#------------------------------------------------------------------------------ #$Date: 2011-10-06 14:27:20 +0300 (Thu, 06 Oct 2011) $ #$Revision: 27511 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/11/2231184.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231184_Fobs loop_ _publ_author_name 'Tigyer, Benjamin R.' 'Zeller, Matthias' 'Zaleski, Curtis M.' _publ_section_title ; Di-\m-acetato-bis(dimethylformamide)pentakis(\m-N,2-dioxidobenzene-1-carboximidato)tetrakis(1-ethylimidazole)pentamanganese(III)manganese(II)--diethyl ether--dimethylforamide--methanol--water (1/1/1/1/0.12) ; _journal_coeditor_code JJ2091 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1041 _journal_page_last m1042 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 103.564 _cell_angle_beta 97.322 _cell_angle_gamma 107.658 _cell_length_a 12.6043 _cell_length_b 17.1875 _cell_length_c 20.9900 _exptl_crystal_F_000 1971.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file jj2091Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 10mz547_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 400.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 84477.56 77936.24 1946.86 o 2 0 0 4.71 35.72 13.55 o 3 0 0 1205.24 1240.16 49.93 o 4 0 0 7739.70 8420.91 177.51 o 5 0 0 11769.23 10953.57 182.29 o 6 0 0 11664.54 11698.45 203.35 o 7 0 0 9892.12 8678.61 173.62 o 8 0 0 4026.07 3416.26 112.16 o 9 0 0 141.97 213.46 50.06 o 10 0 0 11522.50 11312.72 236.68 o 11 0 0 1662.24 1649.73 115.03 o 12 0 0 438.74 411.51 72.47 o 13 0 0 22.84 83.88 31.19 o 14 0 0 498.49 526.00 97.76 o 15 0 0 233.31 183.06 39.44 o -15 1 0 27.19 197.87 54.87 o -14 1 0 1080.57 1240.53 97.98 o -13 1 0 297.75 312.50 60.34 o -12 1 0 361.99 406.82 69.68 o -11 1 0 356.22 398.70 73.08 o -10 1 0 2421.39 2316.76 101.94 o -9 1 0 6787.52 6709.51 234.69 o -8 1 0 430.34 398.65 49.78 o -7 1 0 317.19 313.11 43.47 o -6 1 0 359.85 220.65 60.59 o -5 1 0 6075.74 6525.28 124.50 o -4 1 0 9597.87 8055.54 135.10 o -3 1 0 8692.50 9305.34 141.31 o -2 1 0 1515.01 1853.85 82.67 o -1 1 0 2753.01 3160.70 349.42 o 1 1 0 13145.42 13693.87 345.39 o 2 1 0 5634.03 6943.75 262.59 o 3 1 0 9.36 19.04 35.04 o 4 1 0 3416.03 2503.38 75.22 o 5 1 0 335.81 267.25 40.64 o 6 1 0 3260.81 2892.01 98.33 o 7 1 0 789.97 956.71 67.09 o 8 1 0 3040.88 2966.20 139.90 o 9 1 0 887.83 824.32 70.49 o 10 1 0 1092.04 1210.38 73.96 o 11 1 0 1501.63 1448.93 107.31 o 12 1 0 93.88 171.39 44.02 o 13 1 0 14.25 63.20 28.33 o 14 1 0 741.72 901.33 93.07 o -15 2 0 822.35 853.56 129.29 o -14 2 0 2917.19 3105.76 157.18 o -13 2 0 628.39 525.54 80.45 o -12 2 0 264.82 240.01 61.60 o -11 2 0 516.76 601.09 82.35 o -10 2 0 4032.24 4005.92 127.88 o -9 2 0 55.87 28.12 30.17 o -8 2 0 8191.22 7989.87 167.68 o -7 2 0 3428.67 3229.61 99.99 o -6 2 0 1646.36 1904.71 