#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:25:10 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181233 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/11/2231145.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231145_Fobs loop_ _publ_author_name 'Chelghoum, Meryem' 'Bahnous, Mebarek' 'Bouacida, Sofiane' 'Roisnel, Thierry' 'Belfaitah, Ali' _publ_section_title ; 2-Hydroxymethyl-1,3-dimethylimidazolium iodide ; _journal_coeditor_code HG5062 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1890 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.093 _cell_angle_gamma 90.000 _cell_length_a 7.3428 _cell_length_b 7.2186 _cell_length_c 16.8870 _exptl_crystal_F_000 488.00 _reflns_d_resolution_high 0.7711 _cod_data_source_file hg5062Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' import in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 324.21 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14009.78 15118.01 328.27 o 3 0 0 4520.52 4768.42 127.97 o 4 0 0 928.50 1053.51 29.55 o 5 0 0 12882.70 13214.38 350.17 o 6 0 0 2999.90 3180.37 106.38 o 7 0 0 2572.94 2421.26 91.41 o 8 0 0 4300.56 4345.29 147.16 o 9 0 0 13.80 10.65 11.85 o 1 1 0 7216.75 8375.37 123.64 o 2 1 0 22813.56 24871.07 361.00 o 3 1 0 2926.23 3041.75 44.14 o 4 1 0 29461.32 31453.33 457.54 o 5 1 0 2.05 2.98 2.83 o 6 1 0 4306.40 4312.04 95.42 o 7 1 0 5620.99 5679.25 123.72 o 8 1 0 646.17 631.69 30.04 o 9 1 0 2655.72 2881.95 81.39 o 0 2 0 105111.21 100017.75 1806.27 o 1 2 0 13.79 27.46 3.16 o 2 2 0 17241.65 18064.98 297.17 o 3 2 0 8108.37 8342.92 126.22 o 4 2 0 137.26 134.95 7.57 o 5 2 0 9043.29 8991.40 197.33 o 6 2 0 2020.18 2022.49 53.42 o 7 2 0 2474.22 2397.44 63.80 o 8 2 0 3834.09 3951.24 96.71 o 9 2 0 15.14 -0.10 10.75 o 1 3 0 7074.66 7061.22 221.57 o 2 3 0 11166.92 11822.63 150.30 o 3 3 0 3727.46 3801.18 119.23 o 4 3 0 21995.98 22568.50 330.52 o 5 3 0 148.90 134.77 8.62 o 6 3 0 2478.95 2436.94 60.80 o 7 3 0 3193.51 3073.30 76.04 o 8 3 0 776.68 738.81 48.62 o 9 3 0 2648.94 2661.34 111.90 o 0 4 0 31917.30 32589.21 828.01 o 1 4 0 22.62 18.39 2.67 o 2 4 0 10618.71 10557.76 190.23 o 3 4 0 6436.14 6110.94 93.32 o 4 4 0 28.36 18.85 3.38 o 5 4 0 5466.74 5157.15 105.57 o 6 4 0 1177.61 1290.09 58.26 o 7 4 0 1673.54 