#------------------------------------------------------------------------------ #$Date: 2011-10-06 14:27:20 +0300 (Thu, 06 Oct 2011) $ #$Revision: 27511 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/11/2231150.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231150_Fobs loop_ _publ_author_name 'Mochida, Tomoyuki' _publ_section_title ; 1,1',2,2',3,3',4,4'-Octamethylferrocenium 2,5-dibromo-4-hydroxy-3,6-dioxocyclohexa-1,4-dien-1-olate ; _journal_coeditor_code HY2444 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1012 _journal_volume 67 _journal_year 2011 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.7106 _cell_length_b 10.4938 _cell_length_c 14.9461 _exptl_crystal_F_000 1196.00 _reflns_d_resolution_high 0.7690 _[local]_cod_data_source_file hy2444Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' OctMeBAPnma in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 457.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 69925.38 70806.15 953.51 o 4 0 0 37219.43 35492.59 625.89 o 6 0 0 9218.63 9326.91 232.35 o 8 0 0 2933.80 2459.17 254.56 o 10 0 0 214.67 357.24 100.25 o 12 0 0 69.95 -135.36 135.36 o 14 0 0 2478.16 2200.18 269.05 o 16 0 0 896.95 1122.51 251.32 o 18 0 0 5.76 -44.42 196.68 o 2 1 0 3.88 12.79 13.69 o 4 1 0 12599.81 13398.64 189.83 o 6 1 0 1063.73 1160.73 52.51 o 8 1 0 715.42 616.98 71.69 o 10 1 0 4300.15 4109.60 157.69 o 12 1 0 6387.22 6208.65 254.95 o 14 1 0 24.06 -1.97 105.71 o 16 1 0 1.45 50.07 120.47 o 18 1 0 722.86 662.34 176.16 o 0 2 0 140963.88 148225.80 3383.59 o 2 2 0 6694.68 6615.38 103.41 o 4 2 0 10823.00 10173.18 154.87 o 6 2 0 10549.78 10254.84 167.76 o 8 2 0 16938.64 16826.17 258.74 o 10 2 0 593.25 532.46 86.62 o 12 2 0 218.39 281.63 93.51 o 14 2 0 1250.43 1398.25 135.02 o 16 2 0 703.61 743.39 246.74 o 18 2 0 512.75 497.49 173.49 o 2 3 0 125.35 148.31 46.80 o 4 3 0 2286.19 2243.95 66.93 o 6 3 0 4238.46 4306.59 99.39 o 8 3 0 49.14 9.21 37.43 o 10 3 0 3018.83 2999.91 143.84 o 12 3 0 61.75 42.78 83.54 o 14 3 0 796.81 821.55 203.08 o 16 3 0 11.76 25.18 108.01 o 18 3 0 1141.21 1270.08 205.23 o 0 4 0 83396.40 85689.95 2024.77 o 2 4 0 3132.47 2888.59 169.57 o 4 4 0 8124.59 8013.75 140.86 o 6 4 0 8793.98 8562.12 221.08 o 8 4 0 13108.55 13658.49 225.81 o 10 4 0 488.54 424.37 90.42 o 12 4 0 282.71 241.13 91.87 o 14 4 0 964.59 957.90 129.56 o 16 4 0 673.56 767.96 134.04 o 18 4 0 507.48 281.00 170.32 o 2 5 0 29.58 25.45 49.68 o 4 5 0 3853.29 3931.75 113.16 o 6 5 0 177.67 209.74 45.01 o 8 5 0 395.81 339.29 75.74 o 10 5 0 1841.88 1812.84 130.26 o 12 5 0 3821.57 3801.59 179.99 o 14 5 0 27.66 -17.92 106.97 o 16 5 0 8.61 50.49 119.36 o 0 6 0 209544.38 208530.80 4827.29 o 2 6 0 19503.12 20633.58 1152.96 o 4 6 0 6325.16 6363.01 139.33 o 6 6 0 2988.11 2725.37 97.39 o 8 6 0 2202.78 2066.03 126.73 o 10 6 0 41.06 97.26 83.35 o 12 6 0 62.22 117.40 92.80 o 14 6 0 1261.59 1239.47 149.48 o 16 6 0 593.35 333.51 155.42 o 2 7 0 100.46 97.60 72.90 o 4 7 0 2265.15 2294.12 94.72 o 6 7 0 94.92 92.26 54.34 o 8 7 0 166.54 53.94 104.45 o 10 7 0 2095.13 2238.72 174.41 o 12 7 0 3009.11 3199.44 183.04 o 14 7 0 75.85 -16.67 162.47 o 16 7 0 23.40 -139.11 139.11 o 0 8 0 28297.63 27061.84 810.70 o 2 8 0 1857.61 1976.65 140.99 o 4 8 0 1083.14 1067.09 82.45 o 6 8 0 2625.31 2620.49 183.70 o 8 8 0 4924.72 4807.68 185.94 o 10 8 0 493.07 553.21 109.84 o 12 8 0 130.91 1.41 141.20 o 14 8 0 451.78 217.54 151.40 o 2 9 0 92.29 174.49 79.06 o 4 9 0 303.95 337.44 79.60 o 6 9 0 573.17 574.91 115.99 o 8 9 0 34.47 80.22 92.65 o 10 9 0 741.73 629.75 155.21 o 12 9 0 81.43 9.94 134.50 o 14 9 0 186.26 -20.16 148.57 o 0 10 0 8534.71 9009.49 428.19 o 2 10 0 609.20 607.36 130.67 o 4 10 0 363.40 407.45 129.96 o 6 10 0 1789.77 1899.49 144.85 o 8 10 0 3228.60 3696.33 246.22 o 10 10 0 355.89 513.74 161.77 o 12 10 0 97.62 119.08 161.76 o 2 11 0 29.91 65.14 116.52 o 4 11 0 301.84 198.56 98.37 o 6 11 0 19.08 50.99 125.36 o 8 11 0 22.55 206.60 147.04 o 10 11 0 294.37 503.47 178.71 o 0 12 0 22128.96 24415.12 875.77 o 2 12 0 3783.32 3753.77 230.65 o 4 12 0 105.40 363.59 157.61 o 6 12 0 261.53 210.59 213.89 o 8 12 0 193.89 229.26 171.38 o 2 13 0 49.64 277.19 240.27 o 4 13 0 122.56 -36.08 219.00 o 1 0 1 878.09 871.98 36.28 o 2 0 1 18694.55 19227.82 239.69 o 3 0 1 2146.09 2256.23 57.75 o 4 0 1 8109.82 7967.29 117.83 o 5 0 1 15823.21 16193.20 208.33 o 6 0 1 6866.73 6976.81 121.70 o 7 0 1 3180.26 3312.91 123.28 o 8 0 1 2163.98 1997.28 86.88 o 9 0 1 3383.08 3586.85 184.03 o 10 0 1 5549.31 5858.96 296.36 o 11 0 1 498.23 401.06 90.41 o 12 0 1 580.71 515.11 237.18 o 13 0 1 2720.77 2537.15 305.86 o 14 0 1 25.49 -31.20 195.32 o 15 0 1 869.82 793.90 152.78 o 16 0 1 251.89 426.01 183.12 o 17 0 1 53.06 5.77 138.18 o 18 0 1 25.09 54.72 140.77 o 19 0 1 98.76 25.02 155.59 o 0 1 1 457.11 439.90 14.01 o 1 1 1 21.24 12.49 7.25 o 2 1 1 7368.88 7940.89 80.74 o 3 1 1 20701.84 22337.38 203.22 o 4 1 1 5799.07 5998.11 73.26 o 5 1 1 14365.73 14500.90 142.77 o 6 1 1 570.83 560.29 40.23 o 7 1 1 568.18 616.10 59.30 o 8 1 1 3212.89 3070.86 76.08 o 9 1 1 19.55 -10.14 41.23 o 10 1 1 7076.33 6675.36 140.58 o 11 1 1 1455.34 1468.05 100.35 o 12 1 1 103.30 87.28 67.39 o 13 1 1 2351.90 2293.62 113.01 o 14 1 1 84.86 