 1 48.04 73.11 5.15 o 1 1 1 3129.16 2996.05 42.56 o 3 1 1 2746.21 2647.12 39.55 o 5 1 1 1454.16 1356.03 12.88 o 7 1 1 9310.22 9588.17 111.74 o 9 1 1 58.27 57.09 8.23 o 11 1 1 18094.26 19501.41 252.62 o 13 1 1 208.82 226.79 10.54 o 15 1 1 1852.24 1809.63 36.33 o 17 1 1 11411.17 9899.60 390.51 o 19 1 1 2.04 6.86 5.96 o 21 1 1 5544.64 5166.83 131.79 o 23 1 1 2624.21 2638.80 70.64 o 25 1 1 67.87 38.77 14.45 o 27 1 1 1707.67 1663.96 61.40 o 29 1 1 32.90 28.39 16.42 o 31 1 1 344.95 335.14 50.50 o 33 1 1 219.75 246.62 53.67 o 35 1 1 31.64 31.39 42.88 o -34 2 1 1344.97 1431.46 106.15 o -32 2 1 620.18 567.88 38.10 o -30 2 1 3181.42 3281.85 104.24 o -28 2 1 0.71 -1.17 22.76 o -26 2 1 8728.06 9030.93 180.03 o -24 2 1 1041.97 932.10 52.84 o -22 2 1 607.71 548.12 37.54 o -20 2 1 505.17 443.90 30.74 o -18 2 1 1960.80 1870.37 47.01 o -16 2 1 4496.21 4446.09 70.33 o -14 2 1 411.51 486.49 23.18 o -12 2 1 20251.83 20485.18 236.82 o -10 2 1 4369.35 4649.46 37.75 o -8 2 1 5851.05 5886.93 60.22 o -6 2 1 12279.79 12852.02 144.68 o -4 2 1 452.22 418.96 8.76 o -2 2 1 51016.42 56912.70 376.96 o 0 2 1 449.11 539.97 9.73 o 2 2 1 9633.24 10109.41 116.14 o 4 2 1 1613.97 1672.68 20.82 o 6 2 1 23093.76 25030.27 216.60 o 8 2 1 8429.66 8583.09 79.97 o 10 2 1 167.07 157.96 8.61 o 12 2 1 26554.67 29836.24 590.75 o 14 2 1 6.14 4.00 8.74 o 16 2 1 4558.73 4572.07 87.64 o 18 2 1 224.80 158.22 21.19 o 20 2 1 206.01 231.31 50.35 o 22 2 1 10589.43 10771.79 208.78 o 24 2 1 1896.64 1873.10 68.63 o 26 2 1 5746.89 5734.18 126.54 o 28 2 1 1004.16 1019.43 52.81 o 30 2 1 632.37 642.27 43.58 o 32 2 1 783.06 850.17 83.97 o 34 2 1 21.14 6.78 23.46 o -33 3 1 351.04 271.37 47.43 o -31 3 1 1140.19 1122.19 70.95 o -29 3 1 76.86 99.23 53.08 o -27 3 1 160.43 201.16 41.55 o -25 3 1 1794.98 1810.91 140.98 o -23 3 1 317.23 345.26 48.15 o -21 3 1 174.18 189.52 55.15 o -19 3 1 997.32 1016.29 39.22 o -17 3 1 53.13 71.46 22.58 o -15 3 1 2042.50 1926.97 49.79 o -13 3 1 3821.31 3821.45 58.75 o -11 3 1 12814.12 14756.20 120.33 o -9 3 1 1877.00 1602.26 29.02 o -7 3 1 1844.42 1539.20 25.39 o -5 3 1 21083.84 23942.64 216.46 o -3 3 1 8093.29 7982.77 52.51 o -1 3 1 215.23 293.34 10.11 o 1 3 1 6025.44 6089.24 32.75 o 3 3 1 31.48 60.97 6.63 o 5 3 1 1655.57 1667.91 31.18 o 7 3 1 1063.12 1220.66 26.32 o 9 3 1 6473.64 6756.98 88.18 o 11 3 1 1801.46 1635.27 29.41 o 13 3 1 0.27 6.73 6.70 o 15 3 1 122.37 141.69 18.91 o 17 3 1 4695.48 4838.88 92.68 o 19 3 1 6088.81 5990.66 172.19 o 21 3 1 