#------------------------------------------------------------------------------ #$Date: 2011-10-06 14:27:20 +0300 (Thu, 06 Oct 2011) $ #$Revision: 27511 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/13/2231305.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231305_Fobs loop_ _publ_author_name 'Wang, Chen-Yi' _publ_section_title ; Bis{N-methyl-N'-[1-(pyridin-2-yl)ethylidene]ethane-1,2-diamine}zinc bis(perchlorate) ; _journal_coeditor_code SJ5175 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1038 _journal_page_last m1039 _journal_volume 67 _journal_year 2011 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.461 _cell_angle_gamma 90.000 _cell_length_a 12.7999 _cell_length_b 15.8414 _cell_length_c 13.6869 _exptl_crystal_F_000 1280.00 _reflns_d_resolution_high 0.8766 _[local]_cod_data_source_file sj5175Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21 in P21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 243.28 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 -15 0 45.39 74.76 36.28 o 7 -15 0 178.42 118.19 42.33 o 5 -14 0 384.91 454.63 57.17 o 6 -14 0 41.53 36.28 31.34 o 7 -14 0 144.94 153.93 45.08 o 8 -14 0 13.96 34.63 35.18 o 4 -13 0 73.70 91.81 32.98 o 5 -13 0 483.33 492.02 58.82 o 6 -13 0 84.48 97.85 37.38 o 7 -13 0 430.67 340.84 55.52 o 8 -13 0 122.90 115.45 43.43 o 9 -13 0 9.42 4.40 34.63 o 4 -12 0 159.02 222.64 38.48 o 5 -12 0 1055.68 937.31 78.61 o 6 -12 0 59.94 37.38 33.53 o 7 -12 0 138.45 128.64 39.03 o 8 -12 0 311.68 339.74 55.52 o 9 -12 0 260.69 293.01 54.97 o 10 -12 0 87.75 119.29 46.18 o 3 -11 0 473.31 433.74 47.28 o 4 -11 0 12.43 26.94 25.84 o 5 -11 0 144.08 172.62 37.38 o 6 -11 0 540.05 582.17 62.12 o 7 -11 0 863.40 820.76 75.86 o 8 -11 0 268.09 290.26 51.13 o 9 -11 0 92.49 67.07 38.48 o 10 -11 0 217.54 282.02 56.62 o 11 -11 0 75.23 168.77 53.32 o 3 -10 0 701.76 753.69 57.17 o 4 -10 0 2050.81 2297.91 119.84 o 5 -10 0 121.31 133.04 33.53 o 6 -10 0 67.40 64.87 30.79 o 7 -10 0 392.51 468.93 57.17 o 8 -10 0 548.23 578.88 65.42 o 9 -10 0 83.77 81.91 38.48 o 10 -10 0 414.60 561.28 70.92 o 11 -10 0 2.76 5.50 36.83 o 2 -9 0 2881.56 2907.57 136.34 o 3 -9 0 70.71 48.93 21.99 o 4 -9 0 1026.71 941.70 65.97 o 5 -9 0 287.70 253.98 36.83 o 6 -9 0 1176.61 1128.61 81.36 o 7 -9 0 426.85 447.49 54.97 