#------------------------------------------------------------------------------ #$Date: 2011-10-06 14:27:20 +0300 (Thu, 06 Oct 2011) $ #$Revision: 27511 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/11/2231193.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231193_Fobs loop_ _publ_author_name 'Kraicheva, Ivanka' 'Tsacheva, Ivelina' 'Vodenicharova, Elitsa' 'Tashev, Emil' 'Troev, Kolio' _publ_section_title ; rac-Dimethyl [(9-anthryl)(4-methylanilino)methyl]phosphonate ; _journal_coeditor_code KP2342 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2045 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 100.920 _cell_angle_beta 91.633 _cell_angle_gamma 95.174 _cell_length_a 7.9436 _cell_length_b 11.3889 _cell_length_c 24.0065 _exptl_crystal_F_000 856.00 _reflns_d_resolution_high 0.8115 _[local]_cod_data_source_file kp2342Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 218.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5.74 17.95 9.26 o 2 0 0 43409.14 43041.91 279.19 o 3 0 0 0.95 -4.83 26.21 o 4 0 0 501.77 495.98 44.62 o 5 0 0 0.16 -8.45 40.95 o 6 0 0 1.32 -60.65 60.65 o 7 0 0 146.27 138.85 42.96 o 8 0 0 8.92 -19.48 38.15 o 9 0 0 46.48 35.71 71.42 o -9 1 0 1.38 -8.87 77.82 o -8 1 0 126.42 138.75 45.52 o -7 1 0 39.38 21.65 34.65 o -6 1 0 74.16 75.93 37.77 o -5 1 0 10.08 -39.67 39.67 o -4 1 0 971.08 1022.28 68.71 o -3 1 0 2812.46 2549.95 86.65 o -2 1 0 1298.33 1488.68 53.71 o -1 1 0 20.34 6.43 15.45 o 0 1 0 37.83 35.41 5.64 o 1 1 0 267.29 268.36 23.62 o 2 1 0 681.90 704.37 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