#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:25:46 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181235 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/13/2231303.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231303_Fobs loop_ _publ_author_name 'Saraswathi, B. S.' 'Foro, Sabine' 'Gowda, B. Thimme' _publ_section_title ; N-(2,6-Dichlorophenyl)succinamic acid ; _journal_coeditor_code SJ5173 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1880 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.640 _cell_angle_gamma 90.000 _cell_length_a 4.7130 _cell_length_b 11.9630 _cell_length_c 20.6870 _exptl_crystal_F_000 536.00 _reflns_d_resolution_high 0.8352 _cod_data_source_file sj5173Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' A19 IN P21/N' _shelx_refln_list_code 4 _shelx_f_calc_maximum 182.72 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 41.87 57.66 24.62 o 4 0 0 643.22 465.81 38.76 o 1 1 0 733.74 763.21 10.88 o 2 1 0 757.50 828.69 19.38 o 3 1 0 75.01 35.26 32.53 o 4 1 0 15.53 -21.87 25.46 o 5 1 0 64.82 63.66 59.82 o 1 2 0 492.15 477.76 8.50 o 2 2 0 233.14 209.80 12.55 o 3 2 0 508.77 522.53 21.87 o 4 2 0 33.44 36.88 20.22 o 5 2 0 89.55 56.38 87.84 o 1 3 0 920.30 869.18 9.60 o 2 3 0 0.34 7.62 10.42 o 3 3 0 5.90 -3.93 19.66 o 4 3 0 16.54 36.62 21.37 o 5 3 0 16.95 45.06 63.52 o 1 4 0 1796.34 1826.38 24.70 o 2 4 0 190.95 173.60 11.08 o 3 4 0 739.21 680.17 20.99 o 4 4 0 52.00 71.54 21.50 o 5 4 0 35.29 -16.03 19.58 o 1 5 0 4443.19 4347.34 37.02 o 2 5 0 494.66 565.65 16.46 o 3 5 0 394.89 303.05 18.45 o 4 5 0 124.20 136.70 21.44 o 5 5 0 4.47 3.33 29.89 o 1 6 0 243.79 194.08 6.18 o 2 6 0 263.29 324.79 22.87 o 3 6 0 812.14 763.36 20.80 o 4 6 0 96.23 74.87 28.01 o 5 6 0 0.64 51.99 21.90 o 1 7 0 21.95 37.93 20.96 o 2 7 0 0.06 -6.74 22.96 o 3 7 0 164.44 136.40 27.00 o 4 7 0 53.20 317.40 175.17 o 1 8 0 618.23 723.04 27.38 o 2 8 0 1359.34 1326.88 34.07 o 3 8 0 72.96 -8.83 25.14 o 4 8 0 110.61 123.98 26.30 o 1 9 0 84.45 109.12 24.54 o 2 9 0 26.87 33.53 24.67 o 3 9 0 6.68 29.34 28.01 o 0 10 0 680.64 717.11 27.04 o 1 10 0 1059.35 1105.63 33.06 o 2 10 0 11.44 58.80 26.58 o 4 10 0 0.28 -12.84 23.85 o 1 11 0 265.89 220.93 26.35 o 2 11 0 101.86 143.09 25.70 o 3 11 0 36.29 109.92 25.46 o 0 12 0 67.29 9.86 21.41 o 1 12 0 117.86 253.01 26.29 o 2 12 