#------------------------------------------------------------------------------ #$Date: 2011-10-07 16:37:56 +0300 (Fri, 07 Oct 2011) $ #$Revision: 27934 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/14/2231419.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231419_Fobs loop_ _publ_author_name 'Aliyeva, Khatira N.' 'Maharramov, Abel M.' 'Allahverdiyev, Mirze A.' 'Gurbanov, Atash V.' 'Brito, Iv\'an' _publ_section_title ; 4,6-Dihydroxy-4,6-dimethyl-1,3-diazinane-2-thione ; _journal_coeditor_code BT5602 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2293 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 74.812 _cell_angle_beta 88.670 _cell_angle_gamma 79.708 _cell_length_a 5.2425 _cell_length_b 8.7047 _cell_length_c 9.4370 _exptl_crystal_F_000 188.00 _reflns_d_resolution_high 0.7828 _[local]_cod_data_source_file bt5602Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' A in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 67.17 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 378.96 410.40 3.01 o 2 0 0 3130.75 3361.43 17.93 o 4 0 0 54.35 57.88 1.35 o 5 0 0 6.64 8.96 0.51 o 6 0 0 0.17 -0.41 0.54 o -6 1 0 0.29 0.25 0.34 o -5 1 0 93.31 89.33 1.26 o -4 1 0 9.92 12.17 0.49 o -3 1 0 573.06 593.05 5.17 o -2 1 0 607.56 623.69 3.54 o -1 1 0 552.81 575.15 3.39 o 0 1 0 1124.58 1143.77 5.37 o 1 1 0 175.61 149.00 0.97 o 2 1 0 1.71 0.95 0.19 o 3 1 0 260.73 270.93 2.72 o 4 1 0 53.57 63.38 1.16 o 5 1 0 171.49 167.91 2.56 o 6 1 0 0.00 0.65 0.67 o -6 2 0 6.66 6.42 0.75 o -5 2 0 17.14 18.83 0.66 o -4 2 0 233.92 228.05 1.96 o -3 2 0 425.14 472.74 5.30 o -2 2 0 90.94 75.34 0.79 o -1 2 0 20.52 22.28 0.38 o 0 2 0 1620.72 1716.97 9.26 o 1 2 0 1894.97 2136.54 14.65 o 2 2 0 211.95 217.53 1.51 o 4 2 0 185.08 193.03 1.74 o 5 2 0 117.37 108.34 1.38 o 6 2 0 37.94 42.24 0.98 o -5 3 0 18.22 18.02 0.91 o -4 3 0 251.25 247.36 2.11 o -3 3 0 19.02 17.16 0.61 o -2 3 0 179.22 189.26 1.49 o -1 3 0 134.32 129.72 1.79 o 0 3 0 241.24 230.31 1.51 o 1 3 0 687.46 702.89 5.37 o 2 3 0 103.66 101.35 0.97 o 3 3 0 367.15 377.36 2.54 o 4 3 0 75.17 78.64 1.07 o 5 3 0 17.03 16.61 0.66 o 6 3 0 14.77 14.23 0.70 o -5 4 0 21.37 20.64 2.69 o -4 4 0 0.43 0.40 