#------------------------------------------------------------------------------ #$Date: 2011-10-06 14:27:20 +0300 (Thu, 06 Oct 2011) $ #$Revision: 27511 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/11/2231127.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231127_Fobs loop_ _publ_author_name 'Wang, Chen-Yi' _publ_section_title ; Dichlorido[2-({[3-(cyclohexylazaniumyl)propyl]imino}methyl)-5-methoxyphenolate]zinc ; _journal_coeditor_code HB5943 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1085 _journal_page_last m1086 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.435 _cell_angle_gamma 90.000 _cell_length_a 25.1180 _cell_length_b 10.5430 _cell_length_c 14.9920 _exptl_crystal_F_000 1776.00 _reflns_d_resolution_high 0.7964 _[local]_cod_data_source_file hb5943Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 575.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 75228.39 76461.27 740.45 o 6 0 0 94970.17 96896.45 935.81 o 8 0 0 15274.87 16077.16 199.49 o 10 0 0 578.08 611.37 21.87 o 12 0 0 12125.03 11853.10 142.39 o 14 0 0 5000.29 4925.45 77.52 o 16 0 0 10305.64 10211.92 169.98 o 18 0 0 1392.00 1370.63 87.31 o 20 0 0 1476.82 1550.00 60.11 o 22 0 0 5540.16 5486.00 124.40 o 24 0 0 4600.12 4105.73 177.52 o 26 0 0 2125.05 2029.87 134.10 o 28 0 0 1620.78 1824.70 138.28 o 30 0 0 78.04 119.63 65.28 o 1 1 0 44836.59 45614.54 547.48 o 3 1 0 95944.59 92219.06 788.17 o 5 1 0 1178.58 1275.35 38.71 o 7 1 0 159.86 246.51 12.59 o 9 1 0 16860.65 16646.13 141.00 o 11 1 0 337.96 326.53 12.22 o 13 1 0 32214.37 31938.72 238.37 o 15 1 0 4484.70 4372.48 52.17 o 17 1 0 12091.03 12459.02 152.91 o 19 1 0 5299.14 5281.15 80.85 o 21 1 0 1321.86 1297.43 50.07 o 23 1 0 576.60 583.42 39.08 o 25 1 0 9452.29 9442.72 430.77 o 27 1 0 109.97 127.95 41.65 o 29 1 0 554.80 592.23 66.04 o 31 1 0 4.59 -29.88 41.40 o 0 2 0 4679.74 5255.42 79.63 o 2 2 0 3362.67 3328.44 45.34 o 4 2 0 59647.55 59178.81 574.39 o 6 2 0 2406.89 2151.32 29.34 o 8 2 0 877.00 994.55 20.57 o 10 2 0 20575.86 20124.29 170.19 o 12 2 0 36000.16 34893.79 282.83 o 14 2 0 894.83 754.74 23.06 o 16 2 0 20393.76 20114.28 213.36 o 18 2 0 1947.47 1927.80 40.21 o 20 2 0 10.87 1.67 16.26 o 22 2 0 2983.54 2987.58 89.07 o 24 2 0 1757.81 1704.35 63.41 o 26 2 0 1122.52 1003.31 72.54 o 28 2 0 1522.74 1622.22 234.28 o 30 2 0 165.20 134.79 49.79 o 1 3 0 24175.94 23572.65 243.85 o 3 3 0 542.27 487.93 34.05 o 5 3 