#------------------------------------------------------------------------------ #$Date: 2011-10-06 14:27:20 +0300 (Thu, 06 Oct 2011) $ #$Revision: 27511 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/10/2231090.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231090_Fobs loop_ _publ_author_name 'Sen Gupta, Nalinava' 'Wragg, David S.' 'Tilset, Mats' 'Omtvedt, Jon Petter' _publ_section_title ; 4,7,13,18-Tetraoxa-1,10-diazoniabicyclo[8.5.5]icosane bis(hexafluoridophosphate) ; _journal_coeditor_code FY2005 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1929 _journal_page_last o1930 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.538 _cell_angle_gamma 90.000 _cell_length_a 10.8297 _cell_length_b 16.4853 _cell_length_c 12.6846 _exptl_crystal_F_000 1192.00 _reflns_d_resolution_high 0.7350 _[local]_cod_data_source_file fy2005Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2byc in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 317.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 37684.92 37431.48 257.15 o 4 0 0 67.00 83.44 16.15 o 6 0 0 2282.37 2449.10 60.58 o 8 0 0 1183.52 1334.87 116.34 o 10 0 0 3213.02 3247.78 121.25 o 12 0 0 8.22 37.68 56.53 o 14 0 0 902.94 884.63 151.68 o 1 1 0 515.80 602.38 13.53 o 3 1 0 13746.88 13751.86 162.89 o 5 1 0 1371.58 1382.88 30.16 o 7 1 0 1166.72 1363.59 36.49 o 9 1 0 174.06 177.50 25.10 o 11 1 0 247.58 280.64 51.71 o 13 1 0 14.37 33.37 46.27 o 0 2 0 632.95 540.19 18.98 o 2 2 0 30735.40 29471.77 169.41 o 4 2 0 3074.35 3471.79 41.24 o 6 2 0 814.27 770.11 28.69 o 8 2 0 605.57 525.92 33.04 o 10 2 0 1246.90 1259.24 72.18 o 12 2 0 295.43 274.46 58.03 o 14 2 0 14.30 -24.49 60.29 o 1 3 0 31557.68 32289.61 175.89 o 3 3 0 25344.01 24385.28 157.62 o 5 3 0 4830.25 4678.06 52.17 o 7 3 0 621.05 585.26 31.24 o 9 3 0 10.69 -0.80 15.87 o 11 3 0 7.05 19.27 28.27 o 13 3 0 1233.99 1397.02 116.91 o 0 4 0 96816.51 92734.64 733.75 o 2 4 0 15630.78 15429.46 95.23 o 4 4 0 2627.31 2600.08 53.26 o 6 4 0 4159.13 4428.22 100.30 o 8 4 0 17.20 28.16 16.65 o 10 4 0 2001.76 1852.09 149.17 o 12 4 0 260.44 296.96 49.62 o 14 4 0 94.01 62.18 73.48 o 1 5 0 14225.82 13866.03 91.06 o 3 5 0 70.86 114.09 13.35 o 5 5 0 24.96 66.52 14.06 o 7 5 0 0.02 4.45 14.50 o 9 5 0 1140.58 1152.50 57.00 o 11 