#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:25:46 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181235 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/13/2231347.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231347_Fobs loop_ _publ_author_name 'Smith, Graham' 'Wermuth, Urs D.' _publ_section_title ; Poly[di-\m-aqua-bis(\m-2-amino-4-nitrobenzoato)dicaesium] ; _journal_coeditor_code WM2509 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1047 _journal_page_last m1048 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.903 _cell_angle_gamma 90.000 _cell_length_a 15.3615 _cell_length_b 6.9573 _cell_length_c 18.3714 _exptl_crystal_F_000 1264.00 _reflns_d_resolution_high 0.7380 _cod_data_source_file wm2509Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' gs11gs12 NAACS' _shelx_refln_list_code 4 _shelx_f_calc_maximum 513.14 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 46662.21 44671.85 353.15 o 6 0 0 1649.86 1616.37 42.41 o 8 0 0 3364.97 3484.89 77.58 o 10 0 0 792.48 803.85 65.94 o 12 0 0 21505.32 20719.00 215.32 o 14 0 0 810.26 841.81 87.50 o 16 0 0 24365.14 24444.11 406.31 o 18 0 0 56.46 10.38 142.60 o 2 1 0 4573.98 4640.53 85.38 o 3 1 0 19358.60 20417.62 120.70 o 4 1 0 33677.97 33612.17 189.99 o 5 1 0 6036.72 6135.74 63.55 o 6 1 0 104.89 132.98 19.74 o 7 1 0 24.16 61.09 18.02 o 8 1 0 42349.50 41526.89 274.41 o 9 1 0 2782.30 3172.81 103.12 o 10 1 0 29.57 44.00 26.02 o 11 1 0 1025.37 1042.74 53.38 o 12 1 0 11202.94 11190.70 127.38 o 13 1 0 2750.07 2842.05 82.20 o 14 1 0 452.33 539.08 61.31 o 15 1 0 3137.62 3115.53 90.89 o 16 1 0 9.24 72.78 66.13 o 17 1 0 575.39 609.65 79.17 o 18 1 0 484.11 499.71 82.38 o 19 1 0 1456.53 1371.11 139.99 o 0 2 0 240.99 226.20 72.80 o 1 2 0 6707.48 6582.55 45.54 o 2 2 0 37369.33 38088.05 236.29 o 3 2 0 14.94 34.49 17.19 o 4 2 0 15417.38 15619.23 396.24 o 5 2 0 28596.55 28383.41 216.94 o 6 2 0 33506.50 33453.57 191.46 o 7 2 0 11600.16 11895.52 191.01 o 8 2 0 31.07 56.66 47.77 o 9 2 0 10980.92 11310.32 140.99 o 10 2 0 10547.25 10884.51 129.85 o 11 2 0 9533.87 9318.68 128.84 o 12 2 0 2967.45 3087.54 92.54 o 13 2 0 36.63 57.82 52.65 o 14 2 0 1370.49 1389.93 110.96 o 15 2 0 850.38 787.92 76.75 o 16 2 0 1067.79 1026.71 81.83 o 17 2 0 2829.62 2898.65 106.91 o 18 2 0 3.54 109.11 74.01 o 19 2 0 7.35 30.65 92.43 o 1 3 0 10543.40 10882.23 86.51 o 2 3 0 63263.17 58382.51 376.17 o 3 3 0 2075.19 2001.08 41.48 o 4 3 0 