1560.40 70.62 o 8 4 0 2423.21 2504.23 102.06 o 1 5 0 4625.37 4553.03 63.38 o 2 5 0 5733.00 5548.01 109.60 o 3 5 0 1880.80 1818.51 44.55 o 4 5 0 10073.80 9883.63 148.75 o 5 5 0 81.23 83.98 14.46 o 6 5 0 1793.41 1857.73 74.33 o 7 5 0 1997.82 1777.07 76.64 o 8 5 0 330.21 350.67 34.86 o 0 6 0 13984.42 14132.40 384.93 o 1 6 0 442.02 439.56 21.02 o 2 6 0 3757.64 3873.55 72.73 o 3 6 0 2216.15 2130.09 51.90 o 4 6 0 106.85 120.64 14.16 o 5 6 0 3315.09 3019.95 99.95 o 6 6 0 725.55 772.06 42.89 o 7 6 0 816.96 833.74 48.52 o 1 7 0 2071.95 1939.30 75.89 o 2 7 0 2689.37 2581.98 97.14 o 3 7 0 641.14 649.14 23.22 o 4 7 0 3447.22 3413.94 92.41 o 5 7 0 17.42 22.71 7.60 o 6 7 0 1173.50 1137.70 54.14 o 0 8 0 4696.60 4796.82 159.42 o 1 8 0 249.37 289.90 31.14 o 2 8 0 1556.34 1476.52 70.22 o 3 8 0 824.99 787.93 49.72 o 4 8 0 39.04 34.98 10.45 o 1 9 0 695.62 780.40 51.03 o 2 9 0 918.88 909.88 56.75 o -9 1 1 7.33 3.88 8.41 o -8 1 1 7.95 3.13 6.51 o -7 1 1 32.62 29.34 8.27 o -6 1 1 3.18 0.44 4.32 o -5 1 1 45.45 43.75 5.84 o -4 1 1 1.08 15.28 4.62 o -3 1 1 74.88 86.34 6.83 o -2 1 1 11.33 7.21 2.07 o -1 1 1 10.88 12.40 1.60 o 1 1 1 41.89 19.30 2.11 o 2 1 1 271.07 271.40 6.88 o 3 1 1 192.74 206.09 13.48 o 4 1 1 78.80 81.62 6.29 o 5 1 1 197.22 229.69 11.14 o 6 1 1 23.62 29.54 10.90 o 7 1 1 38.69 34.20 8.26 o 8 1 1 6.30 4.38 6.68 o 9 1 1 19.32 6.82 8.74 o -9 2 1 8.40 31.14 15.87 o -8 2 1 0.98 8.88 7.94 o -7 2 1 84.57 79.62 11.70 o -6 2 1 39.92 48.69 8.95 o -5 2 1 133.71 135.09 8.95 o -4 2 1 84.11 81.67 6.20 o -3 2 1 344.44 358.84 10.81 o -2 2 1 405.92 443.39 10.98 o -1 2 1 87.13 99.08 3.58 o 0 2 1 1407.87 1388.95 16.28 o 1 2 1 114.22 110.06 2.87 o 2 2 1 240.59 258.33 7.84 o 3 2 1 26.50 25.66 3.42 o 4 2 1 10.60 14.20 3.27 o 5 2 1 19.77 11.58 7.43 o 6 2 1 4.89 -4.07 4.07 o 7 2 1 7.37 6.32 6.11 o 8 2 1 0.76 -4.63 6.09 o 9 2 1 0.28 24.91 14.77 o -9 3 1 1.44 -2.81 11.25 o -8 3 1 0.41 -2.21 8.74 o -7 3 1 51.66 29.74 8.73 o -6 3 1 5.05 -3.76 3.76 o -5 3 1 83.80 84.04 7.24 o -4 3 1 3.16 15.10 5.11 o -3 3 1 318.32 339.87 23.91 o -2 3 1 0.05 -1.32 1.32 o -1 3 1 32.74 34.47 1.54 o 0 3 1 65.90 67.58 5.89 o 1 3 1 78.71 67.86 3.40 o 2 3 1 47.68 62.15 3.18 o 3 3 1 55.71 60.16 5.76 o 4 3 1 0.31 5.16 2.80 o 5 3 1 277.25 280.78 11.92 o 6 3 1 0.98 -4.56 4.56 