#------------------------------------------------------------------------------ #$Date: 2011-10-06 14:27:20 +0300 (Thu, 06 Oct 2011) $ #$Revision: 27511 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/12/2231221.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231221_Fobs loop_ _publ_author_name 'Betz, Richard' 'Gerber, Thomas' 'Hosten, Eric' 'Schalekamp, Henk' _publ_section_title ; (2-Hydroxy-4-methoxyphenyl)(2-hydroxyphenyl)methanone ; _journal_coeditor_code LW2071 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2180 _journal_volume 67 _journal_year 2011 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 4.8582 _cell_length_b 14.0236 _cell_length_c 16.8636 _exptl_crystal_F_000 512.00 _reflns_d_resolution_high 0.7494 _[local]_cod_data_source_file lw2071Isup3.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ba264_s in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 110.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3033.67 2976.31 10.24 o 4 0 0 20.67 25.03 2.16 o 6 0 0 3.19 0.65 2.19 o 1 1 0 90.82 88.89 0.77 o 2 1 0 433.75 424.93 4.93 o 3 1 0 455.92 476.99 2.54 o 4 1 0 3.11 1.21 0.96 o 5 1 0 11.31 10.29 1.39 o 6 1 0 14.61 15.54 2.53 o 1 2 0 646.98 612.07 4.58 o 2 2 0 817.68 824.38 4.09 o 3 2 0 133.96 146.73 1.79 o 4 2 0 33.56 34.93 1.67 o 5 2 0 0.74 1.05 1.59 o 6 2 0 132.39 148.12 4.83 o 1 3 0 144.39 128.58 1.67 o 2 3 0 214.73 224.14 3.18 o 3 3 0 328.38 341.29 4.46 o 4 3 0 4.97 5.17 1.53 o 5 3 0 24.70 27.84 2.59 o 6 3 0 47.14 46.79 3.30 o 0 4 0 317.61 286.52 7.56 o 1 4 0 0.65 0.59 0.34 o 2 4 0 380.10 402.44 4.49 o 3 4 0 73.85 76.10 2.59 o 4 4 0 34.26 38.41 2.41 o 5 4 0 1.09 1.02 1.70 o 6 4 0 0.09 -0.31 1.85 o 1 5 0 9.53 8.42 0.48 o 2 5 0 701.42 735.96 9.75 o 3 5 0 23.32 19.45 1.35 o 4 5 0 120.43 117.35 3.44 o 5 5 0 12.25 14.71 2.19 o 6 5 0 0.60 -0.99 1.85 o 0 6 0 1681.53 1759.93 33.05 o 1 6 0 114.74 114.63 1.28 o 2 6 0 189.24 197.32 1.82 o 3 6 0 302.46 278.90 5.14 o 4 6 0 16.43 16.14 1.93 o 5 6 0 22.97 26.73 2.64 o 6 6 0 0.14 -0.88 1.99 o 1 7 0 427.67 470.07 29.60 o 2 7 0 443.95 452.92 2.79 o 3 7 