55.22 71.43 o 15 1 1 350.60 361.88 127.73 o 16 1 1 827.45 978.36 118.95 o 17 1 1 10.13 -84.25 84.25 o 18 1 1 134.51 94.48 105.23 o 19 1 1 87.82 140.54 111.50 o 1 2 1 1922.01 1877.36 39.21 o 2 2 1 28126.17 27664.88 280.34 o 3 2 1 2238.96 2341.73 48.63 o 4 2 1 4211.01 4191.13 68.17 o 5 2 1 1307.04 1289.04 42.56 o 6 2 1 13644.46 13388.81 160.10 o 7 2 1 1330.95 1187.73 48.71 o 8 2 1 3376.08 3343.87 78.22 o 9 2 1 172.70 208.37 40.20 o 10 2 1 1935.28 1988.84 73.44 o 11 2 1 203.26 160.86 57.81 o 12 2 1 987.03 1070.31 90.19 o 13 2 1 14.46 2.52 58.53 o 14 2 1 14.87 -27.93 62.60 o 15 2 1 273.72 223.70 81.46 o 16 2 1 176.13 117.88 82.99 o 17 2 1 69.09 -60.98 90.39 o 18 2 1 28.16 77.05 105.73 o 0 3 1 39093.45 41636.36 715.34 o 1 3 1 84962.67 87705.84 915.55 o 2 3 1 1126.80 1095.17 37.07 o 3 3 1 18511.25 18781.75 194.55 o 4 3 1 3730.20 3611.33 56.46 o 5 3 1 17589.39 17576.38 194.14 o 6 3 1 1588.45 1465.90 51.22 o 7 3 1 5457.45 5889.42 100.80 o 8 3 1 7298.24 7204.30 117.53 o 9 3 1 2106.04 2396.28 129.06 o 10 3 1 7602.54 7642.01 133.46 o 11 3 1 2602.63 2624.17 130.66 o 12 3 1 116.73 75.49 61.40 o 13 3 1 2339.38 2081.79 103.43 o 14 3 1 101.06 132.13 66.38 o 15 3 1 33.31 -20.01 69.93 o 16 3 1 911.56 824.38 95.61 o 17 3 1 112.28 -103.37 103.37 o 18 3 1 417.10 476.68 136.99 o 1 4 1 1445.48 1407.57 64.20 o 2 4 1 16522.98 15695.60 185.12 o 3 4 1 1573.93 1597.61 46.17 o 4 4 1 2651.35 2683.07 52.91 o 5 4 1 1521.00 1505.63 66.40 o 6 4 1 8897.76 8440.12 123.22 o 7 4 1 962.11 922.41 49.99 o 8 4 1 2260.42 2096.27 70.67 o 9 4 1 367.73 492.34 52.48 o 10 4 1 1386.71 1321.99 99.49 o 11 4 1 238.97 272.97 65.68 o 12 4 1 840.09 802.39 78.80 o 13 4 1 8.40 -59.67 59.67 o 14 4 1 32.79 0.19 66.13 o 15 4 1 197.63 228.47 77.53 o 16 4 1 129.61 121.34 79.25 o 17 4 1 84.49 25.26 91.38 o 18 4 1 52.20 16.70 109.04 o 0 5 1 55.76 46.84 52.71 o 1 5 1 238.18 190.40 43.72 o 2 5 1 4261.59 4252.59 92.78 o 3 5 1 11353.34 11436.58 155.32 o 4 5 1 2117.64 2150.98 59.45 o 5 5 1 6842.69 6756.70 96.51 o 6 5 1 118.76 130.26 36.91 o 7 5 1 585.07 625.51 51.32 o 8 5 1 2133.28 2083.25 73.17 o 9 5 1 13.85 -34.40 52.40 o 10 5 1 3511.13 3560.57 137.77 o 11 5 1 1060.08 1108.62 84.03 o 12 5 1 26.93 41.36 59.70 o 13 5 1 1542.27 1562.35 101.16 o 14 5 1 33.58 16.95 69.49 o 15 5 1 278.79 254.95 90.27 o 16 5 1 552.64 713.09 107.50 o 17 5 1 27.26 -16.47 90.14 o 1 6 1 515.94 530.73 64.75 o 2 6 1 7511.84 7127.03 133.49 o 3 6 1 717.48 722.51 58.02 o 4 6 1 1721.46 1761.52 61.19 o 5 6 1 3373.78 3156.76 70.27 o 6 6 1 2817.27 2773.65 67.95 o 7 6 1 1671.42 1797.50 70.01 o 8 6 1 1026.22 1066.21 73.37 o 9 6 1 