0 22.13 134.03 27.06 o 3 12 0 45.44 228.26 27.24 o 2 13 0 19.56 61.03 28.51 o 0 14 0 1.51 42.65 22.92 o 1 14 0 131.42 187.54 29.23 o -5 0 1 28.74 17.57 35.62 o -3 0 1 1143.48 1200.43 34.85 o -1 0 1 1402.50 1430.43 25.32 o 1 0 1 4744.89 4585.67 25.34 o 3 0 1 1424.83 1395.65 36.67 o 5 0 1 105.50 138.93 34.16 o -5 1 1 32.76 62.25 36.87 o -4 1 1 84.98 147.45 20.77 o -3 1 1 969.40 912.78 24.47 o -2 1 1 1939.84 1990.74 24.91 o -1 1 1 438.78 522.81 12.54 o 1 1 1 4.21 1.72 7.99 o 2 1 1 1575.73 1616.41 54.37 o 3 1 1 57.72 108.95 18.66 o 4 1 1 77.11 58.75 22.81 o 5 1 1 2.66 16.01 27.08 o -5 2 1 82.54 82.70 53.67 o -4 2 1 50.90 59.44 22.30 o -3 2 1 490.78 478.73 23.99 o -2 2 1 1533.80 1593.12 17.33 o -1 2 1 3312.47 3387.07 33.49 o 0 2 1 3750.89 3555.47 24.80 o 1 2 1 1605.93 1646.86 17.23 o 2 2 1 8.45 10.95 9.53 o 3 2 1 106.59 123.94 20.53 o 4 2 1 212.09 181.26 23.70 o 5 2 1 1.84 17.81 56.32 o -5 3 1 3.65 22.00 23.92 o -4 3 1 15.66 10.44 21.18 o -3 3 1 177.13 205.20 20.94 o -2 3 1 1.66 1.86 8.41 o -1 3 1 12.22 24.52 7.04 o 0 3 1 588.93 524.14 19.76 o 1 3 1 47.27 67.38 7.19 o 2 3 1 9.51 17.53 12.14 o 3 3 1 0.70 9.44 18.27 o 4 3 1 3.15 7.27 22.35 o 5 3 1 155.11 134.36 22.36 o -5 4 1 1.36 -20.45 20.45 o -4 4 1 295.76 312.36 22.06 o -3 4 1 499.18 607.79 27.87 o -2 4 1 300.66 332.43 12.81 o -1 4 1 74.02 48.52 9.01 o 0 4 1 1451.93 1352.20 25.81 o 1 4 1 514.91 504.33 18.28 o 2 4 1 1050.11 1039.18 21.17 o 3 4 1 0.64 -4.37 16.21 o 4 4 1 46.49 84.02 21.99 o 5 4 1 31.48 0.19 20.59 o -5 5 1 82.00 27.71 46.60 o -4 5 1 68.26 50.42 21.44 o -3 5 1 0.84 -9.61 16.92 o -2 5 1 174.04 198.03 14.21 o -1 5 1 277.79 309.95 11.71 o 0 5 1 1451.34 1240.02 27.61 o 1 5 1 1316.33 1363.72 23.44 o 2 5 1 164.31 135.48 12.76 o 3 5 1 116.84 117.74 16.01 o 4 5 1 274.42 245.14 21.46 o 5 5 1 1.80 53.71 24.23 o -5 6 1 14.01 4.74 67.69 o -4 6 1 145.53 214.57 73.93 o -3 6 1 2237.00 2191.65 28.04 o -2 6 1 87.43 104.89 22.79 o -1 6 1 3.50 -4.69 4.69 o 1 6 1 2433.98 2574.80 31.84 o 2 6 1 1176.49 1055.68 28.44 o 3 6 1 330.95 295.17 18.05 o 4 6 1 13.76 170.51 85.62 o 5 6 1 11.41 62.59 71.42 o -4 7 1 4.57 172.47 133.35 o -3 7 1 242.93 336.46 30.78 o -2 7 1 73.51 86.61 23.44 o -1 7 1 263.91 286.49 23.08 o 1 7 1 0.62 1.27 17.92 o 2 7 1 22.21 6.02 21.39 o 3 7 1 105.03 156.47 26.73 o 4 7 1 140.38 252.34 83.48 o -3 8 1 8.74 48.03 