0 54.43 54.19 1.98 o 4 7 0 22.11 18.52 2.07 o 5 7 0 13.97 12.50 2.16 o 0 8 0 265.67 302.67 5.47 o 1 8 0 179.10 205.57 1.92 o 2 8 0 22.62 21.64 1.46 o 3 8 0 68.08 71.96 2.12 o 4 8 0 38.97 37.98 2.73 o 5 8 0 104.13 111.50 4.12 o 1 9 0 285.68 324.16 2.65 o 2 9 0 429.17 404.31 3.49 o 3 9 0 545.24 535.46 6.90 o 4 9 0 159.49 161.89 4.46 o 5 9 0 8.48 9.32 2.19 o 0 10 0 48.76 47.67 1.93 o 1 10 0 17.98 14.59 0.88 o 2 10 0 65.63 63.02 0.83 o 3 10 0 105.78 106.27 3.75 o 4 10 0 131.05 132.80 4.35 o 5 10 0 11.54 12.07 2.36 o 1 11 0 1.67 1.27 0.81 o 2 11 0 504.33 485.62 3.83 o 3 11 0 30.77 27.92 2.70 o 4 11 0 31.04 28.09 2.90 o 5 11 0 1.52 1.96 1.87 o 0 12 0 810.25 738.95 5.38 o 1 12 0 126.08 115.14 1.84 o 2 12 0 523.04 502.77 4.07 o 3 12 0 149.05 146.04 4.43 o 4 12 0 27.42 28.95 3.04 o 1 13 0 54.78 46.91 2.59 o 2 13 0 2.58 3.11 0.61 o 3 13 0 32.62 31.84 2.70 o 4 13 0 12.75 11.65 2.36 o 0 14 0 88.21 77.35 3.66 o 1 14 0 51.43 49.34 2.81 o 2 14 0 8.01 8.10 0.71 o 3 14 0 0.69 1.16 1.73 o 4 14 0 0.74 1.31 1.99 o 1 15 0 3.84 1.85 1.62 o 2 15 0 2.02 2.73 0.72 o 3 15 0 17.24 21.08 2.64 o 0 16 0 3.00 3.18 2.10 o 1 16 0 2.40 3.92 1.76 o 2 16 0 31.23 38.42 1.72 o 3 16 0 2.86 4.40 1.96 o 1 17 0 16.39 16.62 2.16 o 2 17 0 18.04 20.08 1.35 o 1 18 0 2.12 4.20 1.90 o 1 0 1 45.67 40.65 0.57 o 2 0 1 63.75 70.84 0.99 o 3 0 1 12.11 10.66 0.78 o 4 0 1 6.46 4.21 1.04 o 5 0 1 60.33 65.74 2.29 o 6 0 1 25.99 28.75 2.25 o 0 1 1 13.61 9.41 4.98 o 1 1 1 649.10 654.47 3.80 o 2 1 1 1081.67 1082.27 4.08 o 3 1 1 137.78 141.37 1.24 o 4 1 1 100.86 105.65 1.59 o 5 1 1 23.81 21.70 1.24 o 6 1 1 85.77 85.40 2.32 o 0 2 1 538.09 477.70 41.56 o 1 2 1 1055.75 1058.77 7.54 o 2 2 1 97.96 101.29 0.87 o 3 2 1 255.20 259.06 1.60 o 4 2 1 5.79 4.51 0.74 o 5 2 1 51.49 50.70 1.74 o 6 2 1 20.55 22.19 1.89 o 0 3 1 1725.98 1737.13 11.43 o 1 3 1 1472.27 1492.52 7.68 o 2 3 1 554.53 543.79 3.80 o 3 3 1 682.41 694.97 5.74 o 4 3 1 89.16 88.85 2.14 o 5 3 1 26.61 26.43 1.84 o 6 3 1 8.94 8.34 1.58 o 0 4 1 3772.06 3659.60 26.12 o 1 4 1 269.51 277.97 1.82 o 2 4 1 50.96 49.75 0.59 o 3 4 1 134.52 142.15 1.66 