#------------------------------------------------------------------------------ #$Date: 2011-10-06 14:27:20 +0300 (Thu, 06 Oct 2011) $ #$Revision: 27511 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/12/2231256.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231256_Fobs loop_ _publ_author_name 'Zou, Qin' 'Wang, Jian-fei' 'Lin, Jian-li' _publ_section_title ; Aqua(4-carboxypyridine-2,6-dicarboxylato-\k^3^O^2^,N,O^6^)(1,10-phenanthroline-\k^2^N,N')nickel(II) ; _journal_coeditor_code PV2419 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1043 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.874 _cell_angle_gamma 90.000 _cell_length_a 6.8387 _cell_length_b 13.4214 _cell_length_c 19.6758 _exptl_crystal_F_000 952.00 _reflns_d_resolution_high 0.7706 _[local]_cod_data_source_file pv2419Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Ni(Hptc)(phen)(H2O)] in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 263.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 64222.39 71603.39 805.49 o 3 0 0 2171.87 2163.22 29.69 o 4 0 0 12347.80 12546.77 135.13 o 5 0 0 23.32 28.91 7.03 o 6 0 0 285.01 295.99 14.07 o 7 0 0 2.02 6.37 24.35 o 8 0 0 5.44 -2.16 25.36 o 1 1 0 11360.98 10443.16 55.93 o 2 1 0 1155.60 1094.90 11.75 o 3 1 0 9865.12 9676.62 103.65 o 4 1 0 183.69 168.65 10.37 o 5 1 0 418.25 443.75 13.62 o 6 1 0 354.78 346.59 12.52 o 7 1 0 1057.64 1330.13 44.11 o 8 1 0 340.69 0.46 18.84 o 0 2 0 17.41 34.90 6.07 o 1 2 0 1954.88 1786.22 19.96 o 2 2 0 293.16 355.26 10.28 o 3 2 0 1455.92 1386.24 24.14 o 4 2 0 3144.45 3121.03 39.17 o 5 2 0 1348.36 1407.58 26.08 o 6 2 0 141.64 143.33 15.80 o 7 2 0 876.20 1025.47 53.37 o 8 2 0 120.73 59.22 43.32 o 1 3 0 3667.98 3643.72 37.03 o 2 3 0 470.05 461.16 13.43 o 3 3 0 9302.71 9062.08 70.34 o 4 3 0 332.63 344.46 14.01 o 5 3 0 1083.67 1185.05 53.36 o 6 3 0 344.89 404.57 21.44 o 7 3 0 372.47 349.45 63.89 o 8 3 0 87.51 52.14 42.20 o 0 4 0 104.58 116.57 17.04 o 1 4 0 131.64 153.59 12.65 o 2 4 0 101.15 86.47 10.13 o 3 4 0 798.82 785.45 17.36 o 4 4 0 1893.18 1941.42 29.89 o 5 4 0 1073.34 1203.29 26.56 o 6 4 0 112.88 105.89 32.77 o 7 4 0 294.10 184.47 125.51 o 8 4 0 64.79 -1.86 21.79 o 1 5 0 605.30 453.93 18.43 o 2 5 0 764.43 750.75 17.94 o 3 5 0 496.16 442.74 15.30 o 4 5 0 1470.68 1424.41 25.83 o 5 5 0 144.18 147.68 21.73 o 6 5 0 295.46 281.54 28.18 o 7 5 0 156.16 139.94 53.42 o 8 5 0 7.92 2.97 27.08 o 0 6 0 97.44 90.66 18.54 o 1 6 0 109.55 110.46 14.02 o 2 6 0 646.75 630.21 22.45 o 3 6 0 327.12 356.79 20.07 o 4 6 0 787.43 794.21 22.87 o 5 6 0 8.75 22.76 13.06 o 6 6 0 1578.86 