27.83 o -2 8 1 99.61 146.51 26.15 o -1 8 1 49.33 49.06 23.22 o 0 8 1 51.77 111.89 19.35 o 1 8 1 66.83 91.06 20.67 o 2 8 1 654.52 657.45 28.15 o 3 8 1 0.03 7.05 23.14 o 4 8 1 13.08 51.38 25.84 o -3 9 1 91.32 30.63 29.76 o -2 9 1 65.16 53.22 26.89 o -1 9 1 65.04 57.71 24.10 o 0 9 1 0.10 27.82 19.93 o 1 9 1 5.16 -21.48 21.48 o 2 9 1 187.08 169.18 25.26 o 3 9 1 218.02 164.62 27.65 o 4 9 1 2.60 163.94 25.37 o -4 10 1 211.69 362.08 33.42 o -3 10 1 39.65 80.10 27.95 o -2 10 1 77.31 23.65 26.52 o -1 10 1 4.26 63.14 23.99 o 0 10 1 3.92 28.96 21.82 o 1 10 1 170.11 141.84 25.08 o 2 10 1 104.18 56.87 25.73 o 3 10 1 36.56 97.95 24.05 o -3 11 1 44.43 -28.76 28.76 o -2 11 1 0.15 -27.72 27.72 o -1 11 1 144.76 171.32 27.68 o 0 11 1 306.62 320.52 42.51 o 1 11 1 34.25 75.93 25.34 o 2 11 1 24.74 -25.79 25.81 o 3 11 1 271.88 248.80 29.48 o -3 12 1 0.02 -27.66 27.66 o -1 12 1 72.84 -6.18 26.31 o 0 12 1 4.06 186.94 95.56 o 1 12 1 0.80 -25.14 25.14 o -1 13 1 40.39 26.70 28.50 o 0 13 1 0.16 -7.93 17.14 o 1 13 1 41.03 109.52 18.10 o -1 14 1 30.73 -23.34 29.19 o 0 14 1 17.12 59.23 25.24 o 1 14 1 90.85 344.82 24.93 o -4 0 2 105.70 133.06 32.75 o -2 0 2 2500.05 2513.56 34.91 o 2 0 2 879.60 723.24 19.68 o 4 0 2 755.98 824.29 40.91 o -5 1 2 23.95 -23.75 23.75 o -4 1 2 117.77 69.98 22.37 o -3 1 2 910.69 947.30 24.98 o -2 1 2 575.29 646.39 14.54 o -1 1 2 6137.33 6744.94 21.81 o 1 1 2 1681.88 1623.92 19.47 o 2 1 2 1001.80 941.64 11.29 o 3 1 2 220.37 202.89 19.19 o 4 1 2 0.31 26.84 20.21 o 5 1 2 142.77 175.45 38.09 o -5 2 2 0.53 37.17 31.23 o -4 2 2 10.12 -3.47 25.31 o -3 2 2 8.53 13.18 19.85 o -2 2 2 25.23 37.82 6.37 o -1 2 2 9845.28 9923.24 38.14 o 0 2 2 44.38 58.58 10.06 o 1 2 2 5002.63 5074.58 38.96 o 2 2 2 527.23 534.00 11.10 o 3 2 2 167.94 167.69 19.25 o 4 2 2 214.88 159.18 21.52 o 5 2 2 263.43 339.25 112.11 o -5 3 2 5.18 -17.86 23.52 o -4 3 2 2.11 -11.44 19.63 o -3 3 2 141.26 139.88 20.48 o -2 3 2 91.27 67.34 8.41 o -1 3 2 3164.42 3227.81 15.83 o 0 3 2 1098.66 1097.14 13.50 o 1 3 2 1184.51 1150.20 17.96 o 2 3 2 948.56 902.59 12.74 o 3 3 2 29.41 59.20 20.09 o 4 3 2 3.16 -11.59 20.35 o 5 3 2 7.35 -29.69 31.45 o -5 4 2 2.31 31.63 67.76 o -4 4 2 1.47 14.33 54.69 o -3 4 2 4.32 3.04 17.02 o -2 4 2 1929.07 1900.38 20.78 o -1 4 2 2832.90 2912.11 56.79 o 0 4 2 1361.26 1309.78 14.70 o 1 4 2 21.94 9.28 10.88 