o 4 4 1 2.28 1.69 0.97 o 5 4 1 24.98 27.23 1.93 o 6 4 1 27.04 28.97 2.10 o 0 5 1 1195.62 1162.08 10.97 o 1 5 1 70.20 62.86 0.61 o 2 5 1 326.21 305.43 3.09 o 3 5 1 173.20 176.06 2.35 o 4 5 1 6.65 7.54 1.12 o 5 5 1 14.08 14.50 1.53 o 6 5 1 8.00 8.72 2.27 o 0 6 1 1773.01 1928.19 19.67 o 1 6 1 659.34 649.63 6.92 o 2 6 1 149.36 164.95 1.21 o 3 6 1 122.23 126.68 2.26 o 4 6 1 40.34 40.48 1.80 o 5 6 1 19.51 18.32 1.62 o 6 6 1 2.36 3.38 2.10 o 0 7 1 554.00 576.08 3.32 o 1 7 1 57.91 63.23 0.81 o 2 7 1 363.07 369.99 1.82 o 3 7 1 163.61 164.74 3.16 o 4 7 1 9.94 10.77 1.33 o 5 7 1 25.53 25.28 1.98 o 6 7 1 10.34 8.29 2.36 o 0 8 1 302.92 349.34 4.27 o 1 8 1 144.89 149.83 1.15 o 2 8 1 21.77 22.21 0.60 o 3 8 1 36.31 35.13 1.33 o 4 8 1 116.72 116.17 2.69 o 5 8 1 38.49 41.29 2.15 o 0 9 1 1230.81 1307.05 15.80 o 1 9 1 87.83 83.72 1.51 o 2 9 1 178.21 174.21 1.12 o 3 9 1 823.36 832.08 11.05 o 4 9 1 105.97 107.39 2.71 o 5 9 1 71.97 81.89 2.67 o 0 10 1 291.82 318.74 4.90 o 1 10 1 80.83 80.17 1.04 o 2 10 1 419.66 410.73 2.16 o 3 10 1 49.56 48.34 2.12 o 4 10 1 54.70 53.53 2.28 o 5 10 1 1.88 2.99 1.35 o 0 11 1 217.32 239.40 2.71 o 1 11 1 124.60 137.67 1.32 o 2 11 1 364.74 364.94 3.10 o 3 11 1 106.89 100.81 2.66 o 4 11 1 123.33 129.50 3.11 o 5 11 1 13.23 15.52 1.72 o 0 12 1 37.54 36.66 1.52 o 1 12 1 13.55 11.33 0.67 o 2 12 1 32.17 28.58 0.96 o 3 12 1 19.37 17.63 1.57 o 4 12 1 4.57 5.12 1.41 o 0 13 1 28.10 23.94 1.51 o 1 13 1 53.88 44.77 1.22 o 2 13 1 24.82 22.08 0.82 o 3 13 1 7.14 6.18 1.31 o 4 13 1 12.39 11.04 1.64 o 0 14 1 40.69 32.70 2.23 o 1 14 1 23.91 18.31 1.43 o 2 14 1 3.54 3.44 0.46 o 3 14 1 33.03 32.16 2.23 o 4 14 1 12.13 13.74 1.74 o 0 15 1 58.17 58.05 2.51 o 1 15 1 56.31 51.18 2.09 o 2 15 1 11.25 12.41 1.13 o 3 15 1 19.89 18.31 3.45 o 0 16 1 71.21 68.12 3.69 o 1 16 1 37.65 41.30 2.09 o 2 16 1 6.14 6.08 0.60 o 3 16 1 1.15 1.71 1.40 o 1 17 1 44.34 48.69 2.21 o 2 17 1 8.17 10.16 0.88 o 1 18 1 66.20 81.91 2.55 o 0 0 2 1039.95 991.79 13.62 o 1 0 2 1003.57 894.29 7.48 o 2 0 2 614.84 555.05 3.42 o 3 0 2 53.60 52.39 1.67 o 4 0 2 7.20 5.99 1.02 o 5 0 2 