5 0 14.26 28.76 25.21 o 13 5 0 7.64 0.73 33.05 o 0 6 0 12966.19 13882.00 167.62 o 2 6 0 5598.99 5154.51 51.60 o 4 6 0 16761.17 16117.07 133.52 o 6 6 0 6977.35 7060.36 91.64 o 8 6 0 90.02 100.85 25.60 o 10 6 0 123.01 156.17 30.91 o 12 6 0 109.09 137.08 40.64 o 14 6 0 57.54 133.78 80.08 o 1 7 0 79.39 67.90 11.56 o 3 7 0 12441.65 11994.99 92.15 o 5 7 0 13351.71 13710.57 129.79 o 7 7 0 168.87 204.25 29.31 o 9 7 0 54.57 69.61 26.36 o 11 7 0 193.12 148.80 40.52 o 13 7 0 793.27 839.88 80.93 o 0 8 0 0.20 -10.13 10.13 o 2 8 0 2313.46 2578.01 40.99 o 4 8 0 791.65 734.56 30.15 o 6 8 0 1063.47 1133.98 75.52 o 8 8 0 2600.36 2521.68 101.85 o 10 8 0 208.26 267.09 48.54 o 12 8 0 96.76 108.33 34.91 o 1 9 0 1018.75 1084.86 29.95 o 3 9 0 6323.51 6107.18 68.00 o 5 9 0 4171.40 3983.38 85.28 o 7 9 0 2268.01 2201.82 135.16 o 9 9 0 155.14 123.49 30.81 o 11 9 0 252.35 181.42 35.87 o 13 9 0 271.27 246.83 90.44 o 0 10 0 2164.78 2731.06 83.27 o 2 10 0 2700.30 2693.26 47.19 o 4 10 0 1853.97 1935.52 58.61 o 6 10 0 3859.63 3732.71 99.54 o 8 10 0 1494.36 1324.27 63.80 o 10 10 0 118.57 94.48 31.64 o 12 10 0 332.56 272.36 46.17 o 1 11 0 601.69 673.97 32.67 o 3 11 0 1255.55 1204.08 41.73 o 5 11 0 934.65 932.99 50.06 o 7 11 0 403.75 302.47 37.15 o 9 11 0 772.13 733.55 55.04 o 11 11 0 25.54 31.61 30.22 o 0 12 0 5004.11 4839.65 121.85 o 2 12 0 555.64 596.72 29.49 o 4 12 0 3538.85 3581.02 85.04 o 6 12 0 2189.85 2001.35 80.39 o 8 12 0 218.00 183.71 34.17 o 10 12 0 354.53 371.37 46.64 o 12 12 0 2.41 33.92 65.95 o 1 13 0 3632.37 3528.56 62.66 o 3 13 0 12.56 14.18 19.88 o 5 13 0 16.58 7.01 21.17 o 7 13 0 563.08 611.68 56.43 o 9 13 0 64.39 30.29 28.12 o 11 13 0 154.54 67.46 56.93 o 0 14 0 2071.01 1929.26 167.69 o 2 14 0 41.36 57.97 23.03 o 4 14 0 343.65 272.40 46.55 o 6 14 0 530.68 543.73 56.06 o 8 14 0 84.54 51.48 27.76 o 10 14 0 181.96 214.11 50.58 o 1 15 0 437.80 467.48 43.46 o 3 15 0 586.11 637.38 47.54 o 5 15 0 45.31 39.56 26.47 o 7 15 0 927.52 982.36 64.07 o 9 15 0 243.69 312.90 53.16 o 0 16 0 2726.39 2869.45 112.37 o 2 16 0 1382.25 1359.43 63.69 o 4 16 0 0.07 12.14 26.38 o 6 16 0 624.48 609.99 53.81 o 8 16 0 493.33 469.08 60.78 o 1 17 0 1513.50 1494.34 160.28 o 3 17 0 1.10 1.89 24.34 o 5 17 0 1.37 38.70 27.39 o 7 17 0 4.67 16.14 35.35 o 0 18 0 691.67 