#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:25:46 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181235 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/13/2231342.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231342_Fobs loop_ _publ_author_name 'Win, Yip-Foo' 'Choong, Chen-Shang' 'Ha, Sie-Tiong' 'Yeap, Chin Sing' 'Fun, Hoong-Kun' _publ_section_title ; Octabutylbis[\m~2~-4-(diethylamino)benzoato-\k^2^O:O']bis[4-(diethylamino)benzoato-\kO]di-\m~3~-oxido-tetratin(IV) ; _journal_coeditor_code WM2503 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1018 _journal_page_last m1019 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 102.374 _cell_angle_beta 90.100 _cell_angle_gamma 92.164 _cell_length_a 11.7394 _cell_length_b 14.4449 _cell_length_c 24.3248 _exptl_crystal_F_000 1784.00 _reflns_d_resolution_high 0.8107 _cod_data_source_file wm2503Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' yipfw18_0m in P-1 (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 442.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 78.31 14.14 10.07 o 2 0 0 64407.27 65320.26 1204.62 o 3 0 0 417.42 355.16 31.40 o 4 0 0 880.76 1018.98 49.97 o 5 0 0 424.61 377.59 31.05 o 6 0 0 543.42 685.51 52.62 o 7 0 0 7681.42 7727.17 415.91 o 8 0 0 3785.15 3783.91 100.15 o 9 0 0 6056.04 5667.96 188.94 o 10 0 0 2267.04 2242.05 137.83 o 11 0 0 291.48 327.49 74.40 o 12 0 0 282.01 331.05 81.34 o 13 0 0 93.59 13.45 78.63 o 14 0 0 10989.12 11385.40 451.06 o -14 1 0 6.08 51.84 104.23 o -13 1 0 406.93 367.24 141.53 o -12 1 0 0.56 20.28 54.75 o -11 1 0 1190.57 1151.67 157.23 o -10 1 0 3778.97 3718.26 222.91 o -9 1 0 8816.91 9023.53 236.33 o -8 1 0 35775.36 36482.34 440.28 o -7 1 0 451.73 415.69 48.12 o -6 1 0 15136.45 14681.90 211.71 o -5 1 0 20798.31 20241.29 387.83 o -4 1 0 4479.10 4643.61 85.66 o -3 1 0 3051.74 2910.14 64.55 o -2 1 0 113.06 198.89 21.85 o -1 1 0 45197.78 48206.07 367.14 o 0 1 0 107.14 65.01 15.26 o 1 1 0 54346.68 54527.71 1061.20 o 2 1 0 0.23 -5.36 6.67 o 3 1 0 265.95 325.05 21.27 o 4 1 0 484.36 611.99 34.85 o 5 1 0 2209.10 2417.82 79.47 o 6 1 0 2678.60 2766.76 122.76 o 7 1 0 246.89 163.58 43.63 o 8 1 0 12850.98 12057.69 832.68 o 9 1 0 2662.68 2321.25 117.95 o 10 1 0 504.97 615.08 108.02 o 11 1 0 770.79 668.78 86.75 o 12 1 0 212.90 124.13 63.97 o 13 1 0 8382.25 8790.68 373.70 o 14 1 0 60.99 160.38 91.57 o -14 2 0 27.62 -97.22 68.79 o -13 2 0 1183.71 928.14 193.87 o -12 2 0 2429.35 2587.06 242.55 o -11 2 0 2540.52 2547.71 154.75 o -10 2 0 6848.04 7261.81 223.56 o -9 2 0 2009.06 1916.37 