#------------------------------------------------------------------------------ #$Date: 2011-10-07 16:37:56 +0300 (Fri, 07 Oct 2011) $ #$Revision: 27934 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/14/2231427.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231427_Fobs loop_ _publ_author_name 'Asiri, Abdullah M.' 'Faidallah, Hassan M.' 'Al-Youbi, Abdulrahman O.' 'Ng, Seik Weng' _publ_section_title ; 4-(3,5-Dimethyl-1H-pyrazol-1-yl)benzenesulfonamide ; _journal_coeditor_code BT5610 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2427 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.720 _cell_angle_gamma 90.000 _cell_length_a 7.9649 _cell_length_b 11.7827 _cell_length_c 12.2720 _exptl_crystal_F_000 528.00 _reflns_d_resolution_high 0.8013 _[local]_cod_data_source_file bt5610Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 134.65 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 741.72 765.91 4.72 o 4 0 0 4168.54 4318.77 23.90 o 6 0 0 1040.75 1176.96 10.39 o 8 0 0 43.55 42.74 4.51 o 1 1 0 1906.39 1779.24 9.24 o 3 1 0 26.12 24.94 0.78 o 4 1 0 120.17 133.08 2.88 o 5 1 0 489.93 435.77 6.66 o 6 1 0 656.05 679.38 5.47 o 7 1 0 199.22 195.40 4.14 o 8 1 0 127.92 129.73 4.10 o 9 1 0 19.48 18.44 1.24 o 1 2 0 4230.82 3656.76 10.77 o 2 2 0 182.95 183.11 1.96 o 3 2 0 2.15 11.85 0.87 o 4 2 0 7878.85 7928.34 39.07 o 5 2 0 0.35 3.64 0.67 o 6 2 0 0.76 0.67 0.53 o 7 2 0 1085.28 1114.24 10.48 o 8 2 0 23.28 26.72 1.75 o 9 2 0 116.80 112.50 3.30 o 1 3 0 2391.45 2247.63 7.71 o 2 3 0 6470.97 6187.66 78.27 o 3 3 0 472.51 485.90 7.63 o 4 3 0 330.12 365.72 4.21 o 5 3 0 1295.00 1233.87 12.27 o 6 3 0 847.52 927.37 7.60 o 7 3 0 282.90 267.37 5.05 o 8 3 0 19.93 26.52 1.79 o 9 3 0 637.79 651.96 10.00 o 0 4 0 1188.38 1288.44 14.64 o 1 4 0 201.43 244.44 2.19 o 2 4 0 2004.13 2122.17 8.16 o 3 4 0 1392.73 1378.58 9.23 o 4 4 0 817.68 881.11 15.80 o 5 4 0 436.77 443.18 7.04 o 6 4 0 517.34 503.88 5.93 o 7 4 0 960.62 956.43 12.58 o 8 4 0 341.34 326.59 6.76 o 9 4 0 241.51 228.95 9.47 o 1 5 0 71.69 89.24 1.36 o 2 5 0 326.69 346.55 3.96 o 3 5 0 160.25 163.25 3.26 o 4 5 0 12.60 19.42 1.95 o 5 5 0 521.31 