106.75 o -5 2 0 663.42 511.08 38.00 o -4 2 0 5088.30 4898.95 189.07 o -3 2 0 1936.07 2001.00 57.96 o -2 2 0 6180.79 6827.09 146.44 o -1 2 0 2060.32 2341.34 57.19 o 0 2 0 18078.84 19565.46 667.58 o 1 2 0 18910.79 20977.61 359.80 o 2 2 0 1278.34 904.15 40.08 o 3 2 0 809.18 998.59 48.47 o 4 2 0 2719.03 2541.33 87.61 o 5 2 0 187.07 193.35 34.90 o 6 2 0 10082.32 10052.05 186.82 o 7 2 0 934.55 1152.48 66.65 o 8 2 0 7700.74 7130.40 181.84 o 9 2 0 2735.67 2623.95 109.97 o 10 2 0 507.27 579.70 62.91 o 11 2 0 98.25 241.96 58.61 o 12 2 0 16.57 31.06 54.89 o 13 2 0 705.30 706.07 88.87 o 14 2 0 767.72 1004.47 98.65 o -15 3 0 174.21 245.04 74.18 o -14 3 0 0.06 75.27 35.46 o -13 3 0 1399.55 1511.14 109.33 o -12 3 0 1586.02 1584.10 114.21 o -11 3 0 1119.70 1027.10 66.70 o -10 3 0 1676.96 1366.69 73.55 o -9 3 0 1222.24 1079.80 61.07 o -8 3 0 3818.24 3404.60 107.56 o -7 3 0 2250.54 2251.70 121.09 o -6 3 0 4232.87 4495.80 151.08 o -5 3 0 3.86 4.88 20.62 o -4 3 0 1646.79 1313.70 54.05 o -3 3 0 3870.98 4761.59 102.30 o -2 3 0 20165.40 22862.59 298.37 o -1 3 0 4373.10 5891.10 112.64 o 0 3 0 2536.43 2359.65 147.01 o 1 3 0 5737.73 6755.76 105.06 o 2 3 0 3383.58 3390.54 128.25 o 3 3 0 1821.51 1967.52 75.87 o 4 3 0 4689.28 4330.18 101.82 o 5 3 0 700.17 721.15 116.67 o 6 3 0 2840.78 2361.99 83.92 o 7 3 0 19.18 38.84 29.70 o 8 3 0 4561.99 4439.05 130.25 o 9 3 0 33.11 5.19 22.60 o 10 3 0 1.79 6.97 33.52 o 11 3 0 117.16 101.54 37.13 o 12 3 0 1363.91 1445.43 111.35 o 14 3 0 415.33 336.32 51.99 o -16 4 0 348.53 368.24 89.99 o -15 4 0 3388.06 3677.95 237.95 o -14 4 0 5189.56 6016.34 245.92 o -13 4 0 1359.18 1481.70 120.66 o -12 4 0 25.92 11.81 40.71 o -11 4 0 1490.10 1708.84 77.95 o -10 4 0 801.51 837.06 60.00 o -9 4 0 8470.39 8672.40 188.23 o -8 4 0 1793.75 1721.70 74.03 o -7 4 0 2650.43 2859.75 87.56 o -6 4 0 7547.06 10003.53 440.63 o -5 4 0 877.16 1018.94 69.62 o -4 4 0 652.21 811.00 45.85 o -3 4 0 23298.29 23167.41 514.20 o -2 4 0 38165.09 38591.21 489.70 o -1 4 0 292.37 363.89 25.44 o 0 4 0 2579.68 2037.67 47.49 o 1 4 0 2450.14 1618.93 70.79 o 2 4 0 341.80 453.79 44.29 o 3 4 0 173.34 87.26 22.63 o 4 4 0 1886.95 2521.27 118.47 o 5 4 0 8871.17 8238.18 160.23 o 6 4 0 3813.04 4231.62 114.53 o 7 4 0 288.21 333.46 48.21 o 8 4 0 6.70 -23.84 23.84 o 9 4 0 31.79 90.43 26.73 o 10 4 0 752.78 875.86 60.25 o 11 4 0 1173.23 1147.62 85.97 o 12 4 0 481.40 605.56 79.86 o 13 4 0 14.49 -36.28 36.28 o -16 5 0 1409.43 1566.71 159.67 o -15 5 0 502.52 569.89 223.97 o -14 5 0 272.33 399.42 109.66 o -13 5 0 602.47 988.74 92.82 o -12 5 0 2666.60 3112.94 148.82 o -11 5 0 13.60 30.20 44.92 o -10 5 0 926.39 1029.48 63.31 o -9 5 0 1145.20 1070.19 64.25 o -8 5 0 2086.09 1729.41 75.93 o -7 5 0 152.00 291.08 38.96 o -6 5 0 70.87 54.82 28.56 o -5 5 0 1094.60 1460.95 267.06 o -4 5 0 6539.63 