0 19854.20 20659.62 218.65 o 7 3 0 7003.21 6905.96 89.24 o 9 3 0 24053.90 23811.68 222.94 o 11 3 0 1103.64 1029.88 25.01 o 13 3 0 33707.22 32234.59 267.45 o 15 3 0 8793.02 8549.33 93.41 o 17 3 0 2489.14 2376.41 43.75 o 19 3 0 544.87 512.05 35.95 o 21 3 0 343.20 397.97 33.93 o 23 3 0 31.66 72.12 25.91 o 25 3 0 181.27 145.14 31.87 o 27 3 0 29.94 27.37 39.37 o 29 3 0 1328.45 1373.22 118.18 o 0 4 0 30350.42 28745.62 371.96 o 2 4 0 1396.14 1478.66 35.13 o 4 4 0 21657.26 22630.16 242.17 o 6 4 0 13706.09 13900.60 160.92 o 8 4 0 12730.95 12617.90 150.86 o 10 4 0 8134.06 8210.74 126.87 o 12 4 0 35485.25 35457.45 373.69 o 14 4 0 3268.39 3178.72 56.11 o 16 4 0 7697.04 7507.66 140.87 o 18 4 0 739.42 797.94 42.02 o 20 4 0 27.82 22.08 22.94 o 22 4 0 383.21 393.26 37.42 o 24 4 0 1594.20 1633.21 87.52 o 26 4 0 1093.47 1153.82 60.92 o 28 4 0 1088.60 1159.97 64.01 o 30 4 0 113.66 65.98 46.60 o 1 5 0 27677.59 27459.14 258.52 o 3 5 0 45071.58 44414.99 454.47 o 5 5 0 1418.86 1347.06 37.36 o 7 5 0 3883.91 3995.15 85.72 o 9 5 0 13374.96 13590.67 166.54 o 11 5 0 13807.52 14024.98 173.56 o 13 5 0 16724.79 16106.55 196.37 o 15 5 0 551.29 573.71 43.17 o 17 5 0 3937.97 3935.10 107.59 o 19 5 0 938.50 1015.56 67.37 o 21 5 0 369.15 377.67 37.80 o 23 5 0 175.06 159.95 33.39 o 25 5 0 3679.08 3908.94 104.63 o 27 5 0 1.24 18.20 32.16 o 29 5 0 1693.25 1921.24 85.67 o 0 6 0 15278.65 14106.20 216.03 o 2 6 0 454.12 367.80 25.18 o 4 6 0 4229.19 3875.14 70.89 o 6 6 0 2639.03 2438.12 55.10 o 8 6 0 10354.14 10252.75 195.22 o 10 6 0 4057.72 4133.77 106.13 o 12 6 0 17263.63 17231.57 284.06 o 14 6 0 151.68 168.86 32.19 o 16 6 0 10892.62 10764.17 202.76 o 18 6 0 132.42 101.51 33.55 o 20 6 0 211.51 271.34 43.86 o 22 6 0 2296.11 2486.89 101.05 o 24 6 0 1125.63 1184.49 169.48 o 26 6 0 1028.66 1130.18 78.85 o 28 6 0 1362.40 1588.50 105.32 o 1 7 0 7048.50 6690.21 93.07 o 3 7 0 6879.96 6761.30 94.03 o 5 7 0 12.83 30.17 15.79 o 7 7 0 721.07 654.62 32.50 o 9 7 0 7024.08 7182.44 194.74 o 11 7 0 86.71 97.30 27.70 o 13 7 0 1777.22 1669.59 71.87 o 15 7 0 5558.63 5387.75 134.17 o 17 7 0 25.99 1.16 30.90 o 19 7 0 592.78 640.57 56.99 o 21 7 0 1709.93 1577.23 83.06 o 23 7 0 9.51 13.32 45.83 o 25 7 0 1380.48 1446.68 123.81 o 0 8 0 6411.11 6291.00 175.59 o 2 8 0 29.76 46.07 16.30 o 4 8 0 3201.32 3035.90 63.27 o 6 8 0 355.35 375.01 28.79 o 8 8 0 739.64 715.44 37.07 o 10 8 0 1924.39 1885.04 114.33 o 12 8 0 4398.25 4249.45 