#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:26:07 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181236 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/14/2231436.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231436_Fobs loop_ _publ_author_name 'Asiri, Abdullah M.' 'Al-Youbi, Abdulrahman O.' 'Faidallah, Hassan M.' 'Alamry, Khalid A.' 'Ng, Seik Weng' _publ_section_title ; (E)-2-Methyl-5-(thiophen-2-ylmethylidene)cyclopentan-1-one ; _journal_coeditor_code BT5619 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2443 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.469 _cell_angle_gamma 90.000 _cell_length_a 12.0667 _cell_length_b 11.0576 _cell_length_c 7.3003 _exptl_crystal_F_000 408.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file bt5619Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 188.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 126.52 120.42 3.48 o 3 0 0 786.42 825.01 25.76 o 4 0 0 182.39 166.38 7.90 o 5 0 0 959.34 1100.67 15.87 o 6 0 0 1210.86 1292.60 19.13 o 7 0 0 1134.87 1160.58 21.45 o 8 0 0 125.69 113.75 5.96 o 9 0 0 580.61 550.03 14.80 o 10 0 0 45.74 56.32 4.76 o 11 0 0 288.76 294.59 25.06 o 12 0 0 37.96 48.29 8.71 o 13 0 0 738.92 763.72 38.07 o 14 0 0 320.99 308.63 25.01 o 15 0 0 68.35 75.16 13.03 o 1 1 0 1398.50 1391.95 43.39 o 2 1 0 3230.54 3312.02 40.67 o 3 1 0 71.96 88.75 4.01 o 4 1 0 538.08 547.99 9.94 o 5 1 0 1115.10 1149.83 13.36 o 6 1 0 76.25 66.77 3.51 o 7 1 0 21.02 33.94 2.06 o 8 1 0 100.43 97.59 3.45 o 9 1 0 60.10 59.91 3.03 o 10 1 0 679.75 667.88 9.67 o 11 1 0 123.71 119.88 4.24 o 12 1 0 66.81 79.69 5.68 o 13 1 0 2.39 1.37 8.06 o 14 1 0 13.60 20.35 5.56 o 15 1 0 5.15 14.43 4.73 o 0 2 0 5.62 2.87 1.26 o 1 2 0 321.18 298.09 5.52 o 2 2 0 266.09 236.49 4.67 o 3 2 0 521.51 552.90 12.33 o 4 2 0 1406.61 1378.00 23.66 o 5 2 0 3351.62 3725.70 51.49 o 6 2 0 5.07 2.39 1.33 o 7 2 0 117.56 128.70 5.91 o 8 2 0 7.61 4.34 1.50 o 9 2 0 1188.31 1136.89 21.50 o 10 2 0 1442.00 1340.29 24.72 o 11 2 0 262.70 239.99 9.90 o 12 2 0 336.21 383.23 13.22 o 13 2 0 131.15 145.80 8.45 o 14 2 0 36.87 34.24 6.63 o 15 2 0 399.97 408.49 21.47 o 1 3 0 312.73 264.00 7.32 o 2 3 