#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:25:28 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181234 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/12/2231277.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231277_Fobs loop_ _publ_author_name 'Reiss, Guido J.' 'Meyer, Michaela K.' _publ_section_title ; Diisopropylammonium methanesulfonate ; _journal_coeditor_code QM2018 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2169 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.816 _cell_angle_gamma 90.000 _cell_length_a 8.8815 _cell_length_b 8.5354 _cell_length_c 14.5784 _exptl_crystal_F_000 432.00 _reflns_d_resolution_high 0.7108 _cod_data_source_file qm2018Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title EXP_150 _shelx_refln_list_code 4 _shelx_f_calc_maximum 131.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2945.54 2655.18 7.23 o 4 0 0 562.65 642.90 3.80 o 6 0 0 35.47 39.54 0.89 o 8 0 0 822.33 790.62 6.81 o 10 0 0 28.96 26.26 1.96 o 12 0 0 101.98 117.85 3.69 o 2 1 0 524.03 531.96 1.79 o 3 1 0 669.91 772.64 3.84 o 4 1 0 104.34 100.61 1.05 o 5 1 0 53.25 53.99 0.58 o 6 1 0 73.31 64.36 0.73 o 7 1 0 63.54 59.15 0.92 o 8 1 0 0.93 0.23 0.90 o 9 1 0 346.82 337.69 3.05 o 10 1 0 2.91 3.49 1.12 o 11 1 0 6.08 5.53 1.38 o 12 1 0 25.53 25.89 2.29 o 0 2 0 4417.15 4339.13 17.56 o 1 2 0 1928.40 1972.00 9.56 o 2 2 0 226.34 235.02 0.84 o 3 2 0 481.51 499.71 2.75 o 4 2 0 1475.54 1388.67 6.27 o 5 2 0 322.57 338.85 1.95 o 6 2 0 135.93 125.64 0.99 o 7 2 0 162.96 157.01 1.45 o 8 2 0 1437.36 1395.49 6.47 o 9 2 0 46.68 45.61 1.44 o 10 2 0 1.43 0.54 1.13 o 11 2 0 62.56 62.94 1.94 o 12 2 0 16.92 16.47 2.14 o 1 3 0 452.05 517.28 2.86 o 2 3 0 16.91 28.49 0.58 o 3 3 0 430.44 401.23 1.54 o 4 3 0 21.84 27.79 0.42 o 5 3 0 740.87 698.58 5.62 o 6 3 0 526.87 521.38 3.95 o 7 3 0 18.94 17.31 0.94 o 8 3 0 90.32 88.74 1.61 o 9 3 0 280.35 279.25 4.16 o 10 3 0 41.94 42.85 1.61 o 11 3 0 0.46 0.87 1.19 o 0 4 0 373.55 383.36 3.00 o 1 4 0 1001.69 1056.75 5.92 o 2 4 0 301.90 340.38 1.26 o 3 4 0 1178.60 1189.01 3.88 o 4 4 0 1815.49 1808.16 5.58 o 5 4 0 1328.55 1365.49 6.21 o 6 4 0 112.09 108.57 1.38 o 7 4 0 56.03 58.36 1.69 o 8 4 0 297.26 309.74 3.99 o 9 4 0 25.38 24.25 1.43 o 10 4 0 4.18 4.15 1.46 o 11 4 0 51.68 46.90 2.49 o 1 5 0 15.83 23.99 0.53 o 2 5 