#------------------------------------------------------------------------------ #$Date: 2011-10-06 14:27:20 +0300 (Thu, 06 Oct 2011) $ #$Revision: 27511 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/12/2231246.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231246_Fobs loop_ _publ_author_name 'Betz, Richard' 'Gerber, Thomas' 'Hosten, Eric' 'Schalekamp, Henk' _publ_section_title ; Pyridine-2,3-diamine ; _journal_coeditor_code OM2449 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2154 _journal_volume 67 _journal_year 2011 _space_group_IT_number 106 _symmetry_space_group_name_Hall 'P 4c -2ab' _symmetry_space_group_name_H-M 'P 42 b c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 16.4670 _cell_length_b 16.4670 _cell_length_c 3.9064 _exptl_crystal_F_000 464.00 _reflns_d_resolution_high 0.7501 _[local]_cod_data_source_file om2449Isup3.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ba262_s in P4(2)bc' _shelx_refln_list_code 4 _shelx_f_calc_maximum 85.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x, z+1/2' '-x, -y, z' 'y, -x, z+1/2' '-x+1/2, y+1/2, z' '-y+1/2, -x+1/2, z+1/2' 'x+1/2, -y+1/2, z' 'y+1/2, x+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 1327.29 743.86 311.54 o 0 2 0 394.28 383.17 4.68 o 1 2 0 146.02 136.91 0.96 o 1 3 0 21.49 21.98 0.36 o 2 3 0 557.45 507.42 4.00 o 3 3 0 240.37 251.22 3.91 o 0 4 0 1266.12 1289.05 16.95 o 1 4 0 0.23 0.50 0.22 o 2 4 0 59.86 53.52 1.13 o 3 4 0 744.20 669.15 4.98 o 4 4 0 3930.76 3832.01 48.70 o 1 5 0 0.27 0.45 0.21 o 2 5 0 102.18 93.63 0.69 o 3 5 0 1129.61 1060.64 8.00 o 4 5 0 1564.85 1502.39 18.03 o 5 5 0 641.71 603.62 11.03 o 0 6 0 124.69 136.95 1.46 o 1 6 0 15.76 16.41 0.40 o 2 6 0 651.74 717.92 5.44 o 3 6 0 745.02 741.78 7.31 o 4 6 0 105.45 112.43 1.27 o 5 6 0 970.99 1023.89 12.65 o 6 6 0 990.33 1022.78 19.93 o 1 7 0 378.52 408.25 2.86 o 2 7 0 1524.31 1675.91 11.13 o 3 7 0 20.88 19.35 0.48 o 4 7 0 26.37 23.62 0.50 o 5 7 0 0.04 -0.13 0.30 o 6 7 0 15.72 14.39 0.47 o 7 7 0 256.88 284.02 7.35 o 0 8 0 2992.99 3418.19 34.03 o 1 8 0 1066.51 1139.77 8.55 o 2 8 0 288.14 298.78 2.21 o 3 8 0 74.34 95.18 0.98 o 4 8 0 726.04 847.88 10.16 o 5 8 0 65.99 76.28 1.32 o 6 8 0 8.73 7.37 0.38 o 7 8 0 31.34 31.61 0.64 o 8 8 0 15.83 19.66 0.88 o 1 9 0 477.62 498.66 4.27 o 2 9 0 168.79 181.27 1.31 o 3 9 0 298.71 318.25 2.59 o 4 9 0 171.54 191.45 1.85 o 5 9 0 29.41 32.63 0.74 o 6 9 0 12.21 10.36 0.42 o 7 9 0 68.45 67.29 1.42 o 8 9 0 402.27 412.07 6.66 o 9 9 0 1133.49 1135.51 32.31 o 0 10 0 0.00 -0.31 0.54 o 1 10 0 436.21 476.62 3.53 o 2 10 0 817.46 962.90 6.93 o 3 10 0 77.90 85.91 0.73 o 4 10 0 171.92 