o 8 -9 0 891.22 1050.00 84.66 o 9 -9 0 61.89 76.41 36.28 o 10 -9 0 543.27 704.77 76.41 o 11 -9 0 14.29 35.18 39.03 o 12 -9 0 132.45 91.81 48.93 o 2 -8 0 162.41 140.73 24.74 o 3 -8 0 9.15 25.84 18.69 o 4 -8 0 171.12 104.45 25.84 o 5 -8 0 345.48 474.97 48.38 o 6 -8 0 1016.96 892.78 67.07 o 7 -8 0 110.78 91.26 31.88 o 8 -8 0 958.11 1195.13 86.86 o 9 -8 0 74.30 85.76 37.93 o 10 -8 0 208.06 234.19 52.23 o 11 -8 0 11.70 39.58 37.38 o 12 -8 0 127.49 30.24 40.13 o 2 -7 0 4134.07 3734.38 157.23 o 3 -7 0 5629.97 5176.90 207.25 o 4 -7 0 91.67 139.63 26.39 o 5 -7 0 124.69 128.64 28.04 o 6 -7 0 1030.21 1129.16 76.96 o 7 -7 0 140.80 106.10 33.53 o 8 -7 0 27.67 29.69 30.24 o 9 -7 0 42.79 28.59 32.98 o 10 -7 0 232.72 184.16 46.18 o 11 -7 0 355.58 406.26 65.42 o 12 -7 0 185.14 156.68 51.68 o 13 -7 0 17.17 -18.14 35.18 o 1 -6 0 3699.01 3338.57 133.04 o 2 -6 0 1709.56 1937.83 89.61 o 3 -6 0 3145.69 2957.60 133.04 o 4 -6 0 2997.25 2955.40 124.79 o 5 -6 0 1463.43 1479.35 86.31 o 6 -6 0 325.66 214.95 34.08 o 7 -6 0 689.75 689.37 63.22 o 8 -6 0 998.60 818.56 73.12 o 9 -6 0 452.84 457.93 59.37 o 10 -6 0 154.48 134.14 41.23 o 11 -6 0 1.94 37.38 36.83 o 12 -6 0 110.26 114.90 46.18 o 13 -6 0 245.59 242.44 59.37 o 1 -5 0 12810.66 9408.79 332.59 o 2 -5 0 466.69 617.91 39.58 o 3 -5 0 1897.09 1873.51 91.81 o 4 -5 0 4.57 12.64 14.84 o 5 -5 0 1712.31 2105.50 108.85 o 6 -5 0 622.13 754.93 29.20 o 7 -5 0 2690.38 2639.30 137.98 o 8 -5 0 223.71 257.28 42.33 o 9 -5 0 789.72 838.35 75.86 o 10 -5 0 111.40 137.98 42.88 o 11 -5 0 878.41 835.60 86.31 o 12 -5 0 29.53 43.43 37.93 o 13 -5 0 64.79 86.31 46.73 o 1 -4 0 3494.90 3402.89 131.39 o 2 -4 0 2180.36 2455.14 102.25 o 3 -4 0 3285.87 4555.14 179.22 o 4 -4 0 2239.73 2849.85 125.34 o 5 -4 0 13612.14 13674.78 315.99 o 6 -4 0 628.88 579.08 58.82 o 7 -4 0 477.99 564.99 29.47 o 8 -4 0 16.57 -3.87 12.20 o 9 -4 0 1987.09 1956.52 119.84 o 10 -4 0 112.38 126.99 41.78 o 11 -4 0 370.21 337.54 58.82 o 12 -4 0 69.67 31.88 38.48 o 13 -4 0 544.79 524.45 76.41 o 2 -3 0 5476.18 6025.69 227.59 o 3 -3 0 3448.77 4034.54 150.08 o 4 -3 0 1414.11 2137.39 96.75 o 5 -3 0 761.10 1071.85 36.30 o 6 -3 0 4876.59 5221.37 134.33 o 7 -3 0 5897.20 5135.64 134.72 o 8 -3 0 296.85 263.51 22.70 o 9 -3 0 1302.62 1282.31 52.68 o 10 -3 0 291.91 306.75 50.58 o 11 -3 