0 121.39 160.66 4.64 o 3 3 0 123.78 111.68 3.61 o 4 3 0 674.98 688.03 16.22 o 5 3 0 56.17 81.03 5.52 o 6 3 0 74.10 71.29 5.53 o 7 3 0 1579.81 1653.48 25.99 o 8 3 0 222.96 224.24 7.62 o 9 3 0 238.42 226.73 9.16 o 10 3 0 31.07 36.64 4.06 o 11 3 0 36.37 31.42 3.92 o 12 3 0 6.56 8.56 2.56 o 13 3 0 29.97 35.09 4.68 o 14 3 0 31.85 23.77 5.59 o 15 3 0 141.43 138.78 17.37 o 0 4 0 1961.08 2027.35 43.20 o 1 4 0 3456.21 3533.23 38.85 o 2 4 0 10.43 13.42 1.86 o 3 4 0 1476.67 1553.04 20.84 o 4 4 0 120.47 146.37 4.72 o 5 4 0 233.48 339.60 12.33 o 6 4 0 30.37 38.64 4.53 o 7 4 0 114.55 96.22 7.18 o 8 4 0 7.77 11.64 3.31 o 9 4 0 17.30 20.55 3.15 o 10 4 0 428.87 456.83 14.39 o 11 4 0 28.76 34.98 5.25 o 12 4 0 181.82 189.50 9.95 o 13 4 0 87.81 95.22 7.50 o 14 4 0 283.54 322.74 18.47 o 1 5 0 714.16 747.99 14.67 o 2 5 0 150.87 202.37 10.17 o 3 5 0 1084.22 1176.04 16.32 o 4 5 0 359.77 340.66 7.78 o 5 5 0 153.65 163.22 5.36 o 6 5 0 975.25 915.42 19.32 o 7 5 0 508.05 512.49 17.86 o 8 5 0 546.09 562.18 29.35 o 9 5 0 1.08 2.82 2.02 o 10 5 0 171.47 156.78 8.68 o 11 5 0 0.91 2.65 1.97 o 12 5 0 189.26 211.89 10.93 o 13 5 0 10.29 0.69 2.93 o 14 5 0 3.12 2.83 4.30 o 0 6 0 3579.67 3711.11 76.01 o 1 6 0 7.15 9.92 1.99 o 2 6 0 4.93 13.67 2.11 o 3 6 0 663.54 691.24 14.27 o 4 6 0 734.24 784.81 13.64 o 5 6 0 631.57 596.96 11.44 o 6 6 0 638.73 683.56 12.94 o 7 6 0 365.86 370.91 15.82 o 8 6 0 5.91 5.28 3.24 o 9 6 0 158.08 158.05 14.11 o 10 6 0 40.85 53.66 5.52 o 11 6 0 67.70 51.69 7.84 o 12 6 0 49.67 46.47 5.55 o 13 6 0 43.28 46.68 5.83 o 14 6 0 73.36 109.28 13.61 o 1 7 0 27.60 47.90 3.84 o 2 7 0 288.45 325.20 10.13 o 3 7 0 511.25 526.28 13.13 o 4 7 0 7.03 1.31 1.51 o 5 7 0 747.54 784.13 22.55 o 6 7 0 757.18 732.68 15.06 o 7 7 0 757.96 739.03 10.28 o 8 7 0 1610.08 1523.04 37.55 o 9 7 0 104.27 96.05 9.14 o 10 7 0 16.00 20.84 3.80 o 11 7 0 174.25 160.35 12.41 o 12 7 0 48.85 40.79 5.36 o 13 7 0 0.18 -0.21 7.24 o 0 8 0 14.62 29.84 4.23 o 1 8 0 208.25 213.99 8.74 o 2 8 0 156.69 159.38 7.54 o 3 8 0 13.50 10.45 2.23 o 4 8 0 12.14 10.80 2.69 o 5 8 0 45.78 51.14 4.98 o 6 8 0 428.75 380.80 12.71 o 7 8 0 21.10 21.10 2.37 o 8 8 0 107.82 105.94 9.62 o 9 8 0 10.03 6.78 3.80 