117.86 o 14 8 0 673.43 632.63 53.26 o 16 8 0 3007.87 3046.66 105.86 o 18 8 0 155.04 170.76 40.47 o 20 8 0 3.10 -15.41 33.31 o 22 8 0 136.39 117.91 44.62 o 24 8 0 751.93 805.78 83.13 o 1 9 0 4551.24 4539.15 80.80 o 3 9 0 3869.45 3681.31 96.18 o 5 9 0 978.80 872.91 37.72 o 7 9 0 1054.82 1049.07 45.72 o 9 9 0 1433.15 1417.51 82.33 o 11 9 0 131.47 116.14 33.95 o 13 9 0 4610.12 4291.78 164.17 o 15 9 0 1768.84 1814.58 85.04 o 17 9 0 133.43 96.83 38.18 o 19 9 0 182.36 93.45 40.38 o 21 9 0 823.88 716.92 74.77 o 23 9 0 2.01 -6.18 40.13 o 0 10 0 10206.35 10242.20 264.83 o 2 10 0 203.99 241.50 27.25 o 4 10 0 1367.63 1377.96 48.11 o 6 10 0 1655.46 1734.18 85.76 o 8 10 0 1315.81 1323.11 72.43 o 10 10 0 780.03 880.82 63.31 o 12 10 0 3099.65 3196.19 111.59 o 14 10 0 18.98 36.75 37.03 o 16 10 0 556.89 556.29 61.17 o 18 10 0 2.81 89.17 41.66 o 20 10 0 106.74 66.58 41.62 o 1 11 0 1577.67 1557.47 89.31 o 3 11 0 5950.47 5868.24 102.94 o 5 11 0 79.69 73.63 29.70 o 7 11 0 727.57 699.63 59.75 o 9 11 0 2269.29 2184.36 91.69 o 11 11 0 258.35 230.99 46.27 o 13 11 0 1882.30 2161.40 97.88 o 15 11 0 245.51 282.92 51.17 o 17 11 0 284.92 253.49 52.28 o 0 12 0 952.05 1067.68 89.40 o 2 12 0 278.45 345.39 48.18 o 4 12 0 805.43 802.92 77.02 o 6 12 0 472.27 439.67 54.53 o 8 12 0 15.96 16.52 33.75 o 10 12 0 238.49 228.08 64.64 o 12 12 0 392.42 399.74 57.45 o 1 13 0 491.75 509.08 74.29 o 3 13 0 180.39 198.10 62.07 o 5 13 0 20.28 14.79 50.17 o -31 1 1 67.76 22.69 43.43 o -29 1 1 0.32 -42.19 35.33 o -27 1 1 176.41 167.59 45.80 o -25 1 1 21.97 41.64 26.80 o -23 1 1 354.35 419.03 36.07 o -21 1 1 522.84 543.98 29.98 o -19 1 1 591.98 613.16 29.51 o -17 1 1 299.00 286.77 21.22 o -15 1 1 4292.79 4410.15 82.82 o -13 1 1 1638.00 1705.05 27.60 o -11 1 1 12.40 12.04 6.29 o -9 1 1 15586.43 15664.80 134.58 o -7 1 1 6161.04 6486.25 63.04 o -5 1 1 52689.27 53204.28 454.63 o -3 1 1 11240.53 11241.37 103.98 o -1 1 1 12.45 -2.34 4.53 o 1 1 1 11216.75 11146.78 148.07 o 3 1 1 465.38 604.70 13.80 o 5 1 1 152.61 203.20 9.52 o 7 1 1 4090.73 4322.69 53.39 o 9 1 1 8627.51 8629.02 81.66 o 11 1 1 1915.81 1834.58 27.88 o 13 1 1 64.33 87.46 9.67 o 15 1 1 44.13 36.26 9.51 o 17 1 1 12.80 33.29 10.11 o 19 1 1 518.36 516.13 34.49 o 21 1 1 1353.66 1429.58 51.23 o 23 1 1 285.82 300.39 65.44 o 25 1 1 190.93 195.56 51.94 o 27 1 1 992.21 925.74 71.00 o 29 1 1 304.23 335.66 69.95 o 31 1 1 445.70 426.99 66.05 o -30 2 1 1.72 -31.50 