o 2 4 2 1761.93 1673.48 27.16 o 3 4 2 511.44 477.37 19.88 o 4 4 2 345.19 419.80 22.38 o 5 4 2 95.05 133.50 30.65 o -5 5 2 11.02 7.18 21.84 o -4 5 2 37.50 -3.36 19.74 o -3 5 2 47.58 68.67 18.44 o -2 5 2 193.04 247.07 16.28 o -1 5 2 7326.43 7714.80 54.99 o 0 5 2 2057.92 2320.80 41.01 o 1 5 2 187.21 241.54 13.52 o 2 5 2 6.22 -0.41 8.37 o 3 5 2 0.75 7.85 14.70 o 4 5 2 64.12 68.98 26.51 o 5 5 2 115.40 200.36 26.16 o -5 6 2 18.31 78.62 26.49 o -4 6 2 31.12 18.54 20.90 o -3 6 2 305.86 335.65 37.36 o -2 6 2 359.43 334.78 25.97 o -1 6 2 29.94 31.38 4.22 o 0 6 2 1422.57 1409.42 34.66 o 1 6 2 47.37 52.37 15.28 o 2 6 2 226.57 181.80 19.87 o 3 6 2 233.66 270.31 17.08 o 4 6 2 382.35 453.33 30.99 o 5 6 2 2.09 51.81 38.15 o -4 7 2 120.45 105.36 53.42 o -3 7 2 16.78 -27.27 27.27 o -2 7 2 28.72 3.48 23.95 o -1 7 2 1174.84 1272.63 30.97 o 0 7 2 10.28 45.98 16.77 o 1 7 2 1462.53 1445.73 28.00 o 2 7 2 739.39 744.70 26.77 o 3 7 2 29.16 13.21 23.12 o 4 7 2 2.16 -1.81 24.79 o -4 8 2 8.59 49.15 26.70 o -3 8 2 16.63 38.71 30.27 o -2 8 2 91.62 96.12 25.87 o -1 8 2 495.50 449.68 26.53 o 0 8 2 1779.85 1819.98 30.77 o 1 8 2 0.49 -7.52 18.92 o 2 8 2 48.22 23.27 23.18 o 3 8 2 7.16 20.26 22.55 o -4 9 2 6.81 113.90 28.63 o -3 9 2 1.95 51.31 29.56 o -2 9 2 60.98 5.70 25.27 o -1 9 2 24.06 28.82 24.41 o 0 9 2 572.05 550.65 24.17 o 1 9 2 470.30 541.13 24.70 o 2 9 2 155.28 209.60 25.33 o 3 9 2 144.70 253.84 25.12 o 4 9 2 25.78 146.48 26.28 o -3 10 2 12.16 14.36 31.03 o -2 10 2 5.29 50.06 27.14 o -1 10 2 12.07 4.83 24.70 o 0 10 2 11.02 -21.47 21.47 o 1 10 2 19.30 45.86 21.87 o 2 10 2 117.18 66.07 26.06 o 3 10 2 660.74 556.56 30.36 o -3 11 2 18.43 76.88 31.22 o -2 11 2 1.63 98.91 26.47 o -1 11 2 10.75 -2.53 27.43 o 0 11 2 0.75 19.49 22.08 o 1 11 2 426.83 388.01 27.04 o 2 11 2 226.63 219.26 29.36 o -3 12 2 1.43 37.25 26.34 o -2 12 2 0.00 136.76 27.41 o -1 12 2 0.95 7.67 25.07 o 0 12 2 890.39 915.24 27.91 o 1 12 2 0.97 91.81 16.60 o 2 12 2 0.54 46.61 24.65 o 3 12 2 11.45 41.97 20.84 o -2 13 2 31.37 166.82 26.71 o 0 13 2 0.97 15.09 15.17 o 1 13 2 83.00 179.47 111.86 o 2 13 2 25.26 17.94 26.97 o -1 14 2 66.43 223.43 28.30 o 0 14 2 5.41 27.08 41.16 o 1 14 2 23.38 122.51 86.15 o -5 0 3 437.81 473.70 38.58 o -3 0 3 1.42 0.00 30.51 o -1 0 3 33386.70 34508.51 52.37 o 1 0 3 13542.85 13256.40 32.20 o 3 0 3 165.81 174.27 