0.32 o -3 4 0 42.86 42.95 0.78 o -2 4 0 26.75 21.46 0.50 o -1 4 0 41.89 42.59 0.67 o 0 4 0 104.76 107.14 1.01 o 1 4 0 1721.84 1835.01 14.84 o 2 4 0 34.03 43.52 0.66 o 3 4 0 222.99 233.42 1.85 o 4 4 0 1.58 2.45 0.34 o 5 4 0 88.08 84.76 1.81 o 6 4 0 1.69 2.24 0.54 o -5 5 0 0.15 1.32 1.01 o -4 5 0 23.67 24.73 0.99 o -3 5 0 12.26 12.90 0.58 o -2 5 0 122.93 118.13 1.21 o -1 5 0 97.17 97.58 1.37 o 0 5 0 0.01 0.13 0.24 o 1 5 0 246.93 235.32 1.80 o 2 5 0 203.69 181.44 1.53 o 3 5 0 14.70 15.73 0.54 o 4 5 0 31.70 29.94 0.74 o 5 5 0 48.85 48.85 1.27 o 6 5 0 0.59 0.62 0.52 o -4 6 0 12.35 14.67 1.98 o -3 6 0 22.63 24.45 0.99 o -2 6 0 58.15 56.00 0.87 o -1 6 0 146.82 143.93 1.41 o 0 6 0 14.31 13.41 0.52 o 1 6 0 0.05 -0.11 0.34 o 2 6 0 92.12 87.56 1.07 o 3 6 0 94.97 94.67 1.15 o 4 6 0 8.46 8.53 0.83 o 5 6 0 0.29 -0.08 0.46 o 6 6 0 19.19 17.04 1.00 o -4 7 0 6.84 6.21 0.75 o -3 7 0 30.58 31.43 1.16 o -2 7 0 2.77 2.51 0.78 o -1 7 0 9.97 9.85 0.49 o 0 7 0 124.16 116.72 1.36 o 1 7 0 113.77 109.36 1.31 o 2 7 0 2.13 1.79 0.35 o 3 7 0 80.29 79.27 1.52 o 4 7 0 49.08 50.22 1.33 o 5 7 0 0.96 0.55 0.50 o -3 8 0 27.50 24.90 1.34 o -2 8 0 22.23 21.44 1.05 o -1 8 0 0.16 -0.05 0.80 o 0 8 0 26.44 26.83 0.76 o 1 8 0 52.88 52.99 1.03 o 2 8 0 11.48 11.19 0.87 o 3 8 0 9.37 9.25 0.77 o 4 8 0 3.86 4.05 0.66 o 5 8 0 78.81 80.38 1.80 o -2 9 0 2.62 1.87 0.61 o -1 9 0 10.44 10.46 0.91 o 0 9 0 34.37 33.78 0.90 o 1 9 0 4.36 4.62 0.58 o 2 9 0 76.61 75.04 1.59 o 3 9 0 64.49 62.39 1.55 o 4 9 0 0.00 -0.33 0.54 o -1 10 0 4.90 4.39 1.79 o 0 10 0 36.93 41.00 1.98 o 1 10 0 26.86 30.69 1.09 o 2 10 0 32.28 35.02 1.20 o 3 10 0 35.66 36.40 1.28 o -3 -10 1 49.15 50.16 1.46 o -2 -10 1 35.95 36.24 1.30 o -1 -10 1 0.45 2.88 0.90 o 0 -10 1 6.49 6.05 2.45 o -4 -9 1 23.57 24.50 1.13 o -3 -9 1 0.16 -0.14 0.80 o -2 -9 1 47.49 46.84 1.29 o -1 -9 1 71.54 72.45 1.28 o 0 -9 1 0.05 0.05 1.51 o 1 -9 1 2.10 1.79 0.64 o 2 -9 1 2.57 2.12 0.67 o -5 -8 1 37.34 34.11 1.28 o -4 -8 1 59.96 56.74 1.45 o -3 -8 1 3.12 3.94 0.71 o -2 -8 1 0.22 0.50 0.34 o -1 -8 1 4.20 5.90 0.50 o 0 -8 1 88.32 86.08 1.25 o 1 -8 1 32.91 29.25 1.20 o 2 -8 1 21.75 20.99 1.51 o 3 -8 1 7.87 9.41 1.72 o -5 -7 1 13.94 14.52 0.98 o -4 -7 