Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 2231153
Preview
| Coordinates | 2231153.cif |
|---|---|
| Structure factors | 2231153.hkl |
| Original IUCr paper | HTML |
| Chemical name | Bis[μ~2~-bis(diphenylphosphanyl)methane-κ^2^<i>P</i>:<i>P</i>']bis(μ~4~- diphenylphosphinato-κ^4^<i>O</i>:<i>O</i>:<i>O</i>':<i>O</i>')bis[μ~2~- trifluoromethanesulfonato(0.546/0.454)]- κ^2^<i>O</i>:<i>O</i>';κ^2^<i>O</i>:<i>O</i>-tetrasilver(I) acetonitrile disolvate |
|---|---|
| Formula | C80 H70 Ag4 F6 N2 O10 P6 S2 |
| Calculated formula | C80 H70 Ag4 F6 N2 O10 P6 S2 |
| Title of publication | Bis[μ~2~-bis(diphenylphosphanyl)methane-κ^2^<i>P</i>:<i>P</i>']bis(μ~4~-diphenylphosphinato-κ^4^<i>O</i>:<i>O</i>:<i>O</i>':<i>O</i>')bis[μ~2~-trifluoromethanesulfonato(0.546/0.454)]-κ^2^<i>O</i>:<i>O</i>';κ^2^<i>O</i>:<i>O</i>-tetrasilver(I) acetonitrile disolvate |
| Authors of publication | Tang, Li-ping; Jia, Chen; Huang, Li-li; Xie, Jia-Li |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2011 |
| Journal volume | 67 |
| Journal issue | 8 |
| Pages of publication | m1141 - m1142 |
| a | 11.73 ± 0.007 Å |
| b | 15.169 ± 0.009 Å |
| c | 23.688 ± 0.012 Å |
| α | 90° |
| β | 96.967 ± 0.007° |
| γ | 90° |
| Cell volume | 4184 ± 4 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 8 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0706 |
| Residual factor for significantly intense reflections | 0.055 |
| Weighted residual factors for significantly intense reflections | 0.1335 |
| Weighted residual factors for all reflections included in the refinement | 0.1443 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.011 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181233 (current) | 2016-04-03 | hkl/2/23/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23/11. |
2231153.cif 2231153.hkl |
| 176798 | 2016-02-21 | cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23. |
2231153.cif 2231153.hkl |
| 120072 | 2014-07-11 | Adding DOIs to range 2 structures. | 2231153.cif 2231153.hkl |
| 88064 | 2013-08-29 | Adding _cod_database_fobs_code data item to all COD CIFs that have Fobs deposited and did not have this data item yet. | 2231153.cif 2231153.hkl |
| 27511 | 2011-10-06 | hkl/ Committing assigned Fobs data for the recently deposited coordinates from IUCr journals. |
2231153.cif 2231153.hkl |
| 27061 | 2011-09-29 | ../uploads/cif-deposit/cod/cif Adding structures of 2231153 via cif-deposit CGI script. |
2231153.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.