24.68 o 5 0 3 174.25 36.42 36.79 o -5 1 3 2.69 11.68 35.73 o -4 1 3 1.43 -7.69 26.32 o -3 1 3 159.76 177.30 21.21 o -2 1 3 23.63 59.45 8.53 o -1 1 3 11079.63 11696.63 28.68 o 0 1 3 4237.06 4558.92 30.24 o 1 1 3 3747.85 3626.83 33.67 o 2 1 3 2251.77 2154.16 23.47 o 3 1 3 302.33 258.50 20.58 o 4 1 3 19.10 15.37 20.30 o 5 1 3 41.75 39.37 49.95 o -5 2 3 58.86 5.74 23.09 o -4 2 3 1083.18 1067.43 57.32 o -3 2 3 107.41 127.28 19.97 o -2 2 3 511.29 551.78 9.75 o -1 2 3 2187.49 2132.55 23.54 o 0 2 3 24.25 19.96 8.29 o 1 2 3 335.98 309.19 6.44 o 2 2 3 1862.55 1828.03 16.47 o 3 2 3 19.25 20.82 18.44 o 4 2 3 23.62 15.92 31.13 o 5 2 3 5.06 18.65 72.64 o -5 3 3 14.24 80.67 36.04 o -4 3 3 0.47 25.15 23.62 o -3 3 3 645.86 674.22 75.51 o -2 3 3 5.81 -0.21 4.90 o -1 3 3 406.44 397.56 8.65 o 0 3 3 606.29 621.13 12.06 o 1 3 3 82.11 69.62 4.71 o 2 3 3 45.52 41.30 9.03 o 3 3 3 275.88 235.54 26.89 o 4 3 3 41.12 24.64 19.83 o 5 3 3 0.15 -21.43 21.43 o -5 4 3 4.98 26.78 26.76 o -4 4 3 587.93 564.58 32.33 o -3 4 3 30.29 46.10 19.54 o -2 4 3 1486.87 1371.44 19.56 o -1 4 3 413.51 362.88 10.47 o 0 4 3 2445.19 2400.22 40.66 o 1 4 3 477.97 484.99 11.88 o 2 4 3 2951.09 3094.88 25.40 o 3 4 3 643.06 545.46 21.35 o 4 4 3 9.69 34.38 19.72 o 5 4 3 115.73 162.34 26.11 o -5 5 3 0.25 133.61 26.93 o -4 5 3 699.52 728.91 52.24 o -3 5 3 10.15 16.13 20.40 o -2 5 3 596.69 573.64 17.44 o -1 5 3 620.61 626.44 12.32 o 0 5 3 117.52 143.52 11.90 o 1 5 3 1083.24 1082.14 16.90 o 2 5 3 203.10 138.79 9.22 o 3 5 3 143.74 108.92 14.87 o 4 5 3 35.65 7.64 20.91 o 5 5 3 9.90 70.74 20.56 o -5 6 3 0.21 109.81 42.82 o -4 6 3 405.05 402.32 24.21 o -3 6 3 587.09 619.77 21.43 o -2 6 3 49.31 65.38 11.90 o -1 6 3 90.66 61.22 12.63 o 0 6 3 578.67 447.25 14.26 o 1 6 3 1491.18 1424.96 20.58 o 2 6 3 1025.91 929.31 25.78 o 3 6 3 5.04 -14.59 14.59 o 4 6 3 0.84 33.10 25.41 o 5 6 3 2.24 10.47 15.84 o -4 7 3 63.20 141.66 90.80 o -3 7 3 5.50 19.92 30.93 o -2 7 3 103.54 100.88 25.71 o -1 7 3 45.91 46.00 23.87 o 0 7 3 239.77 274.03 31.21 o 1 7 3 509.47 422.35 39.48 o 2 7 3 45.37 54.10 19.99 o 3 7 3 52.14 48.10 21.41 o 4 7 3 49.17 56.08 24.03 o -4 8 3 132.20 296.25 33.24 o -3 8 3 284.94 354.51 33.63 o -2 8 3 71.64 38.57 26.81 o -1 8 3 67.76 34.10 23.61 o 0 8 3 414.11 384.95 55.77 o 1 8 3 773.54 687.89 24.33 o 2 8 3 833.90 731.06 27.46 o 3 8 3 