200.26 209.50 24.45 o 5 3 0 1048.30 1028.65 42.39 o 6 3 0 4969.87 4998.99 89.85 o 7 3 0 2.32 71.39 63.44 o 8 3 0 438.46 431.68 58.10 o 9 3 0 578.53 630.12 66.96 o 10 3 0 5857.94 5754.38 137.12 o 11 3 0 1742.65 1624.44 88.58 o 12 3 0 518.43 481.51 62.32 o 13 3 0 245.16 280.45 59.60 o 14 3 0 16162.55 16330.04 231.71 o 15 3 0 1531.43 1556.01 83.67 o 16 3 0 133.01 80.55 65.93 o 17 3 0 1237.42 1223.84 86.73 o 18 3 0 8352.67 8295.06 187.36 o 19 3 0 97.54 100.98 121.99 o 0 4 0 380.30 409.41 33.50 o 1 4 0 21247.93 21409.49 196.06 o 2 4 0 22106.48 21492.42 231.49 o 3 4 0 21849.29 21977.76 249.44 o 4 4 0 764.80 799.34 40.42 o 5 4 0 238.25 255.35 52.06 o 6 4 0 37311.07 36726.32 236.71 o 7 4 0 75.51 180.35 62.83 o 8 4 0 750.58 770.94 70.79 o 9 4 0 1082.11 1100.25 78.46 o 10 4 0 19779.36 19724.39 343.89 o 11 4 0 1271.26 1612.59 91.95 o 12 4 0 1287.64 1306.58 72.40 o 13 4 0 1767.36 1865.11 86.95 o 14 4 0 1319.02 1372.64 79.31 o 15 4 0 1565.56 1614.85 98.11 o 16 4 0 88.95 132.56 89.04 o 17 4 0 1462.98 1471.15 115.02 o 18 4 0 1672.39 1545.37 197.96 o 1 5 0 198.42 218.10 39.99 o 2 5 0 4386.69 4563.84 108.48 o 3 5 0 6435.55 6299.50 125.31 o 4 5 0 1042.12 1084.52 61.03 o 5 5 0 13240.59 13189.41 138.41 o 6 5 0 511.92 556.87 57.83 o 7 5 0 8939.73 8698.20 164.04 o 8 5 0 172.98 360.28 66.27 o 9 5 0 13328.70 13229.75 179.45 o 10 5 0 36.72 199.71 70.96 o 11 5 0 3737.74 3651.74 131.49 o 12 5 0 46.74 128.81 80.42 o 13 5 0 1598.03 1659.29 99.58 o 14 5 0 1471.16 1394.61 102.78 o 15 5 0 64.18 64.94 84.24 o 16 5 0 237.94 211.66 88.18 o 0 6 0 18730.11 18877.62 291.80 o 1 6 0 1785.28 1903.92 74.92 o 2 6 0 68.07 64.13 54.14 o 3 6 0 8120.99 8112.79 139.73 o 4 6 0 2011.16 2166.35 75.68 o 5 6 0 353.24 378.21 56.34 o 6 6 0 898.90 976.04 69.95 o 7 6 0 740.63 801.01 65.64 o 8 6 0 163.00 160.97 59.55 o 9 6 0 337.14 409.09 66.44 o 10 6 0 114.37 169.00 71.96 o 11 6 0 2450.49 2395.19 111.65 o 12 6 0 1421.67 1421.79 101.33 o 13 6 0 2619.83 2619.87 243.09 o 14 6 0 65.16 117.70 142.88 o 15 6 0 1525.92 1437.60 192.40 o 1 7 0 3459.35 3559.52 78.26 o 2 7 0 2256.74 2221.95 86.43 o 3 7 0 1107.30 1216.52 85.40 o 4 7 0 4997.78 4917.77 127.29 o 5 7 0 3460.72 3456.86 113.00 o 6 7 0 458.40 446.72 76.46 o 7 7 0 230.74 215.02 68.26 o 8 7 0 7440.38 7897.12 213.47 o 9 7 0 439.36 667.47 112.92 o 10 7 0 367.80 565.10 112.85 o 11 7 0 2086.56 2033.90 144.21 o 0 8 0 306.66 428.37 97.38 o 1 8 0 183.86 147.42 58.04 o 2 8 0 67.14 54.59 60.62 o 