#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:25:10 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181233 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/11/2231171.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231171_Fobs loop_ _publ_author_name 'Todorov, Petar' 'Calmes, Monique' 'Shivachev, Boris L.' 'Nikolova, Rosica P.' _publ_section_title ; (R)-Methyl {[(2-carboxybicyclo[2.2.2]octan-1-yl)ammonio]methyl}phosphonate dichloromethane 0.25-solvate ; _journal_coeditor_code IS2751 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2152 _journal_page_last o2153 _journal_volume 67 _journal_year 2011 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.3520 _cell_length_b 12.7553 _cell_length_c 24.1148 _exptl_crystal_F_000 1249.00 _reflns_d_resolution_high 0.8680 _cod_data_source_file is2751Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title exp1 _shelx_refln_list_code 4 _shelx_f_calc_maximum 323.63 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 104734.89 118061.63 409.25 o 4 0 0 532.99 394.51 21.75 o 6 0 0 37.75 49.06 13.47 o 8 0 0 805.78 777.21 109.01 o 10 0 0 99.04 102.64 41.26 o 1 1 0 533.61 472.67 22.56 o 2 1 0 6935.60 7517.73 133.23 o 3 1 0 173.72 127.52 8.56 o 4 1 0 19.76 43.24 5.70 o 5 1 0 2883.26 3036.20 137.08 o 6 1 0 859.49 774.82 39.38 o 7 1 0 2.23 0.22 11.63 o 8 1 0 1270.50 1412.05 128.44 o 9 1 0 44.72 73.08 15.26 o 10 1 0 616.55 588.02 257.71 o 0 2 0 29634.45 32132.32 198.59 o 1 2 0 35674.11 35191.03 234.52 o 2 2 0 15668.75 15760.58 416.96 o 3 2 0 40.81 63.70 7.74 o 4 2 0 1834.86 1633.34 43.45 o 5 2 0 40.15 53.56 11.30 o 6 2 0 1140.94 1034.11 51.07 o 7 2 0 119.62 103.72 12.79 o 8 2 0 55.28 43.53 10.91 o 9 2 0 184.59 140.56 23.84 o 10 2 0 30.01 -5.07 18.60 o 1 3 0 5415.43 5699.75 76.85 o 2 3 0 3694.70 4415.90 173.98 o 3 3 0 3641.82 4000.63 161.24 o 4 3 0 269.68 249.44 14.09 o 5 3 0 255.17 255.67 15.23 o 6 3 0 929.40 1053.77 52.59 o 7 3 0 272.54 322.40 28.16 o 8 3 0 2330.84 2509.67 137.97 o 9 3 0 95.58 193.92 41.24 o 10 3 0 443.99 309.83 51.76 o 0 4 0 16600.60 16666.13 283.03 o 1 4 0 3277.71 3128.17 125.46 o 2 4 0 4722.08 3897.32 179.17 o 3 4 0 369.87 361.24 32.35 o 4 4 0 1118.55 890.67 24.94 o 5 4 0 52.39 39.23 7.67 o 6 4 0 376.16 385.79 19.70 o 7 4 0 1746.16 1778.81 101.26 