1 28.30 28.17 1.07 o -3 -7 1 43.17 50.23 0.96 o -2 -7 1 73.98 67.34 1.08 o -1 -7 1 24.16 20.01 0.74 o 0 -7 1 247.54 242.83 2.10 o 1 -7 1 16.30 15.10 0.87 o 2 -7 1 1.13 1.09 0.50 o 3 -7 1 37.53 34.88 1.37 o 4 -7 1 32.77 35.64 1.37 o -6 -6 1 10.28 10.52 1.23 o -5 -6 1 33.31 33.91 1.18 o -4 -6 1 5.22 4.18 0.52 o -3 -6 1 13.74 13.65 0.58 o -2 -6 1 74.86 70.89 1.15 o -1 -6 1 129.60 136.38 1.43 o 0 -6 1 19.97 17.27 0.56 o 1 -6 1 49.75 50.21 0.79 o 2 -6 1 120.67 117.42 2.45 o 3 -6 1 5.14 4.81 1.06 o 4 -6 1 16.26 14.89 0.93 o -6 -5 1 7.65 7.88 1.04 o -5 -5 1 5.15 4.56 0.47 o -4 -5 1 562.23 561.03 3.82 o -3 -5 1 3.77 5.07 0.38 o -2 -5 1 315.75 335.85 2.41 o 0 -5 1 443.13 431.95 2.80 o 1 -5 1 0.57 1.20 0.22 o 2 -5 1 138.98 132.02 1.22 o 3 -5 1 0.02 -0.22 0.38 o 4 -5 1 55.92 56.18 2.64 o 5 -5 1 2.58 2.83 0.60 o -6 -4 1 23.48 24.20 1.46 o -5 -4 1 8.21 9.27 0.56 o -4 -4 1 108.51 109.07 1.31 o -3 -4 1 0.58 0.27 0.24 o -2 -4 1 104.59 117.44 1.17 o -1 -4 1 408.68 455.94 2.84 o 0 -4 1 889.63 991.13 5.31 o 1 -4 1 863.64 865.12 4.74 o 2 -4 1 155.51 165.70 2.69 o 3 -4 1 103.06 98.21 1.08 o 4 -4 1 4.96 5.04 0.58 o 5 -4 1 0.06 -0.10 0.68 o -6 -3 1 0.60 1.30 0.47 o -5 -3 1 0.01 -0.12 0.32 o -4 -3 1 519.38 533.61 3.53 o -3 -3 1 634.58 648.18 3.89 o -2 -3 1 1516.41 1627.20 8.64 o -1 -3 1 668.41 714.84 3.98 o 0 -3 1 107.56 110.10 0.94 o 1 -3 1 247.38 235.15 3.22 o 2 -3 1 0.23 -0.05 0.17 o 3 -3 1 2.59 3.27 0.29 o 4 -3 1 146.86 133.18 2.85 o 5 -3 1 108.59 105.64 1.97 o -6 -2 1 1.80 1.56 0.46 o -5 -2 1 30.68 34.04 0.81 o -4 -2 1 254.02 245.12 2.02 o -3 -2 1 65.24 72.43 0.88 o -2 -2 1 571.05 583.93 3.32 o -1 -2 1 98.34 100.14 1.35 o 0 -2 1 626.95 739.94 3.84 o 1 -2 1 334.23 326.18 1.53 o 2 -2 1 374.08 389.98 2.36 o 3 -2 1 167.53 145.98 1.32 o 4 -2 1 6.94 7.32 0.45 o 5 -2 1 39.75 37.79 1.15 o 6 -2 1 10.91 12.64 0.85 o -6 -1 1 0.14 -0.19 0.40 o -5 -1 1 17.18 16.21 0.62 o -3 -1 1 659.03 713.88 4.09 o -2 -1 1 216.03 231.27 1.69 o -1 -1 1 1328.81 1435.61 9.11 o 0 -1 1 896.62 910.78 4.19 o 1 -1 1 1913.91 1980.41 18.73 o 2 -1 1 93.58 104.60 2.30 o 3 -1 1 1003.36 1063.12 5.81 o 4 -1 1 3.43 3.47 0.33 o 5 -1 1 0.13 -0.06 0.27 o 6 -1 1 0.54 0.71 0.61 o -6 0 1 25.70 25.47 