o 10 8 0 6.17 5.01 5.05 o 11 8 0 29.84 24.20 4.24 o 12 8 0 1.62 -2.54 2.78 o 1 9 0 0.24 1.47 1.91 o 2 9 0 91.84 101.69 7.71 o 3 9 0 894.61 897.71 24.12 o 4 9 0 1512.33 1537.83 33.08 o 5 9 0 128.78 135.41 8.46 o 6 9 0 8.44 15.94 2.96 o 7 9 0 515.57 534.92 15.35 o 8 9 0 139.07 132.76 15.67 o 9 9 0 379.27 381.52 19.73 o 10 9 0 60.84 60.61 8.49 o 11 9 0 86.99 86.69 8.04 o 12 9 0 24.65 27.05 6.18 o 0 10 0 147.97 128.39 13.14 o 1 10 0 173.42 163.47 11.86 o 2 10 0 115.70 123.20 13.77 o 3 10 0 107.34 135.52 19.67 o 4 10 0 258.99 244.16 12.50 o 5 10 0 75.00 81.18 13.10 o 6 10 0 0.00 2.24 2.01 o 7 10 0 14.17 6.43 4.72 o 8 10 0 24.47 16.33 6.79 o 9 10 0 47.88 42.61 9.97 o 10 10 0 15.82 13.92 7.37 o 1 11 0 106.49 108.93 9.16 o 2 11 0 7.49 12.07 3.42 o 3 11 0 11.14 14.41 5.62 o 4 11 0 216.50 218.23 12.57 o 5 11 0 226.70 224.14 12.49 o 6 11 0 355.46 384.93 15.99 o 7 11 0 346.86 345.24 26.87 o 8 11 0 250.43 297.82 25.50 o 9 11 0 165.02 174.56 20.30 o 0 12 0 46.45 40.68 8.44 o 1 12 0 44.09 54.19 6.95 o 2 12 0 166.71 187.34 14.07 o 3 12 0 11.41 15.84 4.49 o 4 12 0 8.19 9.13 3.62 o 5 12 0 20.04 24.24 7.27 o 6 12 0 76.25 75.20 13.35 o 7 12 0 49.99 66.26 12.59 o 1 13 0 5.79 1.98 4.89 o 2 13 0 110.33 81.35 8.61 o 3 13 0 201.59 208.10 36.06 o 4 13 0 103.29 117.24 22.17 o 5 13 0 66.44 72.44 13.21 o 0 14 0 139.97 128.69 16.41 o 1 14 0 316.37 339.93 18.78 o 2 14 0 150.11 140.92 12.05 o 3 14 0 229.22 233.84 20.25 o -15 1 1 135.23 120.77 15.13 o -14 1 1 15.15 20.09 4.99 o -13 1 1 180.60 199.11 9.11 o -12 1 1 120.71 142.09 5.65 o -11 1 1 65.20 70.71 4.06 o -10 1 1 2.70 -0.09 1.15 o -9 1 1 571.31 565.05 9.52 o -8 1 1 1292.60 1275.93 16.61 o -7 1 1 3135.36 3182.58 25.25 o -6 1 1 21.02 8.45 0.81 o -5 1 1 739.40 692.53 7.21 o -4 1 1 694.93 673.23 7.41 o -3 1 1 1684.60 1711.41 11.77 o -2 1 1 1947.76 1924.82 15.62 o -1 1 1 1514.64 1494.33 27.19 o 0 1 1 156.95 163.71 3.17 o 1 1 1 27.61 25.70 1.39 o 2 1 1 2559.52 2568.61 26.29 o 3 1 1 434.04 400.41 7.47 o 4 1 1 1657.80 1670.49 24.64 o 5 1 1 1149.32 1178.36 23.81 o 6 1 1 724.13 669.90 12.26 o 7 1 1 2671.36 2691.56 33.42 o 8 1 1 864.60 821.92 11.14 o 9 1 1 207.84 194.91 5.03 o 10 1 1 50.08 66.22 2.94 o 11 1 1 