37.57 35.42 1.97 o 6 0 2 58.75 56.87 3.64 o 0 1 2 2290.61 2240.86 18.29 o 1 1 2 12227.42 11311.54 40.08 o 2 1 2 1171.62 1130.97 8.00 o 3 1 2 360.89 395.18 2.12 o 4 1 2 1.54 1.30 0.67 o 5 1 2 34.90 34.41 1.63 o 6 1 2 5.41 7.24 1.63 o 0 2 2 970.45 972.71 7.13 o 1 2 2 3821.12 3652.65 30.32 o 2 2 2 553.66 561.25 5.21 o 3 2 2 629.14 609.48 2.50 o 4 2 2 84.67 83.82 1.72 o 5 2 2 55.28 55.35 1.82 o 6 2 2 3.68 3.55 2.16 o 0 3 2 3261.28 3182.64 27.37 o 1 3 2 284.06 278.09 1.95 o 2 3 2 483.35 514.32 4.20 o 3 3 2 57.84 58.36 1.05 o 4 3 2 9.91 7.56 0.92 o 5 3 2 93.49 98.68 2.55 o 6 3 2 14.22 11.48 2.41 o 0 4 2 475.32 481.42 5.56 o 1 4 2 64.01 66.24 0.61 o 2 4 2 88.39 99.64 1.29 o 3 4 2 135.03 124.73 2.11 o 4 4 2 66.88 63.31 1.99 o 5 4 2 91.49 95.22 2.60 o 6 4 2 2.36 0.97 2.10 o 0 5 2 512.76 506.69 5.40 o 1 5 2 757.65 818.23 7.51 o 2 5 2 240.63 242.07 2.15 o 3 5 2 26.52 30.50 1.20 o 4 5 2 57.15 52.07 2.23 o 5 5 2 5.36 5.20 1.30 o 6 5 2 32.96 34.32 3.32 o 0 6 2 1376.86 1457.09 9.17 o 1 6 2 150.91 168.05 0.89 o 2 6 2 93.44 93.34 0.75 o 3 6 2 79.42 81.60 1.42 o 4 6 2 75.13 72.23 2.14 o 5 6 2 2.86 2.34 1.22 o 6 6 2 2.20 -0.57 2.07 o 0 7 2 21.22 23.80 0.94 o 1 7 2 153.99 154.67 1.01 o 2 7 2 16.16 14.22 0.56 o 3 7 2 65.13 64.11 1.41 o 4 7 2 65.18 64.44 2.12 o 5 7 2 0.41 -0.62 1.17 o 0 8 2 1635.18 1923.72 20.38 o 1 8 2 147.05 162.31 1.11 o 2 8 2 78.41 68.45 0.84 o 3 8 2 806.74 824.83 17.50 o 4 8 2 129.78 126.12 2.71 o 5 8 2 1.16 0.89 1.26 o 0 9 2 95.48 100.35 1.52 o 1 9 2 63.18 72.48 1.02 o 2 9 2 31.12 29.93 0.86 o 3 9 2 86.15 84.33 2.39 o 4 9 2 95.42 93.96 2.64 o 5 9 2 31.19 38.10 2.43 o 0 10 2 111.89 117.36 1.75 o 1 10 2 5.30 5.73 0.55 o 2 10 2 459.71 456.03 5.69 o 3 10 2 591.98 604.30 7.98 o 4 10 2 113.85 118.63 2.92 o 5 10 2 37.42 41.46 2.26 o 0 11 2 149.89 144.72 1.91 o 1 11 2 12.03 11.30 0.66 o 2 11 2 423.65 412.71 4.28 o 3 11 2 95.37 92.53 2.57 o 4 11 2 36.67 39.52 2.20 o 5 11 2 5.93 5.34 1.50 o 0 12 2 249.18 218.20 2.31 o 1 12 2 10.68 8.76 0.66 o 2 12 2 131.29 129.45 2.39 o 3 12 2 38.85 38.02 1.98 o 4 12 2 0.19 -0.08 1.26 o 0 13 2 150.90 