171.30 1.72 o 5 10 0 2.81 4.00 0.40 o 6 10 0 1.23 0.63 0.36 o 7 10 0 6.97 7.67 0.46 o 8 10 0 17.98 16.66 0.62 o 9 10 0 25.83 26.07 0.74 o 10 10 0 970.11 963.64 25.37 o 1 11 0 67.51 72.67 0.71 o 2 11 0 128.45 136.16 1.62 o 3 11 0 65.52 59.18 0.77 o 4 11 0 59.66 59.77 0.95 o 5 11 0 39.82 38.69 0.79 o 6 11 0 42.00 47.49 0.74 o 7 11 0 2.47 0.56 0.34 o 8 11 0 42.47 39.53 0.93 o 9 11 0 0.76 0.01 0.61 o 10 11 0 710.78 686.39 12.08 o 11 11 0 39.22 43.06 1.39 o 0 12 0 48.07 54.32 1.17 o 1 12 0 175.15 191.66 1.42 o 2 12 0 204.15 209.27 1.87 o 3 12 0 2.18 3.15 0.45 o 4 12 0 600.83 599.39 6.68 o 5 12 0 1.37 0.23 0.42 o 6 12 0 97.96 94.77 1.36 o 7 12 0 22.50 20.93 0.78 o 8 12 0 251.15 248.55 4.20 o 9 12 0 383.00 348.22 5.78 o 10 12 0 12.47 12.54 0.72 o 11 12 0 68.84 66.26 1.45 o 12 12 0 9.46 11.29 1.02 o 1 13 0 185.65 180.72 1.46 o 2 13 0 49.18 46.86 0.94 o 3 13 0 159.78 151.13 1.34 o 4 13 0 1721.29 1645.65 15.68 o 5 13 0 0.43 -0.53 0.53 o 6 13 0 218.55 199.34 1.66 o 7 13 0 0.85 -0.16 0.51 o 8 13 0 0.31 -0.51 0.51 o 9 13 0 48.31 47.79 1.39 o 10 13 0 4.34 2.79 0.54 o 11 13 0 13.58 12.66 0.75 o 12 13 0 71.93 65.60 1.28 o 13 13 0 124.16 120.09 4.40 o 0 14 0 76.93 72.12 1.37 o 1 14 0 0.31 -0.54 0.54 o 2 14 0 283.97 281.88 1.80 o 3 14 0 593.79 576.25 3.13 o 4 14 0 0.05 0.15 0.52 o 5 14 0 3.75 4.15 0.53 o 6 14 0 27.82 32.72 0.83 o 7 14 0 0.01 -0.51 0.51 o 8 14 0 0.09 -0.50 0.50 o 9 14 0 18.86 14.31 0.65 o 10 14 0 6.94 7.33 0.71 o 11 14 0 127.08 114.23 2.04 o 12 14 0 58.16 55.41 1.14 o 13 14 0 15.84 14.66 0.82 o 14 14 0 70.16 65.05 1.76 o 1 15 0 4.14 3.08 0.56 o 2 15 0 256.37 244.85 1.82 o 3 15 0 128.22 135.08 1.33 o 4 15 0 14.55 15.68 0.65 o 5 15 0 1.81 1.11 0.55 o 6 15 0 1029.23 966.75 10.91 o 7 15 0 61.36 57.39 0.92 o 8 15 0 28.35 25.68 0.76 o 9 15 0 41.80 37.47 1.02 o 10 15 0 0.08 -0.36 0.68 o 11 15 0 0.02 -0.68 0.68 o 12 15 0 19.76 16.57 0.84 o 13 15 0 0.00 -0.48 0.74 o 14 15 0 3.92 2.82 0.80 o 15 15 0 2.43 1.48 1.17 o 0 16 0 19.90 16.14 1.27 o 1 16 0 4.81 4.22 0.61 o 2 16 0 114.69 105.44 1.13 o 3 16 0 138.82 143.05 1.31 o 4 16 0 51.50 59.58 1.24 o 5 16 0 297.24 286.58 2.47 o 6 16 0 3.56 4.75 0.57 o 7 16 0 88.40 89.08 1.31 o 8 16 0 6.70 6.68 0.69 o 9 16 0 0.12 -0.24 0.68 o 10 16 0 7.49 7.33 0.76 o 11 16 0 40.53 39.17 1.13 o 12 16 0 99.94 102.31 1.44 o 13 16 0 0.85 0.82 0.78 o 14 16 0 1.69 1.36 0.81 o 15 16 0 5.64 5.43 0.86 o 1 17 0 0.20 0.16 0.61 o 2 17 0 22.16 23.86 0.93 o 3 17 0 5.27 6.67 0.63 o 4 17 0 367.35 326.79 4.16 o 5 17 0 0.17 0.66 0.83 o 6 17 0 0.03 0.66 0.56 o 7 17 0 5.18 6.63 0.71 o 8 17 0 14.76 14.28 0.78 o 9 17 0 31.64 34.06 1.05 o 10 17 0 45.45 44.82 1.92 o 11 17 