#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:25:10 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181233 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/11/2231140.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231140_Fobs loop_ _publ_author_name 'Dai, Jun' 'Pan, Rong-Kun' 'Yang, Juan' _publ_section_title ; Tetrakis(\m-4-tert-butylbenzoato)-\k^3^O:O,O';\k^3^O,O':O';\k^4^O:O'-bis[aquabis(4-tert-butylbenzoato-\k^2^O,O')(4-tert-butylbenzoic acid-\kO)praseodymium(III)] ; _journal_coeditor_code HG5053 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1160 _journal_page_last m1161 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.073 _cell_angle_gamma 90.000 _cell_length_a 35.1940 _cell_length_b 9.3857 _cell_length_c 27.9560 _exptl_crystal_F_000 3600.00 _reflns_d_resolution_high 0.8402 _cod_data_source_file hg5053Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' y in P2(1)/c New: P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 789.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 622906.38 465434.69 22494.71 o 4 0 0 18468.32 14881.41 746.89 o 5 0 0 171.00 112.98 87.87 o 6 0 0 201997.59 184248.84 6143.54 o 7 0 0 88.85 193.82 88.23 o 8 0 0 1262.02 3558.66 401.69 o 9 0 0 266.21 335.16 114.89 o 10 0 0 74399.20 80593.70 2758.26 o 11 0 0 202.59 746.89 251.06 o 12 0 0 50796.79 64053.71 2236.33 o 13 0 0 111.44 555.51 151.98 o 14 0 0 226264.75 261990.22 8791.23 o 16 0 0 225299.33 270990.81 9108.70 o 18 0 0 26884.39 30560.52 1199.80 o 19 0 0 79.89 601.56 192.57 o 20 0 0 48354.66 53729.36 2413.29 o 21 0 0 487.08 1291.97 254.20 o 22 0 0 12725.82 17990.06 1245.87 o 23 0 0 294.21 496.24 226.13 o 24 0 0 353.95 483.28 458.18 o 25 0 0 14.09 194.57 395.41 o 26 0 0 241.51 495.84 470.73 o 27 0 0 148.93 307.54 445.63 o 28 0 0 12543.55 14285.15 1324.33 o 29 0 0 155.16 69.04 464.46 o 30 0 0 12053.48 14988.11 1405.92 o 31 0 0 351.61 790.83 577.43 o 32 0 0 15038.46 17919.20 1606.77 o 33 0 0 546.43 916.36 615.09 o 34 0 0 15764.25 18371.10 1682.08 o 35 0 0 527.42 589.98 558.60 o 36 0 0 13352.57 16732.95 1675.81 o 37 0 0 328.36 1638.15 709.24 o 38 0 0 5082.91 6596.52 1142.31 o 39 0 0 195.34 772.00 696.68 o 40 0 0 2128.97 2918.54 928.91 o 1 1 0 655.42 456.05 219.67 o 2 1 0 14629.68 9884.11 1522.03 o 3 1 0 292.09 225.95 67.34 o 4 1 0 90915.48 102631.50 5121.57 o 5 1 0 24.56 -15.51 60.64 o 6 1 0 1507.09 2472.43 163.92 o 7 1 0 21.46 -30.34 108.24 o 8 1 0 82663.53 