138.84 2.83 o 1 13 2 203.46 194.79 2.25 o 2 13 2 106.14 101.84 1.63 o 3 13 2 13.77 14.65 1.60 o 4 13 2 15.79 14.74 1.68 o 0 14 2 24.95 22.47 2.17 o 1 14 2 6.32 4.16 1.18 o 2 14 2 7.40 6.28 0.79 o 3 14 2 63.98 64.65 2.50 o 4 14 2 1.90 -0.16 1.33 o 0 15 2 62.65 57.52 2.44 o 1 15 2 19.63 20.28 1.67 o 2 15 2 67.61 60.23 1.66 o 3 15 2 43.34 43.73 2.40 o 0 16 2 8.33 10.43 2.27 o 1 16 2 5.76 7.55 1.29 o 2 16 2 52.79 53.38 1.97 o 3 16 2 3.91 4.79 1.52 o 1 17 2 8.34 13.34 1.14 o 2 17 2 6.50 6.88 1.19 o 1 18 2 0.21 1.90 1.00 o 1 0 3 1364.16 1291.14 13.32 o 2 0 3 16.64 19.42 0.59 o 3 0 3 151.91 151.33 1.69 o 4 0 3 38.72 36.17 1.62 o 5 0 3 31.39 31.04 1.94 o 6 0 3 4.13 2.78 2.19 o 0 1 3 3776.79 3657.12 21.48 o 1 1 3 7445.12 7248.21 52.22 o 2 1 3 503.38 513.41 3.19 o 3 1 3 204.39 202.75 1.68 o 4 1 3 82.07 80.49 1.73 o 5 1 3 111.93 116.35 3.84 o 6 1 3 4.29 4.87 1.61 o 0 2 3 3211.78 3235.21 29.00 o 1 2 3 2326.41 2356.32 17.50 o 2 2 3 971.16 968.75 6.19 o 3 2 3 393.71 396.05 3.41 o 4 2 3 27.98 32.21 1.39 o 5 2 3 44.96 44.41 2.23 o 6 2 3 2.59 2.36 2.10 o 0 3 3 102.87 94.23 12.70 o 1 3 3 2511.65 2463.33 17.00 o 2 3 3 64.60 65.62 0.94 o 3 3 3 15.77 17.57 0.77 o 4 3 3 57.04 54.80 1.55 o 5 3 3 14.51 14.58 1.24 o 6 3 3 1.10 2.39 2.05 o 0 4 3 99.13 80.32 3.60 o 1 4 3 177.00 180.87 3.80 o 2 4 3 1433.12 1540.36 13.54 o 3 4 3 100.82 101.18 1.92 o 4 4 3 324.97 327.10 3.62 o 5 4 3 40.64 44.11 2.08 o 6 4 3 7.53 4.89 2.27 o 0 5 3 305.27 315.10 1.89 o 1 5 3 665.45 708.93 4.06 o 2 5 3 290.36 327.96 2.32 o 3 5 3 63.26 67.55 1.46 o 4 5 3 4.08 5.22 2.03 o 5 5 3 11.07 10.71 1.44 o 6 5 3 12.25 13.44 2.59 o 0 6 3 55.77 58.23 1.03 o 1 6 3 58.50 62.31 0.67 o 2 6 3 268.87 250.84 1.83 o 3 6 3 413.61 416.63 6.12 o 4 6 3 135.69 135.99 2.66 o 5 6 3 48.35 52.81 3.01 o 6 6 3 5.40 7.19 2.41 o 0 7 3 446.25 454.92 2.29 o 1 7 3 1060.80 1143.04 5.34 o 2 7 3 125.11 123.52 1.01 o 3 7 3 21.13 19.66 1.01 o 4 7 3 29.71 30.31 1.75 o 5 7 3 19.28 21.12 1.70 o 0 8 3 24.14 30.29 1.26 o 1 8 3 0.49 0.01 0.36 o 2 8 3 509.59 504.72 7.34 o 3 8 3 93.53 91.78 1.71 o 4 8 3 20.43 22.84 1.70 o 5 8 3 