0 582.06 597.16 3.14 o 3 5 0 156.39 161.82 1.24 o 4 5 0 13.12 13.17 0.66 o 5 5 0 383.49 368.58 2.65 o 6 5 0 156.05 158.63 2.50 o 7 5 0 0.08 2.66 1.67 o 8 5 0 112.78 107.03 2.43 o 9 5 0 8.28 6.89 1.68 o 10 5 0 60.57 61.92 2.71 o 11 5 0 2.84 2.77 1.73 o 0 6 0 317.71 300.60 4.38 o 1 6 0 248.84 267.56 1.64 o 2 6 0 24.62 30.86 0.78 o 3 6 0 360.66 362.95 2.04 o 4 6 0 591.04 562.06 3.34 o 5 6 0 33.34 32.90 1.20 o 6 6 0 3.60 2.58 1.16 o 7 6 0 155.65 160.70 2.77 o 8 6 0 142.51 149.33 2.84 o 9 6 0 45.96 57.29 2.13 o 10 6 0 0.54 0.16 1.84 o 1 7 0 0.14 2.44 0.76 o 2 7 0 227.65 230.83 3.01 o 3 7 0 45.73 54.41 1.12 o 4 7 0 111.71 97.57 1.49 o 5 7 0 48.99 46.56 1.40 o 6 7 0 310.15 281.81 2.93 o 7 7 0 4.68 4.42 1.49 o 8 7 0 15.74 18.29 1.85 o 9 7 0 29.55 34.29 2.60 o 0 8 0 510.18 497.03 4.98 o 1 8 0 265.68 253.06 2.55 o 2 8 0 4.91 8.36 0.93 o 3 8 0 194.82 190.39 2.06 o 4 8 0 52.44 58.22 1.44 o 5 8 0 97.02 97.30 2.00 o 6 8 0 65.34 76.76 1.91 o 7 8 0 78.38 92.91 2.56 o 8 8 0 0.09 0.00 1.70 o 9 8 0 89.18 93.90 2.77 o 1 9 0 35.99 38.48 1.51 o 2 9 0 227.07 216.87 2.50 o 3 9 0 2.84 1.97 1.19 o 4 9 0 28.49 24.09 1.24 o 5 9 0 36.32 33.94 1.63 o 6 9 0 21.72 20.59 1.70 o 7 9 0 15.99 12.17 1.86 o 8 9 0 41.51 41.08 2.39 o 0 10 0 7.28 11.26 2.17 o 1 10 0 161.82 161.92 2.53 o 2 10 0 3.26 4.72 1.23 o 3 10 0 195.16 199.28 3.20 o 4 10 0 9.29 8.56 1.68 o 5 10 0 102.84 116.86 3.68 o 6 10 0 23.86 23.52 2.06 o 1 11 0 32.90 32.75 1.77 o 2 11 0 59.20 54.04 2.18 o 3 11 0 0.22 1.41 1.60 o 4 11 0 21.32 19.93 2.23 o 0 12 0 19.40 19.36 2.25 o -11 0 1 280.65 264.17 7.06 o -9 0 1 4.00 4.76 1.56 o -7 0 1 350.31 348.57 3.33 o -5 0 1 522.53 551.94 4.81 o -3 0 1 1246.24 1139.59 8.44 o 3 0 1 675.45 706.32 2.27 o 5 0 1 1.10 0.26 0.40 o 7 0 1 19.11 18.71 0.92 o 9 0 1 267.14 250.44 3.95 o 11 0 1 397.62 397.91 7.25 o -12 1 1 59.29 65.95 2.50 o -11 1 1 0.85 0.62 1.26 o -10 1 1 734.33 699.34 4.38 o -9 1 1 65.68 59.90 1.43 o -8 1 1 401.54 383.71 2.34 o -7 1 1 56.26 47.34 0.95 o -6 1 1 1.93 4.02 0.55 o -5 1 1 23.86 25.89 0.43 o -4 1 1 4.52 11.22 0.29 o -3 1 1 116.51 107.18 1.03 o -2 1 1 16022.20 15585.50 169.65 o 2 1 1 5112.31 5044.41 22.57 o 3 1 1 415.38 420.22 1.48 o 4 1 1 458.80 476.43 2.45 o 5 1 1 2.69 4.43 0.35 o 6 1 1 1201.15 1149.39 6.26 o 7 1 1 49.49 45.33 0.91 o 8 1 1 710.92 691.51 5.48 o 9 1 1 0.09 0.37 0.94 