0 2.67 3.26 0.78 o 12 17 0 6.42 8.19 0.83 o 13 17 0 12.95 14.09 0.92 o 0 18 0 40.34 41.73 2.17 o 1 18 0 22.43 21.93 2.00 o 2 18 0 3.31 3.12 0.81 o 3 18 0 92.47 92.48 2.55 o 4 18 0 6.85 7.38 0.72 o 5 18 0 50.56 48.71 1.44 o 6 18 0 12.52 9.72 0.82 o 7 18 0 11.42 13.66 0.78 o 8 18 0 21.39 23.75 0.94 o 9 18 0 0.60 -0.31 0.82 o 10 18 0 27.83 34.76 1.69 o 11 18 0 15.82 16.92 0.92 o 12 18 0 45.01 52.85 1.30 o 1 19 0 13.11 17.95 2.58 o 2 19 0 2.58 7.15 2.05 o 3 19 0 22.49 24.04 3.31 o 4 19 0 15.98 18.02 1.85 o 5 19 0 1.10 2.74 0.93 o 6 19 0 15.78 14.71 1.35 o 7 19 0 39.08 42.65 1.53 o 8 19 0 3.65 3.43 0.77 o 9 19 0 3.62 6.09 1.10 o 10 19 0 1.09 0.17 0.80 o 11 19 0 123.49 142.18 2.67 o 0 20 0 34.07 53.14 6.60 o 1 20 0 0.51 2.71 1.46 o 2 20 0 22.35 35.02 4.00 o 3 20 0 12.22 18.41 3.33 o 4 20 0 15.23 16.31 3.57 o 5 20 0 0.01 6.26 3.09 o 6 20 0 10.42 11.66 1.92 o 7 20 0 2.53 2.11 0.76 o 8 20 0 0.05 0.17 0.78 o 9 20 0 28.74 32.05 1.53 o 1 21 0 11.67 30.41 8.34 o 2 21 0 22.91 37.25 5.05 o 3 21 0 22.80 29.59 3.53 o 4 21 0 9.91 23.40 4.31 o 5 21 0 21.36 29.45 3.66 o 6 21 0 14.56 15.62 0.97 o 1 2 1 562.27 514.32 3.35 o 1 3 1 7316.60 7104.40 41.27 o 2 3 1 1477.53 1374.10 8.09 o 0 4 1 3361.94 3245.96 37.82 o 1 4 1 1680.38 1554.00 10.34 o 2 4 1 5.15 5.73 0.16 o 3 4 1 836.87 885.33 5.59 o 1 5 1 242.99 261.94 1.89 o 2 5 1 59.25 64.91 0.82 o 3 5 1 398.04 417.43 3.40 o 4 5 1 66.89 74.24 0.55 o 0 6 1 290.03 295.15 4.48 o 1 6 1 185.82 196.63 2.00 o 2 6 1 168.29 162.19 1.42 o 3 6 1 108.19 117.33 1.12 o 4 6 1 1046.96 1146.80 10.15 o 5 6 1 711.77 723.28 6.02 o 1 7 1 218.42 234.98 2.25 o 2 7 1 12.09 11.19 0.27 o 3 7 1 229.64 243.14 2.20 o 4 7 1 161.39 172.60 1.66 o 5 7 1 328.89 335.98 2.58 o 6 7 1 203.26 195.33 1.72 o 0 8 1 318.80 338.12 4.32 o 1 8 1 222.31 243.93 2.32 o 2 8 1 1246.01 1398.10 13.44 o 3 8 1 203.99 216.32 1.81 o 4 8 1 17.28 14.26 0.33 o 5 8 1 370.37 362.65 3.31 o 6 8 1 298.16 307.46 2.69 o 7 8 1 99.69 99.53 1.23 o 1 9 1 299.65 318.36 2.44 o 2 9 1 136.56 149.14 1.41 o 3 9 1 246.77 240.12 2.04 o 4 9 1 94.57 88.98 0.82 o 5 9 1 204.84 202.21 1.78 o 6 9 1 43.98 42.05 0.50 o 7 9 1 213.62 218.04 1.82 o 8 9 1 38.25 31.17 0.57 o 0 10 1 996.24 1086.28 17.26 o 1 10 1 285.70 299.95 2.55 o 2 10 1 163.22 161.44 1.42 o 3 10 1 142.26 150.77 1.26 o 4 10 1 26.72 31.06 0.48 o 5 10 1 113.59 118.91 1.05 o 6 10 1 94.91 87.33 0.94 o 7 10 1 89.63 84.46 0.95 o 8 10 1 174.92 184.95 2.04 o 9 10 1 316.45 290.39 2.71 o 1 11 1 468.95 470.09 3.68 o 2 11 1 1.67 2.45 0.37 o 3 11 1 60.70 55.81 0.51 o 4 11 1 201.54 189.06 1.82 o 5 11 1 38.41 40.52 0.54 o 6 11 1 25.67 20.59 0.67 o 7 11 1 8.80 6.71 0.38 o 8 11 1 