30.15 -5.58 21.31 o -3 9 3 21.34 -28.23 28.78 o -2 9 3 20.93 54.26 28.18 o -1 9 3 142.04 148.57 25.28 o 0 9 3 1.81 18.34 20.64 o 1 9 3 163.77 209.86 21.46 o 2 9 3 9.92 -22.71 22.71 o 3 9 3 10.38 -4.33 21.42 o -4 10 3 24.49 -3.52 22.82 o -3 10 3 12.25 25.99 30.87 o -2 10 3 69.68 86.42 27.93 o -1 10 3 401.38 398.72 29.72 o 0 10 3 1870.22 1936.23 36.49 o 1 10 3 34.97 22.00 20.83 o 2 10 3 143.79 76.10 23.23 o 3 10 3 4.18 -20.01 20.01 o -2 11 3 91.92 -21.01 28.43 o -1 11 3 32.66 -2.53 27.83 o 0 11 3 226.92 177.98 23.65 o 1 11 3 60.07 74.14 24.40 o 2 11 3 70.33 16.56 24.68 o 3 11 3 94.92 179.57 24.13 o -3 12 3 33.18 78.02 27.97 o -2 12 3 58.24 1.04 29.70 o -1 12 3 6.31 53.34 28.36 o 0 12 3 95.35 327.03 117.38 o 1 12 3 9.25 80.01 20.97 o 2 12 3 23.58 1.49 24.10 o -1 13 3 4.84 36.97 30.55 o 0 13 3 17.41 277.60 118.19 o 1 13 3 36.75 97.61 15.74 o 2 13 3 0.63 62.72 27.47 o 0 14 3 107.46 27.06 30.26 o -4 0 4 254.40 179.85 33.13 o -2 0 4 1.20 12.55 23.15 o 0 0 4 200.78 201.50 14.87 o 2 0 4 603.94 745.68 15.49 o 4 0 4 1.36 -26.48 26.48 o -5 1 4 45.20 15.08 28.08 o -4 1 4 221.98 160.94 24.50 o -3 1 4 220.11 201.21 19.09 o -2 1 4 176.24 204.81 10.34 o -1 1 4 564.67 604.33 13.39 o 0 1 4 2735.27 2756.81 51.95 o 1 1 4 4968.16 4322.25 29.44 o 2 1 4 20.81 16.28 8.20 o 3 1 4 335.74 294.25 14.78 o 4 1 4 58.63 116.83 20.64 o 5 1 4 22.71 4.62 39.57 o -5 2 4 5.23 16.90 32.46 o -4 2 4 1.26 30.23 21.30 o -3 2 4 436.31 451.51 22.41 o -2 2 4 2819.74 2909.11 21.00 o -1 2 4 7136.40 7294.99 25.24 o 0 2 4 81.60 66.72 7.72 o 1 2 4 446.07 448.06 5.41 o 2 2 4 2133.76 2455.41 12.74 o 3 2 4 1893.20 1946.14 27.09 o 4 2 4 0.08 14.21 41.62 o 5 2 4 43.93 -8.19 22.02 o -5 3 4 11.94 70.52 38.55 o -4 3 4 209.87 187.98 45.57 o -3 3 4 2.36 -18.70 18.70 o -2 3 4 660.79 722.02 14.54 o -1 3 4 4030.35 4244.92 27.97 o 0 3 4 1301.38 1163.22 18.12 o 1 3 4 274.40 238.45 5.42 o 2 3 4 706.09 674.27 11.53 o 3 3 4 117.24 123.85 24.48 o 4 3 4 802.69 851.22 25.56 o 5 3 4 289.84 244.62 24.08 o -5 4 4 4.30 62.19 30.69 o -4 4 4 215.23 243.56 29.81 o -3 4 4 187.97 198.18 40.56 o -2 4 4 673.12 792.07 14.24 o -1 4 4 94.62 135.48 7.52 o 0 4 4 3000.77 2938.53 36.72 o 1 4 4 163.38 146.81 6.34 o 2 4 4 62.24 58.07 8.65 o 3 4 4 13.95 10.32 13.96 o 4 4 4 9.35 16.97 18.78 o 5 4 4 11.15 68.80 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