571.45 5.05 o 6 5 0 12.40 13.27 0.98 o 7 5 0 57.48 55.73 2.02 o 8 5 0 349.92 330.05 5.31 o 9 5 0 1105.21 1124.28 38.64 o 0 6 0 760.79 778.20 17.40 o 1 6 0 89.35 83.25 1.67 o 2 6 0 147.90 170.62 3.48 o 3 6 0 127.97 125.21 5.95 o 4 6 0 1159.15 1147.37 11.30 o 5 6 0 169.35 163.93 2.84 o 6 6 0 215.50 213.19 3.87 o 7 6 0 492.28 525.05 6.07 o 8 6 0 6.94 3.51 0.70 o 9 6 0 22.31 30.13 2.36 o 1 7 0 359.26 391.88 5.96 o 2 7 0 2171.12 2110.84 13.34 o 3 7 0 171.46 168.96 3.49 o 4 7 0 342.89 367.07 4.61 o 5 7 0 98.60 99.87 3.46 o 6 7 0 530.86 540.07 7.34 o 7 7 0 0.01 0.15 0.41 o 8 7 0 392.34 395.94 5.34 o 0 8 0 2708.52 2629.20 78.39 o 1 8 0 240.32 215.19 4.49 o 2 8 0 85.32 85.87 2.31 o 3 8 0 5.85 5.58 0.69 o 4 8 0 864.23 872.21 11.34 o 5 8 0 330.96 360.55 6.41 o 6 8 0 284.08 297.16 6.39 o 7 8 0 12.41 14.80 1.30 o 8 8 0 103.06 96.98 2.91 o 1 9 0 17.06 23.30 1.18 o 2 9 0 2867.92 2722.17 12.90 o 3 9 0 386.17 375.07 5.58 o 4 9 0 506.29 492.99 6.09 o 5 9 0 64.41 64.56 2.09 o 6 9 0 1.19 1.07 0.78 o 7 9 0 134.17 139.68 4.24 o 0 10 0 1792.21 1869.30 19.05 o 1 10 0 595.69 607.51 6.93 o 2 10 0 231.41 231.64 4.92 o 3 10 0 170.95 190.24 4.14 o 4 10 0 250.09 236.08 5.02 o 5 10 0 3.18 1.20 0.87 o 6 10 0 7.41 8.98 1.20 o 7 10 0 180.44 179.18 3.96 o 1 11 0 52.20 50.52 2.48 o 2 11 0 273.95 297.14 6.62 o 3 11 0 236.98 233.72 5.71 o 4 11 0 11.45 12.77 1.16 o 5 11 0 82.34 87.42 3.08 o 6 11 0 3.07 2.16 0.47 o 0 12 0 64.73 69.21 4.02 o 1 12 0 3.87 3.84 0.83 o 2 12 0 19.87 23.42 3.11 o 3 12 0 130.50 120.71 4.88 o 4 12 0 27.34 24.67 1.78 o 5 12 0 0.02 -0.02 0.37 o 1 13 0 0.84 1.59 0.87 o 2 13 0 126.83 138.71 3.85 o 3 13 0 43.42 40.81 3.49 o 4 13 0 974.02 986.00 8.73 o 0 14 0 126.46 133.71 5.87 o 1 14 0 153.76 138.20 3.06 o 2 14 0 519.98 469.00 11.13 o -9 0 1 186.90 201.31 10.99 o -7 0 1 33.89 23.22 2.24 o -5 0 1 365.23 288.11 7.63 o -3 0 1 3244.85 3131.67 19.36 o -1 0 1 23.20 23.38 1.07 o 1 0 1 1671.29 1546.83 10.64 o 3 0 1 389.52 384.21 4.16 o 5 0 1 541.96 596.90 12.51 o 7 0 1 100.69 114.94 5.43 o 9 0 1 356.75 353.19 9.57 o -9 1 1 9.76 13.38 1.34 o -8 1 1 4.73 3.87 0.98 o -7 1 1 439.88 420.78 6.61 o -6 1 1 1386.95 