275.85 273.03 7.60 o 12 1 1 30.68 39.98 4.28 o 13 1 1 61.58 65.88 13.60 o 14 1 1 70.51 75.80 9.07 o -15 2 1 2.17 2.06 3.54 o -14 2 1 41.18 41.41 14.72 o -13 2 1 24.30 10.20 3.59 o -12 2 1 24.66 27.05 3.58 o -11 2 1 50.67 50.63 4.60 o -10 2 1 302.69 302.15 10.55 o -9 2 1 71.34 80.09 4.51 o -8 2 1 8.27 4.48 0.76 o -7 2 1 74.62 73.34 2.69 o -6 2 1 63.83 81.49 2.13 o -5 2 1 1415.88 1522.64 12.57 o -4 2 1 730.50 733.64 7.67 o -3 2 1 1306.74 1415.59 17.60 o -2 2 1 768.80 797.97 13.71 o -1 2 1 2051.91 2111.76 41.13 o 0 2 1 13295.34 12671.12 113.85 o 1 2 1 3.94 3.05 0.69 o 2 2 1 871.01 814.20 11.13 o 3 2 1 810.97 828.69 14.94 o 4 2 1 2247.95 2287.22 26.04 o 5 2 1 1052.80 1195.30 19.17 o 6 2 1 32.75 26.00 2.06 o 7 2 1 101.37 106.71 2.90 o 8 2 1 4.40 3.21 0.87 o 9 2 1 0.77 0.27 0.60 o 10 2 1 228.80 224.52 9.57 o 11 2 1 47.00 45.14 8.51 o 12 2 1 84.50 97.72 9.95 o 13 2 1 91.34 87.19 9.42 o 14 2 1 0.63 2.89 4.43 o -15 3 1 70.59 61.58 8.56 o -14 3 1 19.71 13.68 6.56 o -13 3 1 0.16 7.51 2.88 o -12 3 1 3.28 4.47 3.58 o -11 3 1 471.95 473.44 14.43 o -10 3 1 850.22 800.97 18.50 o -9 3 1 18.33 17.35 2.81 o -8 3 1 2598.65 2499.32 30.39 o -7 3 1 40.61 31.62 2.75 o -6 3 1 460.59 480.22 9.99 o -5 3 1 2413.28 2489.41 25.53 o -4 3 1 696.26 675.28 13.16 o -3 3 1 294.79 312.45 7.85 o -2 3 1 1760.28 1830.87 40.40 o -1 3 1 0.92 3.80 1.98 o 0 3 1 527.93 562.94 9.39 o 1 3 1 715.73 763.21 9.97 o 2 3 1 2738.27 2843.64 26.72 o 3 3 1 1396.67 1385.28 15.28 o 4 3 1 3.42 9.47 0.97 o 5 3 1 823.21 780.16 17.95 o 6 3 1 211.87 220.87 14.64 o 7 3 1 262.57 242.08 13.46 o 8 3 1 1272.34 1225.00 23.31 o 9 3 1 74.16 61.44 5.14 o 10 3 1 58.21 67.41 5.62 o 11 3 1 80.70 82.99 6.39 o 12 3 1 36.52 35.68 7.56 o 13 3 1 4.79 6.64 2.72 o 14 3 1 7.85 8.53 4.24 o -15 4 1 253.45 289.92 23.76 o -14 4 1 125.89 139.63 8.98 o -13 4 1 150.76 147.47 8.92 o -12 4 1 19.86 17.34 3.30 o -11 4 1 229.50 222.62 10.43 o -10 4 1 944.77 858.29 19.84 o -9 4 1 163.03 142.79 7.42 o -8 4 1 83.77 75.03 5.13 o -7 4 1 111.20 109.10 5.17 o -6 4 1 10.95 6.62 0.69 o -5 4 1 112.35 113.17 4.11 o -4 4 1 0.78 3.32 1.11 o -3 4 1 1057.80 1101.21 31.27 o -2 4 1 196.02 174.86 10.57 o -1 4 1 67.61 37.86 4.86 o 0 4 1 