1739.61 38.75 o 7 6 0 95.63 -0.28 20.37 o 8 6 0 184.99 -2.42 24.62 o 1 7 0 3350.14 3290.60 43.34 o 2 7 0 525.43 505.29 24.09 o 3 7 0 379.87 359.65 18.72 o 4 7 0 62.88 68.56 15.02 o 5 7 0 41.24 64.65 18.41 o 6 7 0 45.01 44.76 18.05 o 7 7 0 0.39 -14.33 17.90 o 8 7 0 46.43 26.57 40.85 o 0 8 0 84.51 120.40 25.09 o 1 8 0 1531.92 1559.20 38.74 o 2 8 0 10.62 16.23 14.16 o 3 8 0 0.21 13.46 13.06 o 4 8 0 38.54 33.06 16.01 o 5 8 0 15.43 2.88 11.48 o 6 8 0 75.82 122.62 22.82 o 7 8 0 0.53 2.13 22.83 o 1 9 0 426.41 376.74 25.64 o 2 9 0 219.41 235.74 26.43 o 3 9 0 47.86 53.91 16.65 o 4 9 0 58.27 80.80 20.91 o 5 9 0 2.12 -2.04 14.19 o 6 9 0 11.56 -1.72 19.16 o 7 9 0 14.18 12.72 19.53 o 0 10 0 60.50 36.73 26.84 o 1 10 0 178.02 198.07 25.16 o 2 10 0 37.35 63.74 21.37 o 3 10 0 854.39 849.68 35.14 o 4 10 0 1.82 26.36 17.90 o 5 10 0 205.24 191.29 41.98 o 6 10 0 51.63 25.26 23.25 o 7 10 0 11.57 5.50 19.60 o 1 11 0 175.23 169.65 26.39 o 2 11 0 220.85 181.67 41.49 o 3 11 0 0.84 -1.07 10.81 o 4 11 0 6.71 8.83 15.68 o 5 11 0 1.82 10.77 18.71 o 6 11 0 116.87 50.43 30.64 o 0 12 0 41.98 18.98 28.83 o 1 12 0 25.74 12.75 21.14 o 2 12 0 2.09 2.42 13.67 o 3 12 0 106.85 88.05 24.36 o 4 12 0 184.01 187.13 27.30 o 5 12 0 45.34 13.83 22.09 o 6 12 0 173.63 100.55 52.18 o 1 13 0 879.83 965.68 46.65 o 2 13 0 186.79 171.28 26.87 o 3 13 0 45.52 56.28 25.95 o 4 13 0 11.56 8.74 19.97 o 5 13 0 179.49 50.26 37.03 o 0 14 0 779.71 729.26 61.18 o 1 14 0 440.01 408.28 52.42 o 2 14 0 442.49 524.27 35.88 o 3 14 0 14.93 1.43 18.87 o 4 14 0 111.82 84.39 36.75 o 5 14 0 61.68 41.22 36.73 o 1 15 0 714.27 810.09 47.72 o 2 15 0 1.41 -5.39 21.45 o 3 15 0 1193.54 1277.86 53.05 o 4 15 0 32.40 27.19 25.84 o 0 16 0 773.21 816.14 74.36 o 1 16 0 1.90 11.35 26.62 o 2 16 0 67.12 76.25 33.77 o 3 16 0 3.94 -7.28 23.62 o 1 17 0 404.66 409.38 48.96 o -8 1 1 40.08 4.24 19.94 o -7 1 1 57.69 50.32 23.51 o -6 1 1 84.30 73.88 30.68 o -5 1 1 91.46 97.87 8.76 o -4 1 1 1199.99 1169.22 18.56 o -3 1 1 845.16 955.37 27.89 o -2 1 1 3349.03 3281.12 28.94 o -1 1 1 1517.16 1377.89 14.28 o 1 1 1 233.97 197.73 4.32 o 2 1 1 31228.84 31307.63 572.75 o 3 1 1 686.98 705.07 17.62 o 4 1 1 3162.98 3336.85 35.59 o 5 1 1 3.23 6.19 6.56 o 6 1 1 213.60 235.40 10.43 o 7 1 1 24.30 18.98 10.84 o 8 1 1 5.01 26.30 26.68 o -8 2 1 3.27 0.35 14.76 o -7 2 1 185.71 159.93 63.77 o -6 2 1 94.23 102.74 9.76 o -5 2 1 634.24 616.93 26.71 o -4 2 1 323.93 358.24 12.07 o -3 2 1 1990.07 2019.08 32.51 o -2 2 1 835.90 789.80 13.07 o -1 2 1 2313.88 2201.65 22.21 o 0 2 1 398.75 411.88 7.53 o 1 2 1 7716.32 7419.89 44.71 o 2 2 1 407.54 