104812.44 2897.45 o 9 1 0 276.42 202.45 116.47 o 10 1 0 60524.36 53607.68 1549.71 o 11 1 0 733.90 712.10 148.44 o 12 1 0 59670.51 56917.19 1419.14 o 13 1 0 439.52 576.97 109.48 o 14 1 0 6066.99 6218.01 248.44 o 15 1 0 369.05 353.55 111.12 o 16 1 0 21091.05 22545.83 646.23 o 17 1 0 332.02 557.14 111.38 o 18 1 0 2861.30 3353.82 201.21 o 19 1 0 90.10 185.81 127.02 o 20 1 0 45735.82 42138.43 1136.73 o 21 1 0 11.33 654.63 199.03 o 22 1 0 41505.39 48839.01 1553.09 o 23 1 0 363.03 835.03 226.24 o 24 1 0 50112.82 46742.37 1521.37 o 25 1 0 669.71 1266.13 269.67 o 26 1 0 25240.67 24218.63 2118.29 o 27 1 0 238.61 721.22 342.22 o 28 1 0 27960.61 28460.88 1382.46 o 29 1 0 719.38 1259.47 405.63 o 30 1 0 9368.58 8588.00 828.49 o 31 1 0 399.49 731.31 386.04 o 32 1 0 943.97 1128.33 445.75 o 33 1 0 55.16 -341.65 341.65 o 34 1 0 380.53 641.14 441.17 o 35 1 0 60.14 -376.59 376.59 o 36 1 0 150.30 689.54 449.66 o 37 1 0 26.83 -86.06 445.22 o 38 1 0 3175.89 4146.36 1032.47 o 39 1 0 14.81 -222.45 564.88 o 0 2 0 240101.42 228374.08 10920.98 o 1 2 0 85.26 17.72 112.59 o 2 2 0 2730.31 5573.47 439.35 o 3 2 0 814.46 578.27 104.93 o 4 2 0 2316.14 2157.41 138.50 o 5 2 0 558.91 288.31 90.74 o 6 2 0 3908.13 6295.02 199.92 o 7 2 0 80.04 255.34 120.49 o 8 2 0 18749.24 17372.96 494.40 o 9 2 0 2281.65 1739.89 131.69 o 10 2 0 3309.42 4523.13 199.37 o 11 2 0 1096.77 1509.77 332.19 o 12 2 0 7690.62 5232.50 301.54 o 13 2 0 1.31 142.88 152.72 o 14 2 0 22799.41 27857.39 916.61 o 15 2 0 90.46 349.71 166.45 o 16 2 0 35401.01 37944.59 1204.18 o 17 2 0 361.95 164.30 161.34 o 18 2 0 31450.21 28054.14 797.61 o 19 2 0 1129.16 966.59 160.44 o 20 2 0 20626.02 23938.63 872.10 o 21 2 0 563.01 301.09 201.66 o 22 2 0 7867.37 8912.47 500.87 o 23 2 0 1824.60 2262.92 323.30 o 24 2 0 840.61 817.80 321.46 o 25 2 0 1893.71 1523.67 513.69 o 26 2 0 1.74 378.38 251.48 o 27 2 0 218.90 624.06 279.70 o 28 2 0 6292.56 7620.83 698.74 o 29 2 0 6.29 255.29 348.20 o 30 2 0 7499.56 8720.87 1148.59 o 31 2 0 1.18 241.21 345.25 o 32 2 0 12003.99 13584.84 976.90 o 33 2 0 177.87 44.08 375.00 o 34 2 0 8724.42 7763.62 815.94 o 35 2 0 355.90 448.60 434.32 o 36 2 0 4705.75 5790.03 747.57 o 37 2 0 353.24 7.93 627.64 o 38 2 0 1687.40 1875.33 947.74 o 39 2 0 323.95 494.40 490.47 o 1 3 0 7860.08 6799.50 372.72 o 2 3 0 10391.36 11239.82 520.78 o 4 3 0 14253.71 12483.64 571.16 o 5 3 0 4364.78 5069.87 240.38 o 6 3 0 2990.01 2361.67 262.31 o 7 3 0 586.42 596.82 104.40 