o 8 4 0 65.22 58.93 18.85 o 9 4 0 6.68 24.32 16.37 o 10 4 0 20.27 44.37 61.28 o 1 5 0 225.23 407.50 27.09 o 2 5 0 3065.13 2888.15 228.34 o 3 5 0 1620.79 1523.37 33.42 o 4 5 0 48.05 89.28 15.79 o 5 5 0 287.30 320.68 16.07 o 6 5 0 1222.94 1112.28 41.41 o 7 5 0 156.50 238.95 33.28 o 8 5 0 484.91 401.56 58.47 o 9 5 0 158.87 124.93 33.80 o 10 5 0 19.87 -62.36 62.36 o 0 6 0 4765.84 4659.65 247.29 o 1 6 0 2102.85 2298.11 45.59 o 2 6 0 1091.51 1148.99 46.39 o 3 6 0 2893.12 3429.41 63.27 o 4 6 0 906.84 1096.05 36.19 o 5 6 0 2265.55 2536.87 163.53 o 6 6 0 185.88 178.44 20.38 o 7 6 0 143.04 91.18 43.04 o 8 6 0 24.47 -25.99 25.99 o 9 6 0 18.37 12.62 16.00 o 1 7 0 306.18 320.42 18.69 o 2 7 0 1867.18 1560.76 42.32 o 3 7 0 17.26 23.54 11.64 o 4 7 0 1902.07 1911.52 207.68 o 5 7 0 1454.04 1583.83 83.81 o 6 7 0 847.90 785.70 130.98 o 7 7 0 38.25 0.71 31.65 o 8 7 0 41.52 45.42 24.64 o 9 7 0 18.53 4.27 13.80 o 0 8 0 1.57 20.33 11.80 o 1 8 0 5712.04 5455.89 108.92 o 2 8 0 18.92 61.55 11.69 o 3 8 0 3293.76 3708.17 113.57 o 4 8 0 75.20 68.10 28.26 o 5 8 0 489.35 1078.33 153.36 o 6 8 0 4.51 -15.75 22.61 o 7 8 0 13.46 26.82 28.61 o 8 8 0 5.13 9.96 23.41 o 9 8 0 19.01 -31.57 40.44 o 1 9 0 118.76 86.16 12.60 o 2 9 0 74.26 74.38 13.57 o 3 9 0 4.50 15.92 14.14 o 4 9 0 89.16 148.38 33.18 o 5 9 0 120.79 88.38 23.52 o 6 9 0 27.32 -10.97 15.07 o 7 9 0 209.27 144.22 32.63 o 8 9 0 24.64 -1.37 16.70 o 0 10 0 280.12 282.98 34.35 o 1 10 0 28.22 164.67 36.52 o 2 10 0 301.03 296.52 32.39 o 3 10 0 2.34 66.33 34.12 o 4 10 0 129.14 116.97 50.66 o 5 10 0 0.41 4.69 18.75 o 6 10 0 17.80 -5.60 16.44 o 7 10 0 8.71 -20.52 20.52 o 1 11 0 48.14 36.06 10.16 o 2 11 0 558.68 654.77 52.19 o 3 11 0 0.43 26.04 23.14 o 4 11 0 27.65 23.94 16.69 o 5 11 0 349.54 354.97 51.27 o 6 11 0 19.95 13.68 16.85 o 7 11 0 219.92 153.50 28.13 o 0 12 0 73.09 75.80 27.40 o 1 12 0 74.81 100.69 17.26 o 2 12 0 56.19 96.99 24.80 o 3 12 0 151.68 109.65 19.70 o 4 12 0 46.07 68.57 16.29 o 5 12 0 48.12 28.77 14.42 o 6 12 0 96.04 35.80 23.69 o 1 13 0 19.73 16.95 10.64 o 2 13 0 31.25 13.22 13.45 o 3 13 0 9.38 18.86 15.04 o 4 13 0 19.88 28.25 13.76 o 0 14 0 0.52 141.16 67.80 o 1 14 0 2.28 -5.46 14.83 o 2 14 0 1.51 -0.59 12.73 o 3 14 0 2.20 -13.10 24.45 o 1 0 1 423.22 353.43 10.97 o 2 0 1 33910.24 36232.59 383.65 