6953.84 140.39 o -3 5 0 15541.57 16156.48 312.07 o -2 5 0 30103.51 30932.83 405.38 o -1 5 0 6619.00 6907.20 192.90 o 0 5 0 6702.78 6098.25 108.71 o 1 5 0 3423.97 3461.83 69.18 o 2 5 0 288.47 73.03 17.03 o 3 5 0 1981.45 1995.50 100.81 o 4 5 0 6790.59 5915.37 182.97 o 5 5 0 1851.42 2162.52 79.64 o 6 5 0 7026.02 6670.30 159.85 o 7 5 0 10241.79 9359.73 194.39 o 8 5 0 72.26 116.01 32.88 o 9 5 0 450.92 448.62 52.47 o 10 5 0 319.86 257.26 36.24 o 11 5 0 101.51 101.65 83.52 o 12 5 0 689.05 839.08 164.38 o 13 5 0 1487.37 1459.97 176.53 o -16 6 0 56.05 200.63 65.89 o -15 6 0 2.50 35.44 103.72 o -14 6 0 45.97 45.54 78.83 o -13 6 0 291.65 349.62 62.64 o -12 6 0 682.31 772.70 92.89 o -11 6 0 348.98 523.43 71.74 o -10 6 0 8105.15 8212.80 184.93 o -9 6 0 36.49 77.82 28.55 o -8 6 0 808.08 723.25 54.99 o -7 6 0 971.87 974.96 56.43 o -6 6 0 1137.07 1310.58 71.27 o -5 6 0 122.23 97.27 30.61 o -4 6 0 158.60 141.73 30.66 o -3 6 0 5198.72 4871.25 103.63 o -2 6 0 2164.57 1776.97 58.56 o -1 6 0 37704.91 38409.22 717.13 o 0 6 0 613.56 516.92 25.81 o 1 6 0 6.11 40.27 14.95 o 2 6 0 399.92 313.06 27.12 o 3 6 0 5448.66 4939.55 117.61 o 4 6 0 1190.45 1569.47 92.30 o 5 6 0 1633.55 1572.75 66.89 o 6 6 0 1611.09 1665.24 73.25 o 7 6 0 349.44 311.21 43.37 o 8 6 0 3.75 16.46 18.68 o 9 6 0 266.78 259.84 51.44 o 10 6 0 1489.79 1188.68 188.28 o 11 6 0 203.18 328.22 109.94 o 12 6 0 1219.75 1360.40 175.21 o 13 6 0 0.27 -1.01 56.40 o -16 7 0 1484.98 1960.50 192.67 o -15 7 0 16.66 173.25 85.72 o -14 7 0 142.19 192.28 82.74 o -13 7 0 227.60 231.15 49.43 o -12 7 0 875.83 1114.87 93.96 o -11 7 0 28.46 82.28 23.11 o -10 7 0 61.13 119.20 34.48 o -9 7 0 3.90 29.15 25.86 o -8 7 0 777.50 617.36 55.34 o -7 7 0 1030.51 1057.52 59.79 o -6 7 0 37.16 120.88 86.48 o -5 7 0 205.14 365.12 41.20 o -4 7 0 23057.60 23541.81 340.21 o -3 7 0 176.81 79.56 29.65 o -2 7 0 41380.87 42256.33 621.27 o -1 7 0 11338.71 11179.32 203.07 o 0 7 0 2504.26 2122.57 100.02 o 1 7 0 2005.25 1844.15 58.53 o 2 7 0 107.26 97.00 47.15 o 3 7 0 648.44 494.11 32.32 o 4 7 0 4781.08 4439.92 105.85 o 5 7 0 654.09 818.89 71.33 o 6 7 0 3037.93 2831.35 93.70 o 7 7 0 485.34 456.03 45.51 o 8 7 0 26.64 20.97 34.68 o 9 7 0 885.14 683.79 95.16 o 10 7 0 0.82 21.55 76.23 o 11 7 0 219.87 260.25 100.18 o 12 7 0 430.28 513.28 129.50 o -16 8 0 73.42 44.05 60.11 o -15 8 0 1714.44 1644.83 172.36 o -14 8 0 2527.08 2399.92 193.60 o -13 8 0 15.71 36.48 100.85 o -12 8 0 9523.61 9032.20 259.11 o -11 8 0 7851.41 7911.60 188.45 o -10 8 0 1011.15 1283.78 72.99 o -9 8 0 1856.63 1858.85 83.68 o -8 8 0 972.12 1018.78 66.17 o -7 8 0 3.20 -31.47 31.47 o -6 8 0 15813.57 15335.60 256.24 o -5 8 0 3253.73 3399.99 100.35 o -4 8 0 33626.45 34911.26 480.49 o -3 8 0 5.18 101.20 45.88 o -2 8 0 33200.40 36856.84 491.63 o -1 8 0 20639.45 20996.54 494.55 o 0 8 0 