555.84 103.63 o 2 18 0 120.65 71.00 29.31 o 4 18 0 193.74 153.79 47.87 o 6 18 0 61.91 104.53 43.07 o 1 19 0 58.77 58.83 44.27 o 3 19 0 18.29 -27.15 27.15 o 5 19 0 147.71 132.77 42.13 o 7 19 0 286.89 169.58 88.56 o 2 20 0 11.13 27.32 62.18 o 4 20 0 456.27 464.89 61.76 o 6 20 0 34.55 75.10 51.71 o 1 21 0 21.69 -31.09 64.06 o 3 21 0 61.52 70.66 81.02 o 5 21 0 36.26 22.61 70.66 o -13 1 1 24.93 110.11 52.61 o -11 1 1 5792.05 6052.90 123.06 o -9 1 1 17405.50 17398.91 198.36 o -7 1 1 2075.93 1962.70 41.52 o -5 1 1 3890.77 4227.55 51.12 o -3 1 1 5713.00 5505.05 55.43 o -1 1 1 781.22 829.06 16.60 o 1 1 1 1246.66 1309.71 18.66 o 3 1 1 847.84 770.25 19.51 o 5 1 1 1959.67 1800.99 37.40 o 7 1 1 12225.47 12136.10 109.81 o 9 1 1 8510.92 8731.39 116.14 o 11 1 1 3548.86 3618.27 206.32 o 13 1 1 130.92 87.49 50.29 o -14 2 1 232.86 248.61 69.86 o -12 2 1 650.64 583.69 61.71 o -10 2 1 1915.23 2075.47 72.25 o -8 2 1 4243.31 3885.09 71.87 o -6 2 1 6677.27 6529.74 86.95 o -4 2 1 647.62 588.95 18.49 o -2 2 1 2297.18 2492.60 36.23 o 0 2 1 1791.82 1545.11 18.59 o 2 2 1 12185.01 12385.40 101.03 o 4 2 1 46.86 22.16 10.81 o 6 2 1 401.66 540.63 23.74 o 8 2 1 12448.46 12411.04 134.99 o 10 2 1 8738.67 9100.14 344.34 o 12 2 1 524.97 799.71 91.93 o -13 3 1 23.42 59.35 35.84 o -11 3 1 448.19 576.21 57.60 o -9 3 1 4493.52 4621.96 96.73 o -7 3 1 2475.33 2624.95 56.52 o -5 3 1 1605.15 1865.18 31.81 o -3 3 1 3516.88 3233.00 51.76 o -1 3 1 4059.03 3700.81 33.44 o 1 3 1 90.13 99.21 9.67 o 3 3 1 3501.67 3379.93 43.26 o 5 3 1 424.53 349.81 17.93 o 7 3 1 1484.09 1649.58 45.41 o 9 3 1 291.44 250.23 32.35 o 11 3 1 430.88 437.61 92.93 o 13 3 1 325.31 351.97 77.72 o -14 4 1 46.68 -32.97 67.83 o -12 4 1 689.11 620.24 77.35 o -10 4 1 2692.31 2503.16 77.67 o -8 4 1 10590.72 10698.06 126.52 o -6 4 1 2699.64 2507.72 51.62 o -4 4 1 10.28 18.47 10.86 o -2 4 1 1611.12 1690.65 24.56 o 0 4 1 8669.80 8473.42 61.25 o 2 4 1 3516.96 3157.17 33.44 o 4 4 1 8042.79 7915.94 66.41 o 6 4 1 8390.92 8586.04 81.65 o 8 4 1 436.04 543.78 41.55 o 10 4 1 1113.65 1147.56 59.69 o 12 4 1 1336.52 1325.39 87.16 o -13 5 1 113.28 71.02 42.77 o -11 5 1 703.08 708.27 53.66 o -9 5 1 241.29 306.66 38.21 o -7 5 1 1209.70 1191.29 42.46 o -5 5 1 22535.82 22764.63 173.90 o -3 5 1 12105.13 11892.93 102.13 o -1 5 1 4760.60 4773.16 51.38 o 1 5 1 402.85 425.83 21.56 o 3 5 1 4372.12 4295.13 44.08 o 5 5 1 18816.86 18768.28 127.18 o 7 5 1 11989.47 12593.32 249.12 o 9 5 1 3840.76 3830.60 154.07 o 11 5 1 50.47 58.36 28.70 o 13 5 1 889.52 1078.24 100.70 o -14 6 1 851.86 1092.92 292.52 o -12 6 1 190.93 105.23 38.56 o -10 6 1 935.74 889.03 55.49 o -8 6 1 855.18 976.45 51.90 o -6 6 1 3981.07 3904.14 66.76 o -4 6 1 3246.80 3095.07 58.49 o -2 6 1 5126.68 4939.45 51.86 o 0 6 1 148.89 149.79 12.79 o 2 6 1 0.41 -4.93 8.36 o 4 6 1 439.16 460.18 17.09 o 6 6 1 12.75 34.53 18.35 o 8 6 1 35.08 10.47 20.55 o 10 6 1 483.91 495.87 46.26 o 12 6 1 416.42 377.49 116.73 o -13 7 1 1589.34 1587.88 122.46 o -11 7 1 35.45 -5.54 24.08 o -9 7 1 1361.66 1114.47 57.72 o -7 7 1 509.46 577.96 40.87 o -5 7 1 2144.45 2259.94 49.86 o -3 7 1 303.05 325.59 18.82 o -1 7 1 3015.80 2814.25 44.67 o 1 7 1 740.19 733.54 37.37 o 3 7 1 389.56 370.63 18.24 o 5 7 1 4928.53 4800.77 87.46 o 7 7 1 475.10 547.11 41.62 o 9 7 1 207.74 162.18 31.62 o 11 7 1 325.78 267.12 40.63 o 13 7 1 57.66 59.28 41.60 o -12 8 1 473.04 449.40 71.72 o -10 8 1 295.32 291.01 39.23 o -8 8 1 1823.84 2041.95 69.91 o -6 8 1 13493.94 13036.52 135.78 o -4 8 1 5877.46 5739.92 86.30 o -2 8 1 429.78 549.24 23.42 o 0 8 1 481.71 547.23 22.02 o 2 8 1 619.83 572.07 22.37 o 4 8 1 20916.52 20954.64 164.64 o 6 8 1 9236.78 9516.67 137.64 o 8 8 1 337.06 309.87 37.37 o 10 8 1 92.32 44.87 26.74 o 12 8 1 1399.94 1450.00 79.20 o -11 9 1 36.61 34.03 27.39 o -9 9 1 211.68 190.44 33.15 o -7 9 1 1.89 2.18 19.99 o -5 9 1 8689.70 9093.58 109.39 o -3 9 1 14587.12 14748.20 115.88 o -1 9 1 3183.30 3249.80 68.07 o 1 9 1 2.37 26.22 11.51 o 3 9 1 204.22 198.56 16.82 o 5 9 1 2398.18 2385.02 66.85 o 7 9 1 183.18 206.93 38.39 o 9 9 1 248.69 282.90 38.34 o 11 9 1 70.40 64.68 29.74 o 13 9 1 332.65 268.50 97.04 o -12 10 1 21.93 43.45 31.65 o -10 10 1 73.44 88.67 30.34 o -8 10 1 93.12 95.36 28.13 o -6 10 1 1.20 11.74 20.73 o -4 10 1 647.82 721.73 34.96 o -2 10 1 1801.21 1766.63 38.76 o 0 10 1 3626.32 3670.31 55.75 o 2 10 1 908.05 836.74 29.59 o 4 10 1 135.26 113.71 24.50 o 6 10 1 1291.29 1245.08 57.70 o 8 10 1 35.52 7.95 24.07 o 10 10 1 12.13 -13.08 25.43 o 12 10 1 2.21 -23.47 28.61 o -11 11 1 448.35 429.91 59.94 o -9 11 1 90.23 115.65 30.95 