407.68 10.18 o 3 2 1 813.54 898.37 16.60 o 4 2 1 105.45 122.65 11.23 o 5 2 1 118.37 128.82 9.78 o 6 2 1 10.16 8.68 12.35 o 7 2 1 675.54 772.61 25.90 o 8 2 1 75.78 35.43 31.36 o -8 3 1 161.84 -0.53 17.42 o -7 3 1 118.49 61.21 29.42 o -6 3 1 139.39 162.91 10.90 o -5 3 1 7.80 20.20 26.58 o -4 3 1 861.80 843.85 21.32 o -3 3 1 546.93 550.45 18.84 o -2 3 1 2157.93 2081.38 27.57 o -1 3 1 57.85 65.92 10.47 o 0 3 1 6210.69 5913.18 49.50 o 1 3 1 983.64 867.27 15.12 o 2 3 1 187.14 183.91 9.50 o 3 3 1 2016.17 2063.75 24.93 o 4 3 1 657.68 736.06 18.34 o 5 3 1 4.81 -22.79 32.71 o 6 3 1 15.28 18.55 11.29 o 7 3 1 339.49 410.56 25.53 o 8 3 1 1.78 -7.15 22.56 o -8 4 1 0.89 3.25 26.78 o -7 4 1 962.70 1049.26 80.75 o -6 4 1 15.71 33.52 27.85 o -5 4 1 1229.17 1375.42 27.09 o -4 4 1 29.47 36.70 10.40 o -3 4 1 2581.78 2408.59 28.75 o -2 4 1 30.53 25.77 11.49 o -1 4 1 3732.30 3629.53 42.71 o 0 4 1 248.21 219.90 14.79 o 1 4 1 6.88 12.03 8.30 o 2 4 1 140.65 141.68 11.12 o 3 4 1 5089.27 5171.60 45.70 o 4 4 1 443.80 456.11 17.61 o 5 4 1 257.16 266.60 23.21 o 6 4 1 181.60 214.46 42.16 o 7 4 1 434.97 448.72 29.83 o 8 4 1 42.63 -1.55 20.61 o -8 5 1 489.80 581.63 166.56 o -7 5 1 91.66 -1.55 23.99 o -6 5 1 295.66 296.71 27.49 o -5 5 1 8.72 15.03 10.89 o -4 5 1 7852.96 8452.39 82.30 o -3 5 1 22.61 30.34 9.64 o -2 5 1 1474.64 1317.28 26.88 o -1 5 1 2063.45 1938.33 28.28 o 0 5 1 2067.08 1929.33 33.26 o 1 5 1 887.05 786.90 20.85 o 2 5 1 59.17 44.34 9.14 o 3 5 1 359.38 311.13 18.34 o 4 5 1 466.73 460.79 20.10 o 5 5 1 119.22 119.97 16.23 o 6 5 1 42.81 55.32 34.07 o 7 5 1 120.19 121.92 43.20 o 8 5 1 87.75 1.40 21.63 o -8 6 1 110.30 3.63 26.15 o -7 6 1 113.10 5.62 29.02 o -6 6 1 122.47 135.82 19.01 o -5 6 1 87.07 76.86 16.64 o -4 6 1 591.46 625.66 23.01 o -3 6 1 88.71 62.46 15.66 o -2 6 1 215.39 211.95 16.95 o -1 6 1 1436.63 1228.07 29.39 o 0 6 1 795.48 867.60 21.78 o 1 6 1 145.82 104.24 14.46 o 2 6 1 44.37 33.71 14.51 o 3 6 1 3677.33 3584.32 44.42 o 4 6 1 1619.54 1696.07 32.53 o 5 6 1 7.40 23.99 13.84 o 6 6 1 940.69 1048.91 37.18 o 7 6 1 0.95 -0.29 20.79 o 8 6 1 142.41 2.63 24.59 o -8 7 1 35.81 14.88 37.66 o -7 7 1 155.62 89.82 43.70 o -6 7 1 164.61 170.15 28.59 o -5 7 1 278.28 337.20 22.79 o -4 7 1 3371.60 3467.90 47.47 o -3 7 1 15.43 25.02 11.82 o -2 7 1 5629.57 5354.03 61.49 o -1 7 1 2262.69 2171.51 37.28 o 0 7 1 10706.83 10566.49 96.74 o 1 7 1 623.75 579.13 21.76 o 2 7 1 4180.28 3951.78 45.57 o 3 7 1 118.94 114.67 16.80 o 4 7 1 1894.41 1853.51 35.08 o 5 7 1 698.71 753.54 27.38 o 6 7 1 738.41 818.32 37.04 o 7 7 1 30.49 40.01 22.22 o 8 7 1 7.97 9.10 