5369.65 5801.60 277.10 o 1 8 0 8.99 24.41 14.09 o 2 8 0 34.82 84.17 14.85 o 3 8 0 391.75 403.42 31.55 o 4 8 0 6660.80 6353.15 132.61 o 5 8 0 3272.78 3052.06 97.53 o 6 8 0 2775.59 2680.45 156.77 o 7 8 0 1433.89 1398.08 120.34 o 8 8 0 2036.90 1861.14 141.02 o 9 8 0 1848.58 1634.50 125.08 o 10 8 0 25.42 -28.94 69.67 o 11 8 0 1.12 10.41 71.10 o -16 9 0 4.68 26.63 53.20 o -15 9 0 1809.03 1812.06 179.30 o -14 9 0 1166.47 1349.67 173.55 o -13 9 0 2917.61 2987.16 212.71 o -12 9 0 3237.48 3471.87 152.26 o -11 9 0 170.96 186.99 35.08 o -10 9 0 37.59 19.29 23.83 o -9 9 0 1280.07 1323.86 74.06 o -8 9 0 14151.89 14087.46 255.83 o -7 9 0 16942.59 16296.46 278.23 o -6 9 0 157.87 148.25 45.86 o -5 9 0 1423.05 1143.26 63.24 o -4 9 0 4941.68 5270.00 233.04 o -3 9 0 2081.69 3069.58 100.47 o -2 9 0 22693.81 22443.66 461.01 o -1 9 0 540.54 762.37 110.15 o 0 9 0 444.15 411.76 39.87 o 1 9 0 1016.44 970.60 42.08 o 2 9 0 550.65 418.02 29.90 o 3 9 0 1988.46 1901.10 78.77 o 4 9 0 682.52 713.42 95.01 o 5 9 0 976.57 929.42 109.24 o 6 9 0 4.39 -28.63 41.88 o 7 9 0 175.29 204.30 77.69 o 8 9 0 90.06 51.50 44.78 o 9 9 0 18.68 5.61 31.24 o 11 9 0 232.85 364.61 92.66 o -16 10 0 650.89 711.61 138.14 o -15 10 0 12.61 223.02 228.40 o -14 10 0 280.99 240.10 89.35 o -13 10 0 532.68 557.14 110.63 o -12 10 0 2447.69 2496.94 126.46 o -11 10 0 5723.88 5369.74 152.39 o -10 10 0 25.98 19.91 21.81 o -9 10 0 1075.40 1080.64 71.89 o -8 10 0 226.62 278.27 52.85 o -7 10 0 941.09 923.14 63.77 o -6 10 0 220.40 248.00 40.49 o -5 10 0 5880.60 5208.31 128.87 o -4 10 0 691.91 937.59 122.40 o -3 10 0 3867.48 4344.81 175.50 o -2 10 0 380.59 585.04 74.09 o -1 10 0 133.04 274.37 33.79 o 0 10 0 3964.96 3585.61 88.93 o 1 10 0 5655.45 5233.10 200.83 o 2 10 0 780.93 798.81 94.96 o 3 10 0 3613.77 3607.03 176.72 o 4 10 0 1665.03 1509.53 126.15 o 5 10 0 9941.60 8550.33 291.78 o 6 10 0 5550.50 5410.26 228.78 o 7 10 0 763.92 644.88 97.76 o 8 10 0 141.98 147.22 48.15 o 9 10 0 26.23 -16.63 19.41 o 10 10 0 2670.45 2883.54 258.15 o -15 11 0 564.08 462.49 108.90 o -14 11 0 1732.27 1914.84 168.35 o -13 11 0 1326.29 1322.54 160.78 o -12 11 0 55.90 64.37 46.94 o -11 11 0 353.85 405.71 49.86 o -10 11 0 223.36 195.12 36.68 o -9 11 0 1001.62 855.11 62.32 o -8 11 0 1502.56 1500.27 79.08 o -7 11 0 118.21 118.18 36.71 o -6 11 0 3551.49 2974.36 102.56 o -5 11 0 1841.92 2201.18 87.51 o -4 11 0 14814.02 15372.03 269.66 o -3 11 0 8194.10 7859.68 161.80 o -2 11 0 559.52 749.10 72.09 o -1 11 0 738.55 485.48 104.96 o 0 11 0 80.44 24.21 48.06 o 1 11 0 62.70 48.02 51.69 o 2 11 0 176.52 184.77 66.45 o 3 11 0 46.89 -75.46 79.98 o 4 11 0 5870.40 5648.52 233.72 o 5 11 0 456.48 416.60 82.99 o 6 11 0 1298.73 1277.17 122.09 o 7 11 0 1336.98 1392.09 117.77 o 8 11 0 37.16 32.84 28.85 o 9 11 0 101.12 89.28 22.43 o 10 11 0 74.93 293.79 