39.13 o -28 2 1 41.85 79.50 42.29 o -26 2 1 46.04 50.97 26.60 o -24 2 1 12.80 -14.01 21.79 o -22 2 1 1382.11 1231.51 60.75 o -20 2 1 1113.98 1097.43 47.09 o -18 2 1 876.32 850.78 68.93 o -16 2 1 612.76 635.33 23.02 o -14 2 1 3158.54 3128.42 55.83 o -12 2 1 3335.50 3119.55 44.54 o -10 2 1 136.07 146.53 16.52 o -8 2 1 3838.34 3755.98 50.80 o -6 2 1 42.13 95.52 8.80 o -4 2 1 22682.42 23187.82 236.55 o -2 2 1 733.66 709.36 20.60 o 0 2 1 38607.18 37482.89 367.54 o 2 2 1 57745.50 56322.90 474.14 o 4 2 1 1368.31 1336.09 22.18 o 6 2 1 22298.30 22851.29 184.17 o 8 2 1 7794.31 8252.15 78.19 o 10 2 1 348.81 407.93 14.69 o 12 2 1 11329.22 12035.85 122.88 o 14 2 1 2237.78 2236.65 38.76 o 16 2 1 259.61 273.44 16.70 o 18 2 1 58.67 28.65 12.91 o 20 2 1 445.87 428.22 32.81 o 22 2 1 54.20 71.34 23.79 o 24 2 1 1955.13 1894.10 66.09 o 26 2 1 8.62 -10.70 34.00 o 28 2 1 97.67 87.47 42.52 o 30 2 1 64.23 84.88 47.52 o -29 3 1 77.62 41.10 48.72 o -27 3 1 98.32 56.08 31.08 o -25 3 1 362.24 381.10 38.98 o -23 3 1 927.48 1057.36 52.66 o -21 3 1 34.07 38.89 22.77 o -19 3 1 415.98 366.37 24.32 o -17 3 1 266.02 275.12 20.95 o -15 3 1 512.28 538.83 28.87 o -13 3 1 0.43 -2.44 10.66 o -11 3 1 2890.30 3146.51 51.35 o -9 3 1 10872.89 11373.26 120.72 o -7 3 1 390.37 339.00 17.14 o -5 3 1 22034.88 24237.27 252.81 o -3 3 1 543.40 520.06 19.27 o -1 3 1 4867.77 5665.06 98.22 o 1 3 1 273.75 298.96 20.28 o 3 3 1 103.89 90.72 10.39 o 5 3 1 647.91 787.49 25.55 o 7 3 1 29.13 -11.48 6.05 o 9 3 1 11.45 22.96 7.39 o 11 3 1 3420.77 3758.21 48.96 o 13 3 1 1300.60 1331.41 29.15 o 15 3 1 85.92 89.85 12.59 o 17 3 1 173.87 206.31 20.98 o 19 3 1 746.18 738.85 33.54 o 21 3 1 89.61 72.68 23.54 o 23 3 1 32.90 -16.87 27.09 o 25 3 1 30.39 -32.91 23.99 o 27 3 1 8.65 -39.33 48.56 o 29 3 1 42.14 94.01 60.78 o -30 4 1 0.00 -27.04 44.42 o -28 4 1 4.66 -39.28 28.08 o -26 4 1 243.60 183.30 37.20 o -24 4 1 5.87 4.23 31.32 o -22 4 1 209.34 251.05 33.27 o -20 4 1 2603.52 2557.19 73.17 o -18 4 1 50.07 99.20 22.48 o -16 4 1 1.84 4.28 12.56 o -14 4 1 44.89 32.47 13.06 o -12 4 1 11488.64 11524.88 147.58 o -10 4 1 801.88 837.78 30.25 o -8 4 1 17.78 11.15 10.53 o -6 4 1 2064.56 2190.10 44.64 o -4 4 1 1300.04 1228.38 44.67 o -2 4 1 4423.46 4880.85 70.94 o 0 4 1 7164.32 7472.40 85.61 o 2 4 1 389.14 285.91 21.22 o 4 4 1 805.48 714.12 25.05 o 6 4 1 3942.76 3894.98 74.26 o 8 4 1 93.84 107.63 23.29 o 10 4 1 196.39 203.30 16.16 o 12 4 