3 8 0 1489.59 1430.37 93.75 o 4 8 0 403.22 552.13 100.34 o 5 8 0 3738.59 3462.46 154.30 o 6 8 0 1471.43 1380.04 122.96 o 7 8 0 1932.65 2324.67 144.75 o 1 9 0 3573.87 3587.99 164.95 o 2 9 0 448.26 507.73 156.05 o 3 9 0 2276.70 2091.38 192.78 o -19 0 1 27.69 119.12 147.40 o -17 0 1 143.72 367.46 118.06 o -15 0 1 22884.90 22384.95 258.22 o -13 0 1 5759.71 5624.72 135.43 o -11 0 1 56042.14 54090.68 318.65 o -9 0 1 824.79 877.10 64.81 o -7 0 1 11325.92 11169.99 151.00 o -5 0 1 494.93 606.03 43.66 o -3 0 1 13978.79 13782.85 133.69 o 3 0 1 21.59 218.14 20.33 o 5 0 1 179826.45 163475.45 2750.78 o 7 0 1 5344.39 5588.11 105.76 o 9 0 1 12683.52 12763.21 172.86 o 11 0 1 14.89 52.34 63.18 o 13 0 1 4902.54 4753.59 181.39 o 15 0 1 70.39 46.91 70.38 o 17 0 1 15742.48 15875.16 290.86 o 19 0 1 1440.13 1635.71 192.98 o -19 1 1 2976.54 2878.44 118.00 o -18 1 1 2365.60 2405.75 105.14 o -17 1 1 958.43 921.58 82.74 o -16 1 1 573.70 626.06 72.17 o -15 1 1 2054.96 2100.80 112.17 o -14 1 1 2729.27 2891.02 86.90 o -13 1 1 45.53 75.10 54.71 o -12 1 1 8588.77 8528.01 126.34 o -11 1 1 1287.33 1401.16 63.05 o -10 1 1 608.54 615.91 32.86 o -9 1 1 475.91 541.87 43.05 o -8 1 1 11609.08 12205.34 309.19 o -7 1 1 40750.30 39206.21 315.74 o -6 1 1 283.52 344.66 40.70 o -5 1 1 1887.75 1937.93 62.33 o -4 1 1 1085.35 1138.90 38.78 o -3 1 1 57424.30 57425.83 524.38 o -2 1 1 11262.03 11884.78 71.01 o -1 1 1 2006.23 1899.60 40.23 o 1 1 1 6703.63 7288.77 62.09 o 2 1 1 20275.53 21042.78 316.00 o 3 1 1 1789.77 1990.49 38.80 o 4 1 1 46851.20 46459.51 235.81 o 5 1 1 4747.89 4618.81 40.80 o 6 1 1 3915.48 4137.53 39.98 o 7 1 1 559.98 646.51 25.22 o 8 1 1 9481.97 9738.86 87.86 o 9 1 1 26360.57 25920.81 206.58 o 10 1 1 851.16 943.24 49.63 o 11 1 1 1.66 48.57 52.20 o 12 1 1 706.84 684.61 61.57 o 13 1 1 15838.27 15651.43 151.88 o 14 1 1 3298.80 3264.72 87.56 o 15 1 1 391.34 483.96 61.18 o 16 1 1 1485.49 1415.30 85.75 o 17 1 1 722.11 799.11 80.39 o 18 1 1 486.59 600.87 95.79 o 19 1 1 18.22 76.39 106.92 o -20 2 1 763.90 720.22 229.82 o -19 2 1 1847.58 1890.85 125.03 o -18 2 1 1931.88 1779.91 101.55 o -17 2 1 841.28 885.78 81.21 o -16 2 1 2782.69 2788.19 102.20 o -15 2 1 2592.02 2666.18 113.54 o -14 2 1 392.95 490.50 60.35 o -13 2 1 6.32 28.08 52.97 o -12 2 1 2880.64 2834.09 89.35 o -11 2 1 614.36 826.32 57.22 o -10 2 1 14748.98 14599.63 144.67 o -9 2 1 14162.58 14649.23 131.02 o -8 2 1 1955.89 2080.56 87.04 o -7 2 1 1683.32 1730.47 