366.98 363.74 3.61 o 9 11 1 89.68 92.74 0.91 o 10 11 1 69.90 63.23 0.88 o 0 12 1 378.44 377.93 6.12 o 1 12 1 338.43 337.83 2.40 o 2 12 1 358.01 344.53 3.19 o 3 12 1 236.36 243.43 1.54 o 4 12 1 169.74 167.80 1.15 o 5 12 1 43.77 37.04 0.57 o 6 12 1 105.10 104.72 0.99 o 7 12 1 422.35 411.49 4.44 o 8 12 1 119.93 118.15 1.40 o 9 12 1 49.15 45.26 0.66 o 10 12 1 159.06 155.89 1.50 o 11 12 1 276.85 256.08 2.90 o 1 13 1 75.27 74.20 0.75 o 2 13 1 230.01 217.87 1.70 o 3 13 1 281.68 284.87 2.04 o 4 13 1 30.28 28.47 0.56 o 5 13 1 20.56 22.02 0.52 o 6 13 1 437.42 409.82 3.97 o 7 13 1 42.93 43.86 0.64 o 8 13 1 202.92 196.20 1.84 o 9 13 1 116.89 111.21 1.32 o 10 13 1 32.83 31.78 0.64 o 11 13 1 87.14 83.37 1.20 o 12 13 1 9.69 8.65 0.51 o 0 14 1 14.48 13.42 0.81 o 1 14 1 323.11 320.00 2.97 o 2 14 1 0.70 -0.38 0.45 o 3 14 1 181.19 166.28 1.65 o 4 14 1 128.10 136.94 1.24 o 5 14 1 201.65 191.64 1.35 o 6 14 1 72.83 67.12 0.71 o 7 14 1 30.67 28.67 0.64 o 8 14 1 66.96 67.62 0.82 o 9 14 1 226.86 222.15 2.28 o 10 14 1 11.95 10.24 0.51 o 11 14 1 16.60 16.45 0.56 o 12 14 1 26.00 22.08 0.64 o 13 14 1 18.64 15.81 0.58 o 1 15 1 35.13 37.44 0.71 o 2 15 1 57.59 51.79 0.71 o 3 15 1 18.60 16.26 0.56 o 4 15 1 691.44 640.90 4.91 o 5 15 1 104.87 104.59 0.84 o 6 15 1 25.40 23.19 0.59 o 7 15 1 22.51 20.25 0.71 o 8 15 1 52.55 47.56 0.72 o 9 15 1 30.02 30.48 0.69 o 10 15 1 47.94 45.78 0.74 o 11 15 1 22.41 21.50 0.63 o 12 15 1 15.60 16.14 0.58 o 13 15 1 5.38 5.31 0.55 o 14 15 1 8.70 8.19 0.59 o 0 16 1 5.44 5.40 0.93 o 1 16 1 30.32 32.48 0.89 o 2 16 1 9.61 8.55 0.54 o 3 16 1 161.86 159.09 1.62 o 4 16 1 53.67 51.84 0.84 o 5 16 1 73.21 73.88 1.05 o 6 16 1 25.50 22.10 0.59 o 7 16 1 42.02 36.66 0.92 o 8 16 1 26.48 25.79 0.66 o 9 16 1 47.26 44.97 0.75 o 10 16 1 15.58 17.35 0.58 o 11 16 1 2.23 2.30 0.52 o 12 16 1 2.63 2.22 0.54 o 13 16 1 31.03 32.31 0.82 o 14 16 1 22.05 25.35 0.78 o 1 17 1 28.99 34.70 1.59 o 2 17 1 85.59 82.53 1.34 o 3 17 1 22.45 20.21 1.23 o 4 17 1 130.02 136.16 1.97 o 5 17 1 17.92 17.37 0.61 o 6 17 1 51.29 43.92 0.75 o 7 17 1 31.22 34.20 0.71 o 8 17 1 6.79 6.22 0.51 o 9 17 1 18.73 19.92 0.60 o 10 17 1 0.96 1.58 0.51 o 11 17 1 39.33 45.87 0.81 o 12 17 1 6.18 7.39 0.59 o 13 17 1 3.56 1.85 0.59 o 0 18 1 22.93 27.34 3.12 o 1 18 1 1.35 3.78 1.29 o 2 18 1 14.92 14.23 0.69 o 3 18 1 42.64 41.43 0.77 o 4 18 1 5.99 8.02 0.55 o 5 18 1 51.69 52.99 0.87 o 6 18 1 4.17 5.11 0.61 o 7 18 1 78.35 76.30 1.21 o 8 18 1 56.84 65.02 1.01 o 9 18 1 4.66 4.78 0.53 o 10 18 1 33.31 36.36 0.81 o 11 18 1 11.48 10.65 0.67 o 1 19 1 4.61 8.03 1.45 o 2 19 1 4.40 5.35 0.65 o 3 19 1 0.93 1.08 0.56 o 4 19 1 79.14 73.49 0.97 o 