1046.07 1123.81 77.88 o 10 6 1 2215.46 2308.25 100.27 o 11 6 1 214.42 201.99 62.75 o 12 6 1 443.36 336.32 70.81 o 13 6 1 1655.55 1653.78 107.31 o 14 6 1 28.73 157.90 84.84 o 15 6 1 469.98 388.51 125.90 o 16 6 1 131.70 139.52 93.15 o 17 6 1 32.70 149.14 116.26 o 0 7 1 682.74 443.42 86.89 o 1 7 1 87.84 94.37 56.86 o 2 7 1 2598.02 2725.03 91.13 o 3 7 1 6188.83 5876.03 117.50 o 4 7 1 1375.19 1267.84 61.05 o 5 7 1 4391.63 4566.12 90.24 o 6 7 1 54.31 72.65 44.26 o 7 7 1 161.15 153.25 61.36 o 8 7 1 1138.31 1260.27 81.33 o 9 7 1 12.79 -53.38 53.38 o 10 7 1 2209.01 2428.49 135.23 o 11 7 1 754.75 797.42 80.11 o 12 7 1 11.57 -11.52 74.11 o 13 7 1 1098.89 1043.47 111.40 o 14 7 1 3.44 -69.08 82.93 o 15 7 1 196.45 71.07 172.38 o 16 7 1 326.72 244.46 142.72 o 1 8 1 373.78 312.36 65.43 o 2 8 1 4503.29 4377.09 134.40 o 3 8 1 347.18 398.46 56.57 o 4 8 1 412.26 489.30 55.60 o 5 8 1 526.56 627.06 52.45 o 6 8 1 2199.68 2178.86 103.55 o 7 8 1 350.16 354.82 64.36 o 8 8 1 629.40 704.03 73.02 o 9 8 1 6.45 22.23 62.03 o 10 8 1 584.67 708.14 135.00 o 11 8 1 24.50 136.30 80.32 o 12 8 1 208.53 131.89 88.42 o 13 8 1 3.50 -53.82 96.81 o 14 8 1 3.82 18.87 103.43 o 15 8 1 87.05 143.41 117.21 o 0 9 1 1513.95 1366.33 195.64 o 1 9 1 5957.82 5770.81 201.43 o 2 9 1 221.90 155.15 59.28 o 3 9 1 2261.01 2402.63 86.88 o 4 9 1 539.33 658.44 55.49 o 5 9 1 4041.23 4387.69 112.01 o 6 9 1 25.97 17.57 55.80 o 7 9 1 1477.50 1481.18 91.40 o 8 9 1 1723.77 2013.16 166.51 o 9 9 1 883.32 762.14 95.82 o 10 9 1 1558.01 1616.26 119.64 o 11 9 1 979.69 889.05 117.95 o 12 9 1 5.58 51.73 101.73 o 13 9 1 718.59 487.57 123.09 o 14 9 1 0.76 -110.23 110.23 o 1 10 1 222.42 151.14 71.64 o 2 10 1 1861.80 1958.89 92.56 o 3 10 1 194.36 185.78 56.93 o 4 10 1 134.74 160.37 61.61 o 5 10 1 211.84 194.29 65.44 o 6 10 1 984.00 1054.10 99.40 o 7 10 1 239.63 243.91 82.15 o 8 10 1 199.06 148.53 83.41 o 9 10 1 16.01 37.62 93.46 o 10 10 1 119.95 113.89 137.85 o 11 10 1 113.99 -31.27 98.88 o 12 10 1 160.77 155.34 114.07 o 0 11 1 252.83 526.50 125.70 o 1 11 1 20.15 15.20 78.26 o 2 11 1 456.24 744.02 97.00 o 3 11 1 1218.66 1309.86 86.07 o 4 11 1 225.91 152.41 78.40 o 5 11 1 1367.12 1548.08 114.96 o 6 11 1 44.19 23.86 77.37 o 7 11 1 200.94 74.02 97.14 o 8 11 1 384.71 380.80 123.88 o 9 11 1 29.47 -32.08 104.14 o 10 11 1 407.68 243.66 113.55 o 11 11 1 283.59 337.17 126.62 o 1 12 1 43.96 155.84 80.79 o 2 12 1 505.65 630.28 95.27 o 3 12 1 32.39 125.50 93.04 o 4 12 1 84.58 95.41 85.63 o 5 12 1 398.92 611.02 117.30 o 6 12 1 182.27 -36.26 103.30 o 7 12 1 191.90 221.29 112.31 o 8 12 1 61.92 64.68 118.46 o 9 12 1 71.36 118.22 