o -7 11 1 423.51 391.34 40.59 o -5 11 1 171.28 183.21 29.30 o -3 11 1 7.72 -13.13 13.13 o -1 11 1 133.16 138.01 19.65 o 1 11 1 543.77 439.10 24.92 o 3 11 1 122.26 109.46 26.38 o 5 11 1 350.46 374.85 39.30 o 7 11 1 2.84 -20.73 20.73 o 9 11 1 199.44 205.05 36.03 o 11 11 1 1734.63 1917.35 104.30 o -12 12 1 174.60 153.56 80.08 o -10 12 1 915.46 1014.69 90.44 o -8 12 1 455.16 439.70 44.50 o -6 12 1 663.89 710.95 48.92 o -4 12 1 1270.67 1388.72 56.77 o -2 12 1 493.60 457.32 28.98 o 0 12 1 5490.01 5387.16 76.61 o 2 12 1 62.36 49.74 18.27 o 4 12 1 2377.46 2375.90 71.80 o 6 12 1 1262.76 1305.16 72.07 o 8 12 1 918.26 844.06 58.22 o 10 12 1 570.91 627.04 57.90 o 12 12 1 74.53 34.86 74.43 o -11 13 1 58.13 2.31 34.32 o -9 13 1 20.17 5.75 33.55 o -7 13 1 6.82 -9.13 21.92 o -5 13 1 185.49 228.16 39.57 o -3 13 1 133.95 142.18 28.25 o -1 13 1 400.85 363.99 26.48 o 1 13 1 92.54 90.74 20.79 o 3 13 1 4154.07 4244.13 94.04 o 5 13 1 122.66 89.24 26.30 o 7 13 1 605.84 645.33 51.25 o 9 13 1 74.50 86.33 39.71 o 11 13 1 48.35 14.42 38.45 o -10 14 1 1949.01 1719.78 105.37 o -8 14 1 601.21 654.47 65.42 o -6 14 1 400.27 379.38 56.30 o -4 14 1 4.53 41.00 23.34 o -2 14 1 787.01 799.48 45.16 o 0 14 1 4355.28 4075.35 70.18 o 2 14 1 404.90 347.63 37.32 o 4 14 1 818.40 782.99 50.73 o 6 14 1 172.06 193.73 34.44 o 8 14 1 147.07 174.37 37.78 o 10 14 1 1063.03 957.12 69.57 o -9 15 1 869.92 889.51 79.36 o -7 15 1 967.21 1072.65 101.57 o -5 15 1 46.39 57.99 26.67 o -3 15 1 298.13 306.29 44.19 o -1 15 1 4.31 11.88 25.78 o 1 15 1 556.00 524.93 43.33 o 3 15 1 295.93 357.98 40.20 o 5 15 1 325.64 346.59 41.72 o 7 15 1 384.55 426.81 47.12 o 9 15 1 1039.65 1053.99 71.61 o -8 16 1 41.63 24.08 36.57 o -6 16 1 62.82 -0.87 28.75 o -4 16 1 100.31 133.98 32.03 o -2 16 1 12.33 -3.56 22.16 o 0 16 1 172.63 133.81 26.94 o 2 16 1 1320.19 1190.26 76.56 o 4 16 1 28.30 42.24 27.18 o 6 16 1 570.10 612.40 54.21 o 8 16 1 171.66 144.80 38.46 o -7 17 1 313.33 331.37 54.57 o -5 17 1 23.79 9.61 31.17 o -3 17 1 9.14 6.16 30.60 o -1 17 1 1590.01 1702.80 110.93 o 1 17 1 11.07 -19.09 22.24 o 3 17 1 511.66 469.81 47.07 o 5 17 1 1007.45 1000.74 64.69 o 7 17 1 896.64 961.31 67.62 o -6 18 1 0.93 -24.87 31.95 o -4 18 1 194.28 175.01 43.40 o -2 18 1 32.15 8.93 40.30 o 0 18 1 681.62 876.15 