61.44 o -6 2 1 32051.66 32480.11 229.84 o -5 2 1 45991.89 45121.19 204.90 o -4 2 1 43799.96 44362.86 209.10 o -3 2 1 28306.75 29299.14 127.94 o -2 2 1 2715.26 2935.19 45.07 o -1 2 1 7766.58 8468.24 70.73 o 0 2 1 51.25 101.52 15.91 o 1 2 1 13649.28 13478.81 94.92 o 2 2 1 27320.44 27886.55 207.31 o 3 2 1 536.16 562.67 20.69 o 4 2 1 1839.79 1961.87 38.40 o 5 2 1 5727.07 5817.07 73.37 o 6 2 1 4067.23 3858.07 67.36 o 7 2 1 5857.73 5481.63 92.36 o 8 2 1 2331.37 2427.63 75.02 o 9 2 1 3387.66 3467.14 88.37 o 10 2 1 9726.45 9777.62 123.00 o 11 2 1 15604.11 15139.53 180.81 o 12 2 1 11544.87 11529.04 183.11 o 13 2 1 535.86 605.18 58.53 o 14 2 1 509.95 537.15 64.61 o 15 2 1 4720.70 4769.79 115.58 o 16 2 1 2499.64 2431.00 98.02 o 17 2 1 846.82 882.76 81.99 o 18 2 1 1563.35 1689.15 98.97 o 19 2 1 123.99 190.59 143.98 o -19 3 1 109.74 157.19 128.39 o -18 3 1 636.39 651.83 82.96 o -17 3 1 2855.60 2754.36 108.74 o -16 3 1 425.08 424.43 72.28 o -15 3 1 1686.82 1612.13 84.65 o -14 3 1 1253.22 1264.09 76.19 o -13 3 1 23636.68 22692.88 241.78 o -12 3 1 274.33 329.13 57.57 o -11 3 1 469.86 493.37 56.02 o -10 3 1 1897.26 2237.87 75.76 o -9 3 1 23343.97 23396.30 204.63 o -8 3 1 83.17 139.16 55.25 o -7 3 1 265.21 299.25 51.20 o -6 3 1 113.67 140.63 20.37 o -5 3 1 1707.14 1587.21 55.23 o -4 3 1 1636.57 1591.39 38.66 o -3 3 1 359.18 330.47 37.66 o -2 3 1 546.42 553.76 24.38 o -1 3 1 46337.68 45325.74 214.94 o 0 3 1 9317.19 9330.57 56.35 o 1 3 1 1149.31 1212.51 30.60 o 2 3 1 5120.00 5215.28 61.18 o 3 3 1 48849.99 47716.95 273.08 o 4 3 1 1511.99 1435.86 48.71 o 5 3 1 92.43 84.13 18.06 o 6 3 1 1455.70 1504.22 60.90 o 7 3 1 42017.68 41536.84 243.83 o 8 3 1 27.42 144.95 60.29 o 9 3 1 580.70 631.50 69.67 o 10 3 1 12.48 63.55 59.48 o 11 3 1 5.97 47.96 63.76 o 12 3 1 707.92 700.57 76.31 o 13 3 1 76.83 158.93 72.49 o 14 3 1 190.82 177.36 59.04 o 15 3 1 6769.38 6643.68 130.87 o 16 3 1 967.04 917.84 78.53 o 17 3 1 19.72 24.87 66.08 o 18 3 1 407.63 286.88 96.59 o 19 3 1 4900.52 4532.23 195.15 o -18 4 1 218.61 287.74 168.30 o -17 4 1 3951.23 3803.19 148.17 o -16 4 1 944.07 1062.18 98.84 o -15 4 1 9.05 43.99 81.40 o -14 4 1 1916.23 1863.49 100.49 o -13 4 1 9.31 45.63 59.29 o -12 4 1 7044.86 7093.63 134.48 o -11 4 1 11.81 77.84 50.64 o -10 4 1 1314.05 1872.28 81.04 o -9 4 1 8547.78 8884.74 216.14 o -8 4 1 2940.63 2944.31 92.84 o -7 4 1 815.33 857.69 66.28 o -6 4 1 130.00 174.83 31.89 o -5 4 1 41807.37 40903.74 367.52 