5 19 1 4.51 4.13 0.55 o 6 19 1 76.66 77.30 1.40 o 7 19 1 12.81 12.84 0.80 o 8 19 1 24.18 28.33 0.77 o 9 19 1 105.33 119.83 1.19 o 10 19 1 4.07 4.65 0.66 o 0 20 1 7.31 9.97 1.91 o 1 20 1 26.49 31.52 1.65 o 2 20 1 18.25 24.46 1.60 o 3 20 1 22.22 22.17 1.53 o 4 20 1 23.70 27.16 1.22 o 5 20 1 19.83 20.01 0.88 o 6 20 1 12.40 11.27 1.09 o 7 20 1 14.96 19.39 0.78 o 8 20 1 14.80 17.17 0.94 o 1 21 1 23.46 29.54 2.46 o 2 21 1 8.25 16.54 2.68 o 3 21 1 8.28 13.05 2.14 o 4 21 1 25.30 28.88 1.43 o 0 0 2 646.02 598.98 17.32 o 1 1 2 601.58 628.56 5.07 o 0 2 2 1804.51 1727.38 19.28 o 1 2 2 72.19 70.12 1.03 o 2 2 2 133.36 117.81 1.37 o 1 3 2 583.02 575.70 5.33 o 2 3 2 197.68 191.52 1.67 o 3 3 2 2203.43 2284.57 21.12 o 0 4 2 313.62 308.22 4.44 o 1 4 2 134.33 133.62 1.19 o 2 4 2 978.99 958.73 6.47 o 3 4 2 157.94 159.81 1.48 o 4 4 2 239.17 254.92 3.28 o 1 5 2 1473.43 1508.92 11.23 o 2 5 2 459.67 449.53 3.43 o 3 5 2 199.37 192.99 1.57 o 4 5 2 32.05 31.38 0.54 o 5 5 2 279.60 286.54 3.78 o 0 6 2 324.52 355.16 3.33 o 1 6 2 526.00 532.12 3.45 o 2 6 2 19.20 21.12 0.38 o 3 6 2 560.23 560.64 4.71 o 4 6 2 3.47 2.97 0.27 o 5 6 2 60.56 60.68 0.98 o 6 6 2 157.74 162.08 2.42 o 1 7 2 154.97 176.94 1.57 o 2 7 2 50.13 48.08 0.45 o 3 7 2 6.99 6.93 0.28 o 4 7 2 48.17 45.73 0.73 o 5 7 2 31.12 31.40 0.62 o 6 7 2 14.18 15.98 0.62 o 7 7 2 307.32 331.28 4.57 o 0 8 2 18.05 18.45 0.72 o 1 8 2 203.31 195.55 1.84 o 2 8 2 147.01 142.98 1.58 o 3 8 2 45.55 39.96 0.61 o 4 8 2 267.39 275.81 2.59 o 5 8 2 79.43 74.51 0.95 o 6 8 2 6.38 6.19 0.37 o 7 8 2 85.92 88.10 1.65 o 8 8 2 8.76 10.72 2.05 o 1 9 2 139.31 135.44 1.93 o 2 9 2 170.31 170.06 1.87 o 3 9 2 98.81 93.20 1.02 o 4 9 2 76.16 67.73 0.91 o 5 9 2 320.22 332.67 4.40 o 6 9 2 10.64 8.38 0.38 o 7 9 2 195.35 199.16 2.47 o 8 9 2 99.39 92.13 0.90 o 9 9 2 25.17 26.65 0.96 o 0 10 2 67.16 67.37 1.36 o 1 10 2 437.33 453.53 5.02 o 2 10 2 133.10 125.52 1.54 o 3 10 2 3.60 3.25 0.35 o 4 10 2 45.96 44.95 0.74 o 5 10 2 1.92 1.32 0.34 o 6 10 2 55.39 57.28 0.85 o 7 10 2 230.44 219.33 1.94 o 8 10 2 91.41 89.18 0.88 o 9 10 2 61.81 55.32 0.69 o 10 10 2 14.67 8.77 0.58 o 1 11 2 88.55 90.70 1.26 o 2 11 2 36.59 35.16 0.59 o 3 11 2 251.20 261.93 2.96 o 4 11 2 540.05 533.29 6.77 o 5 11 2 58.10 55.56 0.65 o 6 11 2 189.27 180.44 2.41 o 7 11 2 35.53 33.58 0.70 o 8 11 2 39.55 35.23 0.65 o 9 11 2 53.95 52.01 0.85 o 10 11 2 33.32 28.40 0.66 o 11 11 2 43.56 37.32 1.13 o 0 12 2 536.51 546.38 9.17 o 1 12 2 285.05 288.86 3.71 o 2 12 2 128.38 128.06 1.57 o 3 12 2 237.98 232.11 2.53 o 4 12 2 110.73 113.17 1.21 o 5 12 2 111.26 107.15 1.28 o 6 12 2 232.48 218.92 1.96 o 7 12 2 55.71 54.82 0.80 o 8 12 