1 2166.88 2043.49 38.90 o 14 4 1 770.01 870.94 43.54 o 16 4 1 5273.70 5118.76 83.78 o 18 4 1 1.57 19.44 20.98 o 20 4 1 410.32 462.10 30.77 o 22 4 1 51.21 37.41 27.11 o 24 4 1 554.21 520.69 44.24 o 26 4 1 51.64 30.89 30.52 o 28 4 1 34.23 60.72 61.42 o -29 5 1 0.42 18.45 33.77 o -27 5 1 30.85 16.89 32.78 o -25 5 1 127.88 110.19 33.54 o -23 5 1 40.38 74.36 28.86 o -21 5 1 213.77 196.40 38.09 o -19 5 1 123.59 86.05 30.24 o -17 5 1 830.56 778.12 151.63 o -15 5 1 771.34 832.97 40.03 o -13 5 1 9.83 -1.71 12.95 o -11 5 1 20.20 30.44 13.91 o -9 5 1 276.63 319.52 40.97 o -7 5 1 5314.40 5768.51 106.84 o -5 5 1 5181.17 5973.03 88.68 o -3 5 1 365.29 389.06 21.32 o -1 5 1 9345.95 10684.11 133.10 o 1 5 1 1517.83 1838.53 38.31 o 3 5 1 611.02 736.74 40.79 o 5 5 1 722.25 821.37 29.77 o 7 5 1 203.16 118.87 21.40 o 9 5 1 109.06 100.88 14.66 o 11 5 1 596.72 668.78 42.57 o 13 5 1 175.70 240.65 31.72 o 15 5 1 36.30 81.78 39.56 o 17 5 1 401.22 354.13 39.87 o 19 5 1 162.64 142.10 28.06 o 21 5 1 267.73 286.63 34.64 o 23 5 1 44.28 55.40 28.78 o 25 5 1 76.32 17.34 29.62 o 27 5 1 42.09 5.94 31.17 o 29 5 1 39.48 84.42 46.16 o -28 6 1 5.66 29.12 43.31 o -26 6 1 55.70 105.47 44.89 o -24 6 1 0.30 -2.11 34.06 o -22 6 1 169.59 199.02 77.34 o -20 6 1 581.95 483.01 49.64 o -18 6 1 994.35 983.58 60.35 o -16 6 1 42.13 42.71 27.35 o -14 6 1 204.87 143.51 30.59 o -12 6 1 3604.91 3509.59 72.81 o -10 6 1 3213.84 3190.57 84.72 o -8 6 1 216.66 250.69 22.12 o -6 6 1 5920.19 6164.24 96.31 o -4 6 1 2130.57 2075.94 52.13 o -2 6 1 1780.04 1687.76 59.29 o 0 6 1 5713.92 6034.78 82.74 o 2 6 1 32.18 4.02 10.89 o 4 6 1 3625.01 3371.05 65.26 o 6 6 1 1779.65 1742.49 45.64 o 8 6 1 2330.07 2344.97 73.13 o 10 6 1 1770.11 1753.36 47.37 o 12 6 1 835.51 875.44 50.73 o 14 6 1 35.11 27.13 25.58 o 16 6 1 267.10 167.85 56.28 o 18 6 1 15.61 5.58 28.52 o 20 6 1 58.62 53.99 48.88 o 22 6 1 29.81 23.92 36.38 o 24 6 1 15.04 -43.53 34.25 o 26 6 1 86.61 43.56 44.18 o 28 6 1 62.25 77.05 45.10 o -25 7 1 56.01 69.42 43.77 o -23 7 1 170.83 153.71 44.58 o -21 7 1 0.88 12.72 64.96 o -19 7 1 620.98 674.87 64.32 o -17 7 1 1071.31 1038.13 63.41 o -15 7 1 78.04 92.78 32.00 o -13 7 1 733.58 728.75 51.14 o -11 7 1 207.51 181.96 24.27 o -9 7 1 6300.55 6396.16 108.00 o -7 7 1 2653.24 2774.97 64.01 o -5 7 1 1789.60 1793.84 50.33 o -3 7 1 60.19 44.50 16.76 o -1 7 1 1175.80 1242.49 37.85 o 1 7 1 6196.53 5953.97 115.77 o 3 7 1 2597.22 2502.52 