193.85 161.37 5.18 o 1 4 1 257.45 218.20 5.22 o 2 4 1 9.49 13.08 1.37 o 3 4 1 598.08 646.60 13.97 o 4 4 1 0.06 3.25 0.76 o 5 4 1 45.69 44.85 2.03 o 6 4 1 43.24 36.56 3.63 o 7 4 1 18.08 20.84 3.02 o 8 4 1 256.32 238.76 12.00 o 9 4 1 380.66 335.84 12.25 o 10 4 1 858.95 772.52 19.91 o 11 4 1 150.78 169.16 9.36 o 12 4 1 5.68 6.03 3.97 o 13 4 1 151.98 159.80 9.85 o 14 4 1 244.12 273.86 24.31 o -14 5 1 25.67 25.39 5.35 o -13 5 1 36.33 31.98 4.40 o -12 5 1 33.80 26.30 4.19 o -11 5 1 0.05 -0.19 1.66 o -10 5 1 0.08 1.66 1.86 o -9 5 1 2.03 1.06 1.68 o -8 5 1 517.43 465.29 13.54 o -7 5 1 154.04 140.48 9.05 o -6 5 1 461.75 479.73 7.89 o -5 5 1 322.00 331.94 6.90 o -4 5 1 92.64 67.30 7.70 o -3 5 1 419.27 477.59 20.41 o -2 5 1 30.46 49.95 6.31 o -1 5 1 418.70 472.58 13.37 o 0 5 1 158.99 176.04 6.01 o 1 5 1 8.18 11.35 1.61 o 2 5 1 53.69 47.87 2.70 o 3 5 1 216.31 255.40 6.26 o 4 5 1 139.40 108.15 3.87 o 5 5 1 600.05 621.73 10.99 o 6 5 1 178.66 187.88 5.12 o 7 5 1 426.27 389.28 15.63 o 8 5 1 488.24 450.80 17.58 o 9 5 1 37.29 33.99 5.36 o 10 5 1 244.00 218.49 15.56 o 11 5 1 28.37 25.10 4.01 o 12 5 1 2.04 2.07 2.30 o 13 5 1 0.00 2.46 3.83 o 14 5 1 36.52 31.67 8.96 o -14 6 1 346.64 365.72 22.72 o -13 6 1 90.91 92.10 7.57 o -12 6 1 208.67 244.39 11.73 o -11 6 1 109.35 107.64 8.74 o -10 6 1 193.29 214.93 10.19 o -9 6 1 0.08 0.03 2.08 o -8 6 1 73.63 72.92 7.33 o -7 6 1 23.00 24.19 1.47 o -6 6 1 159.31 129.79 5.19 o -5 6 1 14.97 5.30 1.50 o -4 6 1 245.66 226.11 9.09 o -3 6 1 207.99 228.75 14.71 o -2 6 1 221.94 216.15 8.96 o -1 6 1 4059.64 4181.39 48.10 o 0 6 1 1748.33 1889.06 26.58 o 1 6 1 2170.45 2117.53 28.54 o 2 6 1 8.32 6.31 1.39 o 3 6 1 825.18 791.15 11.87 o 4 6 1 165.09 144.27 5.45 o 5 6 1 10.32 4.89 1.33 o 6 6 1 11.31 14.78 2.35 o 7 6 1 37.55 26.79 4.80 o 8 6 1 24.68 33.42 5.78 o 9 6 1 1.43 6.03 3.12 o 10 6 1 100.57 106.79 7.72 o 11 6 1 81.69 78.14 9.08 o 12 6 1 277.23 284.40 13.55 o 13 6 1 86.54 93.92 8.12 o -13 7 1 28.93 35.98 5.12 o -12 7 1 27.49 32.59 4.82 o -11 7 1 129.10 127.45 8.46 o -10 7 1 56.20 48.08 5.30 o -9 7 1 122.05 114.25 9.96 o -8 7 1 4.86 6.56 3.43 o -7 7 1 76.47 66.21 4.28 o -6 7 1 500.69 469.02 10.43 o -5 7 1 2.95 1.04 