0 528.79 505.76 65.42 o 12 -3 0 16.10 23.64 35.73 o 13 -3 0 31.95 40.13 38.48 o 14 -3 0 33.44 80.81 45.63 o 2 -2 0 7371.70 7397.29 263.87 o 4 -2 0 6251.65 7754.95 182.03 o 5 -2 0 11157.67 12949.14 303.46 o 6 -2 0 1733.00 1587.76 51.11 o 7 -2 0 1315.21 1346.77 72.29 o 8 -2 0 2742.92 2798.04 85.28 o 9 -2 0 714.07 598.83 35.80 o 10 -2 0 427.56 442.52 34.08 o 11 -2 0 375.86 288.06 52.23 o 12 -2 0 710.04 765.79 83.56 o 13 -2 0 179.47 96.20 45.08 o 14 -2 0 54.15 82.46 48.38 o 3 -1 0 16454.91 17417.94 605.81 o 4 -1 0 4622.01 5248.91 162.17 o 5 -1 0 56.67 102.25 15.39 o 6 -1 0 11655.55 11763.01 283.51 o 7 -1 0 439.02 459.27 59.37 o 8 -1 0 1421.55 1424.68 67.89 o 9 -1 0 86.12 61.18 23.64 o 10 -1 0 679.78 719.80 43.20 o 11 -1 0 406.73 349.49 33.36 o 12 -1 0 179.87 199.01 48.93 o 13 -1 0 15.53 14.29 34.63 o 14 -1 0 106.67 134.14 49.48 o 2 0 0 2681.14 3391.89 114.35 o 3 0 0 12906.96 14096.63 313.35 o 4 0 0 10428.64 10274.47 232.28 o 5 0 0 6065.41 6383.76 149.35 o 6 0 0 108.32 107.17 10.99 o 7 0 0 121.85 122.35 12.10 o 8 0 0 4084.18 3860.27 144.03 o 9 0 0 31.44 61.57 23.64 o 10 0 0 17.99 3.50 20.07 o 11 0 0 14.61 -0.58 18.23 o 12 0 0 55.49 5.06 20.27 o 13 0 0 0.07 -7.15 38.48 o 14 0 0 206.98 183.61 54.42 o 1 1 0 1620.46 1844.39 45.46 o 2 1 0 31383.38 32737.91 766.24 o 3 1 0 16324.65 17334.54 334.21 o 4 1 0 4355.87 4766.26 114.80 o 5 1 0 87.57 114.80 7.11 o 6 1 0 11417.07 11773.09 220.31 o 7 1 0 544.12 584.00 31.92 o 8 1 0 1248.16 1246.26 66.52 o 9 1 0 99.14 136.34 28.04 o 10 1 0 665.90 658.04 53.32 o 11 1 0 393.74 323.80 42.88 o 12 1 0 159.08 169.83 29.14 o 13 1 0 14.65 5.72 22.03 o 14 1 0 106.44 89.61 49.48 o 0 2 0 12872.40 15555.42 509.61 o 1 2 0 15075.74 15556.01 360.35 o 2 2 0 7595.47 7675.22 168.89 o 3 2 0 6035.44 5936.01 113.87 o 4 2 0 5966.36 7285.74 140.77 o 5 2 0 10946.94 12601.34 291.84 o 6 2 0 1584.86 1426.36 47.62 o 7 2 0 1451.59 1481.17 92.08 o 8 2 0 2576.64 2764.36 80.83 o 9 2 0 675.45 567.88 48.38 o 10 2 0 439.94 435.94 46.73 o 11 2 0 396.83 341.39 43.98 o 12 2 0 730.77 559.63 53.32 o 13 2 0 213.50 123.34 29.83 o 14 2 0 40.08 22.84 25.20 o 1 3 0 32986.48 33194.78 604.56 o 2 3 0 6244.82 6753.15 138.74 o 3 3 0 3118.70 3560.88 73.50 o 4 3 0 1412.27 2012.68 45.13 o 5 3 0 634.11 987.95 26.14 o 6 3 0 5017.41 5292.93 133.46 o 7 3 0 5812.16 