o 8 3 0 20683.72 21566.77 537.79 o 9 3 0 15.30 161.50 106.38 o 10 3 0 7816.19 10199.98 428.28 o 11 3 0 98.83 -96.59 98.07 o 12 3 0 11552.75 11000.71 406.39 o 13 3 0 1603.76 1350.31 144.22 o 14 3 0 7187.27 8478.12 433.63 o 15 3 0 3702.40 4040.61 310.33 o 16 3 0 488.95 676.84 319.78 o 17 3 0 1918.44 2447.55 307.77 o 18 3 0 433.96 776.03 218.57 o 19 3 0 3218.65 2888.42 358.30 o 20 3 0 5735.00 6373.95 429.50 o 21 3 0 1923.41 1741.67 282.78 o 22 3 0 8907.53 9875.04 547.19 o 23 3 0 317.45 282.63 230.19 o 24 3 0 998.11 1695.14 318.51 o 25 3 0 24.21 128.42 248.72 o 26 3 0 1765.22 2574.26 396.25 o 27 3 0 432.93 654.10 282.60 o 28 3 0 6406.38 6775.25 527.09 o 29 3 0 1509.82 1103.15 329.71 o 30 3 0 1032.16 1729.25 456.87 o 31 3 0 1278.92 1527.57 511.53 o 32 3 0 88.37 563.08 546.05 o 33 3 0 890.82 1509.10 474.32 o 34 3 0 2.00 315.85 389.87 o 35 3 0 694.02 1587.50 514.76 o 36 3 0 530.60 1160.00 487.95 o 37 3 0 325.71 1188.12 503.36 o 38 3 0 743.11 1065.28 511.90 o 0 4 0 1123.57 1393.37 313.82 o 1 4 0 590.28 579.14 320.10 o 2 4 0 2633.57 2184.20 257.30 o 3 4 0 8784.78 8933.21 478.76 o 5 4 0 11691.53 11217.92 752.54 o 6 4 0 2385.28 1370.94 201.52 o 7 4 0 21004.90 21640.07 629.63 o 8 4 0 139.03 -40.35 110.44 o 9 4 0 21361.37 20619.16 548.74 o 10 4 0 2604.07 3045.25 188.39 o 11 4 0 8165.97 9600.58 370.32 o 12 4 0 2817.98 5094.21 435.75 o 13 4 0 4861.27 5272.15 414.01 o 14 4 0 665.39 467.38 171.28 o 15 4 0 478.99 627.83 148.71 o 16 4 0 72.18 430.71 200.49 o 17 4 0 120.16 33.89 185.99 o 18 4 0 449.04 413.56 215.82 o 19 4 0 388.31 325.99 218.06 o 20 4 0 64.66 161.15 213.46 o 21 4 0 4822.29 5065.92 694.02 o 22 4 0 3322.34 4300.32 404.24 o 23 4 0 14483.82 15048.57 707.39 o 24 4 0 3184.54 3132.24 391.45 o 25 4 0 5538.59 5590.86 480.41 o 26 4 0 74.76 569.45 286.09 o 27 4 0 1147.62 1623.61 341.78 o 28 4 0 378.33 324.40 291.39 o 29 4 0 892.31 537.18 410.40 o 30 4 0 51.35 -199.31 283.17 o 31 4 0 596.45 1065.54 884.98 o 32 4 0 195.91 411.36 405.92 o 33 4 0 126.52 35.83 381.51 o 34 4 0 214.21 -361.69 361.69 o 35 4 0 21.06 -298.93 375.00 o 36 4 0 136.42 -386.04 386.04 o 37 4 0 443.39 359.79 472.52 o 1 5 0 14395.53 14335.82 707.87 o 2 5 0 1483.67 2327.10 303.99 o 3 5 0 20702.12 17976.46 825.34 o 4 5 0 4305.47 5628.99 593.12 o 5 5 0 5734.41 5360.07 627.64 o 6 5 0 1756.46 2480.43 254.26 o 7 5 0 179.42 171.27 133.81 o 8 5 0 5730.32 6937.56 321.82 o 9 5 0 479.16 510.56 116.74 o 10 5 0 9691.12 10855.95 400.33 