o 10 1 1 140.20 138.10 3.04 o 11 1 1 7.02 7.07 1.72 o 12 1 1 44.31 40.55 3.15 o -12 2 1 1.16 0.88 1.63 o -11 2 1 216.42 221.84 3.71 o -10 2 1 16.33 17.49 1.22 o -9 2 1 13.23 11.64 1.11 o -8 2 1 60.22 58.81 1.29 o -7 2 1 131.00 133.75 1.42 o -6 2 1 34.88 31.83 0.75 o -5 2 1 25.49 29.60 0.54 o -4 2 1 161.51 164.68 0.87 o -3 2 1 39.20 26.90 0.67 o -2 2 1 10.38 15.14 0.26 o -1 2 1 26.48 35.62 0.50 o 0 2 1 350.89 308.88 2.28 o 1 2 1 3830.82 3760.64 15.08 o 2 2 1 471.06 471.95 2.51 o 3 2 1 23.40 36.02 0.47 o 4 2 1 232.35 233.22 1.51 o 5 2 1 15.16 20.62 0.57 o 6 2 1 0.76 1.78 0.46 o 7 2 1 539.28 531.64 2.56 o 8 2 1 3.39 3.79 1.01 o 9 2 1 158.14 162.10 3.39 o 10 2 1 25.08 24.26 1.51 o 11 2 1 69.86 65.39 2.12 o -11 3 1 54.69 50.49 1.96 o -10 3 1 96.62 100.63 1.82 o -9 3 1 0.08 1.12 1.02 o -8 3 1 51.17 53.32 1.29 o -7 3 1 114.69 113.53 1.77 o -6 3 1 1730.96 1694.59 9.96 o -5 3 1 244.72 245.66 1.89 o -4 3 1 554.81 527.53 2.40 o -3 3 1 51.85 48.10 0.63 o -2 3 1 2746.73 2808.37 13.78 o -1 3 1 17.79 22.67 0.33 o 0 3 1 1366.12 1397.42 5.30 o 1 3 1 956.83 958.67 4.11 o 2 3 1 839.95 827.76 4.05 o 3 3 1 3983.89 4081.17 12.06 o 4 3 1 715.58 737.23 2.82 o 5 3 1 17.86 19.65 0.61 o 6 3 1 1207.24 1197.04 3.90 o 7 3 1 134.37 121.99 1.72 o 8 3 1 1.38 1.33 1.02 o 9 3 1 52.78 54.09 1.54 o 10 3 1 94.95 97.93 2.57 o 11 3 1 78.71 86.18 2.83 o -11 4 1 0.12 0.00 1.58 o -10 4 1 87.69 82.65 2.00 o -9 4 1 51.78 45.98 1.48 o -8 4 1 3.06 3.90 1.18 o -7 4 1 1241.14 1238.00 8.18 o -6 4 1 106.99 109.77 1.43 o -5 4 1 254.76 257.12 1.70 o -4 4 1 275.93 269.62 1.44 o -3 4 1 44.35 65.15 0.69 o -2 4 1 63.19 76.90 0.70 o -1 4 1 755.28 767.83 3.76 o 0 4 1 116.46 107.89 0.90 o 1 4 1 622.73 724.52 3.92 o 2 4 1 416.25 415.31 1.80 o 3 4 1 5.65 9.94 0.46 o 4 4 1 553.94 585.76 1.89 o 5 4 1 711.07 658.97 2.95 o 6 4 1 108.06 98.46 1.43 o 7 4 1 624.60 631.97 5.94 o 8 4 1 216.47 226.57 3.51 o 9 4 1 141.77 144.89 3.08 o 10 4 1 0.80 0.56 1.80 o 11 4 1 0.79 0.72 1.87 o -11 5 1 5.53 9.10 1.82 o -10 5 1 36.40 33.88 1.83 o -9 5 1 17.40 21.70 1.57 o -8 5 1 179.37 178.38 2.88 o -7 5 1 27.38 28.14 1.71 o -6 5 1 899.56 903.33 10.20 o -5 5 1 2214.94 2185.38 12.77 o -4 5 1 89.84 92.39 1.05 o -3 5 1 1.39 1.19 0.40 o -2 5 1 752.99 715.12 3.66 o -1 5 1 5.06 9.02 0.54 o 0 5 1 32.23 24.75 0.59 o 1 5 1 48.61 46.69 0.81 o 2 5 1 130.84 