120.59 o 2 18 1 3.01 -1.11 27.12 o 4 18 1 999.10 897.40 62.08 o 6 18 1 54.94 69.01 33.10 o 8 18 1 355.29 242.12 95.15 o -7 19 1 323.52 304.30 94.21 o -5 19 1 285.73 266.91 50.68 o -3 19 1 43.17 131.56 53.09 o 1 19 1 8.89 40.45 50.40 o 3 19 1 397.17 470.33 51.42 o 5 19 1 140.84 134.20 37.01 o 7 19 1 166.02 45.22 69.72 o -6 20 1 673.65 637.80 122.47 o -4 20 1 121.19 146.07 74.90 o -2 20 1 0.07 -11.31 58.41 o 0 20 1 5.84 20.73 64.06 o 2 20 1 0.17 -20.26 41.95 o 4 20 1 322.21 289.10 49.50 o 6 20 1 115.87 220.45 98.92 o -3 21 1 5.95 111.17 83.85 o -1 21 1 1.07 26.38 67.83 o 1 21 1 15.86 68.77 71.60 o 3 21 1 85.74 110.23 77.25 o 5 21 1 863.59 792.31 148.85 o -2 22 1 296.44 296.76 110.23 o 0 22 1 58.49 66.89 84.79 o -14 0 2 60.86 14.13 74.43 o -12 0 2 133.63 98.11 48.27 o -10 0 2 47.50 55.07 34.59 o -8 0 2 14.72 29.56 21.50 o -6 0 2 65.78 76.76 19.15 o -4 0 2 6850.01 7381.50 93.98 o -2 0 2 100505.33 93336.45 879.45 o 0 0 2 30754.93 30422.71 211.02 o 2 0 2 46553.59 44772.77 313.44 o 4 0 2 0.82 -8.37 8.37 o 6 0 2 5303.56 5459.59 93.75 o 8 0 2 35.05 10.98 21.91 o 10 0 2 932.29 853.54 116.82 o 12 0 2 3136.65 3295.46 216.68 o -13 1 2 273.73 305.80 67.50 o -11 1 2 292.39 278.89 38.52 o -9 1 2 131.51 67.35 24.93 o -7 1 2 191.11 198.08 18.89 o -5 1 2 2746.68 2677.79 40.98 o -3 1 2 404.87 430.97 19.37 o 1 1 2 53457.93 51952.81 269.01 o 3 1 2 4456.45 4735.23 47.87 o 5 1 2 187.86 235.69 17.77 o 7 1 2 19.17 15.99 13.16 o 9 1 2 206.80 229.54 31.49 o 11 1 2 387.56 371.57 63.97 o 13 1 2 57.62 130.63 55.85 o -14 2 2 283.25 248.24 68.61 o -12 2 2 84.17 13.43 32.12 o -10 2 2 240.37 249.27 33.72 o -8 2 2 1606.12 1711.70 59.00 o -6 2 2 821.26 815.67 36.54 o -4 2 2 3026.02 3118.74 40.43 o -2 2 2 791.62 817.33 24.02 o 0 2 2 23487.10 22451.99 131.62 o 2 2 2 2552.91 2711.85 37.69 o 4 2 2 5416.15 5645.61 57.03 o 6 2 2 2042.54 2211.92 53.63 o 8 2 2 1245.73 1287.38 51.58 o 10 2 2 451.06 425.34 48.56 o 12 2 2 186.59 121.72 67.83 o -13 3 2 164.00 139.19 60.34 o -11 3 2 554.38 460.00 53.04 o -9 3 2 266.19 263.53 42.76 o -7 3 2 3.27 -12.68 12.68 o -5 3 2 872.55 1121.73 26.32 o -3 3 2 190.44 110.77 10.36 o -1 3 2 55533.59 54129.84 261.04 o 1 3 2 19461.46 18897.92 122.03 o 3 3 2 7867.88 7397.58 60.33 o 5 3 2 695.20 727.89 23.77 o 7 3 2 87.37 18.58 15.12 o 9 