2 29.84 30.85 0.62 o 9 12 2 170.56 159.85 1.82 o 10 12 2 7.70 7.33 0.48 o 11 12 2 13.85 12.10 0.72 o 12 12 2 51.49 47.69 2.16 o 1 13 2 162.30 165.37 2.07 o 2 13 2 6.85 6.53 0.40 o 3 13 2 4.12 3.91 0.40 o 4 13 2 119.83 108.56 1.32 o 5 13 2 21.21 22.02 0.61 o 6 13 2 2.92 1.80 0.47 o 7 13 2 7.33 5.75 0.52 o 8 13 2 121.55 115.49 1.23 o 9 13 2 39.35 38.22 0.98 o 10 13 2 69.17 63.72 0.96 o 11 13 2 7.97 5.71 0.73 o 12 13 2 13.97 15.38 0.95 o 13 13 2 8.56 9.17 0.91 o 0 14 2 391.77 398.85 7.52 o 1 14 2 215.29 210.11 2.72 o 2 14 2 27.47 26.81 0.67 o 3 14 2 81.10 81.41 1.36 o 4 14 2 3.80 2.50 0.46 o 5 14 2 0.62 0.77 0.48 o 6 14 2 5.06 4.85 0.59 o 7 14 2 172.52 167.57 2.36 o 8 14 2 27.83 28.92 0.76 o 9 14 2 44.88 44.59 1.45 o 10 14 2 69.95 70.73 1.36 o 11 14 2 97.68 96.44 2.36 o 12 14 2 3.11 3.55 0.55 o 13 14 2 16.90 19.36 0.75 o 14 14 2 25.62 24.90 1.35 o 1 15 2 11.03 10.55 0.53 o 2 15 2 4.94 3.78 0.48 o 3 15 2 11.37 11.36 0.55 o 4 15 2 11.15 11.16 0.60 o 5 15 2 31.96 29.92 1.13 o 6 15 2 24.81 23.84 0.92 o 7 15 2 61.16 58.71 1.43 o 8 15 2 273.09 267.35 3.19 o 9 15 2 9.11 10.45 0.61 o 10 15 2 69.31 69.21 1.83 o 11 15 2 13.76 13.97 0.69 o 12 15 2 35.19 35.64 1.52 o 13 15 2 24.79 26.42 0.94 o 0 16 2 120.15 117.33 2.64 o 1 16 2 55.06 51.66 1.07 o 2 16 2 11.17 10.92 0.60 o 3 16 2 35.17 34.80 0.98 o 4 16 2 23.05 21.49 0.96 o 5 16 2 25.82 25.59 0.77 o 6 16 2 19.92 19.91 0.79 o 7 16 2 111.86 117.74 1.62 o 8 16 2 61.19 64.63 0.95 o 9 16 2 63.03 63.73 0.96 o 10 16 2 18.55 17.64 0.71 o 11 16 2 15.79 14.13 0.72 o 12 16 2 1.01 1.51 0.67 o 1 17 2 0.13 1.46 0.63 o 2 17 2 15.84 17.69 1.50 o 3 17 2 3.89 4.63 0.73 o 4 17 2 19.89 17.30 1.07 o 5 17 2 25.95 24.56 0.99 o 6 17 2 27.24 28.46 1.16 o 7 17 2 9.15 10.38 0.64 o 8 17 2 12.02 14.19 0.77 o 9 17 2 56.10 64.12 1.06 o 10 17 2 23.65 21.59 0.82 o 11 17 2 7.34 6.89 0.81 o 0 18 2 16.69 18.20 1.68 o 1 18 2 0.76 0.83 0.59 o 2 18 2 33.16 39.12 1.45 o 3 18 2 20.83 19.40 1.24 o 4 18 2 42.37 47.71 1.64 o 5 18 2 55.40 57.70 1.40 o 6 18 2 41.15 42.83 1.39 o 7 18 2 9.43 11.53 0.79 o 8 18 2 17.41 17.44 0.77 o 9 18 2 26.30 27.84 0.93 o 1 19 2 21.65 30.52 1.97 o 2 19 2 21.60 24.56 1.82 o 3 19 2 17.23 21.70 1.81 o 4 19 2 50.39 48.24 1.47 o 5 19 2 58.07 60.53 2.06 o 6 19 2 9.24 10.05 1.05 o 7 19 2 17.32 22.29 2.17 o 0 20 2 75.26 90.21 3.16 o 1 20 2 9.23 16.82 3.70 o 2 20 2 26.25 29.85 2.71 o 3 20 2 76.06 86.02 2.69 o 0 2 3 140.16 133.43 1.56 o 1 2 3 206.35 194.99 1.43 o 1 3 3 57.18 59.18 0.71 o 2 3 3 42.30 39.40 0.58 o 0 4 3 859.54 836.52 14.41 o 1 4 3 149.87 145.43 1.48 o 2 4 3 220.16 223.17 2.33 o 3 4 3 21.51 21.33 0.60 o 1 5 3 208.95 207.11 2.10 o 2 5 3 