o 11 5 0 400.47 618.55 132.44 o 12 5 0 1118.75 2122.53 222.17 o 13 5 0 3597.81 3605.20 268.14 o 14 5 0 108.44 293.19 162.53 o 15 5 0 7493.17 8763.22 501.01 o 16 5 0 63.62 364.58 300.44 o 17 5 0 6865.79 6666.42 458.85 o 18 5 0 2494.74 4083.39 725.77 o 19 5 0 7836.98 8581.52 534.80 o 20 5 0 5755.81 6290.58 479.26 o 21 5 0 4571.43 4685.72 435.59 o 22 5 0 3691.35 5291.91 465.99 o 23 5 0 1437.87 954.86 298.78 o 24 5 0 6903.58 7913.69 1041.27 o 25 5 0 460.52 543.81 275.13 o 26 5 0 4046.65 4494.49 469.05 o 27 5 0 16.32 207.90 282.35 o 28 5 0 893.32 628.31 333.22 o 29 5 0 243.27 -6.18 318.04 o 30 5 0 314.75 271.00 322.11 o 31 5 0 873.28 1279.73 375.57 o 32 5 0 143.92 292.86 335.70 o 33 5 0 1656.58 1001.65 485.59 o 34 5 0 24.57 -63.59 403.79 o 35 5 0 1872.04 3089.69 635.93 o 0 6 0 7787.24 9132.20 834.76 o 1 6 0 391.18 502.17 250.49 o 2 6 0 9280.98 10001.45 617.67 o 3 6 0 2513.21 2655.48 360.71 o 4 6 0 6038.09 7794.90 950.88 o 5 6 0 5239.70 3928.93 884.98 o 6 6 0 1777.83 2053.44 228.41 o 7 6 0 12227.10 11656.97 526.77 o 8 6 0 1120.01 1665.07 334.29 o 9 6 0 11493.59 11536.94 513.91 o 10 6 0 572.97 890.29 190.58 o 11 6 0 5481.90 5738.25 322.66 o 12 6 0 317.92 516.28 293.30 o 13 6 0 3188.73 3577.35 891.25 o 14 6 0 804.14 1201.13 318.61 o 15 6 0 399.63 418.31 240.42 o 16 6 0 7035.93 8435.29 536.08 o 17 6 0 11.28 142.36 227.83 o 18 6 0 11481.50 12435.73 664.29 o 19 6 0 50.32 212.33 250.97 o 20 6 0 5694.78 5981.68 535.47 o 21 6 0 1984.40 1908.62 336.24 o 22 6 0 3316.61 3627.33 432.12 o 23 6 0 7083.70 7632.10 862.48 o 24 6 0 3964.96 5807.99 517.28 o 25 6 0 4014.93 3888.15 463.62 o 26 6 0 399.32 425.29 299.76 o 27 6 0 1004.00 1530.67 363.74 o 28 6 0 740.84 963.54 348.95 o 29 6 0 546.57 471.49 333.34 o 30 6 0 2576.79 2320.83 415.90 o 31 6 0 460.91 153.35 334.42 o 32 6 0 3429.08 3343.23 502.65 o 33 6 0 130.04 -129.80 257.86 o 1 7 0 5154.60 4542.22 476.96 o 2 7 0 4218.32 6060.99 536.96 o 3 7 0 564.26 343.56 288.07 o 4 7 0 8102.52 9819.30 461.42 o 5 7 0 81.77 50.81 250.15 o 6 7 0 15524.95 16776.16 611.28 o 7 7 0 53.99 212.59 185.94 o 8 7 0 17239.32 18597.24 658.32 o 9 7 0 377.82 302.68 186.54 o 10 7 0 8070.39 9972.87 454.88 o 11 7 0 818.40 491.93 204.36 o 12 7 0 4413.75 5834.52 568.11 o 13 7 0 2424.75 1861.85 390.25 o 14 7 0 1689.58 1913.85 397.98 o 15 7 0 4239.44 3797.87 493.08 o 16 7 0 388.71 663.29 346.82 o 17 7 0 1578.02 1245.07 357.08 o 18 7 0 203.60 -8.62 323.47 o 19 7 0 1004.67 646.03 365.30 