o 3 0 1 2053.43 2335.83 33.10 o 4 0 1 3163.88 3068.53 45.13 o 5 0 1 929.28 1005.35 54.39 o 6 0 1 109.88 121.33 16.16 o 7 0 1 32.61 37.38 11.87 o 8 0 1 10.66 2.55 25.71 o 9 0 1 22.65 40.27 12.44 o 10 0 1 65.42 59.05 14.98 o -10 1 1 12.95 75.42 18.65 o -9 1 1 190.26 153.94 31.24 o -8 1 1 166.08 286.24 26.36 o -7 1 1 390.56 334.50 23.40 o -6 1 1 78.90 178.72 16.61 o -5 1 1 376.74 389.34 32.02 o -4 1 1 1359.09 1120.40 27.69 o -3 1 1 3635.16 3602.86 70.34 o -2 1 1 2246.53 2213.19 52.14 o -1 1 1 3075.01 2678.82 96.89 o 0 1 1 451.54 535.76 16.45 o 1 1 1 3185.09 2914.76 59.89 o 2 1 1 2330.68 2254.71 49.47 o 3 1 1 3712.42 3660.66 50.87 o 4 1 1 1398.88 1179.98 31.27 o 5 1 1 395.58 436.56 41.12 o 6 1 1 66.59 154.59 19.41 o 7 1 1 353.21 318.75 25.98 o 8 1 1 170.94 313.01 28.29 o 9 1 1 191.22 178.07 19.54 o 10 1 1 12.55 36.33 14.58 o -10 2 1 10.49 36.32 25.82 o -9 2 1 14.28 28.60 20.49 o -8 2 1 359.54 407.23 37.10 o -7 2 1 285.21 351.46 24.76 o -6 2 1 505.63 647.71 42.27 o -5 2 1 203.35 168.39 12.32 o -4 2 1 2211.15 2144.32 58.50 o -3 2 1 1396.04 1289.30 37.92 o -2 2 1 960.26 805.47 49.71 o -1 2 1 4963.64 5745.69 159.47 o 0 2 1 580.64 1012.76 75.41 o 1 2 1 4991.29 5973.30 142.14 o 2 2 1 979.27 807.70 43.25 o 3 2 1 1445.22 1296.45 30.70 o 4 2 1 2189.16 1928.34 55.52 o 5 2 1 197.96 240.62 23.48 o 6 2 1 468.76 531.21 57.17 o 7 2 1 292.70 355.32 69.31 o 8 2 1 335.35 415.95 30.26 o 9 2 1 17.13 54.84 12.51 o 10 2 1 8.83 -3.26 32.62 o -10 3 1 38.32 143.29 32.33 o -9 3 1 51.09 71.09 24.35 o -8 3 1 11.16 116.54 35.03 o -7 3 1 765.91 897.76 43.59 o -6 3 1 183.56 154.67 12.95 o -5 3 1 705.10 863.53 27.98 o -4 3 1 883.52 870.27 54.60 o -3 3 1 770.88 840.56 34.49 o -2 3 1 2541.60 2769.12 141.54 o -1 3 1 4099.68 4631.03 139.17 o 0 3 1 12.69 80.90 9.17 o 1 3 1 3918.35 4326.21 86.94 o 2 3 1 2620.19 2851.80 113.50 o 3 3 1 713.03 787.73 41.23 o 4 3 1 802.23 830.66 26.52 o 5 3 1 651.81 828.25 39.77 o 6 3 1 200.84 203.45 25.42 o 7 3 1 760.76 811.96 41.18 o 8 3 1 6.98 70.09 18.21 o 9 3 1 55.26 94.69 22.82 o 10 3 1 35.71 55.07 49.52 o -10 4 1 18.03 101.26 70.10 o -9 4 1 208.59 167.40 41.77 o -8 4 1 111.17 103.00 22.87 o -7 4 1 968.11 1004.15 49.14 o -6 4 1 515.06 548.88 23.72 o -5 4 1 196.46 190.59 12.97 o -4 4 1 203.51 288.15 18.26 o -3 4 1 1354.16 1103.46 