120.87 0.95 o 3 5 1 803.00 836.97 3.71 o 4 5 1 344.42 357.80 2.75 o 5 5 1 0.26 0.00 0.87 o 6 5 1 647.16 634.70 4.60 o 7 5 1 140.18 152.14 3.24 o 8 5 1 0.37 0.62 1.37 o 9 5 1 64.55 66.99 2.32 o 10 5 1 105.27 109.61 2.87 o -10 6 1 123.05 127.26 3.53 o -9 6 1 0.05 0.00 1.65 o -8 6 1 11.22 9.51 1.62 o -7 6 1 62.92 64.29 2.08 o -6 6 1 331.42 312.85 3.99 o -5 6 1 0.02 0.52 1.12 o -4 6 1 490.18 512.89 3.92 o -3 6 1 21.63 21.27 0.87 o -2 6 1 50.96 47.37 0.82 o -1 6 1 6.01 7.94 0.56 o 0 6 1 1.45 3.67 0.54 o 1 6 1 336.71 326.09 1.96 o 2 6 1 334.95 328.60 2.29 o 3 6 1 0.98 0.00 0.65 o 4 6 1 822.32 810.54 6.06 o 5 6 1 0.30 0.20 0.89 o 6 6 1 134.68 127.39 2.47 o 7 6 1 30.02 25.25 1.74 o 8 6 1 308.50 313.19 6.41 o 9 6 1 0.45 1.62 1.78 o 10 6 1 4.31 5.18 1.84 o -10 7 1 40.25 41.71 2.42 o -9 7 1 134.00 137.73 3.06 o -8 7 1 2.46 1.83 1.67 o -7 7 1 10.20 12.16 1.67 o -6 7 1 16.65 21.09 1.52 o -5 7 1 114.24 121.64 2.08 o -4 7 1 0.13 0.33 0.86 o -3 7 1 64.61 52.88 1.24 o -2 7 1 108.25 107.56 1.88 o -1 7 1 1636.60 1587.05 18.88 o 0 7 1 105.69 103.66 1.28 o 1 7 1 0.50 0.06 0.71 o 2 7 1 898.35 907.99 6.58 o 3 7 1 87.41 94.09 1.26 o 4 7 1 3.73 4.85 0.88 o 5 7 1 30.21 30.94 1.27 o 6 7 1 15.59 17.13 1.35 o 7 7 1 78.52 80.18 2.31 o 8 7 1 5.09 5.98 1.73 o 9 7 1 24.37 25.06 1.84 o -9 8 1 1.67 2.18 1.81 o -8 8 1 27.35 27.94 2.04 o -7 8 1 0.11 0.62 1.60 o -6 8 1 13.60 17.42 1.52 o -5 8 1 14.64 16.90 1.40 o -4 8 1 119.56 131.37 2.03 o -3 8 1 2.88 2.29 0.93 o -2 8 1 685.56 688.77 6.28 o -1 8 1 1.80 1.03 0.97 o 0 8 1 341.79 332.04 3.03 o 1 8 1 44.70 40.79 1.18 o 2 8 1 4.57 2.70 0.98 o 3 8 1 0.91 0.88 0.90 o 4 8 1 267.96 250.51 2.61 o 5 8 1 27.88 28.29 1.32 o 6 8 1 0.69 1.88 1.32 o 7 8 1 0.29 0.00 1.63 o 8 8 1 61.96 67.27 2.44 o -8 9 1 5.49 4.33 1.86 o -7 9 1 16.79 15.86 1.89 o -6 9 1 7.56 8.12 1.54 o -5 9 1 84.99 93.25 2.24 o -4 9 1 13.32 14.35 1.38 o -3 9 1 28.82 24.12 1.12 o -2 9 1 13.69 12.46 1.11 o -1 9 1 251.21 246.49 2.79 o 0 9 1 21.29 21.48 1.51 o 1 9 1 282.94 275.66 2.72 o 2 9 1 18.62 23.61 1.28 o 3 9 1 270.94 267.87 3.78 o 4 9 1 0.13 0.43 1.15 o 5 9 1 13.10 12.45 1.53 o 6 9 1 29.45 28.77 1.82 o 7 9 1 143.22 161.01 3.25 o -6 10 1 52.76 51.99 2.40 o -5 10 1 8.15 7.98 1.75 o -4 10 1 84.83 87.31 2.37 o -3 10 1 1.38 0.52 1.64 o -2 10 1 44.86 39.72 1.56 o -1 10 1 4.03 2.95 1.34 o 0 10 1 123.26 