2300.29 2475.98 66.14 o 23 3 1 1516.20 1572.49 62.16 o 25 3 1 642.22 690.17 59.72 o 27 3 1 79.64 72.72 40.11 o 29 3 1 37.33 37.83 25.30 o 31 3 1 11.11 10.23 21.09 o 33 3 1 80.25 88.76 80.96 o -32 4 1 1.13 11.79 18.94 o -30 4 1 770.99 675.59 61.94 o -28 4 1 388.72 400.79 67.49 o -26 4 1 111.05 115.88 42.66 o -24 4 1 124.39 114.13 42.62 o -22 4 1 83.75 87.89 33.89 o -20 4 1 1721.75 1740.90 65.66 o -18 4 1 1019.23 857.17 29.23 o -16 4 1 834.59 824.24 23.83 o -14 4 1 4071.97 4067.26 65.08 o -12 4 1 6473.75 6216.52 75.64 o -10 4 1 888.36 831.50 20.61 o -8 4 1 1631.95 1840.40 33.21 o -6 4 1 618.91 579.61 17.42 o -4 4 1 19986.68 22240.66 288.58 o -2 4 1 1011.13 1196.16 24.93 o 0 4 1 79.80 122.45 10.92 o 2 4 1 1513.71 1608.60 30.63 o 4 4 1 385.99 338.08 12.40 o 6 4 1 24.73 29.63 9.52 o 8 4 1 3373.88 3633.32 53.60 o 10 4 1 1978.13 2076.33 45.79 o 12 4 1 214.25 217.70 14.38 o 14 4 1 15224.91 15867.46 242.02 o 16 4 1 104.23 88.56 20.84 o 18 4 1 7847.07 7784.86 235.90 o 20 4 1 49.97 39.62 17.06 o 22 4 1 1060.41 1022.77 60.03 o 24 4 1 136.95 157.48 55.90 o 26 4 1 59.04 67.51 32.48 o 28 4 1 548.75 564.85 52.50 o 30 4 1 386.31 355.84 81.24 o 32 4 1 254.84 183.03 115.36 o -31 5 1 1016.47 1065.10 75.58 o -29 5 1 496.25 509.48 52.03 o -27 5 1 1413.67 1576.99 80.73 o -25 5 1 892.44 884.88 77.87 o -23 5 1 304.71 271.08 65.04 o -21 5 1 9.73 15.28 14.29 o -19 5 1 333.42 320.83 97.16 o -17 5 1 80.22 69.62 29.39 o -15 5 1 41.60 32.19 9.80 o -13 5 1 3634.90 3414.01 83.73 o -11 5 1 23.11 21.79 9.05 o -9 5 1 1673.78 1723.70 40.89 o -7 5 1 11425.60 11249.42 237.03 o -5 5 1 2994.84 2720.25 59.77 o -3 5 1 225.29 238.39 13.54 o -1 5 1 15745.19 14706.64 296.04 o 1 5 1 111.18 130.07 12.70 o 3 5 1 1063.93 992.08 26.38 o 5 5 1 236.66 244.21 11.30 o 7 5 1 2649.29 2457.98 46.67 o 9 5 1 1958.82 2016.82 51.01 o 11 5 1 1487.05 1353.25 32.19 o 13 5 1 308.70 302.15 23.09 o 15 5 1 3604.38 3479.67 80.98 o 17 5 1 4574.82 4511.07 116.68 o 19 5 1 335.04 348.41 68.11 o 21 5 1 946.70 971.37 60.89 o 23 5 1 87.53 87.20 34.98 o 25 5 1 526.49 539.34 55.20 o 27 5 1 279.36 243.03 128.80 o 29 5 1 273.56 211.62 72.65 o -28 6 1 85.54 58.68 42.20 o -26 6 1 762.39 805.36 57.11 o -24 6 1 1.35 8.35 15.77 o -22 6 1 2383.50 2289.03 107.45 o -20 6 1 788.57 881.35 51.76 o -18 6 1 4454.14 4392.41 145.18 o -16 6 1 59.91 78.30 33.79 o -14 6 1 98.51 83.80 18.45 o -12 6 1 4862.58 5150.28 90.27 o -10 6 1 165.92 110.62 26.00 o -8 6 1 5106.67 4995.56 112.38 o -6 6 1 4204.89 4014.00 