90.80 o -15 12 0 2439.04 2279.70 192.93 o -14 12 0 136.89 132.13 71.45 o -13 12 0 227.16 158.13 78.04 o -12 12 0 221.01 222.78 34.47 o -11 12 0 54.68 12.59 35.75 o -10 12 0 495.80 518.12 57.38 o -9 12 0 14.83 16.23 35.96 o -8 12 0 173.98 200.05 40.80 o -7 12 0 456.13 494.27 55.06 o -6 12 0 975.99 959.56 67.54 o -5 12 0 3704.18 3706.13 115.47 o -4 12 0 1733.64 1840.59 77.86 o -3 12 0 409.39 543.14 37.63 o -2 12 0 262.35 340.37 24.00 o -1 12 0 2278.70 2060.49 136.24 o 0 12 0 2007.94 2026.42 135.62 o 1 12 0 2187.39 2121.45 205.11 o 2 12 0 83.33 85.20 55.69 o 3 12 0 540.27 649.05 101.20 o 4 12 0 1424.73 1144.22 129.88 o 5 12 0 99.63 57.57 45.98 o 6 12 0 23.73 -20.54 29.84 o 7 12 0 62.68 56.55 35.24 o 8 12 0 1808.43 1896.65 135.55 o 9 12 0 588.21 743.06 150.69 o -15 13 0 263.76 296.23 82.48 o -14 13 0 149.51 200.50 73.39 o -13 13 0 136.29 229.34 76.31 o -12 13 0 120.23 138.09 27.90 o -11 13 0 1.82 -13.97 15.12 o -10 13 0 467.35 491.99 55.26 o -9 13 0 565.49 729.76 68.29 o -8 13 0 1665.06 1730.92 84.98 o -7 13 0 6222.14 6268.64 165.10 o -6 13 0 4741.21 4503.10 129.71 o -5 13 0 527.14 578.25 49.68 o -4 13 0 4350.16 4105.74 130.54 o -3 13 0 1.33 30.97 59.87 o -2 13 0 548.16 592.28 94.73 o -1 13 0 18.93 -5.08 69.42 o 0 13 0 45.44 -44.97 44.97 o 1 13 0 76.29 67.78 53.38 o 2 13 0 983.76 924.00 119.64 o 3 13 0 4587.02 4196.34 209.38 o 4 13 0 1167.13 1042.88 112.66 o 5 13 0 979.65 1019.44 121.94 o 6 13 0 82.99 47.78 34.11 o 7 13 0 43.53 94.80 35.61 o 8 13 0 406.78 397.38 98.03 o -15 14 0 16.30 24.46 42.13 o -14 14 0 1842.26 1803.43 157.81 o -13 14 0 352.71 410.77 93.98 o -12 14 0 933.48 1001.77 80.96 o -11 14 0 386.62 513.89 71.31 o -10 14 0 23.47 1.39 24.62 o -9 14 0 786.85 791.67 70.42 o -8 14 0 7872.19 7578.04 186.33 o -7 14 0 752.07 1079.84 124.63 o -6 14 0 1248.68 1268.71 72.43 o -5 14 0 2773.43 2587.56 105.02 o -4 14 0 2207.73 2200.09 150.95 o -3 14 0 125.94 32.78 65.41 o -2 14 0 8.80 -27.47 54.53 o -1 14 0 217.96 126.66 64.91 o 0 14 0 1694.52 1476.03 128.14 o 1 14 0 2103.14 1809.86 138.62 o 2 14 0 1536.33 1510.50 130.94 o 3 14 0 260.35 346.11 110.44 o 4 14 0 285.24 312.86 74.53 o 5 14 0 715.63 781.88 107.68 o 6 14 0 99.66 148.18 87.06 o 7 14 0 318.98 239.88 49.93 o 8 14 0 1618.30 1594.81 167.91 o -14 15 0 12.79 0.90 33.21 o -13 15 0 127.90 310.51 156.72 o -12 15 0 150.74 221.58 40.02 o -11 15 0 405.28 364.08 58.29 o -10 15 0 13.80 12.33 53.47 o -9 15 0 7.39 -1.57 22.65 o -8 15 0 821.18 864.25 73.11 o -7 15 0 4819.12 4254.27 150.95 o -6 15 0 2165.59 2283.35 157.48 o -5 15 0 375.77 339.92 84.34 o -4 15 0 793.27 717.11 110.75 o -3 15 0 1010.59 1045.80 130.07 o -2 15 0 29.75 28.37 56.58 o -1 15 0 46.99 14.07 90.51 o 0 15 0 2.99 -14.21 47.71 o 1 15 0 12.88 40.55 52.08 o 2 15 0 50.24 133.07 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