78.38 o -2 4 1 805.26 1054.59 63.81 o -1 4 1 883.91 1085.67 62.58 o 0 4 1 4545.86 4492.30 128.17 o 1 4 1 942.75 1237.24 92.94 o 2 4 1 836.53 1052.03 48.51 o 3 4 1 1290.93 1110.99 53.16 o 4 4 1 173.81 182.71 11.47 o 5 4 1 190.84 171.53 10.98 o 6 4 1 519.71 593.41 33.53 o 7 4 1 951.72 1025.37 51.62 o 8 4 1 109.81 141.76 40.34 o 9 4 1 208.37 262.97 48.48 o 10 4 1 16.71 48.93 47.18 o -9 5 1 0.71 26.15 22.17 o -8 5 1 9.21 7.37 19.73 o -7 5 1 141.89 138.25 38.60 o -6 5 1 85.89 144.92 25.68 o -5 5 1 170.28 157.14 12.99 o -4 5 1 1263.19 1528.24 32.71 o -3 5 1 1196.32 1384.26 31.95 o -2 5 1 2265.32 2276.04 196.48 o -1 5 1 4072.49 3700.21 170.81 o 0 5 1 4463.30 4677.11 248.60 o 1 5 1 4224.49 4113.23 288.25 o 2 5 1 2266.06 2661.52 194.51 o 3 5 1 1186.74 1215.15 55.17 o 4 5 1 1208.12 1314.42 35.92 o 5 5 1 147.51 129.19 13.18 o 6 5 1 103.31 241.57 34.20 o 7 5 1 153.66 197.94 49.76 o 8 5 1 11.92 48.83 30.60 o 9 5 1 0.03 -27.20 27.20 o 10 5 1 2.26 -64.81 64.81 o -9 6 1 0.27 15.09 18.30 o -8 6 1 31.59 2.81 38.54 o -7 6 1 308.66 297.14 58.43 o -6 6 1 98.55 150.85 23.88 o -5 6 1 953.13 1023.84 66.16 o -4 6 1 98.17 115.18 13.78 o -3 6 1 2965.58 3126.50 53.63 o -2 6 1 974.87 1071.25 45.13 o -1 6 1 2850.47 2836.45 76.40 o 0 6 1 1957.41 2129.78 68.28 o 1 6 1 3027.78 3023.01 86.90 o 2 6 1 951.62 932.67 35.36 o 3 6 1 3014.14 3060.18 76.34 o 4 6 1 93.69 109.77 17.00 o 5 6 1 945.04 983.74 78.68 o 6 6 1 106.64 167.57 37.10 o 7 6 1 299.69 165.73 30.69 o 8 6 1 30.66 -5.40 19.49 o 9 6 1 0.47 -9.02 20.23 o -9 7 1 68.34 9.64 39.18 o -8 7 1 38.81 27.86 25.61 o -7 7 1 134.88 107.59 42.57 o -6 7 1 722.39 710.05 123.22 o -5 7 1 263.85 259.70 30.71 o -4 7 1 106.61 142.00 17.73 o -3 7 1 166.24 223.80 16.38 o -2 7 1 76.62 135.81 13.84 o -1 7 1 119.37 132.34 11.70 o 0 7 1 1588.74 1449.73 68.67 o 1 7 1 133.27 139.22 12.27 o 2 7 1 86.91 115.53 14.27 o 3 7 1 183.93 197.14 22.48 o 4 7 1 97.35 147.25 37.97 o 5 7 1 270.96 307.12 34.53 o 6 7 1 704.84 690.65 67.90 o 7 7 1 122.36 41.18 44.50 o 8 7 1 33.99 35.47 24.46 o 9 7 1 73.07 71.08 27.50 o -9 8 1 14.85 11.04 33.94 o -8 8 1 3.09 3.37 19.67 o -7 8 1 190.93 178.11 37.96 o -6 8 1 133.08 107.75 29.52 o -5 8 1 1105.17 1706.21 91.48 o -4 8 1 251.13 261.54 44.11 o -3 8 1 671.84 685.03 111.91 o -2 8 1 310.94 327.88 22.30 o -1 8 1 