70.42 o -4 6 1 994.31 863.50 26.82 o -2 6 1 5041.77 4611.16 142.66 o 0 6 1 67.76 50.48 16.75 o 2 6 1 1932.51 1700.91 39.91 o 4 6 1 2634.27 2420.82 38.21 o 6 6 1 27.11 33.32 17.65 o 8 6 1 187.38 200.64 53.56 o 10 6 1 227.59 246.24 43.01 o 12 6 1 3401.74 3579.49 74.91 o 14 6 1 0.08 4.04 14.49 o 16 6 1 275.27 310.90 68.40 o 18 6 1 284.31 271.30 94.47 o 20 6 1 350.20 328.63 50.92 o 22 6 1 1509.90 1472.61 67.00 o 24 6 1 72.38 37.99 25.48 o 26 6 1 1009.35 969.53 80.37 o -25 7 1 0.05 15.80 24.98 o -23 7 1 333.86 297.24 161.36 o -21 7 1 114.39 77.22 49.23 o -19 7 1 204.50 164.93 66.81 o -17 7 1 41.17 52.77 27.69 o -15 7 1 778.60 788.90 44.57 o -13 7 1 75.88 57.78 30.44 o -11 7 1 231.37 202.54 32.99 o -9 7 1 297.75 343.85 42.03 o -7 7 1 2144.72 1930.75 71.18 o -5 7 1 2394.86 2442.43 70.44 o -3 7 1 3063.58 2886.78 91.90 o -1 7 1 283.20 279.86 33.43 o 1 7 1 1858.64 1978.46 63.24 o 3 7 1 2669.95 2665.65 67.69 o 5 7 1 448.06 415.64 37.80 o 7 7 1 54.92 59.97 27.62 o 9 7 1 530.85 595.45 33.49 o 11 7 1 183.82 196.95 27.11 o 13 7 1 78.50 92.77 37.66 o 15 7 1 173.59 153.99 80.01 o 17 7 1 120.82 141.45 78.70 o 19 7 1 2785.88 3125.38 196.05 o 21 7 1 107.49 114.91 77.13 o 23 7 1 181.38 124.12 73.34 o -20 8 1 211.52 166.11 135.36 o -18 8 1 21.85 11.90 30.93 o -16 8 1 3397.86 3675.17 158.72 o -14 8 1 188.36 228.62 63.88 o -12 8 1 4.75 16.49 27.65 o -10 8 1 7323.32 7517.82 234.81 o -8 8 1 560.41 500.81 49.32 o -6 8 1 3851.10 3866.27 269.24 o -4 8 1 117.40 164.53 57.15 o -2 8 1 433.63 397.22 42.30 o 0 8 1 1686.25 1504.51 62.82 o 2 8 1 620.17 568.60 52.16 o 4 8 1 1.44 6.01 18.65 o 6 8 1 41.21 31.59 24.03 o 8 8 1 270.05 162.34 90.48 o 10 8 1 7.13 28.45 38.46 o 12 8 1 1764.83 1724.57 115.17 o 14 8 1 438.40 376.10 80.31 o 16 8 1 369.11 326.09 126.15 o 18 8 1 878.57 994.43 90.59 o 20 8 1 2704.15 2984.89 185.19 o -15 9 1 41.02 31.02 26.11 o -13 9 1 1.01 16.64 35.81 o -11 9 1 2006.83 1959.14 175.30 o -9 9 1 18.86 20.79 24.96 o -7 9 1 974.64 981.43 77.40 o -5 9 1 157.60 159.25 87.37 o -3 9 1 1074.91 1206.87 143.43 o -1 9 1 2850.94 2977.42 165.81 o 1 9 1 296.56 321.97 77.35 o 3 9 1 33.68 26.18 42.61 o 7 9 1 556.88 460.47 68.19 o 9 9 1 7.35 8.69 24.35 o 11 9 1 449.26 370.76 76.13 o 13 9 1 149.57 91.76 141.75 o -36 0 2 1181.91 1162.80 132.43 o -34 0 2 229.55 159.26 173.33 o -32 0 2 1008.97 1183.27 97.51 o -30 0 2 64.81 70.34 46.54 o -28 0 2 69.86 45.33 25.89 o -26 0 2 488.93 425.47 47.98 o -24 0 2 1231.29 1033.14 150.57 o -22 0 2 655.95 555.49 34.38 