14.22 17.01 1.64 o 0 9 3 45.82 42.76 1.20 o 1 9 3 62.63 57.89 1.63 o 2 9 3 18.56 16.17 0.76 o 3 9 3 1.21 0.19 1.48 o 4 9 3 4.62 7.06 1.24 o 5 9 3 22.29 23.55 1.92 o 0 10 3 0.14 -0.17 0.73 o 1 10 3 33.52 26.22 1.00 o 2 10 3 518.57 510.89 3.06 o 3 10 3 34.34 31.86 2.24 o 4 10 3 3.93 4.65 1.30 o 5 10 3 31.89 37.19 3.38 o 0 11 3 10.40 10.14 0.92 o 1 11 3 746.67 730.33 3.54 o 2 11 3 9.98 6.62 0.66 o 3 11 3 97.80 93.67 2.52 o 4 11 3 4.51 6.13 1.32 o 5 11 3 1.24 3.78 2.16 o 0 12 3 113.12 113.77 1.86 o 1 12 3 164.42 169.14 1.35 o 2 12 3 59.59 55.72 1.47 o 3 12 3 80.66 80.43 2.54 o 4 12 3 24.73 27.41 2.03 o 0 13 3 15.74 13.07 1.21 o 1 13 3 404.63 381.75 3.04 o 2 13 3 95.18 91.58 1.59 o 3 13 3 19.06 17.96 1.68 o 4 13 3 9.88 11.09 1.67 o 0 14 3 571.94 533.83 5.26 o 1 14 3 50.63 45.50 1.36 o 2 14 3 7.85 7.47 0.95 o 3 14 3 24.33 24.51 2.24 o 4 14 3 15.28 17.93 1.88 o 0 15 3 22.32 20.00 2.39 o 1 15 3 0.63 1.59 0.88 o 2 15 3 37.36 37.01 1.50 o 3 15 3 77.00 75.59 2.84 o 0 16 3 3.59 0.17 1.99 o 1 16 3 2.09 4.25 0.95 o 2 16 3 41.33 43.10 2.93 o 3 16 3 10.29 10.71 1.69 o 0 17 3 8.23 5.94 2.19 o 1 17 3 16.85 17.71 1.25 o 2 17 3 20.39 29.40 2.94 o 1 18 3 0.73 4.21 1.02 o 0 0 4 1902.66 1905.53 29.22 o 1 0 4 7.08 7.03 0.47 o 2 0 4 811.16 763.05 9.91 o 3 0 4 3.49 5.10 0.52 o 4 0 4 5.03 2.93 1.03 o 5 0 4 86.08 82.21 3.81 o 6 0 4 13.99 15.28 2.70 o 0 1 4 57.43 60.35 0.47 o 1 1 4 2655.25 2581.45 12.35 o 2 1 4 256.24 241.79 1.55 o 3 1 4 43.69 39.22 0.80 o 4 1 4 153.62 146.33 1.77 o 5 1 4 62.87 60.79 2.45 o 6 1 4 18.90 20.73 2.03 o 0 2 4 1184.41 1204.23 9.45 o 1 2 4 1568.54 1631.61 13.81 o 2 2 4 1534.56 1623.51 10.96 o 3 2 4 96.03 98.88 1.09 o 4 2 4 236.95 238.60 2.14 o 5 2 4 96.84 91.76 2.32 o 6 2 4 13.19 12.26 1.77 o 0 3 4 465.31 475.06 4.89 o 1 3 4 2918.55 2851.93 21.17 o 2 3 4 648.85 668.35 5.34 o 3 3 4 65.26 65.82 1.03 o 4 3 4 194.63 199.94 2.44 o 5 3 4 3.74 1.43 1.03 o 6 3 4 8.96 8.49 2.39 o 0 4 4 18.93 20.77 0.73 o 1 4 4 896.24 939.24 3.78 o 2 4 4 1144.68 1290.14 10.39 o 3 4 4 140.84 141.02 1.59 o 4 4 4 12.35 12.78 1.28 o 5 4 4 73.21 70.83 2.30 o 6 4 4 