113.84 2.25 o 1 10 1 50.88 52.54 1.81 o 2 10 1 0.01 0.00 1.31 o 3 10 1 0.08 0.17 1.34 o 4 10 1 77.01 80.05 2.85 o 5 10 1 0.76 2.30 2.01 o 6 10 1 1.89 0.61 2.11 o -4 11 1 33.52 34.18 2.93 o -3 11 1 13.54 16.87 2.38 o -2 11 1 48.91 50.91 2.00 o -1 11 1 68.66 74.48 1.99 o 0 11 1 79.00 79.50 2.13 o 1 11 1 15.59 15.26 1.57 o 2 11 1 61.12 61.07 2.46 o 3 11 1 179.68 186.06 3.93 o 4 11 1 9.57 6.99 2.32 o -12 0 2 52.63 45.02 2.96 o -10 0 2 880.82 855.32 7.53 o -8 0 2 621.41 593.46 5.41 o -6 0 2 8.74 17.26 0.98 o -4 0 2 658.01 725.38 3.68 o -2 0 2 15732.62 16485.15 241.06 o 2 0 2 1307.42 1238.98 7.77 o 4 0 2 1907.52 1843.82 13.69 o 6 0 2 151.46 147.48 1.47 o 8 0 2 146.95 149.59 2.22 o 10 0 2 46.11 44.82 2.44 o -12 1 2 27.45 28.09 1.84 o -11 1 2 274.23 269.53 3.57 o -10 1 2 12.43 10.57 1.31 o -9 1 2 251.94 250.54 2.35 o -8 1 2 4.45 5.96 0.90 o -7 1 2 37.81 42.57 0.93 o -6 1 2 226.36 205.22 1.09 o -5 1 2 202.31 229.37 1.12 o -4 1 2 903.94 968.24 5.79 o -3 1 2 302.84 292.64 2.32 o -2 1 2 167.11 203.24 2.34 o -1 1 2 3106.33 3338.04 25.65 o 1 1 2 529.62 504.89 4.02 o 2 1 2 1320.06 1364.68 7.57 o 3 1 2 1080.70 1000.35 6.33 o 4 1 2 294.75 306.56 1.95 o 5 1 2 15.58 18.90 0.44 o 6 1 2 14.49 17.47 0.56 o 7 1 2 351.67 343.39 1.85 o 8 1 2 69.79 63.93 1.19 o 9 1 2 1.09 1.12 0.88 o 10 1 2 0.00 0.66 1.35 o 11 1 2 152.67 145.85 3.13 o -12 2 2 70.55 69.27 2.35 o -11 2 2 46.60 46.93 2.02 o -10 2 2 154.48 148.98 2.12 o -9 2 2 47.76 48.03 1.31 o -8 2 2 201.72 210.68 1.96 o -7 2 2 296.63 300.10 2.90 o -6 2 2 1360.59 1278.99 7.08 o -5 2 2 44.45 54.21 0.91 o -4 2 2 307.36 303.70 1.67 o -3 2 2 436.52 505.83 2.71 o -2 2 2 2821.13 2813.38 14.27 o -1 2 2 458.56 534.60 2.28 o 0 2 2 6096.24 6109.21 21.29 o 1 2 2 1671.66 1686.48 7.97 o 2 2 2 196.95 170.27 1.29 o 3 2 2 185.13 196.51 1.16 o 4 2 2 1072.27 1051.88 3.27 o 5 2 2 1.30 3.61 0.39 o 6 2 2 1244.45 1215.96 6.40 o 7 2 2 168.13 168.08 1.60 o 8 2 2 79.29 76.70 1.61 o 9 2 2 21.41 22.02 1.23 o 10 2 2 14.66 14.65 1.57 o 11 2 2 23.68 22.67 2.25 o -12 3 2 9.77 8.57 1.97 o -11 3 2 1.33 0.48 1.39 o -10 3 2 0.01 0.00 1.12 o -9 3 2 176.05 173.63 1.98 o -8 3 2 370.71 357.92 3.11 o -7 3 2 1082.86 1044.50 5.88 o -6 3 2 26.97 23.13 0.82 o -5 3 2 312.98 298.03 1.52 o -4 3 2 32.04 49.05 0.52 o -3 3 2 227.29 255.78 1.80 o -2 3 2 676.04 655.44 2.68 o -1 3 2 809.16 