1452.21 12.92 o -5 1 1 1031.75 1077.86 12.91 o -4 1 1 1528.55 1681.97 16.63 o -3 1 1 688.99 759.54 5.67 o -2 1 1 156.79 158.50 2.70 o -1 1 1 216.26 203.84 2.42 o 0 1 1 1695.93 1627.36 4.27 o 1 1 1 568.01 578.24 3.19 o 2 1 1 4081.73 3966.82 20.01 o 3 1 1 25.08 12.47 0.52 o 4 1 1 1317.33 1462.66 7.42 o 5 1 1 58.63 66.08 2.40 o 6 1 1 303.01 265.40 3.79 o 7 1 1 1058.89 1090.59 11.33 o 8 1 1 9.02 9.39 1.29 o 9 1 1 1.56 1.48 0.60 o -9 2 1 14.37 11.63 1.61 o -8 2 1 663.23 688.89 8.32 o -7 2 1 253.38 263.01 4.76 o -6 2 1 832.04 892.04 7.37 o -5 2 1 5.50 11.92 0.98 o -4 2 1 622.05 559.67 4.93 o -3 2 1 5.88 10.74 0.54 o -2 2 1 7518.02 6494.25 58.00 o -1 2 1 754.75 748.59 2.46 o 0 2 1 1975.95 1957.22 4.68 o 1 2 1 116.43 108.14 1.19 o 2 2 1 3069.17 3129.23 10.84 o 3 2 1 6.73 8.75 0.44 o 4 2 1 404.44 421.60 5.71 o 5 2 1 699.99 724.07 8.13 o 6 2 1 49.39 63.98 1.76 o 7 2 1 1.13 2.44 0.71 o 8 2 1 416.98 420.63 8.57 o 9 2 1 59.45 61.09 2.41 o -9 3 1 3.61 1.98 0.98 o -8 3 1 107.07 101.45 3.37 o -7 3 1 594.26 562.58 9.89 o -6 3 1 1783.86 1840.26 12.03 o -5 3 1 20.22 20.94 1.81 o -4 3 1 3130.65 3203.91 19.92 o -3 3 1 1.58 2.52 0.34 o -2 3 1 1923.49 1854.55 9.52 o -1 3 1 6.61 11.90 0.48 o 0 3 1 4603.60 4350.85 14.50 o 1 3 1 3.17 4.22 0.28 o 2 3 1 3247.02 3271.05 9.92 o 3 3 1 504.05 611.94 5.04 o 4 3 1 803.68 909.20 13.65 o 5 3 1 2.24 1.15 0.58 o 6 3 1 1899.88 1877.83 18.50 o 7 3 1 11.87 12.14 1.22 o 8 3 1 158.98 151.75 4.93 o 9 3 1 154.74 155.55 3.71 o -9 4 1 149.65 135.68 4.41 o -8 4 1 37.57 42.08 1.82 o -7 4 1 125.10 115.88 2.98 o -6 4 1 1286.00 1319.08 9.63 o -5 4 1 1376.30 1397.49 19.08 o -4 4 1 2410.83 2410.30 46.73 o -3 4 1 11.39 12.62 0.82 o -2 4 1 240.30 216.84 2.24 o -1 4 1 740.39 747.37 9.42 o 0 4 1 658.30 615.59 7.44 o 1 4 1 643.36 610.36 5.18 o 2 4 1 63.97 36.56 1.20 o 3 4 1 343.35 366.28 3.98 o 4 4 1 3847.08 3737.73 77.81 o 5 4 1 280.30 246.72 6.51 o 6 4 1 146.99 136.10 2.71 o 7 4 1 4.12 4.52 0.87 o 8 4 1 820.38 822.40 10.59 o 9 4 1 26.14 27.50 1.95 o -9 5 1 22.73 19.53 1.60 o -8 5 1 336.88 331.44 5.39 o -7 5 1 761.56 751.13 7.39 o -6 5 1 0.85 0.99 0.59 o -5 5 1 175.58 175.90 3.04 o -4 5 1 233.75 