o 7 3 1 30.85 21.17 7.65 o 8 3 1 0.55 -5.02 9.24 o -8 4 1 12.56 10.45 11.95 o -7 4 1 44.67 34.25 14.57 o -6 4 1 4.53 -6.43 6.43 o -5 4 1 0.15 -2.63 3.81 o -4 4 1 61.86 69.67 6.92 o -3 4 1 3.66 -2.07 2.07 o -2 4 1 5.43 -2.01 2.01 o -1 4 1 288.32 343.58 7.54 o 0 4 1 97.48 89.91 4.36 o 1 4 1 946.80 1031.57 18.01 o 2 4 1 0.52 -1.90 1.90 o 3 4 1 25.54 21.17 2.84 o 4 4 1 0.92 -1.87 2.13 o 5 4 1 88.49 77.57 8.88 o 6 4 1 10.57 10.65 9.34 o 7 4 1 4.95 12.36 10.75 o 8 4 1 2.75 10.25 11.55 o -8 5 1 19.36 5.02 11.45 o -7 5 1 5.58 -7.03 8.14 o -6 5 1 76.47 56.45 14.16 o -5 5 1 14.91 3.72 7.13 o -4 5 1 54.03 58.70 7.08 o -3 5 1 199.58 204.01 11.65 o -2 5 1 0.58 3.68 5.93 o -1 5 1 35.99 26.27 5.90 o 0 5 1 2.97 1.85 3.42 o 1 5 1 285.91 247.86 9.13 o 2 5 1 20.41 15.41 4.15 o 3 5 1 20.48 15.07 3.87 o 4 5 1 110.64 111.03 6.32 o 5 5 1 82.08 91.21 14.97 o 6 5 1 89.95 77.65 16.17 o 7 5 1 0.08 0.80 8.64 o 8 5 1 30.37 21.50 13.66 o -7 6 1 43.36 30.34 13.46 o -6 6 1 4.88 -7.43 7.53 o -5 6 1 0.02 -6.13 6.13 o -4 6 1 71.64 65.69 11.65 o -3 6 1 8.48 20.09 9.54 o -2 6 1 5.59 -3.06 3.06 o -1 6 1 177.53 165.49 14.45 o 0 6 1 27.19 25.30 7.81 o 1 6 1 622.24 606.92 24.96 o 2 6 1 1.28 -1.69 6.98 o 3 6 1 6.88 -0.48 3.44 o 4 6 1 0.02 8.18 6.78 o 5 6 1 68.07 53.34 12.96 o 6 6 1 16.38 1.71 7.94 o 7 6 1 1.41 -2.31 8.54 o -6 7 1 34.76 14.67 10.65 o -5 7 1 23.50 15.97 9.44 o -4 7 1 21.63 24.88 10.05 o -3 7 1 131.66 129.07 16.22 o -2 7 1 1.17 17.48 9.84 o -1 7 1 1.90 6.63 7.53 o 0 7 1 13.00 13.33 7.89 o 1 7 1 85.64 94.16 12.83 o 2 7 1 4.19 10.25 8.74 o 3 7 1 0.03 4.92 10.25 o 4 7 1 16.85 10.75 6.53 o 5 7 1 154.02 137.68 14.18 o 6 7 1 20.62 13.96 7.92 o -4 8 1 2.37 8.96 5.93 o -3 8 1 17.36 20.69 12.76 o -2 8 1 26.86 39.18 14.16 o -1 8 1 5.23 -3.31 7.03 o 0 8 1 80.51 86.00 13.77 o 1 8 1 160.88 170.37 17.78 o 2 8 1 8.75 3.31 8.44 o 3 8 1 4.85 14.77 10.25 o 4 8 1 1.81 -0.51 5.17 o -2 9 1 2.31 4.92 10.65 o -1 9 1 0.42 3.72 9.14 o 0 9 1 15.80 12.81 8.09 o 1 9 1 17.30 22.00 13.56 o 2 9 1 19.22 33.25 15.27 o -9 0 2 2003.91 1971.95 89.50 o -8 0 2 2315.98 2155.47 89.70 o -7 0 2 191.41 219.48 24.31 o -6 0 2 13075.35 13628.34 366.64 o -5 0 2 202.44 189.25 18.68 o -4 0 2 9638.76 9833.70 384.07 o -3 0 2 23152.81 23562.75 420.56 o -2 0 2 224.47 207.54 10.90 o -1 0 2 