121.34 o 0 13 1 441.13 668.55 168.39 o 1 13 1 171.67 301.76 167.59 o 2 13 1 456.40 514.39 139.50 o 3 13 1 827.16 697.07 153.03 o 4 13 1 161.31 82.64 135.25 o 5 13 1 583.27 778.59 158.52 o 0 0 2 7564.78 7753.60 148.99 o 1 0 2 36928.48 38580.79 494.44 o 2 0 2 9722.53 9942.46 122.52 o 3 0 2 14852.91 15058.53 216.21 o 4 0 2 3210.17 3107.23 78.69 o 5 0 2 44967.54 48096.95 596.43 o 6 0 2 6674.95 6839.08 133.43 o 7 0 2 215.25 278.16 46.68 o 8 0 2 442.31 532.70 56.11 o 9 0 2 901.36 1036.48 80.23 o 10 0 2 3699.41 3587.90 198.81 o 11 0 2 5786.13 6003.33 194.56 o 12 0 2 517.67 442.59 96.43 o 13 0 2 3214.51 3566.41 170.49 o 14 0 2 476.34 334.88 152.36 o 15 0 2 275.93 192.89 257.89 o 16 0 2 569.02 686.16 254.24 o 17 0 2 12.49 -119.01 119.01 o 18 0 2 57.98 9.36 139.49 o 19 0 2 175.44 -145.45 145.45 o 1 1 2 3173.13 3127.60 41.69 o 2 1 2 13010.83 13215.12 124.09 o 3 1 2 3892.18 3846.88 49.12 o 4 1 2 3858.63 3927.22 52.18 o 5 1 2 4946.19 4800.38 68.80 o 6 1 2 5963.83 5792.08 80.86 o 7 1 2 6756.99 6935.21 95.74 o 8 1 2 4993.01 4980.34 98.20 o 9 1 2 226.46 229.68 40.04 o 10 1 2 142.45 196.58 53.04 o 11 1 2 36.08 35.27 51.23 o 12 1 2 888.41 923.16 89.12 o 13 1 2 3083.20 3020.75 124.81 o 14 1 2 529.25 506.71 82.09 o 15 1 2 1666.55 1622.06 110.53 o 16 1 2 143.33 59.77 93.08 o 17 1 2 57.76 91.81 98.99 o 18 1 2 69.61 76.16 101.98 o 0 2 2 2445.39 2401.23 48.07 o 1 2 2 12.12 -4.71 16.13 o 2 2 2 812.77 848.39 26.46 o 3 2 2 17641.40 18006.61 173.22 o 4 2 2 6938.32 6690.97 98.92 o 5 2 2 20091.60 19696.41 210.76 o 6 2 2 466.00 396.14 33.00 o 7 2 2 1001.96 1136.68 49.91 o 8 2 2 8.80 8.33 37.43 o 9 2 2 65.93 89.06 41.00 o 10 2 2 4630.14 4675.62 107.39 o 11 2 2 4200.13 4204.48 119.12 o 12 2 2 14.29 -5.33 49.29 o 13 2 2 3528.09 3540.24 132.12 o 14 2 2 397.98 396.33 80.76 o 15 2 2 217.16 98.55 76.55 o 16 2 2 187.24 147.46 84.02 o 17 2 2 87.89 20.11 84.41 o 18 2 2 93.40 133.44 151.77 o 1 3 2 4692.01 4589.71 72.18 o 2 3 2 5746.64 5707.22 84.46 o 3 3 2 59.91 70.39 22.96 o 4 3 2 3444.37 3559.10 65.78 o 5 3 2 6840.69 6760.41 100.68 o 6 3 2 5386.31 5493.21 94.33 o 7 3 2 4909.38 4905.70 93.70 o 8 3 2 4762.94 4600.91 96.40 o 9 3 2 77.63 -22.91 48.22 o 10 3 2 852.37 940.40 61.66 o 11 3 2 3702.10 3544.67 99.92 o 12 3 2 755.08 898.35 79.01 o 13 3 2 150.50 208.23 86.34 o 14 3 2 31.53 103.03 67.97 o 15 3 2 1202.39 1056.70 105.12 o 16 3 2 125.36 59.69 81.02 o 17 3 2 12.23 -91.81 91.81 o 18 3 2 25.19 62.96 145.40 o 0 4 2 1207.13 1215.53 117.63 o 1 4 2 15.96 -21.92 22.62 o 2 4 2 804.77 830.28 38.13 o 3 4 2 11203.20 10722.13 153.20 o 4 4 2 4222.88 4071.11 75.75 o 5 4 2 16183.40 