268.31 4.94 o -3 5 1 234.04 259.09 11.36 o -2 5 1 2338.61 2337.01 13.91 o -1 5 1 25.59 42.53 1.42 o 0 5 1 365.50 425.88 6.41 o 1 5 1 100.12 91.41 1.61 o 2 5 1 288.96 340.66 4.58 o 3 5 1 317.48 289.99 3.83 o 4 5 1 30.67 30.44 2.14 o 5 5 1 162.61 157.93 2.66 o 6 5 1 1422.29 1475.55 26.40 o 7 5 1 931.34 939.95 9.70 o 8 5 1 813.49 791.86 7.24 o 9 5 1 20.00 20.70 2.12 o -9 6 1 202.14 194.13 6.04 o -8 6 1 11.38 14.98 1.19 o -7 6 1 39.06 43.68 2.30 o -6 6 1 12.65 11.38 1.12 o -5 6 1 1035.70 1039.64 8.51 o -4 6 1 221.91 243.63 3.77 o -3 6 1 30.94 43.82 2.04 o -2 6 1 130.57 124.81 2.61 o -1 6 1 355.88 338.73 4.19 o 0 6 1 149.42 185.33 2.86 o 1 6 1 355.44 293.78 2.90 o 2 6 1 4.25 7.01 0.76 o 3 6 1 122.26 135.36 3.38 o 4 6 1 932.24 980.03 10.86 o 5 6 1 1857.49 1797.62 20.27 o 6 6 1 1457.44 1450.09 16.18 o 7 6 1 0.26 0.88 0.65 o 8 6 1 435.10 451.49 6.13 o 9 6 1 582.08 574.54 8.68 o -8 7 1 64.09 57.56 1.94 o -7 7 1 168.37 189.86 3.74 o -6 7 1 0.36 0.57 0.84 o -5 7 1 2.77 1.67 0.68 o -4 7 1 182.45 181.22 3.07 o -3 7 1 1194.91 1165.52 11.12 o -2 7 1 239.85 215.46 3.75 o -1 7 1 2.99 6.44 0.82 o 0 7 1 1026.50 1108.85 10.21 o 1 7 1 32.80 20.16 1.13 o 2 7 1 57.66 89.62 3.32 o 3 7 1 2010.44 1944.12 16.21 o 4 7 1 1898.23 1808.68 20.82 o 5 7 1 56.40 46.71 2.12 o 6 7 1 20.42 29.41 1.48 o 7 7 1 988.69 1035.66 8.68 o 8 7 1 241.18 226.55 3.53 o -8 8 1 23.95 27.96 1.62 o -7 8 1 15.69 15.85 1.22 o -6 8 1 111.45 111.24 4.06 o -5 8 1 1.69 2.38 0.66 o -4 8 1 39.89 38.68 1.43 o -3 8 1 290.09 279.19 3.68 o -2 8 1 572.20 584.11 5.50 o -1 8 1 4.51 2.86 0.60 o 0 8 1 256.57 255.56 6.31 o 1 8 1 5.95 5.90 0.86 o 2 8 1 3528.52 3596.35 13.90 o 3 8 1 359.78 340.57 4.29 o 4 8 1 86.77 88.74 2.15 o 5 8 1 594.76 629.47 8.54 o 6 8 1 1133.88 1112.64 11.38 o 7 8 1 1.83 1.11 0.72 o 8 8 1 121.40 123.47 3.10 o -7 9 1 62.55 70.54 2.36 o -6 9 1 49.91 61.18 3.25 o -5 9 1 4.36 2.87 0.82 o -4 9 1 517.12 516.15 7.68 o -3 9 1 46.88 45.55 1.79 o -2 9 1 366.64 388.83 4.42 o -1 9 1 712.29 709.55 10.59 o 0 9 1 1839.94 1849.99 11.56 o 1 9 1 151.51 142.14 2.68 o 2 9 1 24.79 25.06 1.19 o 3 9 1 44.89 53.95 1.93 o 4 9 1 2901.19 2743.50 26.03 o 5 9 1 