42975.74 41337.57 737.94 o 2 0 2 34777.60 33904.30 856.44 o 3 0 2 0.14 1.00 3.72 o 4 0 2 10446.08 9687.51 181.87 o 5 0 2 6141.14 6470.63 183.62 o 6 0 2 4338.02 4271.56 134.50 o 7 0 2 3442.98 4005.77 133.00 o 8 0 2 212.95 239.27 28.53 o 9 0 2 1916.70 1882.45 87.29 o -9 1 2 581.72 616.32 51.18 o -8 1 2 2464.55 2439.83 68.92 o -7 1 2 3369.40 3330.71 81.68 o -6 1 2 48.53 40.38 11.05 o -5 1 2 11275.07 11549.30 318.45 o -4 1 2 4294.83 4405.46 73.35 o -3 1 2 8680.95 9321.48 122.12 o -2 1 2 41987.86 42702.58 540.05 o -1 1 2 353.40 376.10 8.75 o 0 1 2 3915.10 4118.39 48.25 o 1 1 2 23952.26 23969.79 283.97 o 2 1 2 9421.84 9620.94 123.30 o 3 1 2 29742.39 31792.38 397.97 o 4 1 2 1675.25 1651.44 33.12 o 5 1 2 4717.05 5096.96 105.43 o 6 1 2 8183.76 8148.02 163.50 o 7 1 2 288.09 301.00 48.17 o 8 1 2 3946.04 3983.45 97.67 o 9 1 2 517.27 577.44 31.25 o -9 2 2 1441.98 1692.29 83.17 o -8 2 2 1647.62 1611.22 52.11 o -7 2 2 425.63 443.70 23.04 o -6 2 2 13431.02 12730.42 250.73 o -5 2 2 659.00 636.24 21.14 o -4 2 2 5843.06 5765.94 92.52 o -3 2 2 12784.70 13810.99 248.82 o -2 2 2 1268.05 1298.03 36.46 o -1 2 2 40137.97 42234.19 532.05 o 0 2 2 3236.41 3316.83 31.46 o 1 2 2 14164.63 14344.19 194.29 o 2 2 2 20731.57 20402.25 624.07 o 4 2 2 8693.23 8355.22 129.45 o 5 2 2 4921.50 5214.55 99.85 o 6 2 2 3867.56 3886.95 87.82 o 7 2 2 3443.12 3495.13 152.43 o 8 2 2 288.74 281.49 21.06 o 9 2 2 1420.32 1465.27 76.24 o -9 3 2 314.83 294.02 35.86 o -8 3 2 2215.72 2056.33 89.40 o -7 3 2 2822.42 2814.48 71.68 o -6 3 2 24.91 22.35 6.56 o -5 3 2 7988.79 8181.03 129.25 o -4 3 2 4204.29 4054.30 67.55 o -3 3 2 4320.91 4385.45 86.29 o -2 3 2 18794.46 18387.80 327.83 o -1 3 2 22.59 26.42 3.91 o 0 3 2 8015.94 7832.61 83.09 o 1 3 2 21476.22 21618.74 224.07 o 2 3 2 1752.57 1918.30 32.02 o 3 3 2 14999.90 14583.12 520.94 o 4 3 2 344.66 333.94 14.40 o 5 3 2 5604.84 5587.30 92.30 o 6 3 2 7386.08 6874.19 140.36 o 7 3 2 71.16 88.11 12.86 o 8 3 2 2726.40 2510.46 101.96 o -8 4 2 1060.93 963.52 56.45 o -7 4 2 445.72 447.41 34.66 o -6 4 2 9215.14 8344.03 239.37 o -5 4 2 677.35 687.13 24.04 o -4 4 2 3336.91 3059.50 52.53 o -3 4 2 6076.37 6158.78 116.73 o -2 4 2 1032.11 1051.47 19.14 o -1 4 2 21888.90 22475.39 328.79 o 0 4 2 2849.30 2854.36 48.40 o 1 4 2 7728.03 7904.83 