34.91 o -7 8 1 204.61 110.55 55.95 o -6 8 1 11.35 -9.52 20.35 o -5 8 1 799.35 887.40 29.84 o -4 8 1 76.26 92.39 20.05 o -3 8 1 2889.89 2819.12 43.67 o -2 8 1 39.18 30.77 17.29 o -1 8 1 7967.31 7674.72 81.28 o 0 8 1 729.58 701.71 25.46 o 1 8 1 5598.64 5471.68 63.44 o 2 8 1 1721.43 1595.32 31.98 o 3 8 1 4900.68 4939.18 56.27 o 4 8 1 392.16 454.35 27.74 o 5 8 1 671.45 760.82 31.66 o 6 8 1 191.82 180.04 29.14 o 7 8 1 167.48 117.72 54.79 o -7 9 1 44.78 23.61 26.01 o -6 9 1 303.06 217.63 142.00 o -5 9 1 158.89 166.59 22.06 o -4 9 1 801.52 841.55 29.25 o -3 9 1 183.33 163.36 19.83 o -2 9 1 3073.26 3140.46 55.52 o -1 9 1 0.24 10.62 14.44 o 0 9 1 3760.69 3622.81 53.54 o 1 9 1 2716.98 2603.37 52.24 o 2 9 1 1888.97 1826.32 36.57 o 3 9 1 248.39 245.03 23.45 o 4 9 1 376.11 433.50 26.22 o 5 9 1 445.24 584.65 30.22 o 6 9 1 416.75 536.05 33.38 o 7 9 1 221.43 137.44 70.79 o -7 10 1 324.59 330.04 119.07 o -6 10 1 100.06 61.92 32.31 o -5 10 1 1142.29 1382.73 46.47 o -4 10 1 64.46 80.16 24.39 o -3 10 1 2021.20 2132.82 44.46 o -2 10 1 903.66 873.80 41.38 o -1 10 1 10537.08 10466.63 113.46 o 0 10 1 499.06 485.94 31.87 o 1 10 1 8538.12 8453.66 101.21 o 2 10 1 1525.99 1502.82 37.44 o 3 10 1 9071.04 9060.47 104.70 o 4 10 1 138.43 157.71 22.19 o 5 10 1 1376.06 1589.21 48.50 o 6 10 1 32.33 20.38 20.74 o 7 10 1 308.31 156.66 77.49 o -6 11 1 430.03 495.68 100.72 o -5 11 1 23.53 8.00 16.52 o -4 11 1 2248.81 2364.14 56.23 o -3 11 1 454.20 493.48 28.99 o -2 11 1 738.19 861.18 38.18 o -1 11 1 2779.72 2670.76 54.15 o 0 11 1 4572.21 4514.14 69.13 o 1 11 1 2.04 10.19 17.29 o 2 11 1 4370.28 4384.21 63.77 o 3 11 1 368.37 393.79 27.32 o 4 11 1 939.95 998.33 36.26 o 5 11 1 2143.84 2327.38 51.01 o 6 11 1 650.10 715.69 92.78 o -6 12 1 56.04 42.37 28.28 o -5 12 1 506.65 628.28 37.39 o -4 12 1 1166.88 1187.39 48.76 o -3 12 1 260.99 306.57 30.45 o -2 12 1 403.74 371.05 33.48 o -1 12 1 654.35 683.14 36.61 o 0 12 1 15.26 25.98 22.42 o 1 12 1 506.30 467.96 33.87 o 2 12 1 58.32 80.81 21.88 o 3 12 1 559.70 612.46 32.84 o 4 12 1 1722.02 1811.81 47.13 o 5 12 1 129.29 44.84 29.26 o 6 12 1 321.71 300.20 117.12 o -5 13 1 117.60 42.36 31.15 o -4 13 1 216.52 257.12 42.23 o -3 13 1 26.33 16.10 19.96 o -2 13 1 282.94 336.84 41.73 o -1 13 1 14.64 -5.87 22.43 o 0 13 1 613.12 674.03 42.43 o 1 13 1 398.76 377.70 35.51 o 2 13 1 420.15 504.51 33.01 o 3 13 1 37.14 42.33 22.32 o 4 13 1 107.54 26.93 23.22 o 5 13 1 22.33 3.96 18.13 o -5 14 1 117.34 87.20 46.32 o -4 14 1 2.49 0.34 15.74 o -3 14 1 951.42 1017.63 47.01 o -2 14 1 0.98 4.49 18.28 o -1 14 1 749.84 820.93 44.58 o 0 14 1 92.20 