5112.68 133.12 o 8 3 0 296.25 238.43 21.51 o 9 3 0 1378.71 1360.06 77.51 o 10 3 0 274.87 163.82 34.63 o 11 3 0 438.75 429.90 47.83 o 12 3 0 11.95 23.64 28.04 o 13 3 0 32.46 12.64 29.14 o 14 3 0 40.63 44.34 26.13 o 0 4 0 406.53 381.52 25.29 o 1 4 0 3479.03 3580.80 87.59 o 2 4 0 2144.88 2493.13 64.89 o 3 4 0 3361.73 4946.82 135.08 o 4 4 0 2394.37 3113.12 74.65 o 5 4 0 14025.63 13517.21 256.95 o 6 4 0 641.87 558.09 18.91 o 7 4 0 585.95 605.68 32.03 o 8 4 0 24.37 8.27 12.71 o 9 4 0 1977.18 1840.53 95.10 o 10 4 0 98.10 79.16 31.34 o 11 4 0 397.70 286.96 42.88 o 12 4 0 63.04 11.54 29.14 o 13 4 0 573.65 656.39 65.97 o 1 5 0 11947.98 9128.02 175.28 o 2 5 0 405.15 557.13 23.52 o 3 5 0 2277.75 2263.44 51.73 o 4 5 0 7.32 6.02 5.99 o 5 5 0 2002.79 2387.85 55.75 o 6 5 0 617.77 708.67 24.27 o 7 5 0 2915.34 2956.32 88.24 o 8 5 0 220.50 210.68 22.78 o 9 5 0 752.61 866.27 44.68 o 10 5 0 110.04 159.42 33.53 o 11 5 0 987.72 1071.99 74.76 o 12 5 0 26.46 45.08 32.98 o 13 5 0 64.85 53.87 34.08 o 0 6 0 349.83 559.40 23.38 o 1 6 0 3649.15 3264.46 59.39 o 2 6 0 1648.20 1908.33 71.19 o 3 6 0 3579.52 3415.27 74.57 o 4 6 0 2692.13 2598.79 62.14 o 5 6 0 1549.36 1623.81 43.68 o 6 6 0 363.33 251.41 15.50 o 7 6 0 769.22 772.23 38.87 o 8 6 0 1014.71 893.73 44.51 o 9 6 0 459.70 447.98 75.04 o 10 6 0 180.36 170.42 35.73 o 11 6 0 2.03 18.69 26.39 o 12 6 0 109.56 64.87 35.18 o 13 6 0 244.05 326.55 50.03 o 1 7 0 1654.04 2107.41 42.67 o 2 7 0 4080.48 3846.11 84.00 o 3 7 0 5773.45 5147.77 108.68 o 4 7 0 70.97 106.07 12.09 o 5 7 0 180.75 117.42 14.18 o 6 7 0 1227.47 1226.17 40.74 o 7 7 0 94.71 74.51 17.68 o 8 7 0 50.97 107.99 29.14 o 9 7 0 33.09 -13.42 18.97 o 10 7 0 196.71 203.95 39.58 o 11 7 0 349.70 360.08 49.48 o 12 7 0 198.55 144.03 40.68 o 13 7 0 16.24 -37.93 30.24 o 0 8 0 9678.85 8938.10 212.34 o 1 8 0 805.21 696.81 21.04 o 2 8 0 167.35 134.87 9.72 o 3 8 0 13.82 16.36 9.26 o 4 8 0 195.07 132.62 14.09 o 5 8 0 338.79 440.78 27.31 o 6 8 0 944.66 918.59 44.45 o 7 8 0 120.88 116.69 46.73 o 8 8 0 872.50 1046.24 52.86 o 9 8 0 99.38 110.22 33.53 o 10 8 0 272.43 211.24 28.91 o 11 8 0 11.77 14.29 29.14 o 12 8 0 133.93 40.68 34.08 o 1 9 0 1235.86 1138.83 29.84 o 2 9 0 3149.62 3153.90 61.14 o 3 9 0 75.07 75.53 12.60 o 4 9 0 1065.29 866.82 33.31 o 5 9 0 285.51 280.13 26.10 o 6 