104.65 o 2 4 2 9822.48 10019.48 129.64 o 4 4 2 5344.86 5199.01 103.12 o 5 4 2 2719.73 2701.12 63.89 o 6 4 2 2435.26 2227.49 84.08 o 7 4 2 2618.42 2691.58 101.76 o 8 4 2 254.13 261.98 30.94 o -8 5 2 1323.29 1286.27 67.80 o -7 5 2 1704.03 1597.37 71.72 o -6 5 2 19.99 19.19 10.85 o -5 5 2 4165.08 4151.63 128.98 o -4 5 2 2268.35 2043.31 46.78 o -3 5 2 2716.32 2557.94 52.79 o -2 5 2 9134.79 8763.37 161.20 o -1 5 2 41.81 59.12 4.57 o 0 5 2 4317.87 4218.55 69.91 o 1 5 2 7854.32 7936.43 124.42 o 2 5 2 1114.73 1155.66 22.56 o 3 5 2 8701.29 8206.63 108.61 o 4 5 2 425.47 416.54 12.12 o 5 5 2 2876.32 2669.78 90.31 o 6 5 2 3703.45 3423.36 114.71 o 7 5 2 69.09 55.75 15.17 o -7 6 2 126.80 159.42 23.51 o -6 6 2 3560.73 3124.42 108.79 o -5 6 2 142.63 153.19 18.48 o -4 6 2 2571.89 2536.48 83.07 o -3 6 2 4034.33 4000.05 115.02 o -2 6 2 113.65 126.92 6.78 o -1 6 2 7571.12 7678.15 223.10 o 0 6 2 1014.21 1036.19 34.24 o 1 6 2 4272.91 4082.46 91.91 o 2 6 2 4765.16 4767.45 142.89 o 3 6 2 0.67 9.08 4.34 o 4 6 2 2932.49 2953.00 69.95 o 5 6 2 1320.44 1216.06 52.23 o 6 6 2 934.86 966.54 49.02 o 7 6 2 1248.43 1196.37 59.77 o -6 7 2 25.40 28.53 12.05 o -5 7 2 1802.22 1645.88 64.39 o -4 7 2 999.30 1032.51 34.50 o -3 7 2 1423.11 1426.18 45.71 o -2 7 2 3797.50 3809.74 128.43 o -1 7 2 105.18 120.64 19.79 o 0 7 2 1611.60 1614.13 48.87 o 1 7 2 2217.62 2147.87 59.70 o 2 7 2 672.64 718.42 42.29 o 3 7 2 4327.38 4295.06 92.12 o 4 7 2 399.41 393.43 22.00 o 5 7 2 1054.53 1105.54 37.99 o 6 7 2 1365.83 1356.60 45.95 o -4 8 2 1131.99 1223.48 38.35 o -3 8 2 1610.05 1723.53 80.76 o -2 8 2 28.73 52.23 16.47 o -1 8 2 2753.06 2717.59 104.97 o 0 8 2 447.35 525.44 28.53 o 1 8 2 1731.43 1764.17 62.73 o 2 8 2 1656.38 1561.40 72.83 o 3 8 2 0.21 10.45 9.74 o 4 8 2 1325.47 1461.27 42.61 o -2 9 2 1059.83 1025.90 60.37 o -1 9 2 17.72 20.39 12.36 o 0 9 2 758.46 743.03 49.42 o 1 9 2 878.78 1004.91 58.66 o 2 9 2 111.24 108.69 24.81 o -9 1 3 1.11 1.56 8.09 o -8 1 3 0.06 -4.90 6.10 o -7 1 3 1.41 -1.70 4.61 o -6 1 3 3.82 2.57 4.77 o -5 1 3 17.56 15.96 4.19 o -4 1 3 96.97 107.10 7.33 o -3 1 3 105.28 95.78 5.30 o -2 1 3 281.87 307.29 7.78 o -1 1 3 196.56 209.47 5.91 o 0 1 3 575.31 560.49 8.71 o 1 1 3 114.62 107.92 2.97 o 2 1 3 461.26 478.10 9.94 o 3 1 3 91.90 86.08 4.83 o 