87.13 29.08 o 1 14 1 11.01 22.94 26.43 o 2 14 1 40.32 16.23 24.49 o 3 14 1 940.91 1009.34 46.64 o 4 14 1 38.19 35.59 24.69 o 5 14 1 10.55 -4.47 21.93 o -4 15 1 446.38 334.16 101.56 o -3 15 1 0.83 2.89 22.13 o -2 15 1 3.75 22.93 26.73 o -1 15 1 158.75 169.14 35.89 o 0 15 1 271.33 305.48 47.10 o 1 15 1 11.98 2.17 23.47 o 2 15 1 21.04 16.02 23.65 o 3 15 1 76.18 58.55 27.93 o 4 15 1 132.14 45.82 28.02 o -3 16 1 173.98 163.43 36.38 o -2 16 1 53.23 30.48 29.29 o -1 16 1 173.73 208.87 40.67 o 0 16 1 20.76 24.04 33.66 o 1 16 1 288.68 275.17 45.02 o 2 16 1 9.58 -0.69 20.20 o 3 16 1 339.22 308.55 87.44 o -1 17 1 396.19 363.91 56.83 o 0 17 1 110.11 130.34 40.52 o 1 17 1 67.35 60.53 33.79 o -8 0 2 718.49 964.87 68.78 o -7 0 2 143.94 63.90 67.47 o -6 0 2 568.67 657.20 44.55 o -5 0 2 26.13 10.71 25.34 o -4 0 2 5584.66 5575.07 146.00 o -3 0 2 567.63 497.25 32.84 o -2 0 2 867.73 877.42 34.27 o -1 0 2 14602.06 13752.07 184.19 o 1 0 2 12355.24 11022.69 262.19 o 2 0 2 69642.73 76452.20 1158.35 o 3 0 2 4138.34 3935.27 49.38 o 4 0 2 27569.26 28582.03 262.75 o 5 0 2 433.43 434.76 26.44 o 6 0 2 14048.13 15224.52 164.75 o 7 0 2 343.45 430.73 22.16 o 8 0 2 229.38 195.88 147.60 o -8 1 2 51.86 3.24 20.35 o -7 1 2 120.34 75.12 43.49 o -6 1 2 36.26 51.61 22.87 o -5 1 2 1142.80 1241.86 37.99 o -4 1 2 2.27 42.16 14.77 o -3 1 2 761.98 750.17 27.00 o -2 1 2 1439.02 1396.34 15.81 o -1 1 2 36326.84 37962.64 861.72 o 1 1 2 12321.91 11465.78 61.54 o 2 1 2 8891.23 8612.72 65.45 o 3 1 2 9498.13 9357.60 106.72 o 4 1 2 5259.11 5246.70 51.47 o 5 1 2 287.17 314.64 12.02 o 6 1 2 1372.39 1542.65 25.41 o 7 1 2 157.48 190.23 15.65 o 8 1 2 550.43 667.14 124.33 o -8 2 2 406.17 469.67 175.39 o -7 2 2 4.99 11.23 22.59 o -6 2 2 712.70 955.69 41.82 o -5 2 2 9.31 7.46 11.54 o -4 2 2 3200.42 3099.96 39.42 o -3 2 2 2159.16 2151.57 25.34 o -2 2 2 1625.37 1423.61 25.68 o -1 2 2 802.59 751.43 13.85 o 0 2 2 975.73 940.54 11.13 o 1 2 2 401.34 374.84 8.46 o 2 2 2 319.66 258.88 8.08 o 3 2 2 3667.22 3763.10 33.08 o 4 2 2 133.27 147.98 12.57 o 5 2 2 921.90 913.09 21.05 o 6 2 2 201.09 183.37 12.39 o 7 2 2 1433.33 1605.83 31.50 o 8 2 2 20.12 4.66 20.99 o -8 3 2 57.12 4.59 27.32 o -7 3 2 831.60 1056.60 51.69 o -6 3 2 212.22 184.42 13.07 o -5 3 2 1966.80 2149.66 59.94 o -4 3 2 185.77 178.81 14.10 o -3 3 2 2981.51 2756.53 31.70 o -2 3 2 630.44 566.20 16.65 o -1 3 2 17686.98 17167.12 128.87 o 0 3 2 125.96 135.87 8.51 o 1 3 2 3203.03 3059.83 24.24 o 2 3 2 7.24 7.89 6.20 o 3 3 2 5542.52 5548.10 53.61 o 4 3 2 2880.50 2931.68 34.01 o 5 3 2 513.47 500.54 20.58 o 6 3 2 178.01 237.62 19.07 