o -4 4 1 4146.90 4145.99 62.87 o -3 4 1 6208.32 6192.22 90.66 o -2 4 1 3174.53 3184.94 86.66 o -1 4 1 47522.47 46402.15 215.77 o 0 4 1 1444.93 1616.79 69.79 o 1 4 1 2981.04 3097.22 59.07 o 2 4 1 6545.93 6314.71 107.54 o 3 4 1 1385.36 1553.29 67.09 o 4 4 1 4342.03 4169.51 102.51 o 5 4 1 1414.07 1400.74 43.32 o 6 4 1 1037.33 1038.57 46.91 o 7 4 1 24591.28 24959.87 250.51 o 8 4 1 3092.35 3190.25 93.31 o 9 4 1 688.39 734.77 74.41 o 10 4 1 1079.45 1120.06 102.41 o 11 4 1 20570.98 20842.09 283.76 o 12 4 1 30.68 142.30 77.10 o 13 4 1 441.39 509.69 100.76 o 14 4 1 731.46 627.86 68.74 o 15 4 1 4629.15 4726.66 143.02 o 16 4 1 763.86 770.11 94.31 o 17 4 1 28.86 97.69 84.02 o 18 4 1 2268.43 2027.73 230.65 o -16 5 1 193.17 247.12 120.31 o -15 5 1 1.42 22.97 82.80 o -14 5 1 492.24 486.01 90.85 o -13 5 1 315.31 382.42 82.63 o -12 5 1 1229.66 1343.70 94.00 o -11 5 1 2006.68 1987.69 97.88 o -10 5 1 381.50 481.47 70.33 o -9 5 1 3493.39 3959.38 153.77 o -8 5 1 7492.88 7330.54 135.01 o -7 5 1 3682.85 3781.80 106.77 o -6 5 1 13650.01 13417.92 163.48 o -5 5 1 269.44 320.15 51.92 o -4 5 1 16804.19 16272.10 149.40 o -3 5 1 1637.87 1681.22 64.95 o -2 5 1 12424.66 12356.09 114.22 o -1 5 1 1077.43 1063.42 48.95 o 0 5 1 2653.40 2643.27 81.98 o 1 5 1 361.00 426.52 45.06 o 2 5 1 1170.94 1141.51 53.97 o 3 5 1 4118.09 4071.32 77.09 o 4 5 1 2894.00 2814.92 75.59 o 5 5 1 1351.57 1304.38 63.66 o 6 5 1 4128.60 4174.04 91.40 o 7 5 1 204.42 255.39 52.69 o 8 5 1 7047.58 6987.93 132.33 o 9 5 1 2178.29 2270.43 93.22 o 10 5 1 9911.32 10024.09 166.89 o 11 5 1 83.98 172.81 75.59 o 12 5 1 4944.79 4992.28 138.17 o 13 5 1 1035.93 1133.61 106.26 o 14 5 1 4109.82 4097.18 196.82 o 15 5 1 972.20 955.46 100.07 o 16 5 1 5.09 23.35 94.90 o 17 5 1 25.29 43.75 160.94 o -15 6 1 2383.58 2447.42 224.93 o -14 6 1 1747.07 1746.15 213.05 o -13 6 1 54.23 107.08 107.23 o -12 6 1 2879.91 3067.83 152.65 o -11 6 1 3517.75 3816.94 166.81 o -10 6 1 2299.55 2142.08 103.06 o -9 6 1 113.79 166.10 74.76 o -8 6 1 1271.76 1308.64 73.22 o -7 6 1 2229.85 2239.26 83.21 o -6 6 1 11.26 45.11 51.56 o -5 6 1 666.39 737.42 63.64 o -4 6 1 1663.63 1633.87 69.59 o -3 6 1 1711.73 1658.20 77.21 o -2 6 1 1711.91 1683.60 61.81 o -1 6 1 377.63 475.53 57.26 o 0 6 1 14668.68 14839.16 139.18 o 1 6 1 8347.10 8349.63 106.68 o 2 6 1 5377.84 5310.71 144.57 o 3 6 1 1.60 34.18 64.61 o 4 6 1 1459.47 1466.43 83.05 o 5 6 1 12134.89 12027.85 147.90 o 6 6 1 6222.68 6213.75 114.97 