120.47 117.78 3.16 o 6 9 1 486.39 511.41 7.13 o 7 9 1 187.76 199.15 4.89 o -7 10 1 17.15 19.43 1.38 o -6 10 1 165.84 194.90 5.19 o -5 10 1 80.36 70.51 2.85 o -4 10 1 456.07 498.19 7.30 o -3 10 1 90.30 103.44 3.43 o -2 10 1 3196.34 3197.78 22.05 o -1 10 1 324.15 346.42 7.58 o 0 10 1 0.24 -0.24 0.46 o 1 10 1 0.90 0.75 0.55 o 2 10 1 3109.51 3005.73 24.60 o 3 10 1 28.80 32.10 2.18 o 4 10 1 814.72 843.99 9.06 o 5 10 1 0.07 0.46 0.50 o 6 10 1 143.67 148.63 4.58 o 7 10 1 13.59 14.40 1.11 o -6 11 1 477.21 502.60 5.69 o -5 11 1 129.44 146.12 3.63 o -4 11 1 1011.24 1035.47 14.60 o -3 11 1 590.94 602.61 11.09 o -2 11 1 90.04 76.75 3.44 o -1 11 1 5.25 6.05 1.14 o 0 11 1 3104.03 3196.91 36.25 o 1 11 1 369.40 369.25 6.36 o 2 11 1 21.26 25.28 2.50 o 3 11 1 99.54 104.42 4.31 o 4 11 1 83.42 84.70 2.93 o 5 11 1 29.13 30.56 1.64 o 6 11 1 107.42 108.71 3.25 o -5 12 1 504.74 491.19 6.33 o -4 12 1 201.69 217.13 4.74 o -3 12 1 11.63 10.03 1.63 o -2 12 1 1965.29 2076.27 29.24 o -1 12 1 318.38 323.79 6.97 o 0 12 1 232.85 255.55 5.36 o 1 12 1 9.68 11.47 1.18 o 2 12 1 309.10 302.11 8.09 o 3 12 1 102.52 89.09 3.27 o 4 12 1 47.60 51.85 1.86 o 5 12 1 285.06 273.72 9.05 o -4 13 1 674.39 679.90 14.18 o -3 13 1 534.15 522.64 32.44 o -2 13 1 33.08 42.53 2.79 o -1 13 1 313.37 310.32 6.31 o 0 13 1 230.37 231.14 5.29 o 1 13 1 373.55 376.98 8.22 o 2 13 1 187.22 196.30 4.83 o 3 13 1 187.50 207.00 4.68 o 4 13 1 3.11 1.39 1.31 o -2 14 1 0.51 0.48 0.49 o -1 14 1 127.23 118.56 3.56 o 0 14 1 27.03 28.29 1.94 o 1 14 1 100.21 94.81 3.45 o 2 14 1 4.64 3.98 1.32 o -8 0 2 71.14 76.03 3.80 o -6 0 2 2864.54 2846.09 22.96 o -4 0 2 1625.07 1566.20 17.30 o -2 0 2 2936.47 2880.09 17.04 o 2 0 2 23.96 16.79 0.47 o 4 0 2 232.98 160.08 3.73 o 6 0 2 704.95 643.04 7.87 o 8 0 2 145.37 152.33 5.52 o -9 1 2 113.15 114.05 2.81 o -8 1 2 1249.86 1320.46 12.38 o -7 1 2 38.00 36.81 2.04 o -6 1 2 599.48 658.61 8.00 o -5 1 2 5.39 4.89 0.85 o -4 1 2 134.06 89.22 2.95 o -3 1 2 29.58 33.00 0.95 o -2 1 2 1459.91 1377.18 4.37 o -1 1 2 508.82 479.32 3.59 o 0 1 2 552.96 549.76 2.64 o 1 1 2 834.87 782.72 4.46 o 2 1 2 1191.83 1048.43 6.48 o 3 1 2 133.72 143.24 1.54 