83.07 82.66 1.02 o 3 5 3 153.10 159.07 1.80 o 4 5 3 2.03 2.56 0.42 o 0 6 3 282.64 265.23 3.03 o 1 6 3 112.93 104.80 1.13 o 2 6 3 364.75 370.40 2.56 o 3 6 3 165.58 163.79 1.84 o 4 6 3 0.90 0.28 0.39 o 5 6 3 8.98 7.60 0.43 o 1 7 3 92.89 91.07 0.94 o 2 7 3 30.95 30.94 0.61 o 3 7 3 116.39 114.19 1.00 o 4 7 3 46.93 42.14 0.70 o 5 7 3 33.15 32.05 0.70 o 6 7 3 104.82 101.42 1.20 o 0 8 3 616.10 631.76 5.51 o 1 8 3 27.63 26.26 0.63 o 2 8 3 240.11 235.09 1.76 o 3 8 3 161.24 158.77 1.41 o 4 8 3 47.94 45.04 0.75 o 5 8 3 62.00 61.15 0.94 o 6 8 3 88.93 82.05 1.00 o 7 8 3 87.57 84.74 1.13 o 1 9 3 44.07 43.32 0.62 o 2 9 3 8.99 8.43 0.47 o 3 9 3 160.34 162.59 1.55 o 4 9 3 287.17 281.98 2.63 o 5 9 3 46.23 45.13 0.93 o 6 9 3 35.48 31.11 0.79 o 7 9 3 26.72 25.36 1.13 o 8 9 3 3.83 1.13 0.58 o 0 10 3 163.58 163.28 2.26 o 1 10 3 17.21 15.01 0.53 o 2 10 3 4.13 2.00 0.43 o 3 10 3 262.75 262.52 3.00 o 4 10 3 59.70 62.56 0.90 o 5 10 3 35.87 31.72 0.99 o 6 10 3 25.90 22.34 1.20 o 7 10 3 47.73 41.51 1.14 o 8 10 3 75.42 66.27 1.05 o 9 10 3 14.63 10.77 0.81 o 1 11 3 8.51 8.01 0.44 o 2 11 3 127.92 122.85 1.26 o 3 11 3 11.09 8.45 0.52 o 4 11 3 178.13 180.04 2.56 o 5 11 3 80.78 82.35 1.04 o 6 11 3 162.74 154.29 1.25 o 7 11 3 9.42 8.96 0.72 o 8 11 3 102.13 95.72 1.29 o 9 11 3 21.65 16.70 1.45 o 10 11 3 2.99 0.86 0.94 o 0 12 3 314.89 315.48 4.49 o 1 12 3 63.06 60.65 0.92 o 2 12 3 191.76 194.10 1.55 o 3 12 3 3.96 2.49 0.47 o 4 12 3 148.78 147.01 2.07 o 5 12 3 3.99 3.82 0.71 o 6 12 3 16.30 12.25 0.96 o 7 12 3 9.32 8.16 0.89 o 8 12 3 4.01 1.85 0.72 o 9 12 3 22.38 21.97 1.31 o 10 12 3 2.06 0.61 0.70 o 11 12 3 26.18 22.92 1.77 o 1 13 3 14.99 13.71 0.70 o 2 13 3 59.89 61.66 1.49 o 3 13 3 0.83 -0.45 0.50 o 4 13 3 121.24 117.61 1.42 o 5 13 3 19.20 18.83 1.38 o 6 13 3 31.64 27.53 1.38 o 7 13 3 42.14 39.90 1.78 o 8 13 3 60.79 61.23 1.48 o 9 13 3 24.38 19.82 1.33 o 10 13 3 65.27 67.31 2.05 o 11 13 3 15.42 14.21 1.56 o 12 13 3 32.23 28.09 2.60 o 0 14 3 20.40 18.08 1.69 o 1 14 3 53.07 53.00 1.21 o 2 14 3 37.18 32.42 1.30 o 3 14 3 4.61 4.62 1.10 o 4 14 3 15.77 15.23 1.20 o 5 14 3 10.16 9.75 1.21 o 6 14 3 31.13 26.94 1.63 o 7 14 3 25.78 27.36 1.64 o 8 14 3 29.61 29.88 1.69 o 9 14 3 23.34 18.92 1.65 o 10 14 3 21.20 22.57 1.72 o 11 14 3 27.79 26.95 1.51 o 1 15 3 26.28 27.19 1.55 o 2 15 3 38.16 40.97 1.95 o 3 15 3 40.52 43.10 2.64 o 4 15 3 7.35 8.25 1.37 o 5 15 3 1.12 1.48 0.79 o 6 15 3 6.31 6.85 1.05 o 7 15 3 9.37 7.85 1.85 o 8 15 3 18.04 16.10 1.62 o 9 15 3 38.55 38.44 2.29 o 0 16 3 11.67 14.06 4.53 o 1 16 3 36.90 41.15 1.55 o 2 16 3 37.23 42.90 2.80 o 3 16 3 8.67 12.95 2.38 o 4 16 3 17.95 21.74 1.99 o 5 16 3 0.50 