631.98 781.78 36.29 o 0 8 1 644.95 669.02 30.08 o 1 8 1 613.94 691.31 34.34 o 2 8 1 313.96 286.03 20.17 o 3 8 1 687.72 979.14 98.59 o 4 8 1 238.75 211.58 37.48 o 5 8 1 1052.22 1258.77 83.97 o 6 8 1 131.65 101.36 23.83 o 7 8 1 174.27 151.11 37.29 o 8 8 1 3.64 15.00 15.78 o 9 8 1 14.32 10.80 37.01 o -8 9 1 12.59 3.55 17.16 o -7 9 1 10.81 13.19 16.55 o -6 9 1 65.32 57.58 17.68 o -5 9 1 47.90 30.96 21.09 o -4 9 1 319.61 344.84 73.67 o -3 9 1 101.24 85.64 17.65 o -2 9 1 146.43 150.88 17.09 o -1 9 1 18.02 18.45 8.36 o 0 9 1 272.51 260.55 21.05 o 1 9 1 20.01 14.21 7.57 o 2 9 1 141.59 180.75 18.42 o 3 9 1 90.89 98.46 20.77 o 4 9 1 306.56 304.10 33.16 o 5 9 1 41.67 31.95 12.65 o 6 9 1 62.11 11.75 14.76 o 7 9 1 10.31 15.82 22.68 o 8 9 1 12.83 7.50 18.44 o -7 10 1 1.30 -12.44 22.53 o -6 10 1 128.64 60.89 16.84 o -5 10 1 20.57 60.99 24.02 o -4 10 1 378.44 363.52 119.05 o -3 10 1 595.30 748.85 60.80 o -2 10 1 104.95 147.46 33.37 o -1 10 1 1239.87 1205.69 48.97 o 0 10 1 57.49 68.67 15.79 o 1 10 1 1252.24 1229.00 49.09 o 2 10 1 105.68 136.82 28.27 o 3 10 1 561.27 756.36 60.77 o 4 10 1 388.49 395.09 38.41 o 5 10 1 13.90 27.46 18.43 o 6 10 1 126.71 72.12 18.56 o 7 10 1 1.41 36.31 42.56 o -7 11 1 26.72 51.76 34.14 o -6 11 1 2.32 21.29 14.69 o -5 11 1 86.19 82.78 22.33 o -4 11 1 118.99 104.66 21.58 o -3 11 1 72.22 68.69 28.63 o -2 11 1 184.67 221.03 32.85 o -1 11 1 10.20 43.20 14.84 o 0 11 1 437.37 433.18 31.42 o 1 11 1 9.23 39.95 14.40 o 2 11 1 160.26 210.93 34.08 o 3 11 1 80.11 71.67 20.12 o 4 11 1 118.23 85.50 19.36 o 5 11 1 91.49 119.15 25.42 o 6 11 1 2.92 6.28 11.89 o 7 11 1 23.87 7.14 12.20 o -6 12 1 65.03 39.92 20.33 o -5 12 1 60.54 42.83 14.14 o -4 12 1 2.70 4.60 12.68 o -3 12 1 7.11 21.91 13.20 o -2 12 1 162.21 190.00 27.71 o -1 12 1 8.08 10.79 11.88 o 0 12 1 204.06 200.48 23.28 o 1 12 1 10.66 13.99 11.88 o 2 12 1 170.21 211.17 33.02 o 3 12 1 3.32 9.21 18.14 o 4 12 1 1.42 -10.43 10.43 o 5 12 1 57.88 36.66 14.28 o 6 12 1 63.67 34.17 22.64 o -4 13 1 8.08 -1.58 10.01 o -3 13 1 10.53 17.32 16.78 o -2 13 1 5.41 2.11 12.92 o -1 13 1 19.27 26.27 11.76 o 0 13 1 5.59 14.09 8.76 o 1 13 1 20.35 36.80 15.53 o 2 13 1 4.70 -15.77 15.77 o 3 13 1 8.23 5.50 23.53 o 4 13 1 10.86 -1.91 24.88 o 5 13 1 5.74 -1.75 14.85 o -3 14 1 47.66 9.33 16.16 o -2 14 1 