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1673.43 74.25 o -5 3 0 21518.20 22179.88 229.48 o -4 3 0 16814.84 15869.07 171.36 o -3 3 0 25021.20 25853.55 237.22 o -2 3 0 22142.85 22965.29 187.89 o -1 3 0 25145.91 28259.87 263.57 o 0 3 0 111.60 124.31 19.78 o 1 3 0 73960.98 73375.40 614.82 o 2 3 0 21758.76 22774.58 219.86 o 3 3 0 45384.79 43873.48 403.67 o 4 3 0 628.13 732.17 35.56 o 5 3 0 53059.22 53935.06 532.47 o 6 3 0 597.98 629.03 36.48 o 7 3 0 204.78 200.65 35.86 o 8 3 0 1839.74 1860.04 119.89 o 9 3 0 7439.34 6624.22 193.96 o 10 3 0 326.17 291.31 54.97 o 11 3 0 5605.02 5741.51 321.04 o 12 3 0 1576.11 1243.82 168.39 o 13 3 0 16.22 -35.89 68.49 o 14 3 0 107.70 65.90 85.67 o -14 4 0 2519.32 2591.87 267.49 o -13 4 0 3897.11 4400.43 291.25 o -12 4 0 1304.98 1399.52 186.23 o -11 4 0 12220.17 12064.93 264.39 o -10 4 0 703.81 607.06 73.51 o -9 4 0 718.82 707.27 74.18 o -8 4 0 21.20 36.67 29.49 o -7 4 0 38.71 6.14 22.37 o -6 4 0 782.94 724.80 45.66 o -5 4 0 5615.31 5691.95 99.41 o -4 4 0 2025.40 2309.49 58.69 o -3 4 0 57579.34 57165.32 472.16 o -2 4 0 482.94 461.03 25.49 o -1 4 0 1648.66 1176.69 46.28 o 0 4 0 1930.32 1839.38 52.36 o 1 4 0 1495.27 1506.81 51.90 o 2 4 0 181.48 242.11 32.21 o 3 4 0 50787.76 52479.14 480.39 o 4 4 0 10530.15 10673.40 170.32 o 5 4 0 68.65 22.72 15.03 o 6 4 0 142.83 113.90 28.84 o 7 4 0 74.23 25.18 20.92 o 8 4 0 1497.92 1491.34 148.42 o 9 4 0 3086.09 3554.46 370.64 o 10 4 0 2430.35 1645.60 770.74 o 11 4 0 17035.45 16418.46 711.88 o 12 4 0 1899.33 1904.20 307.73 o 13 4 0 4780.47 4982.11 307.45 o -14 5 0 296.78 353.63 147.13 o -13 5 0 1450.92 1314.04 321.42 o -12 5 0 3667.86 3557.06 216.54 o -11 5 0 4150.79 4567.11 164.16 o -10 5 0 2139.91 1948.12 111.61 o -9 5 0 69.87 98.00 41.51 o -8 5 0 12399.76 11759.10 243.92 o -7 5 0 9.06 4.24 34.05 o -6 5 0 4471.32 4072.54 92.09 o -5 5 0 3787.26 3441.99 79.51 o -4 5 0 8145.53 8557.68 111.73 o -3 5 0 12841.20 11913.13 129.98 o -2 5 0 25981.14 24995.82 234.47 o -1 5 0 26717.41 25726.02 263.81 o 0 5 0 755.23 712.20 39.91 o 1 5 0 6411.58 6196.03 92.55 o 2 5 0 14885.09 14762.45 172.96 o 3 5 0 3696.12 3382.65 91.65 o 4 5 0 4059.36 3919.50 108.22 o 5 5 0 1740.84 1651.41 78.10 o 6 5 0 442.56 474.17 53.66 o 7 5 0 0.99 1.50 23.00 o 8 5 0 36.19 33.50 27.06 o 9 5 0 57.28 -26.61 25.28 o 10 5 0 9335.59 9524.04 352.32 o 11 5 0 2299.88 2285.24 216.33 o 12 5 0 10521.21 10169.34 401.67 o 13 5 0 262.63 221.61 86.08 o -13 6 0 80.15 125.60 102.92 o -12 6 0 46.42 34.37 67.05 o -11 6 0 534.32 676.39 108.14 o -10 6 0 55.15 81.53 41.87 o -9 6 0 7951.25 8060.80 198.08 o -8 6 0 528.37 440.18 