o 20 7 0 4912.05 4749.48 470.35 o 21 7 0 1702.19 1729.72 363.32 o 22 7 0 9736.86 12110.91 721.20 o 23 7 0 1149.49 1477.65 355.85 o 24 7 0 6410.34 6605.59 786.37 o 25 7 0 140.48 42.52 282.82 o 26 7 0 4944.78 5029.99 861.60 o 27 7 0 9.56 591.39 328.37 o 28 7 0 6077.73 7290.73 685.53 o 29 7 0 30.61 479.81 346.48 o 30 7 0 3426.40 4476.96 548.95 o 31 7 0 55.71 363.26 259.54 o 0 8 0 28648.69 34896.93 2196.75 o 1 8 0 1437.02 1615.88 392.75 o 2 8 0 37183.27 41554.62 1435.29 o 3 8 0 551.25 932.16 265.99 o 4 8 0 24481.47 24977.19 977.63 o 5 8 0 1583.10 2024.13 299.86 o 6 8 0 2901.38 3030.91 311.87 o 7 8 0 775.27 641.26 216.07 o 8 8 0 284.42 665.36 233.25 o 9 8 0 451.99 276.38 205.63 o 10 8 0 2814.07 3434.69 960.29 o 11 8 0 1812.73 1929.93 410.96 o 12 8 0 16856.93 18242.91 1013.97 o 13 8 0 862.35 1192.52 372.48 o 14 8 0 15650.10 17546.76 1003.58 o 15 8 0 282.84 357.02 341.39 o 16 8 0 18140.06 19997.25 1126.62 o 17 8 0 897.50 1156.83 517.81 o 18 8 0 22639.06 22711.57 1203.91 o 19 8 0 704.93 714.35 605.68 o 20 8 0 11868.61 12352.01 911.44 o 21 8 0 50.66 154.00 358.76 o 22 8 0 3011.34 3546.01 575.74 o 23 8 0 46.41 214.67 574.29 o 24 8 0 579.17 498.11 426.88 o 25 8 0 225.35 -288.94 368.04 o 26 8 0 12.22 -291.02 291.02 o 27 8 0 153.13 -108.73 311.90 o 1 9 0 3616.87 3394.80 485.58 o 2 9 0 3671.00 4361.61 351.43 o 3 9 0 6184.96 5651.41 471.62 o 4 9 0 6840.10 7685.61 495.86 o 5 9 0 283.51 45.73 231.38 o 6 9 0 8535.70 10777.26 670.20 o 7 9 0 490.04 293.54 247.24 o 8 9 0 11026.75 13527.98 935.19 o 9 9 0 492.02 418.42 630.78 o 10 9 0 13408.08 15386.04 942.19 o 11 9 0 2592.90 3347.73 935.19 o 12 9 0 11333.10 13035.27 909.11 o 13 9 0 2259.47 1594.48 778.28 o 14 9 0 5695.08 6567.58 1813.89 o 15 9 0 1039.20 1005.36 458.18 o 16 9 0 1687.09 2007.50 490.27 o 17 9 0 2272.64 1668.81 477.98 o 18 9 0 46.23 -5.27 355.48 o 19 9 0 892.42 381.46 367.08 o 20 9 0 2648.96 3453.21 588.10 o 21 9 0 76.68 -22.79 369.27 o 22 9 0 4691.00 4546.77 1289.81 o 23 9 0 203.68 860.47 383.26 o 0 10 0 7483.29 10436.76 872.65 o 1 10 0 132.61 -264.63 264.63 o 2 10 0 5181.93 7161.98 522.59 o 3 10 0 700.26 52.40 257.01 o 4 10 0 1924.89 2168.25 316.62 o 5 10 0 2515.61 1645.72 397.17 o 6 10 0 337.00 260.73 286.20 o 7 10 0 4433.16 3970.47 475.57 o 8 10 0 1.65 297.12 281.14 o 9 10 0 3434.83 2237.86 395.52 o 10 10 0 352.52 316.96 302.84 o 11 10 0 2852.10 2208.77 352.49 o 12 10 0 2324.13 3334.01 394.43 o 13 10 0 1444.27 2307.51 354.24 o 