773.53 3.82 o 0 3 2 50.00 43.51 0.44 o 1 3 2 1273.73 1287.71 7.42 o 2 3 2 1140.46 1206.40 6.54 o 3 3 2 660.33 745.69 3.24 o 4 3 2 410.73 439.47 2.09 o 5 3 2 368.07 378.45 2.47 o 6 3 2 89.48 98.01 1.29 o 7 3 2 1233.69 1224.48 5.82 o 8 3 2 45.21 51.49 1.42 o 9 3 2 8.04 11.03 1.75 o 10 3 2 2.61 0.57 1.70 o 11 3 2 50.08 58.74 2.62 o -11 4 2 0.19 0.00 1.84 o -10 4 2 14.94 16.09 1.37 o -9 4 2 3.37 3.00 1.04 o -8 4 2 161.96 162.11 2.08 o -7 4 2 466.47 460.99 5.31 o -6 4 2 665.40 664.73 6.00 o -5 4 2 306.79 283.95 1.52 o -4 4 2 2258.13 2259.03 8.15 o -3 4 2 290.62 286.02 1.29 o -2 4 2 304.33 338.57 2.34 o -1 4 2 276.84 296.59 2.28 o 0 4 2 97.14 87.43 0.70 o 1 4 2 822.84 851.69 2.87 o 2 4 2 2896.37 2957.32 7.23 o 3 4 2 240.00 244.83 1.12 o 4 4 2 177.17 163.16 1.28 o 5 4 2 252.27 263.67 1.90 o 6 4 2 133.81 141.75 1.73 o 7 4 2 0.20 1.12 0.96 o 8 4 2 446.95 447.86 4.35 o 9 4 2 41.55 48.72 2.10 o 10 4 2 10.83 10.73 2.03 o 11 4 2 0.11 0.00 1.77 o -11 5 2 4.45 2.56 1.81 o -10 5 2 2.50 0.20 1.66 o -9 5 2 95.96 106.65 2.76 o -8 5 2 79.55 77.94 2.10 o -7 5 2 169.15 171.12 3.57 o -6 5 2 203.18 202.22 2.28 o -5 5 2 162.24 159.78 1.66 o -4 5 2 807.87 784.48 3.19 o -3 5 2 99.31 101.29 0.86 o -2 5 2 23.70 24.91 0.48 o -1 5 2 38.33 35.68 0.59 o 0 5 2 7.46 12.41 1.02 o 1 5 2 804.98 846.92 4.46 o 2 5 2 5.69 5.87 0.48 o 3 5 2 34.58 22.36 0.68 o 4 5 2 68.92 78.00 1.19 o 5 5 2 261.77 242.90 2.22 o 6 5 2 543.72 548.51 3.41 o 7 5 2 230.08 221.86 3.31 o 8 5 2 0.63 0.00 1.36 o 9 5 2 22.99 24.91 1.91 o 10 5 2 234.46 241.95 4.38 o -10 6 2 62.47 61.84 2.50 o -9 6 2 9.03 9.02 1.85 o -8 6 2 47.29 46.23 1.96 o -7 6 2 76.55 81.69 2.24 o -6 6 2 240.39 249.88 2.87 o -5 6 2 1.96 1.71 1.01 o -4 6 2 81.58 86.64 1.35 o -3 6 2 1265.06 1260.94 4.28 o -2 6 2 46.43 45.82 0.94 o -1 6 2 90.51 98.38 1.05 o 0 6 2 235.15 230.21 1.47 o 1 6 2 324.58 312.06 2.62 o 2 6 2 421.80 415.46 1.92 o 3 6 2 95.53 96.24 1.15 o 4 6 2 193.82 184.87 1.76 o 5 6 2 296.74 330.40 4.34 o 6 6 2 26.94 30.60 1.35 o 7 6 2 8.50 5.02 1.33 o 8 6 2 44.46 43.61 1.90 o 9 6 2 61.00 70.64 2.53 o 10 6 2 43.79 45.39 2.41 o -10 7 2 0.06 0.00 2.07 o -9 7 2 11.83 9.24 2.13 o -8 7 2 14.92 10.91 1.66 o -7 7 2 82.17 81.12 2.30 o -6 7 2 83.60 86.73 2.05 o -5 7 2 41.96 45.99 1.74 o -4 7 2 1010.06 978.78 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