15823.25 184.89 o 6 4 2 375.06 377.63 38.23 o 7 4 2 1351.81 1505.70 58.85 o 8 4 2 43.57 94.26 41.82 o 9 4 2 58.57 58.83 43.70 o 10 4 2 3428.90 3389.87 99.09 o 11 4 2 3127.27 3369.97 133.93 o 12 4 2 11.49 25.75 60.15 o 13 4 2 2750.43 2747.85 114.64 o 14 4 2 266.49 160.94 87.34 o 15 4 2 180.61 122.39 82.22 o 16 4 2 159.09 95.00 81.49 o 17 4 2 112.28 246.93 108.48 o 18 4 2 68.15 215.06 116.97 o 1 5 2 1720.80 1640.63 58.44 o 2 5 2 5014.76 5123.09 94.91 o 3 5 2 1487.79 1453.22 57.98 o 4 5 2 1578.50 1595.78 54.50 o 5 5 2 2481.12 2496.20 57.27 o 6 5 2 2183.83 2234.95 67.89 o 7 5 2 4123.15 4252.16 94.29 o 8 5 2 2430.53 2594.76 98.92 o 9 5 2 112.41 164.40 50.95 o 10 5 2 30.93 -11.17 56.09 o 11 5 2 20.26 -32.48 56.21 o 12 5 2 395.08 371.16 73.69 o 13 5 2 1939.58 1709.96 115.11 o 14 5 2 351.56 244.37 82.32 o 15 5 2 1005.82 869.25 114.23 o 16 5 2 99.11 23.46 89.14 o 17 5 2 79.18 97.20 98.67 o 0 6 2 653.08 913.53 131.81 o 1 6 2 7744.14 8292.86 142.37 o 2 6 2 2764.54 2939.86 77.51 o 3 6 2 8526.88 8263.44 143.75 o 4 6 2 1367.42 1446.74 57.75 o 5 6 2 12284.87 11702.31 146.34 o 6 6 2 1893.54 1964.09 58.60 o 7 6 2 1.34 104.78 44.36 o 8 6 2 128.05 240.26 52.93 o 9 6 2 246.08 226.56 80.68 o 10 6 2 1170.38 1293.55 101.16 o 11 6 2 2930.23 3011.41 120.54 o 12 6 2 259.61 370.39 82.86 o 13 6 2 1755.38 1702.26 118.63 o 14 6 2 176.46 168.67 88.49 o 15 6 2 197.83 175.09 87.21 o 16 6 2 285.35 336.16 102.90 o 17 6 2 17.73 -75.61 94.42 o 1 7 2 909.20 977.45 63.66 o 2 7 2 2788.60 2695.67 81.96 o 3 7 2 994.26 1011.85 65.70 o 4 7 2 694.59 665.07 52.54 o 5 7 2 1524.95 1579.18 70.44 o 6 7 2 1277.04 1307.37 66.60 o 7 7 2 2244.10 2304.98 81.79 o 8 7 2 1053.95 1143.79 82.75 o 9 7 2 19.96 54.86 57.08 o 10 7 2 38.42 83.91 70.67 o 11 7 2 23.71 102.43 73.92 o 12 7 2 178.52 207.24 76.57 o 13 7 2 1430.31 1420.45 119.14 o 14 7 2 171.89 166.29 92.68 o 15 7 2 840.43 903.60 116.34 o 16 7 2 46.43 14.74 107.54 o 0 8 2 145.52 167.83 89.68 o 1 8 2 71.09 47.05 52.29 o 2 8 2 323.13 392.62 55.60 o 3 8 2 4732.81 4677.15 113.98 o 4 8 2 1000.15 973.01 63.77 o 5 8 2 5399.87 5601.09 119.53 o 6 8 2 86.39 140.39 50.32 o 7 8 2 278.66 145.49 58.01 o 8 8 2 22.66 90.47 67.51 o 9 8 2 178.64 117.98 71.46 o 10 8 2 911.14 943.66 99.22 o 11 8 2 1515.18 1591.20 118.32 o 12 8 2 0.44 8.42 80.02 o 13 8 2 1314.15 1279.51 119.47 o 14 8 2 58.79 144.69 96.09 o 15 8 2 147.08 112.99 115.42 o 1 9 2 706.46 850.78 83.95 o 2 9 2 834.95 888.73 69.16 o 3 9 2 76.03 50.79 52.62 o 4 9 2 381.87 459.01 58.01 o 5 9 2 1367.12 1427.97 75.44 o 6 9 2 686.31 602.15 81.28 o 7 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