3 2 49.80 22.31 21.87 o 11 3 2 21.20 7.62 28.58 o 13 3 2 410.97 510.02 84.48 o -14 4 2 97.03 15.96 48.29 o -12 4 2 540.47 654.50 71.44 o -10 4 2 39.14 4.92 21.89 o -8 4 2 1257.18 1152.02 46.62 o -6 4 2 818.00 831.13 34.02 o -4 4 2 2176.12 2264.12 58.61 o -2 4 2 9715.12 9359.45 74.75 o 0 4 2 365.47 274.58 15.66 o 2 4 2 3329.60 3098.74 47.69 o 4 4 2 11672.82 11412.42 86.50 o 6 4 2 13561.54 13524.86 110.19 o 8 4 2 12.63 -14.47 17.76 o 10 4 2 2050.37 2053.94 93.28 o 12 4 2 61.33 61.01 35.12 o -13 5 2 45.03 1.17 34.64 o -11 5 2 2079.66 1929.08 92.74 o -9 5 2 1.03 14.92 17.90 o -7 5 2 661.12 624.61 40.52 o -5 5 2 1102.64 963.27 33.35 o -3 5 2 19652.13 20240.49 138.57 o -1 5 2 14.03 12.34 6.04 o 1 5 2 1251.71 1193.43 23.45 o 3 5 2 965.05 1078.23 34.34 o 5 5 2 1441.02 1460.07 36.91 o 7 5 2 1054.18 1033.14 62.14 o 9 5 2 10.77 24.57 22.72 o 11 5 2 671.39 754.57 58.01 o 13 5 2 366.87 325.87 70.58 o -12 6 2 15.66 31.67 31.59 o -10 6 2 0.04 -16.11 21.34 o -8 6 2 2062.04 2016.91 55.80 o -6 6 2 5731.44 5807.48 83.88 o -4 6 2 27677.61 26766.03 192.64 o -2 6 2 3866.97 4293.71 48.59 o 0 6 2 1212.17 1275.23 26.26 o 2 6 2 208.64 291.39 22.30 o 4 6 2 4634.30 4313.33 60.89 o 6 6 2 101.29 55.97 21.43 o 8 6 2 332.44 307.33 36.39 o 10 6 2 512.14 389.85 43.89 o 12 6 2 4.76 34.25 33.53 o -13 7 2 121.85 133.80 53.92 o -11 7 2 4.75 7.24 25.29 o -9 7 2 1467.06 1360.19 62.83 o -7 7 2 867.29 935.46 57.75 o -5 7 2 95.72 87.88 17.16 o -3 7 2 7878.10 7943.15 122.65 o -1 7 2 6895.94 7776.47 78.86 o 1 7 2 0.68 0.62 7.83 o 3 7 2 18697.88 18611.27 124.76 o 5 7 2 16911.91 15829.19 173.20 o 7 7 2 476.58 486.01 41.70 o 9 7 2 14.02 3.41 22.12 o 11 7 2 658.37 670.15 66.30 o 13 7 2 425.18 410.09 77.59 o -12 8 2 489.85 601.47 66.40 o -10 8 2 300.86 314.10 39.55 o -8 8 2 471.82 409.23 38.95 o -6 8 2 143.54 189.76 23.16 o -4 8 2 256.30 345.59 24.86 o -2 8 2 642.06 700.11 32.07 o 0 8 2 969.98 1020.80 27.49 o 2 8 2 277.45 350.63 18.80 o 4 8 2 249.02 293.38 22.28 o 6 8 2 2478.87 2513.71 84.72 o 8 8 2 494.80 499.61 44.61 o 10 8 2 293.84 365.34 73.16 o 12 8 2 346.12 373.93 49.09 o -11 9 2 23.02 41.44 32.95 o -9 9 2 0.08 3.00 21.03 o -7 9 2 36.37 24.90 22.42 o -5 9 2 21764.16 22620.27 316.78 o -3 9 2 11247.09 11440.46 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