4.89 2.36 2.24 o 0 5 4 232.97 232.05 2.75 o 1 5 4 351.07 369.71 2.52 o 2 5 4 248.74 252.76 2.29 o 3 5 4 120.80 118.96 1.75 o 4 5 4 416.27 410.34 4.05 o 5 5 4 93.99 96.69 4.57 o 6 5 4 10.70 13.98 2.70 o 0 6 4 163.41 180.07 1.48 o 1 6 4 160.14 197.99 1.12 o 2 6 4 262.73 258.81 1.64 o 3 6 4 29.37 30.40 1.89 o 4 6 4 69.57 71.87 2.14 o 5 6 4 16.60 15.39 1.54 o 6 6 4 14.34 13.01 2.64 o 0 7 4 133.60 134.08 1.41 o 1 7 4 1138.05 1226.80 7.63 o 2 7 4 300.69 305.27 3.22 o 3 7 4 32.18 32.68 1.37 o 4 7 4 158.92 156.23 4.89 o 5 7 4 24.70 24.00 2.95 o 0 8 4 82.55 84.80 1.33 o 1 8 4 303.04 330.71 1.91 o 2 8 4 44.64 38.29 0.89 o 3 8 4 42.73 42.82 1.35 o 4 8 4 11.13 12.43 1.36 o 5 8 4 107.34 102.81 4.37 o 0 9 4 30.25 33.42 1.16 o 1 9 4 7.95 7.43 0.47 o 2 9 4 131.04 117.85 1.38 o 3 9 4 83.51 82.90 2.19 o 4 9 4 95.04 98.76 2.63 o 5 9 4 25.87 25.79 3.10 o 0 10 4 37.67 34.69 1.27 o 1 10 4 118.62 108.71 1.09 o 2 10 4 159.47 142.57 3.74 o 3 10 4 102.58 98.81 2.44 o 4 10 4 85.98 83.32 2.54 o 5 10 4 12.74 14.52 2.44 o 0 11 4 1.96 1.03 0.81 o 1 11 4 293.07 282.48 1.56 o 2 11 4 59.97 61.17 1.36 o 3 11 4 108.61 110.00 2.75 o 4 11 4 86.80 97.39 2.86 o 5 11 4 24.77 28.27 3.38 o 0 12 4 51.22 50.29 1.54 o 1 12 4 121.81 127.27 1.23 o 2 12 4 158.72 156.76 2.13 o 3 12 4 13.75 14.56 2.43 o 4 12 4 25.26 27.75 2.21 o 0 13 4 20.20 17.74 1.53 o 1 13 4 24.36 19.08 1.00 o 2 13 4 91.25 88.29 2.09 o 3 13 4 18.72 15.50 1.60 o 4 13 4 56.38 61.69 2.71 o 0 14 4 12.10 12.37 1.59 o 1 14 4 16.50 15.82 1.01 o 2 14 4 31.13 29.34 1.43 o 3 14 4 1.82 2.57 1.35 o 4 14 4 44.24 51.48 2.59 o 0 15 4 0.27 -0.28 1.90 o 1 15 4 15.78 19.23 2.77 o 2 15 4 6.20 7.00 1.01 o 3 15 4 31.82 36.17 2.25 o 0 16 4 5.67 6.02 2.10 o 1 16 4 17.10 19.21 1.31 o 2 16 4 13.83 15.45 2.33 o 3 16 4 29.29 30.52 2.49 o 0 17 4 19.84 14.80 2.39 o 1 17 4 4.23 7.81 1.01 o 2 17 4 0.84 1.49 1.14 o 1 18 4 21.15 25.90 1.76 o 1 0 5 1415.20 1453.19 11.28 o 2 0 5 674.54 699.14 7.05 o 3 0 5 72.53 75.52 1.33 o 4 0 5 37.93 34.16 1.68 o 5 0 5 4.52 2.95 2.05 o 6 0 5 0.84 0.00 1.99 o 0 1 5 233.76 234.13 1.67 o 1 1 5 2244.84 2292.83 