1.04 o -5 0 1 10.88 9.32 0.51 o -4 0 1 2.11 3.29 0.30 o -3 0 1 45.12 43.21 0.65 o -2 0 1 139.17 128.71 1.02 o -1 0 1 639.68 657.72 2.89 o 0 0 1 32.60 35.01 0.29 o 1 0 1 4512.02 4670.70 42.22 o 2 0 1 248.74 268.59 2.36 o 3 0 1 530.35 574.41 3.49 o 4 0 1 3.12 2.25 0.28 o 5 0 1 0.01 -0.05 0.27 o 6 0 1 11.67 12.50 0.64 o -6 1 1 11.68 13.68 0.86 o -5 1 1 0.01 -0.50 0.34 o -4 1 1 1.76 1.52 0.27 o -3 1 1 305.58 350.14 3.42 o -2 1 1 878.61 948.88 4.98 o -1 1 1 2850.05 2995.65 16.59 o 0 1 1 1061.47 1112.79 5.08 o 1 1 1 311.88 328.94 1.60 o 2 1 1 112.31 109.99 0.97 o 3 1 1 100.35 108.60 1.12 o 4 1 1 17.57 19.01 0.57 o 5 1 1 3.15 4.12 0.39 o 6 1 1 11.86 12.51 1.59 o -6 2 1 3.94 3.97 0.61 o -5 2 1 0.81 0.88 0.38 o -4 2 1 88.97 90.70 1.17 o -3 2 1 296.12 311.44 2.23 o -2 2 1 222.31 240.74 2.33 o -1 2 1 1508.25 1594.50 9.08 o 0 2 1 0.36 0.12 0.22 o 1 2 1 26.89 28.83 0.80 o 2 2 1 0.30 1.20 0.56 o 3 2 1 90.22 91.69 1.00 o 4 2 1 72.41 68.79 1.00 o 5 2 1 12.40 12.17 0.58 o 6 2 1 15.96 16.38 0.70 o -6 3 1 13.58 12.36 1.46 o -5 3 1 0.52 0.01 0.31 o -4 3 1 65.10 66.62 1.04 o -3 3 1 70.95 72.97 0.96 o -2 3 1 6.19 4.44 0.38 o -1 3 1 0.78 1.32 0.21 o 0 3 1 57.20 59.35 0.71 o 1 3 1 413.22 436.70 2.47 o 2 3 1 241.75 240.97 2.04 o 3 3 1 46.53 44.93 0.71 o 4 3 1 228.57 229.33 2.28 o 5 3 1 27.29 28.90 0.83 o 6 3 1 12.34 11.67 0.64 o -5 4 1 17.27 17.70 1.16 o -4 4 1 0.26 0.02 0.28 o -3 4 1 45.51 44.34 0.91 o -2 4 1 125.55 119.13 1.20 o -1 4 1 52.03 48.89 0.69 o 0 4 1 2.63 3.24 0.24 o 1 4 1 366.02 377.45 2.55 o 2 4 1 233.06 234.35 1.65 o 3 4 1 2.82 2.31 0.25 o 4 4 1 3.74 3.92 0.35 o 5 4 1 46.82 46.47 0.95 o 6 4 1 20.12 20.63 0.95 o -5 5 1 6.85 10.27 2.88 o -4 5 1 0.28 0.72 0.52 o -3 5 1 6.02 5.08 0.41 o -2 5 1 20.91 20.02 0.57 o -1 5 1 65.86 62.29 0.83 o 0 5 1 134.64 128.17 1.19 o 1 5 1 102.44 101.42 1.04 o 2 5 1 303.66 304.62 2.08 o 3 5 1 291.22 290.16 2.14 o 4 5 1 0.46 0.48 0.27 o 5 5 1 23.35 22.46 0.95 o 6 5 1 17.11 17.76 0.93 o -4 6 1 0.08 0.35 0.42 o -3 6 1 68.12 68.15 1.48 o -2 6 1 10.60 11.50 0.52 o -1 6 1 40.36 37.25 0.71 o 0 6 1 134.98 136.74 1.34 o 1 6 1 352.68 349.03 2.45 o 2 6 1 68.32 71.23 2.23 o 3 6 1 225.97 216.71 2.47 o 4 6 1 1.58 2.26 0.50 o 5 