84.06 56.59 15.51 o -1 14 1 83.10 59.11 14.43 o 0 14 1 227.13 263.64 23.08 o 1 14 1 81.38 33.36 14.79 o 2 14 1 87.43 48.24 15.65 o 3 14 1 43.39 19.34 11.76 o 0 0 2 14100.28 16398.39 146.51 o 1 0 2 26.42 24.96 5.06 o 2 0 2 10351.20 10606.09 93.08 o 3 0 2 4507.14 3909.49 42.27 o 4 0 2 927.38 839.49 23.11 o 5 0 2 685.84 726.97 37.10 o 6 0 2 1927.23 1935.19 62.56 o 7 0 2 2745.46 2716.63 125.18 o 8 0 2 102.24 102.20 16.56 o 9 0 2 42.11 44.88 15.84 o 10 0 2 40.06 36.21 13.03 o -10 1 2 447.00 516.52 54.33 o -9 1 2 66.62 77.63 16.03 o -8 1 2 2817.28 2944.08 255.04 o -7 1 2 115.52 148.76 22.62 o -6 1 2 3242.59 3335.90 103.49 o -5 1 2 585.07 543.28 26.59 o -4 1 2 948.24 838.37 29.15 o -3 1 2 359.18 383.46 15.03 o -2 1 2 3417.39 2747.03 41.22 o -1 1 2 1604.12 1423.56 38.60 o 0 1 2 14984.31 12418.74 89.15 o 1 1 2 1738.93 1680.13 37.22 o 2 1 2 3581.87 2903.53 74.42 o 3 1 2 297.54 350.13 16.25 o 4 1 2 811.04 686.87 29.50 o 5 1 2 587.12 640.21 25.17 o 6 1 2 3241.30 3432.17 178.03 o 7 1 2 106.06 172.37 27.52 o 8 1 2 2944.64 3158.75 85.44 o 9 1 2 59.65 124.92 20.69 o 10 1 2 436.64 373.88 31.59 o -10 2 2 76.12 94.22 30.11 o -9 2 2 141.62 152.43 21.79 o -8 2 2 233.07 232.68 29.75 o -7 2 2 1049.83 1172.11 70.36 o -6 2 2 3378.96 3404.19 69.80 o -5 2 2 2697.73 2647.67 59.96 o -4 2 2 3975.94 3540.81 89.92 o -3 2 2 2724.06 2557.03 45.85 o -2 2 2 3662.18 3519.31 96.07 o -1 2 2 1130.12 1153.59 34.78 o 0 2 2 15154.31 14193.85 302.72 o 1 2 2 1302.57 1351.79 60.72 o 2 2 2 3372.26 3514.66 150.13 o 3 2 2 2708.95 2404.42 54.48 o 4 2 2 4105.73 3724.54 140.58 o 5 2 2 2725.09 3034.03 57.67 o 6 2 2 3450.77 3654.45 161.56 o 7 2 2 1018.27 1227.32 98.41 o 8 2 2 233.94 231.93 24.94 o 9 2 2 126.13 144.33 22.08 o 10 2 2 82.32 75.27 25.66 o -10 3 2 240.05 372.15 47.92 o -9 3 2 116.08 176.54 28.86 o -8 3 2 1061.78 1188.73 113.56 o -7 3 2 539.23 548.34 40.64 o -6 3 2 1033.86 1140.46 32.75 o -5 3 2 26.61 43.71 6.66 o -4 3 2 542.93 649.48 31.87 o -3 3 2 1360.42 1365.87 75.71 o -2 3 2 6695.29 6617.09 329.79 o -1 3 2 4985.67 4515.48 167.90 o 0 3 2 292.55 243.03 13.52 o 1 3 2 4993.17 5023.18 312.37 o 2 3 2 6453.44 6347.46 205.95 o 3 3 2 1216.57 1339.16 53.57 o 4 3 2 415.30 489.83 27.77 o 5 3 2 19.72 21.24 7.88 o 6 3 2 1075.26 1244.64 56.97 o 7 3 2 594.52 659.59 49.47 o 8 3 2 