o 4 1 2 65.10 49.89 1.58 o 5 1 2 427.74 450.39 6.23 o 6 1 2 780.96 783.82 5.85 o 7 1 2 33.44 29.68 1.80 o 8 1 2 170.06 181.97 4.42 o 9 1 2 15.31 16.61 1.09 o -9 2 2 19.70 17.42 1.41 o -8 2 2 25.95 28.13 1.52 o -7 2 2 337.43 316.65 7.13 o -6 2 2 620.19 639.12 11.34 o -5 2 2 156.08 152.50 3.42 o -4 2 2 1033.20 1075.34 13.33 o -3 2 2 2128.26 2296.39 9.81 o -2 2 2 2091.80 2039.72 8.35 o -1 2 2 830.42 702.64 4.30 o 0 2 2 1429.55 1356.99 6.47 o 1 2 2 6529.13 5531.33 14.95 o 2 2 2 4517.12 4418.95 20.23 o 3 2 2 11.89 7.81 0.48 o 4 2 2 1017.53 1067.00 9.19 o 5 2 2 1100.71 1116.55 10.18 o 6 2 2 15.74 19.71 1.05 o 7 2 2 1343.09 1346.53 10.31 o 8 2 2 2.93 4.31 0.79 o 9 2 2 7.22 5.40 0.85 o -9 3 2 304.70 308.91 6.85 o -8 3 2 17.52 23.59 2.00 o -7 3 2 213.95 217.44 5.10 o -6 3 2 2.68 3.32 0.64 o -5 3 2 129.43 125.34 4.05 o -4 3 2 1784.50 1979.52 12.25 o -3 3 2 145.02 207.16 2.60 o -2 3 2 2258.96 2196.37 9.32 o -1 3 2 1365.68 1143.32 14.76 o 0 3 2 70.05 81.41 1.54 o 1 3 2 3551.12 3487.88 12.00 o 2 3 2 2998.14 2891.34 9.73 o 3 3 2 1793.17 1801.81 18.40 o 4 3 2 686.66 749.42 5.57 o 5 3 2 1266.91 1291.99 14.00 o 6 3 2 266.87 265.05 3.52 o 7 3 2 9.13 10.37 1.15 o 8 3 2 36.97 37.20 2.48 o 9 3 2 263.41 268.31 4.60 o -9 4 2 266.76 258.62 8.44 o -8 4 2 23.07 25.39 1.75 o -7 4 2 187.23 197.51 4.31 o -6 4 2 68.14 48.31 1.90 o -5 4 2 2.68 7.72 0.66 o -4 4 2 53.82 40.80 2.38 o -3 4 2 794.11 786.78 7.17 o -2 4 2 644.33 662.04 6.37 o -1 4 2 11.34 13.30 0.83 o 0 4 2 0.83 2.15 0.33 o 1 4 2 25.96 25.47 1.08 o 2 4 2 173.39 164.05 2.52 o 3 4 2 3776.36 3865.23 15.68 o 4 4 2 1.80 1.77 0.39 o 5 4 2 1416.57 1473.00 14.14 o 6 4 2 57.25 47.58 1.56 o 7 4 2 465.68 465.87 8.01 o 8 4 2 11.65 16.26 1.99 o 9 4 2 98.66 103.37 3.22 o -9 5 2 24.85 35.89 2.06 o -8 5 2 142.09 147.85 3.59 o -7 5 2 36.46 37.31 1.94 o -6 5 2 13.64 16.42 1.31 o -5 5 2 316.81 316.97 4.14 o -4 5 2 57.84 75.84 3.41 o -3 5 2 17.95 15.22 1.15 o -2 5 2 116.78 110.36 2.23 o -1 5 2 4.02 4.76 0.53 o 0 5 2 284.77 353.33 4.18 o 1 5 2 685.24 681.05 7.46 o 2 5 2 724.23 715.62 5.72 o 3 5 2 1372.14 1506.20 13.31 o 4 5 2 36.15 29.64 1.39 o 5 5 2 958.60 973.98 11.31 o 6 5 