6 1 15.43 15.48 0.90 o 6 6 1 3.25 3.87 0.64 o -4 7 1 1.58 1.79 0.78 o -3 7 1 1.71 1.63 0.50 o -2 7 1 170.26 167.42 2.58 o -1 7 1 10.24 10.25 0.50 o 0 7 1 186.18 183.86 1.74 o 1 7 1 47.19 45.14 0.88 o 2 7 1 27.72 30.25 0.90 o 3 7 1 1.26 0.98 0.46 o 4 7 1 26.71 27.62 1.06 o 5 7 1 22.46 19.65 1.00 o -3 8 1 1.68 1.95 0.54 o -2 8 1 125.27 125.83 3.92 o -1 8 1 18.66 17.56 0.67 o 0 8 1 21.94 20.28 0.75 o 1 8 1 28.47 27.32 0.78 o 2 8 1 109.37 105.05 1.78 o 3 8 1 129.37 127.26 2.07 o 4 8 1 11.16 11.33 1.11 o 5 8 1 3.62 4.03 0.71 o -2 9 1 0.99 0.52 1.04 o -1 9 1 20.46 20.92 1.25 o 0 9 1 38.34 37.78 0.96 o 1 9 1 1.50 1.84 0.59 o 2 9 1 0.02 -0.12 0.44 o 3 9 1 55.03 57.75 1.48 o 4 9 1 75.83 78.07 1.80 o -1 10 1 6.11 6.38 2.08 o 0 10 1 8.51 9.34 1.18 o 1 10 1 43.54 46.11 1.30 o 2 10 1 90.19 92.44 2.52 o 3 10 1 45.07 47.60 1.44 o -2 -10 2 78.49 79.92 2.69 o -1 -10 2 4.68 4.20 0.99 o -3 -9 2 52.95 55.13 1.46 o -2 -9 2 9.26 10.49 0.76 o -1 -9 2 59.92 56.63 1.58 o 0 -9 2 27.85 29.26 1.30 o 1 -9 2 2.64 2.23 0.70 o -4 -8 2 28.54 25.75 1.05 o -3 -8 2 66.38 58.98 1.42 o -2 -8 2 2.58 4.29 0.48 o -1 -8 2 13.32 12.07 0.62 o 0 -8 2 28.94 25.54 1.12 o 1 -8 2 81.11 78.20 1.79 o 2 -8 2 88.37 85.38 1.98 o -5 -7 2 0.70 1.00 0.53 o -4 -7 2 22.11 29.07 1.07 o -3 -7 2 0.46 0.78 0.42 o -2 -7 2 179.96 196.23 1.96 o -1 -7 2 120.52 107.35 1.38 o 0 -7 2 1.98 3.00 0.37 o 1 -7 2 121.60 119.95 2.29 o 2 -7 2 5.70 4.91 0.70 o 3 -7 2 3.59 3.16 1.13 o -5 -6 2 73.09 76.04 2.57 o -4 -6 2 2.87 3.31 0.41 o -3 -6 2 54.22 45.47 0.93 o -2 -6 2 11.51 11.31 0.55 o -1 -6 2 284.46 267.05 2.20 o 0 -6 2 9.42 8.53 0.44 o 1 -6 2 42.80 41.99 1.22 o 2 -6 2 2.30 1.96 0.50 o 3 -6 2 215.28 212.47 3.30 o 4 -6 2 0.00 -0.27 0.50 o -6 -5 2 1.52 1.46 0.75 o -5 -5 2 3.06 4.09 0.46 o -4 -5 2 0.87 0.87 0.33 o -3 -5 2 274.42 272.58 2.26 o -2 -5 2 127.88 121.39 1.33 o -1 -5 2 258.83 276.94 3.67 o 0 -5 2 56.37 49.54 0.77 o 1 -5 2 107.51 102.55 1.46 o 2 -5 2 13.10 12.52 0.78 o 3 -5 2 82.76 79.67 1.66 o 4 -5 2 1.46 1.61 0.58 o -6 -4 2 29.64 33.18 1.22 o -5 -4 2 122.21 115.16 1.50 o -4 -4 2 92.18 95.09 1.27 o -3 -4 2 18.36 18.12 0.58 o -1 -4 2 372.90 406.06 3.76 o 0 -4 2 110.65 99.87 1.01 o 1 -4 2 140.01 142.37 