o -20 0 2 54.44 26.16 11.84 o -18 0 2 10350.36 10731.20 158.58 o -16 0 2 9746.33 9774.44 263.49 o -14 0 2 34766.03 36849.47 796.54 o -12 0 2 166.22 168.14 12.18 o -10 0 2 19101.06 21474.37 257.77 o -6 0 2 19963.36 21593.33 230.12 o -4 0 2 10082.94 10928.73 152.85 o 0 0 2 1957.88 2137.69 19.00 o 2 0 2 533.85 573.17 12.82 o 4 0 2 58578.56 65100.94 1318.91 o 6 0 2 58787.32 64764.62 525.00 o 8 0 2 192.64 219.87 13.52 o 10 0 2 20311.00 19195.16 170.19 o 12 0 2 17.32 24.83 9.34 o 14 0 2 16334.97 16931.51 443.75 o 16 0 2 1884.67 1535.97 49.76 o 18 0 2 154.99 155.51 23.08 o 20 0 2 6083.56 5981.87 172.19 o 22 0 2 32.71 33.35 18.34 o 24 0 2 3109.64 3072.57 90.58 o 26 0 2 1535.75 1493.54 67.32 o 28 0 2 23.88 67.23 40.73 o 30 0 2 223.07 198.14 168.89 o 32 0 2 2568.58 2723.94 153.17 o 34 0 2 1397.45 1479.70 140.06 o -35 1 2 260.23 275.76 60.40 o -33 1 2 320.91 354.35 54.09 o -31 1 2 0.13 10.53 18.20 o -29 1 2 207.70 228.02 94.16 o -27 1 2 318.31 253.56 39.14 o -25 1 2 4447.34 4424.45 87.65 o -23 1 2 9.91 12.17 8.32 o -21 1 2 2605.47 2545.08 59.82 o -19 1 2 21852.44 23465.10 268.87 o -17 1 2 1636.48 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186.65 113.29 53.78 o -16 4 21 153.79 90.31 46.28 o -14 4 21 87.66 90.69 37.76 o -12 4 21 234.46 172.36 84.09 o -10 4 21 573.06 573.21 54.09 o -8 4 21 307.99 305.15 91.00 o -6 4 21 28.25 34.54 28.06 o -4 4 21 1.12 6.75 23.45 o -2 4 21 12.46 19.94 26.25 o -24 0 22 406.17 447.85 67.86 o -22 0 22 41.36 35.74 28.95 o -20 0 22 0.45 4.64 26.60 o -18 0 22 1239.85 1185.83 93.42 o -16 0 22 1336.00 1281.97 84.78 o -14 0 22 96.44 99.48 73.06 o -12 0 22 12.18 7.80 18.81 o -10 0 22 3160.14 3339.88 139.76 o -8 0 22 2967.70 3299.34 173.81 o -6 0 22 1466.58 1619.89 103.18 o -4 0 22 1225.28 1230.35 86.63 o -2 0 22 51.20 21.92 33.81 o 0 0 22 356.16 271.35 53.16 o 2 0 22 251.47 298.07 54.52 o -25 1 22 243.11 206.25 69.41 o -23 1 22 1132.12 1158.83 68.66 o -21 1 22 262.96 265.05 64.42 o -19 1 22 284.09 264.05 56.35 o -17 1 22 136.60 97.93 50.54 o -15 1 22 503.14 499.06 55.27 o -13 1 22 2028.12 2272.47 76.48 o -11 1 22 250.80 229.96 51.64 o -9 1 22 83.70 98.53 51.51 o -7 1 22 382.69 356.08 65.84 o -5 1 22 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49.20 o -3 1 23 5.95 19.76 27.61 o -18 2 23 4.45 15.49 18.72 o -16 2 23 0.42 10.06 16.39 o -14 2 23 659.79 686.42 53.98 o -12 2 23 1306.95 1269.69 82.42 o -10 2 23 653.30 799.74 60.37 o -8 2 23 0.55 10.79 15.10 o -6 2 23 747.97 798.43 65.99 o