2 2.33 2.09 0.87 o 7 5 2 103.75 105.97 3.04 o 8 5 2 311.54 332.90 5.34 o 9 5 2 208.26 220.90 4.18 o -9 6 2 141.74 147.94 5.03 o -8 6 2 12.44 11.75 1.07 o -7 6 2 32.40 40.35 1.86 o -6 6 2 337.44 342.06 5.55 o -5 6 2 259.09 263.36 3.60 o -4 6 2 313.50 323.18 4.66 o -3 6 2 322.36 369.53 5.83 o -2 6 2 402.13 365.60 4.46 o -1 6 2 609.67 623.20 5.74 o 0 6 2 1822.21 1838.73 10.02 o 1 6 2 385.69 400.00 4.38 o 2 6 2 3294.83 3619.18 22.82 o 3 6 2 440.90 489.48 6.16 o 4 6 2 275.93 254.76 3.56 o 5 6 2 1.08 0.29 0.52 o 6 6 2 297.79 322.83 4.75 o 7 6 2 154.84 163.92 3.64 o 8 6 2 298.22 303.26 3.96 o -8 7 2 142.05 153.33 3.84 o -7 7 2 0.18 0.84 0.74 o -6 7 2 13.88 16.55 1.42 o -5 7 2 41.50 38.86 1.71 o -4 7 2 1748.25 1705.56 11.55 o -3 7 2 56.70 51.41 2.03 o -2 7 2 1370.90 1340.20 10.90 o -1 7 2 75.00 70.69 1.70 o 0 7 2 943.11 1053.55 8.04 o 1 7 2 424.92 452.21 6.53 o 2 7 2 1296.65 1287.41 13.14 o 3 7 2 17.41 19.54 1.12 o 4 7 2 2822.29 2854.66 62.16 o 5 7 2 112.06 109.88 3.18 o 6 7 2 201.26 204.78 5.62 o 7 7 2 319.63 317.15 4.67 o 8 7 2 12.68 17.05 1.12 o -8 8 2 74.83 80.62 2.70 o -7 8 2 49.09 42.39 1.92 o -6 8 2 307.77 330.86 6.96 o -5 8 2 60.63 54.76 2.51 o -4 8 2 36.15 42.35 1.77 o -3 8 2 193.62 210.69 3.20 o -2 8 2 9.61 14.01 3.45 o -1 8 2 283.32 288.46 4.49 o 0 8 2 508.93 565.79 6.27 o 1 8 2 46.99 40.06 2.09 o 2 8 2 384.58 455.56 5.40 o 3 8 2 94.42 110.99 2.86 o 4 8 2 28.46 23.96 1.49 o 5 8 2 5.30 6.99 0.95 o 6 8 2 517.96 526.41 7.47 o 7 8 2 1.40 1.53 0.64 o 8 8 2 3.43 3.80 0.86 o -7 9 2 12.97 11.37 1.05 o -6 9 2 7.47 8.43 1.02 o -5 9 2 332.34 324.73 5.87 o -4 9 2 93.29 107.82 3.56 o -3 9 2 201.43 199.48 4.53 o -2 9 2 302.33 314.57 4.71 o -1 9 2 55.89 45.12 1.46 o 0 9 2 124.43 137.09 2.65 o 1 9 2 178.29 179.06 3.05 o 2 9 2 94.20 75.22 2.19 o 3 9 2 52.00 42.95 2.45 o 4 9 2 492.79 530.88 7.35 o 5 9 2 245.03 270.42 4.53 o 6 9 2 21.87 22.53 1.42 o 7 9 2 28.39 29.95 1.83 o -7 10 2 173.43 188.74 4.08 o -6 10 2 43.90 54.33 2.69 o -5 10 2 5.86 5.31 0.88 o -4 10 2 12.87 10.81 1.20 o -3 10 2 309.86 290.84 7.52 o -2 10 2 27.45 31.43 2.33 o -1 10 2 674.31 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