52.08 o 5 7 1 61.68 84.46 18.54 o 7 7 1 274.58 220.59 23.21 o 9 7 1 686.16 649.47 33.00 o 11 7 1 711.85 732.15 49.77 o 13 7 1 1641.74 1605.13 71.19 o 15 7 1 23.29 25.31 27.46 o 17 7 1 229.09 243.92 55.80 o 19 7 1 491.80 449.09 99.37 o 21 7 1 2.61 5.86 42.29 o 23 7 1 0.38 -19.63 45.67 o 25 7 1 691.86 898.07 75.26 o -24 8 1 53.34 30.77 44.10 o -22 8 1 18.89 -43.16 36.91 o -20 8 1 502.31 590.54 61.60 o -18 8 1 246.80 251.98 45.69 o -16 8 1 113.17 89.82 35.17 o -14 8 1 358.57 385.73 46.09 o -12 8 1 905.78 1019.90 60.53 o -10 8 1 61.52 54.85 21.94 o -8 8 1 475.39 506.33 32.77 o -6 8 1 72.08 80.44 20.46 o -4 8 1 180.74 141.03 31.57 o -2 8 1 118.87 140.63 19.58 o 0 8 1 35.71 45.55 15.86 o 2 8 1 45.39 40.19 16.01 o 4 8 1 5.26 1.62 14.44 o 6 8 1 1306.10 1368.63 48.07 o 8 8 1 1773.26 1754.25 142.46 o 10 8 1 927.75 908.43 56.95 o 12 8 1 592.29 576.60 49.45 o 14 8 1 1090.90 1077.66 64.33 o 16 8 1 7.07 -7.69 29.20 o 18 8 1 524.81 449.78 53.59 o 20 8 1 185.47 248.45 48.26 o 22 8 1 54.99 66.69 40.34 o 24 8 1 130.24 176.11 49.60 o -23 9 1 137.06 158.76 50.90 o -21 9 1 52.33 61.16 53.22 o -19 9 1 88.57 68.60 40.70 o -17 9 1 191.60 147.04 42.81 o -15 9 1 331.16 345.49 48.57 o -13 9 1 0.23 28.41 30.15 o -11 9 1 440.40 417.09 46.26 o -9 9 1 3213.89 3087.80 99.92 o -7 9 1 52.11 62.89 22.46 o -5 9 1 132.61 104.49 21.00 o -3 9 1 193.31 176.26 27.91 o -1 9 1 780.69 790.55 35.78 o 1 9 1 2.65 -1.44 15.76 o 3 9 1 1042.87 1072.66 40.42 o 5 9 1 1303.09 1336.31 44.98 o 7 9 1 0.50 -30.02 23.53 o 9 9 1 265.04 266.90 40.91 o 11 9 1 254.55 281.30 43.97 o 13 9 1 2606.80 2563.01 98.66 o 15 9 1 28.98 -21.71 30.28 o 17 9 1 541.16 483.58 55.29 o 19 9 1 1.35 -14.43 44.22 o 21 9 1 43.13 19.90 39.63 o 23 9 1 156.62 68.62 44.41 o -20 10 1 25.41 21.86 70.75 o -18 10 1 33.80 -11.74 42.45 o -16 10 1 34.94 -9.48 34.80 o -14 10 1 222.86 220.93 44.26 o -12 10 1 1030.82 1004.64 79.75 o -10 10 1 160.88 237.20 42.72 o -8 10 1 529.54 522.94 49.97 o -6 10 1 1013.72 1022.30 43.69 o -4 10 1 307.71 345.09 30.00 o -2 10 1 62.88 20.49 19.84 o 0 10 1 7.30 8.93 18.82 o 2 10 1 743.86 717.27 37.17 o 4 10 1 8.49 -34.11 21.82 o 6 10 1 600.99 623.25 53.15 o 8 10 1 181.32 140.97 43.58 o 10 10 1 101.20 94.15 47.92 o 12 10 1 2.24 8.63 49.04 o 14 10 1 29.60 25.11 34.15 o 16 10 1 102.01 134.91 82.65 o 18 10 1 93.28 29.59 39.32 o 20 10 1 283.26 181.94 49.60 o -17 11 1 649.69 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