o 7 6 1 281.79 300.75 57.86 o 8 6 1 729.83 725.06 66.78 o 9 6 1 594.71 671.73 69.86 o 10 6 1 1.51 8.28 60.45 o 11 6 1 22.61 40.60 73.54 o 12 6 1 17.36 68.01 81.51 o 13 6 1 799.32 713.87 93.31 o 14 6 1 1711.68 1553.43 135.29 o 15 6 1 62.45 -79.33 155.06 o -11 7 1 6.30 146.89 110.88 o -10 7 1 2564.18 2718.49 192.65 o -9 7 1 723.88 783.12 117.89 o -8 7 1 204.01 415.92 108.93 o -7 7 1 8309.18 8320.87 208.14 o -6 7 1 1090.78 1135.12 112.19 o -5 7 1 67.10 128.03 97.08 o -4 7 1 1743.20 1738.43 91.30 o -3 7 1 9217.69 9058.62 193.49 o -2 7 1 138.04 194.37 68.09 o -1 7 1 623.37 609.86 53.56 o 0 7 1 5133.11 5186.16 100.32 o 1 7 1 747.10 819.35 55.57 o 2 7 1 2731.43 2727.21 80.17 o 3 7 1 2156.22 2242.09 81.29 o 4 7 1 2073.44 2181.31 96.89 o 5 7 1 504.94 560.55 76.67 o 6 7 1 4665.10 4547.39 131.48 o 7 7 1 30.41 88.84 70.75 o 8 7 1 22.46 116.92 78.54 o 9 7 1 4838.80 4743.57 137.00 o 10 7 1 1418.98 1430.79 132.27 o 11 7 1 176.17 147.93 105.82 o -8 8 1 1721.97 1708.00 208.17 o -7 8 1 1745.11 1674.80 135.47 o -6 8 1 4630.06 4473.70 178.43 o -5 8 1 2.44 58.85 100.21 o -4 8 1 3388.65 3367.60 151.19 o -3 8 1 177.68 182.47 73.82 o -2 8 1 3602.74 3409.44 104.15 o -1 8 1 1217.83 1059.24 72.09 o 0 8 1 2690.29 2593.91 87.82 o 1 8 1 3036.99 2991.58 89.21 o 2 8 1 37.37 32.28 61.53 o 3 8 1 1.13 13.83 92.48 o 4 8 1 102.71 98.03 110.61 o 5 8 1 2455.58 2094.95 139.10 o 6 8 1 695.54 845.72 118.86 o 7 8 1 33.70 82.92 112.76 o -3 9 1 297.20 345.29 142.12 o -2 9 1 820.81 818.78 119.31 o -1 9 1 355.49 286.80 92.98 o 0 9 1 2169.75 2202.54 142.38 o 1 9 1 11.34 81.55 152.65 o 2 9 1 3483.49 3722.23 238.09 o -18 0 2 149.14 257.50 118.29 o -16 0 2 1311.85 1442.95 123.70 o -14 0 2 10992.75 10166.41 214.07 o -12 0 2 1273.53 1286.59 84.71 o -10 0 2 68968.30 69147.59 464.03 o -8 0 2 1320.86 1384.16 64.53 o -6 0 2 44392.47 43517.80 208.97 o -4 0 2 1226.80 1267.34 53.57 o -2 0 2 18720.07 18382.51 153.37 o 2 0 2 25726.92 25358.77 101.89 o 4 0 2 0.87 34.00 15.99 o 6 0 2 263315.53 244865.09 5950.95 o 8 0 2 95.10 135.75 52.14 o 10 0 2 24517.27 23483.58 682.09 o 12 0 2 498.95 490.31 89.37 o 14 0 2 433.37 524.67 80.32 o 16 0 2 78.87 105.18 93.50 o 18 0 2 4184.88 4210.80 179.85 o -19 1 2 3170.67 3219.09 144.55 o -18 1 2 4446.10 4404.30 148.14 o -17 1 2 1198.07 1231.14 84.29 o -16 1 2 419.73 378.70 67.04 o -15 1 2 57.74 110.83 62.09 o -14 1 2 12081.14 11340.02 165.26 o -13 1 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