54.82 o -7 6 0 34865.91 34842.27 397.33 o -6 6 0 1343.92 1481.65 64.25 o -5 6 0 16542.26 16029.37 194.42 o -4 6 0 15339.50 14826.83 163.41 o -3 6 0 1081.30 1222.34 49.08 o -2 6 0 4726.94 5755.61 89.28 o -1 6 0 3518.89 3848.16 81.15 o 0 6 0 935.90 927.17 47.00 o 1 6 0 11543.63 11667.55 154.71 o 2 6 0 1731.33 1432.49 69.61 o 3 6 0 9142.94 8414.91 155.19 o 4 6 0 13332.63 12573.02 206.10 o 5 6 0 8825.16 9165.78 215.99 o 6 6 0 1711.83 1854.41 94.83 o 7 6 0 24831.82 24448.32 293.71 o 8 6 0 17.46 9.74 29.43 o 9 6 0 1833.87 1787.15 143.82 o 10 6 0 315.21 289.57 80.37 o 11 6 0 3517.41 3842.70 260.85 o 12 6 0 1171.89 927.98 168.97 o 13 6 0 396.77 209.90 93.49 o -13 7 0 5201.72 5213.02 313.29 o -12 7 0 535.54 522.79 108.92 o -11 7 0 230.67 396.34 94.44 o -10 7 0 676.02 697.97 102.48 o -9 7 0 4247.16 3939.39 180.72 o -8 7 0 7445.29 7914.84 180.43 o -7 7 0 2.18 6.83 32.24 o -6 7 0 8793.84 8879.51 147.57 o -5 7 0 455.26 488.21 41.21 o -4 7 0 125.90 198.18 31.39 o -3 7 0 15576.91 15980.87 184.40 o -2 7 0 6846.82 7779.28 112.91 o -1 7 0 30882.70 31248.24 333.29 o 0 7 0 927.28 809.39 66.92 o 1 7 0 15889.63 17405.91 240.59 o 2 7 0 6156.44 6030.17 108.63 o 3 7 0 810.35 1135.48 83.72 o 4 7 0 8102.06 8337.28 170.08 o 5 7 0 8.72 50.37 41.06 o 6 7 0 22402.30 21722.22 325.73 o 7 7 0 2599.69 2681.72 116.63 o 8 7 0 22040.27 22209.31 533.26 o 9 7 0 1168.41 1167.93 122.77 o 10 7 0 1836.24 1685.86 148.48 o 11 7 0 177.31 52.18 42.21 o 12 7 0 83.45 22.33 56.85 o 13 7 0 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13 0 17045.20 16323.75 362.07 o 0 13 0 1769.52 1687.06 148.86 o 1 13 0 4371.03 4145.01 202.62 o 2 13 0 4590.87 5068.77 263.54 o 3 13 0 1282.50 1129.36 117.71 o 4 13 0 509.00 653.50 94.94 o 5 13 0 61.04 103.17 63.61 o 6 13 0 3031.74 3329.91 180.13 o 7 13 0 1557.39 1681.26 143.21 o 8 13 0 142.90 121.15 112.21 o 9 13 0 791.55 643.62 136.58 o -9 14 0 10244.32 10489.46 410.54 o -8 14 0 60.88 190.47 103.09 o -7 14 0 7813.58 7398.08 260.53 o -6 14 0 132.18 179.96 64.63 o -5 14 0 995.08 896.42 107.45 o -4 14 0 75.31 4.54 47.56 o -3 14 0 986.36 955.93 109.11 o -2 14 0 1271.11 1179.03 119.24 o -1 14 0 136.34 101.50 53.98 o 0 14 0 691.84 631.59 93.03 o 1 14 0 7335.22 6894.19 236.06 o 2 14 0 79.37 84.80 62.92 o 3 14 0 391.81 393.16 98.85 o 4 14 0 955.00 1161.08 135.60 o 5 14 0 9688.09 9344.91 287.63 o 6 14 0 504.87 750.66 109.48 o 7 14 0 5377.73 4717.12 317.38 o 8 14 0 118.68 80.75 53.89 o -7 15 0 41.51 130.59 78.39 o -6 15 0 2485.41 2163.90 173.37 o -5 15 0 47.11 8.76 54.77 o -4 15 0 774.56 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