1.96 1.18 o 6 16 3 36.67 38.50 2.51 o 7 16 3 19.42 18.95 2.10 o 8 16 3 12.51 13.17 1.27 o 1 17 3 36.19 42.55 2.57 o 2 17 3 38.36 43.28 2.91 o 3 17 3 16.62 21.33 2.93 o 4 17 3 11.31 14.07 2.42 o 5 17 3 10.67 16.29 3.00 o 0 0 4 41.95 43.75 4.32 o 1 1 4 27.75 28.15 2.61 o 0 2 4 55.04 57.34 2.96 o 1 2 4 4.67 7.60 1.55 o 2 2 4 184.76 186.81 2.22 o 1 3 4 11.20 14.46 1.95 o 2 3 4 55.60 61.14 2.04 o 3 3 4 54.81 54.88 2.87 o 0 4 4 37.31 42.57 3.29 o 1 4 4 25.97 28.33 2.47 o 2 4 4 100.43 101.85 1.58 o 3 4 4 63.13 68.54 1.27 o 4 4 4 83.22 90.81 1.89 o 1 5 4 54.40 61.30 2.08 o 2 5 4 2.32 2.53 0.98 o 3 5 4 68.46 75.59 1.67 o 4 5 4 10.75 10.50 0.99 o 5 5 4 4.55 3.39 0.94 o 0 6 4 400.96 422.00 2.76 o 1 6 4 20.49 21.80 1.71 o 2 6 4 49.51 50.35 1.47 o 3 6 4 19.22 19.96 2.04 o 4 6 4 20.32 17.70 1.25 o 5 6 4 12.72 12.76 1.08 o 6 6 4 19.75 16.39 1.23 o 1 7 4 17.01 17.25 1.23 o 2 7 4 35.97 40.17 1.51 o 3 7 4 44.11 47.05 1.39 o 4 7 4 51.40 51.68 1.32 o 5 7 4 6.56 6.50 0.90 o 6 7 4 9.60 8.87 0.79 o 7 7 4 31.46 32.10 2.51 o 0 8 4 168.93 175.18 2.77 o 1 8 4 84.22 88.95 1.40 o 2 8 4 179.45 180.89 1.64 o 3 8 4 117.33 119.96 1.81 o 4 8 4 19.89 18.97 1.50 o 5 8 4 23.90 20.57 1.87 o 6 8 4 0.98 0.64 0.67 o 7 8 4 14.24 11.72 1.06 o 8 8 4 109.27 106.88 2.88 o 1 9 4 29.43 24.56 2.00 o 2 9 4 54.23 55.02 1.70 o 3 9 4 5.02 6.17 1.20 o 4 9 4 14.39 15.13 1.50 o 5 9 4 20.00 20.18 2.13 o 6 9 4 80.76 78.31 2.43 o 7 9 4 8.70 7.64 1.47 o 8 9 4 1.52 -1.39 1.39 o 9 9 4 11.97 8.68 2.47 o 0 10 4 9.65 8.86 2.16 o 1 10 4 82.72 87.71 2.56 o 2 10 4 97.74 102.15 2.38 o 3 10 4 9.07 9.55 1.53 o 4 10 4 13.20 16.52 2.11 o 5 10 4 65.72 64.67 2.13 o 6 10 4 40.93 38.32 2.89 o 7 10 4 45.20 41.21 2.34 o 8 10 4 4.48 2.11 1.88 o 9 10 4 2.61 -0.91 1.18 o 1 11 4 20.85 20.58 2.25 o 2 11 4 57.33 67.44 2.67 o 3 11 4 23.85 22.27 2.28 o 4 11 4 182.43 182.60 3.69 o 5 11 4 2.53 2.48 1.59 o 6 11 4 103.72 113.90 2.11 o 7 11 4 41.54 40.41 3.04 o 8 11 4 2.75 -0.12 1.15 o 0 12 4 58.75 64.27 2.60 o 1 12 4 9.87 14.40 2.67 o 2 12 4 93.19 104.53 2.59 o 3 12 4 11.93 13.05 1.74 o 4 12 4 44.30 51.19 3.22 o 5 12 4 13.96 17.29 3.10 o 6 12 4 38.13 41.39 3.79 o 7 12 4 4.67 3.98 2.35 o 1 13 4 0.12 5.16 3.03 o 2 13 4 36.58 38.67 2.44 o 3 13 4 1.87 2.60 1.82 o 4 13 4 10.27 13.65 2.71 o 5 13 4 23.62 29.67 4.30 o 0 14 4 33.81 49.08 8.41 o 1 14 4 14.44 28.02 6.60 o 0 2 5 5.78 3.38 1.18 o 1 2 5 16.64 13.77 0.93 o 1 3 5 101.79 97.52 1.70 o 2 3 5 9.29 8.70 0.88 o 0 4 5 151.59 180.43 5.77 o 1 4 5 16.57 19.09 2.43 o 2 4 5 19.41 17.02 0.91 o 3 4 5 16.22 13.84 0.90 o 1 5 5 65.20 77.19 3.96 o 2 5 5 1.31 1.17 1.13 o 3 5 5 89.74 85.48 2.38 o 0 6 5 5.86 7.48 1.79 o