9 0 1301.46 1289.51 55.05 o 7 9 0 419.64 443.59 33.88 o 8 9 0 876.99 998.52 53.36 o 9 9 0 60.35 16.63 18.85 o 10 9 0 549.34 583.86 44.41 o 11 9 0 12.52 15.39 31.34 o 12 9 0 128.89 201.20 47.28 o 0 10 0 641.24 683.72 50.58 o 1 10 0 1225.97 1273.53 33.56 o 2 10 0 1138.97 1142.18 38.96 o 3 10 0 721.33 704.88 33.27 o 4 10 0 2143.58 2360.70 63.95 o 5 10 0 115.55 104.65 16.43 o 6 10 0 82.00 88.04 21.76 o 7 10 0 408.74 450.19 36.53 o 8 10 0 428.51 359.97 34.67 o 9 10 0 59.36 56.49 53.05 o 10 10 0 414.19 454.57 42.11 o 11 10 0 2.55 -0.55 29.14 o 1 11 0 1372.80 1366.64 44.72 o 2 11 0 1733.91 1471.00 47.72 o 3 11 0 521.84 465.61 26.58 o 4 11 0 21.25 37.54 13.35 o 5 11 0 138.83 163.45 24.40 o 6 11 0 481.48 515.35 38.74 o 7 11 0 869.32 919.47 50.95 o 8 11 0 283.50 250.53 32.32 o 9 11 0 89.91 91.97 26.24 o 10 11 0 194.36 139.03 87.41 o 11 11 0 74.10 43.43 39.58 o 0 12 0 617.55 603.61 57.17 o 1 12 0 625.47 632.07 33.53 o 2 12 0 82.29 105.96 28.60 o 3 12 0 314.58 263.59 22.13 o 4 12 0 112.54 144.96 19.68 o 5 12 0 1178.85 1298.59 47.93 o 6 12 0 76.50 109.35 28.59 o 7 12 0 117.34 67.65 24.06 o 8 12 0 317.23 315.12 37.26 o 9 12 0 240.01 253.23 34.39 o 10 12 0 86.47 68.72 28.52 o 1 13 0 497.46 586.38 30.85 o 2 13 0 300.75 378.77 26.57 o 3 13 0 969.67 990.56 41.61 o 4 13 0 75.06 76.73 18.07 o 5 13 0 502.56 518.78 39.75 o 6 13 0 80.88 36.24 23.11 o 7 13 0 410.79 369.46 38.04 o 8 13 0 131.35 136.27 31.23 o 9 13 0 6.58 3.66 24.68 o 0 14 0 64.59 30.79 26.39 o 1 14 0 416.69 400.50 65.14 o 2 14 0 122.31 108.87 19.40 o 3 14 0 709.66 776.82 38.66 o 4 14 0 20.42 42.83 17.51 o 5 14 0 393.42 322.48 35.60 o 6 14 0 43.30 21.03 41.78 o 7 14 0 145.57 152.12 31.09 o 8 14 0 9.36 -14.57 24.10 o 9 14 0 260.11 323.80 54.42 o 1 15 0 164.96 194.23 30.59 o 2 15 0 268.35 303.84 35.85 o 3 15 0 896.28 964.28 51.56 o 4 15 0 20.33 4.75 17.15 o 5 15 0 258.71 292.29 40.13 o 6 15 0 54.31 23.00 24.66 o 7 15 0 180.84 168.96 70.37 o 0 16 0 535.36 531.05 66.52 o 1 16 0 238.64 178.40 32.26 o 2 16 0 3.50 24.76 21.12 o 3 16 0 173.98 177.42 32.40 o 4 16 0 196.03 199.17 32.15 o 5 16 0 269.46 300.06 38.64 o 6 16 0 88.16 110.44 36.83 o 1 17 0 28.12 23.74 23.70 o 2 17 0 323.77 352.09 40.98 o 3 17 0 87.00 87.70 28.96 o 4 17 0 63.90 160.52 51.13 o 0 18 0 339.17 312.25 57.17 o 1 18 0 21.38 -0.05 24.06 