1.29 o 2 -4 2 75.78 75.78 1.40 o 3 -4 2 5.07 4.13 0.53 o 4 -4 2 62.28 62.54 1.51 o 5 -4 2 0.04 0.13 0.49 o -6 -3 2 18.38 20.47 1.51 o -5 -3 2 67.56 63.10 1.08 o -4 -3 2 2.74 2.73 0.35 o -3 -3 2 103.80 112.69 1.20 o -2 -3 2 32.87 34.57 0.62 o -1 -3 2 1647.72 1796.07 9.09 o 0 -3 2 0.36 0.30 0.19 o 1 -3 2 210.91 213.47 3.16 o 2 -3 2 19.38 16.20 0.67 o 3 -3 2 30.26 30.53 0.66 o 4 -3 2 3.00 2.89 0.51 o 5 -3 2 0.61 0.30 0.46 o -6 -2 2 12.20 13.18 0.87 o -5 -2 2 2.98 2.31 0.35 o -4 -2 2 198.16 203.00 1.79 o -3 -2 2 159.11 153.83 1.37 o -2 -2 2 1.73 2.69 0.26 o -1 -2 2 481.76 501.36 2.86 o 0 -2 2 481.77 505.30 4.65 o 1 -2 2 19.89 23.85 0.65 o 2 -2 2 2.97 2.91 0.23 o 3 -2 2 5.11 4.73 0.32 o 4 -2 2 119.21 116.90 1.26 o 5 -2 2 3.44 4.03 0.58 o 6 -2 2 11.75 11.86 0.91 o -6 -1 2 50.02 53.37 1.45 o -5 -1 2 14.69 13.49 2.01 o -4 -1 2 140.74 137.59 1.88 o -3 -1 2 123.15 113.11 1.51 o -2 -1 2 7.77 6.90 0.54 o -1 -1 2 23.94 22.48 0.42 o 0 -1 2 0.23 0.30 0.14 o 1 -1 2 200.36 195.92 3.37 o 2 -1 2 461.50 474.46 2.75 o 3 -1 2 0.91 1.12 0.21 o 4 -1 2 191.09 190.21 1.70 o 5 -1 2 30.40 30.41 0.75 o 6 -1 2 5.23 4.38 0.78 o -6 0 2 6.58 7.69 0.72 o -5 0 2 10.85 9.70 0.70 o -4 0 2 13.00 10.75 0.46 o -3 0 2 2.47 3.59 0.26 o -2 0 2 227.33 209.96 1.39 o -1 0 2 1099.62 1172.97 18.02 o 0 0 2 102.44 112.05 0.85 o 1 0 2 683.96 711.86 3.70 o 2 0 2 675.66 709.49 5.26 o 3 0 2 7.29 5.82 0.33 o 4 0 2 46.65 45.34 0.82 o 5 0 2 1.51 2.38 0.33 o 6 0 2 0.19 0.64 0.45 o -6 1 2 0.36 0.54 0.92 o -5 1 2 26.98 26.76 1.00 o -4 1 2 29.10 29.86 0.67 o -3 1 2 70.15 74.10 0.86 o -2 1 2 15.57 12.62 0.32 o -1 1 2 572.99 599.05 2.66 o 0 1 2 116.33 121.21 1.01 o 1 1 2 161.85 163.10 1.11 o 2 1 2 53.66 53.05 0.75 o 3 1 2 360.65 358.65 3.92 o 4 1 2 7.15 6.37 0.40 o 5 1 2 0.11 0.95 0.66 o 6 1 2 4.33 7.32 1.51 o -6 2 2 3.82 3.47 0.62 o -5 2 2 6.01 4.08 0.56 o -4 2 2 11.49 11.92 0.51 o -3 2 2 92.03 90.20 1.01 o -2 2 2 373.18 389.98 2.42 o -1 2 2 76.44 89.14 0.80 o 0 2 2 1386.02 1461.39 8.90 o 1 2 2 215.69 205.23 2.02 o 2 2 2 28.23 25.66 0.90 o 3 2 2 99.62 98.48 1.06 o 4 2 2 89.39 83.62 1.12 o 5 2 2 1.09 0.74 0.28 o 6 2 2 5.52 5.94 0.66 o -6 3 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