18.02 o 2 1 5 179.61 183.15 1.11 o 3 1 5 13.71 12.97 0.54 o 4 1 5 198.10 200.83 3.20 o 5 1 5 12.03 9.84 1.62 o 6 1 5 1.06 0.49 1.56 o 0 2 5 637.35 592.22 3.50 o 1 2 5 1843.43 1855.83 12.76 o 2 2 5 123.07 154.29 1.63 o 3 2 5 21.31 17.21 0.61 o 4 2 5 16.70 14.90 0.93 o 5 2 5 111.64 113.92 2.21 o 6 2 5 20.48 22.33 2.10 o 0 3 5 49.35 43.48 0.55 o 1 3 5 2954.04 3021.02 14.45 o 2 3 5 214.36 233.45 2.06 o 3 3 5 180.50 181.41 1.94 o 4 3 5 164.24 157.52 3.97 o 5 3 5 29.72 28.15 2.21 o 6 3 5 0.10 -0.51 2.10 o 0 4 5 170.40 164.41 2.21 o 1 4 5 1023.75 1155.47 6.63 o 2 4 5 101.55 99.95 1.01 o 3 4 5 23.23 23.14 0.85 o 4 4 5 66.83 69.69 2.15 o 5 4 5 12.07 13.89 2.41 o 6 4 5 2.62 1.22 2.27 o 0 5 5 47.17 47.77 3.61 o 1 5 5 924.06 1019.75 7.80 o 2 5 5 139.96 123.31 1.08 o 3 5 5 17.31 16.18 0.90 o 4 5 5 4.38 5.69 1.09 o 5 5 5 133.23 130.42 4.66 o 6 5 5 5.92 8.01 2.50 o 0 6 5 2.17 3.66 0.47 o 1 6 5 0.25 0.37 0.28 o 2 6 5 912.16 974.92 6.00 o 3 6 5 144.62 148.33 2.23 o 4 6 5 54.10 58.84 1.93 o 5 6 5 19.21 18.72 2.50 o 0 7 5 50.20 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1.46 o 0 3 20 0.02 -0.90 0.90 o 1 3 20 13.92 15.17 1.71 o 2 3 20 0.58 -0.44 1.45 o 0 4 20 8.83 8.26 0.89 o 1 4 20 5.64 3.62 1.43 o 2 4 20 0.81 1.28 2.19 o 0 5 20 63.59 68.60 1.73 o 1 5 20 1.77 0.25 2.14 o 2 5 20 25.50 29.91 3.32 o 0 6 20 6.78 5.19 1.29 o 1 6 20 5.31 3.53 1.36 o 2 6 20 4.34 6.36 2.39 o 0 7 20 30.44 40.23 1.54 o 1 7 20 8.38 7.63 2.03 o 0 8 20 93.05 85.74 5.01 o 1 8 20 13.40 13.93 5.33 o 1 0 21 74.15 80.68 3.92 o 2 0 21 12.83 13.15 2.59 o 0 1 21 8.74 7.09 0.89 o 1 1 21 17.12 14.54 2.33 o 2 1 21 23.15 23.83 3.76 o 0 2 21 41.79 33.47 1.31 o 1 2 21 15.66 12.87 2.36 o 2 2 21 0.68 -0.81 1.49 o 0 3 21 4.18 2.11 0.84 o 1 3 21 3.41 -0.11 2.05 o 2 3 21 11.99 16.76 2.73 o 0 4 21 3.84 0.60 1.03 o 1 4 21 1.73 -0.32 1.42 o 0 5 21 8.57 8.86 1.24 o 1 5 21 3.87 1.59 2.20 o 0 6 21 40.23 41.71 2.51 o 1 6 21 30.53 28.31 2.40 o 0 0 22 165.55 168.72 10.20 o 0 1 22 27.06 24.59 1.26 o 1 1 22 18.29 13.38 2.41 o 0 2 22 1.54 -0.80 0.80 o 1 2 22 4.01 1.51 2.24 o 0 3 22 0.01 -0.92 0.92 o