4 1 3 54.57 55.35 5.62 o 5 1 3 38.77 37.56 5.61 o 6 1 3 19.17 10.38 11.60 o 7 1 3 6.73 5.71 6.21 o 8 1 3 0.30 -4.22 5.75 o 9 1 3 1.68 -4.21 7.32 o -9 2 3 17.37 27.32 15.67 o -8 2 3 11.19 0.08 6.56 o -7 2 3 68.48 61.90 11.03 o -6 2 3 35.99 38.90 8.38 o -5 2 3 283.89 305.71 12.68 o -4 2 3 74.15 76.63 9.29 o -3 2 3 336.29 372.76 12.72 o -2 2 3 50.19 52.24 3.97 o -1 2 3 176.52 182.67 5.09 o 0 2 3 216.31 223.90 5.03 o 1 2 3 31.63 25.87 2.04 o 2 2 3 46.80 46.66 3.05 o 3 2 3 89.17 95.51 5.69 o 4 2 3 22.10 34.66 4.62 o 5 2 3 129.66 160.09 9.65 o 6 2 3 4.15 -2.72 4.29 o 7 2 3 95.15 89.22 13.46 o 8 2 3 15.22 4.11 10.85 o 9 2 3 15.92 6.63 11.65 o -8 3 3 0.40 1.61 10.35 o -7 3 3 0.60 -2.85 5.28 o -6 3 3 0.03 -2.16 6.18 o -5 3 3 2.29 -2.84 3.17 o -4 3 3 42.50 41.75 5.02 o -3 3 3 3.13 -0.65 1.38 o -2 3 3 37.68 30.18 3.30 o -1 3 3 36.62 35.38 2.78 o 0 3 3 113.32 116.42 2.99 o 1 3 3 138.71 124.20 3.59 o 2 3 3 213.99 214.12 6.87 o 3 3 3 9.21 12.45 2.82 o 4 3 3 6.53 5.68 2.76 o 5 3 3 9.46 3.12 3.33 o 6 3 3 11.14 7.42 5.40 o 7 3 3 2.50 3.68 6.29 o 8 3 3 1.09 -8.84 8.84 o -8 4 3 17.29 6.53 10.85 o -7 4 3 0.49 0.40 8.24 o -6 4 3 30.74 38.07 13.36 o -5 4 3 84.25 79.54 13.86 o -4 4 3 21.14 22.00 3.84 o -3 4 3 20.80 30.28 11.20 o -2 4 3 30.24 40.22 6.38 o -1 4 3 20.25 14.66 2.16 o 0 4 3 131.12 126.83 3.29 o 1 4 3 17.71 17.65 1.58 o 2 4 3 13.78 10.28 1.88 o 3 4 3 2.97 2.51 3.55 o 4 4 3 15.67 14.65 4.85 o 5 4 3 39.21 37.87 6.89 o 6 4 3 54.12 29.43 11.55 o 7 4 3 38.97 7.03 9.54 o 8 4 3 1.28 5.42 9.74 o -7 5 3 0.30 -7.13 7.53 o -6 5 3 2.82 -4.12 7.13 o -5 5 3 1.84 13.16 8.44 o -4 5 3 0.41 -3.07 3.07 o -3 5 3 42.47 43.63 5.03 o -2 5 3 39.48 41.16 3.96 o -1 5 3 340.02 321.49 9.21 o 0 5 3 19.69 19.69 5.99 o 1 5 3 498.20 497.07 13.58 o 2 5 3 6.14 1.73 2.56 o 3 5 3 194.14 201.81 7.73 o 4 5 3 133.68 144.53 9.70 o 5 5 3 2.56 -1.31 7.03 o 6 5 3 0.41 2.71 7.63 o 7 5 3 0.09 3.21 8.94 o -7 6 3 0.96 0.90 8.94 o -6 6 3 48.10 46.51 14.46 o -5 6 3 52.85 31.14 10.45 o -4 6 3 28.64 12.96 7.84 o -3 6 3 3.60 -3.92 4.82 o -2 6 3 46.55 56.85 6.53 o -1 6 3 5.94 2.64 2.47 o 0 6 3 76.28 71.01 16.98 o 1 6 3 6.05 -2.80 12.46 o 2 6 3 7.46 17.18 7.23 o 3 6 3 0.13 0.18 6.83 o 4 6 3 19.95 21.17 9.39 o 5 6 3 18.76 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