1125.42 1276.73 56.25 o 9 3 2 125.54 208.96 28.55 o 10 3 2 235.38 153.39 37.52 o -10 4 2 15.88 59.38 53.89 o -9 4 2 50.87 9.54 22.99 o -8 4 2 323.24 333.79 58.30 o -7 4 2 169.69 206.86 17.54 o -6 4 2 579.88 684.58 27.02 o -5 4 2 780.06 893.56 29.46 o -4 4 2 323.41 326.38 17.86 o -3 4 2 2597.96 2481.52 129.81 o -2 4 2 5323.76 4988.56 364.28 o -1 4 2 2321.35 2023.24 107.21 o 0 4 2 13929.35 14013.79 472.62 o 1 4 2 2236.50 2012.26 118.84 o 2 4 2 4935.28 4749.43 235.90 o 3 4 2 2784.41 2755.55 135.71 o 4 4 2 277.01 285.44 15.01 o 5 4 2 790.98 877.63 31.75 o 6 4 2 611.97 736.69 38.55 o 7 4 2 188.74 261.70 31.60 o 8 4 2 322.53 417.44 68.17 o 9 4 2 48.11 78.16 28.37 o 10 4 2 24.19 0.95 16.22 o -9 5 2 69.20 91.81 37.26 o -8 5 2 612.60 412.09 55.47 o -7 5 2 11.70 16.40 9.96 o -6 5 2 1421.78 1318.41 55.24 o -5 5 2 824.64 891.04 33.95 o -4 5 2 1101.27 1177.66 30.98 o -3 5 2 2605.41 2878.49 38.91 o -2 5 2 701.25 582.39 70.51 o -1 5 2 6097.13 5516.93 133.97 o 0 5 2 2.94 117.80 13.42 o 1 5 2 6189.90 5805.15 357.46 o 2 5 2 723.60 784.39 56.29 o 3 5 2 2507.76 2582.45 73.10 o 4 5 2 1133.75 1140.32 37.53 o 5 5 2 725.55 707.79 24.75 o 6 5 2 1428.01 1497.37 83.02 o 7 5 2 23.30 23.36 14.33 o 8 5 2 617.63 490.41 62.48 o 9 5 2 76.59 46.05 37.31 o 10 5 2 105.60 46.55 65.60 o -9 6 2 49.31 9.55 45.29 o -8 6 2 121.91 126.07 28.81 o -7 6 2 132.06 156.55 19.37 o -6 6 2 2292.84 2252.47 93.01 o -5 6 2 300.57 457.36 49.46 o -4 6 2 1503.34 1690.39 49.16 o -3 6 2 76.69 69.87 12.01 o -2 6 2 330.94 380.84 20.72 o -1 6 2 1050.78 1100.86 32.23 o 0 6 2 19.36 24.97 10.03 o 1 6 2 983.57 985.15 35.94 o 2 6 2 291.08 345.34 21.53 o 3 6 2 47.07 59.90 13.41 o 4 6 2 1577.11 1708.42 62.33 o 5 6 2 364.26 405.83 29.97 o 6 6 2 2292.84 2169.29 118.78 o 7 6 2 136.05 133.04 50.97 o 8 6 2 128.42 128.13 35.74 o 9 6 2 46.56 79.06 32.05 o -9 7 2 58.00 44.88 42.13 o -8 7 2 190.14 149.92 34.17 o -7 7 2 227.81 195.62 40.35 o -6 7 2 201.19 200.04 23.51 o -5 7 2 1212.20 1212.35 75.09 o -4 7 2 415.03 354.47 22.88 o -3 7 2 835.02 813.66 30.40 o -2 7 2 919.83 676.45 28.55 o -1 7 2 77.98 81.20 10.53 o 0 7 2 865.46 864.53 30.75 o 1 7 2 82.21 97.14 11.05 o 2 7 2 1006.82 796.32 29.81 o 3 7 2 830.34 906.96 47.83 o 4 7 2 453.57 459.41 41.32 o 5 7 2 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