14 10 0 4232.77 4674.58 459.94 o 15 10 0 239.80 193.30 272.54 o 16 10 0 4285.09 4594.92 882.21 o 17 10 0 14.12 -293.96 293.96 o 1 11 0 6766.76 5831.56 535.50 o 2 11 0 457.63 482.11 329.25 o 3 11 0 4265.85 3890.66 392.62 o 4 11 0 1023.98 933.89 360.05 o 5 11 0 1884.44 1085.94 375.69 o 6 11 0 856.71 1114.00 381.74 o -40 1 1 93.86 -167.17 435.79 o -39 1 1 367.08 344.15 462.49 o -38 1 1 621.91 224.25 436.21 o -37 1 1 329.89 18.83 421.62 o -36 1 1 612.52 193.71 402.70 o -35 1 1 362.73 272.43 702.96 o -34 1 1 1498.18 985.15 447.19 o -33 1 1 1289.08 1923.48 479.68 o -32 1 1 5074.36 5059.61 634.46 o -31 1 1 1438.04 1898.78 480.15 o -30 1 1 2819.45 2149.47 466.94 o -29 1 1 95.48 451.71 357.08 o -28 1 1 666.63 650.28 365.64 o -27 1 1 2.85 13.10 281.58 o -26 1 1 247.57 644.89 317.11 o -25 1 1 78.52 44.92 207.68 o -24 1 1 128.12 737.31 239.10 o -23 1 1 1512.52 1374.23 258.15 o -22 1 1 2751.59 2967.11 300.89 o -21 1 1 6959.58 5955.08 767.50 o -20 1 1 9521.08 8991.96 426.69 o -19 1 1 5548.05 5842.17 213.69 o -18 1 1 2528.99 3010.35 182.77 o -17 1 1 692.52 194.21 105.19 o -16 1 1 7348.29 6175.03 390.45 o -15 1 1 7769.56 6574.49 255.07 o -14 1 1 12257.44 12992.26 402.11 o -13 1 1 2220.32 3544.21 239.60 o -12 1 1 6209.70 7831.53 352.00 o -11 1 1 5207.56 3492.45 241.97 o -10 1 1 16456.61 15430.00 532.29 o -9 1 1 5486.98 6331.29 288.26 o -8 1 1 27983.12 29800.89 892.57 o -7 1 1 16763.91 15011.39 1383.95 o -6 1 1 6972.69 5705.29 372.80 o -5 1 1 22.40 41.41 53.04 o -4 1 1 231.09 138.87 91.01 o -3 1 1 9873.32 8775.31 344.81 o -2 1 1 40252.06 37382.40 1851.55 o -1 1 1 29484.71 15402.35 803.38 o 0 1 1 19469.79 12989.36 476.71 o 1 1 1 7029.35 4949.26 342.07 o 2 1 1 11678.91 8862.31 489.56 o 3 1 1 30891.06 16801.99 853.59 o 4 1 1 151443.33 105615.81 6747.16 o 5 1 1 130052.29 94275.54 7280.65 o 6 1 1 102384.41 91072.70 4300.42 o 7 1 1 19220.09 10487.91 564.88 o 8 1 1 10677.26 9204.25 351.50 o 9 1 1 26.61 -75.88 75.88 o 10 1 1 2.74 -76.11 76.11 o 11 1 1 10714.81 8177.64 285.64 o 12 1 1 8013.83 5339.97 221.66 o 13 1 1 10932.02 11059.06 357.82 o 14 1 1 10104.94 9550.37 330.74 o 15 1 1 8183.39 7673.73 409.48 o 16 1 1 26.25 -15.07 99.47 o 17 1 1 212.43 210.40 109.82 o 18 1 1 1924.61 1746.80 172.13 o 19 1 1 2454.58 2416.54 186.29 o 20 1 1 8260.44 9012.55 371.31 o 21 1 1 3035.90 3914.15 324.16 o 22 1 1 683.68 941.62 269.21 o 23 1 1 802.98 1224.13 279.55 o 24 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