o -8 -15 1 13.93 7.70 37.38 o -7 -15 1 44.99 71.47 37.38 o -6 -15 1 616.75 680.58 73.67 o -9 -14 1 1.54 0.00 32.43 o -8 -14 1 518.40 501.91 66.52 o -7 -14 1 2.00 -17.04 29.69 o -6 -14 1 22.21 23.09 30.24 o -5 -14 1 2.84 -9.90 25.84 o 5 -14 1 80.33 79.71 33.53 o 6 -14 1 549.17 560.73 65.97 o 7 -14 1 69.07 37.38 37.38 o 8 -14 1 217.21 223.19 51.68 o -10 -13 1 306.46 339.74 65.97 o -9 -13 1 39.39 40.68 39.03 o -8 -13 1 23.71 -6.60 31.34 o -7 -13 1 62.83 10.99 32.43 o -6 -13 1 823.47 771.28 74.21 o -5 -13 1 69.77 4.40 26.94 o 4 -13 1 377.83 311.15 46.73 o 5 -13 1 7.17 -36.28 24.19 o 6 -13 1 275.79 301.26 50.03 o 7 -13 1 98.72 78.61 36.83 o 8 -13 1 306.51 323.80 56.62 o 9 -13 1 4.77 0.55 32.43 o -10 -12 1 1.39 21.99 35.73 o -9 -12 1 5.40 -44.53 29.69 o -8 -12 1 260.40 230.89 50.03 o -7 -12 1 445.95 402.96 54.97 o -6 -12 1 534.73 422.20 56.07 o -5 -12 1 96.08 63.22 31.88 o -4 -12 1 2030.21 1777.31 108.30 o 4 -12 1 1333.71 1387.54 87.96 o 5 -12 1 256.66 301.81 46.73 o 6 -12 1 435.38 324.35 50.58 o 7 -12 1 79.33 119.29 37.93 o 8 -12 1 299.47 247.38 50.03 o 9 -12 1 156.25 182.51 48.93 o 10 -12 1 188.71 163.82 48.38 o -11 -11 1 90.06 16.49 36.28 o -10 -11 1 266.29 229.24 53.32 o -9 -11 1 403.19 394.71 61.02 o -8 -11 1 148.70 203.40 44.53 o -7 -11 1 450.66 464.53 59.37 o -6 -11 1 646.88 623.40 64.87 o -5 -11 1 445.18 448.59 53.32 o -4 -11 1 580.91 692.12 60.47 o 3 -11 1 1220.76 1192.38 78.06 o 4 -11 1 717.44 737.75 62.67 o 5 -11 1 43.32 35.18 26.94 o 6 -11 1 432.10 521.15 57.17 o 7 -11 1 847.12 1016.47 80.26 o 8 -11 1 54.52 20.34 31.88 o 9 -11 1 114.67 118.74 41.78 o 10 -11 1 81.76 74.21 40.68 o 11 -11 1 115.92 135.24 48.93 o -12 -10 1 73.03 32.43 47.28 o -11 -10 1 177.90 345.79 63.77 o -10 -10 1 1.72 20.34 34.08 o -9 -10 1 237.29 261.68 51.13 o -8 -10 1 30.96 13.74 30.79 o -7 -10 1 742.87 762.49 70.92 o -6 -10 1 88.91 88.51 34.08 o -5 -10 1 340.81 228.69 39.03 o -4 -10 1 873.52 1062.10 76.41 o -3 -10 1 3708.00 3468.31 158.87 o 3 -10 1 18.06 37.38 23.09 o 4 -10 1 106.96 83.56 27.49 o 5 -10 1 3215.36 3252.81 154.48 o 6 -10 1 120.28 175.37 37.38 o 7 -10 1 94.20 143.48 37.93 o 8 -10 1 18.05 32.98 31.34 o 9 -10 1 532.48 603.61 70.37 o 10 -10 1 175.02 206.70 50.03 o 11 -10 1 46.49 -1.10 36.28 o 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