o 7 3 2 6.96 -1.44 12.83 o 8 3 2 78.12 57.74 34.88 o -8 4 2 140.13 1.61 23.05 o -7 4 2 104.20 -2.48 20.58 o -6 4 2 57.91 41.76 29.76 o -5 4 2 377.81 374.90 16.06 o -4 4 2 3571.87 3865.51 44.76 o -3 4 2 521.89 562.99 16.83 o -2 4 2 7252.76 7014.24 66.60 o -1 4 2 16.56 30.53 9.87 o 0 4 2 9.51 11.43 8.26 o 1 4 2 2119.18 2137.91 26.27 o 2 4 2 1549.88 1390.19 20.07 o 3 4 2 54.76 86.59 10.52 o 4 4 2 60.09 118.62 14.84 o 5 4 2 1508.17 1594.70 35.42 o 6 4 2 6.62 13.47 22.79 o 7 4 2 249.46 264.16 49.51 o 8 4 2 4.27 -0.98 19.29 o -8 5 2 16.07 -2.09 23.73 o -7 5 2 234.22 0.96 19.41 o -6 5 2 506.41 468.72 21.85 o -5 5 2 2481.92 2727.23 41.19 o -4 5 2 8.41 18.76 10.76 o -3 5 2 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30.73 18.91 o -3 3 22 16.00 23.09 17.59 o -2 3 22 270.05 272.23 69.40 o -1 3 22 131.15 11.18 18.38 o 0 3 22 594.05 706.02 48.66 o 1 3 22 88.12 -1.78 37.12 o 2 3 22 279.44 2.14 41.05 o 3 3 22 152.78 -0.89 28.14 o -4 4 22 6.81 11.83 16.34 o -3 4 22 102.62 90.25 31.03 o -2 4 22 95.48 59.43 34.72 o -1 4 22 338.30 416.98 81.72 o 0 4 22 192.78 1.27 25.37 o 1 4 22 142.56 3.82 30.28 o 2 4 22 126.57 -0.79 26.74 o 3 4 22 47.52 29.61 44.41 o -3 5 22 6.14 8.84 13.37 o -2 5 22 161.65 59.63 52.30 o -1 5 22 4.13 2.93 20.41 o 0 5 22 167.64 144.93 57.19 o 1 5 22 137.15 6.68 33.04 o 2 5 22 87.76 1.54 47.18 o 3 5 22 91.75 68.06 66.75 o -3 6 22 196.08 136.22 47.31 o -2 6 22 10.19 7.35 19.83 o -1 6 22 7.97 3.01 17.15 o 0 6 22 88.69 48.18 28.70 o 1 6 22 40.74 22.27 21.78 o 2 6 22 30.13 -0.49 26.62 o 3 6 22 110.49 53.09 52.12 o -2 7 22 14.28 14.31 33.66 o -1 7 22 62.14 10.24 21.82 o 0 7 22 180.42 180.41 51.53 o 1 7 22 62.18 59.77 28.72 o 2 7 22 47.96 8.21 53.19 o -2 8 22 28.94 65.31 38.35 o -1 8 22 3.31 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90.14 30.23 o -2 0 24 216.59 16.42 45.33 o 1 0 24 168.99 -2.86 44.26 o -3 1 24 84.47 112.41 20.35 o -2 1 24 185.25 20.35 46.05 o -1 1 24 25.69 19.99 48.90 o 0 1 24 7.11 6.07 44.62 o 1 1 24 167.56 0.36 33.91 o 2 1 24 25.82 -1.78 44.98 o -3 2 24 44.51 74.31 34.00 o -2 2 24 322.10 291.01 185.09 o -1 2 24 167.76 6.25 31.05 o 0 2 24 105.70 -0.71 35.70 o -2 3 24 4.75 4.18 19.00 o -1 3 24 427.24 491.96 290.93 o 0 3 24 1.34 9.80 41.57 o -2 4 24 138.07 -6.69 23.96 o -1 4 24 142.22 15.24 35.46 o 0 4 24 235.51 -4.74 39.19 o 1 4 24 5.63 -8.92 52.83 o -1 5 24 54.27 1.88 24.84 o 0 5 24 111.62 -1.77 29.76 o 1 5 24 64.28 -1.54 30.41 o -1 1 25 68.55 6.78 45.33 o 1 1 25 0.05 0.71 39.27 o 0 2 25 74.15 -3.93 45.33 o 1 2 25 10.11 2.50 46.76 o -1 3 25 16.04 1.78 39.62 o 0 3 25 154.86 -0.71 37.48 o