1.49 o -4 7 1 201.37 204.19 9.28 o -3 7 1 26.67 21.21 2.84 o -2 7 1 1.90 -0.66 2.18 o -1 7 1 71.31 70.15 4.55 o 0 7 1 91.34 111.37 8.15 o 1 7 1 206.01 233.48 8.42 o 2 7 1 36.83 29.77 3.11 o 3 7 1 130.94 123.53 7.27 o 4 7 1 905.23 847.33 15.30 o 5 7 1 76.99 78.34 4.84 o 6 7 1 141.00 122.26 5.65 o 7 7 1 52.63 36.40 3.39 o 8 7 1 11.72 16.53 4.41 o 9 7 1 27.81 25.83 5.39 o 10 7 1 11.15 14.81 4.36 o 11 7 1 44.82 61.67 6.63 o 12 7 1 65.71 67.29 6.98 o 13 7 1 92.32 106.25 10.58 o -13 8 1 65.03 67.56 8.03 o -12 8 1 326.44 327.12 21.43 o -11 8 1 107.07 90.24 7.55 o -10 8 1 44.92 54.66 6.72 o -9 8 1 84.16 65.33 10.82 o -8 8 1 0.01 -0.18 1.15 o -7 8 1 50.85 62.94 3.78 o -6 8 1 42.26 47.84 4.71 o -5 8 1 1158.10 1096.01 25.28 o -4 8 1 1655.60 1616.18 32.79 o -3 8 1 21.77 22.05 3.57 o -2 8 1 582.15 538.76 14.56 o -1 8 1 1275.07 1223.96 19.80 o 0 8 1 1031.05 1026.24 20.29 o 1 8 1 541.69 503.91 13.60 o 2 8 1 505.80 522.83 16.97 o 3 8 1 39.59 32.35 3.58 o 4 8 1 1706.79 1621.30 68.20 o 5 8 1 965.91 956.66 19.63 o 6 8 1 0.35 0.74 1.34 o 7 8 1 194.97 196.40 7.32 o 8 8 1 0.22 -3.04 3.15 o 9 8 1 171.73 195.72 13.72 o 10 8 1 177.27 165.31 13.09 o 11 8 1 196.80 194.63 11.65 o 12 8 1 279.29 284.02 17.06 o -12 9 1 13.59 11.50 5.82 o -11 9 1 23.73 33.43 8.00 o -10 9 1 19.87 17.13 6.44 o -9 9 1 13.78 7.65 4.95 o -8 9 1 3.00 -2.70 4.27 o -7 9 1 169.60 174.72 8.91 o -6 9 1 11.58 13.01 2.83 o -5 9 1 740.49 723.27 21.05 o -4 9 1 2.64 1.75 2.02 o -3 9 1 137.86 138.59 9.04 o -2 9 1 80.47 73.57 5.68 o -1 9 1 502.71 483.58 14.00 o 0 9 1 13.82 4.38 2.56 o 1 9 1 557.48 559.51 15.25 o 2 9 1 132.70 136.15 7.37 o 3 9 1 62.30 47.68 5.48 o 4 9 1 293.59 289.59 27.93 o 5 9 1 8.13 7.08 5.37 o 6 9 1 98.78 92.10 6.63 o 7 9 1 191.67 198.23 8.06 o 8 9 1 17.06 15.65 7.29 o 9 9 1 0.05 -0.06 3.24 o 10 9 1 54.61 48.84 7.68 o 11 9 1 0.39 2.51 7.18 o -11 10 1 689.87 729.12 41.60 o -10 10 1 162.49 174.00 19.41 o -9 10 1 17.63 37.47 9.02 o -8 10 1 2.17 -0.48 4.07 o -7 10 1 155.16 138.96 16.40 o -6 10 1 23.06 37.57 4.75 o -5 10 1 8.13 8.31 2.80 o -4 10 1 13.95 16.50 3.69 o -3 10 1 814.62 808.22 26.55 o -2 10 1 162.09 177.10 8.80 o -1 10 1 20.42 20.61 3.28 o 0 10 1 1515.31 1443.87 34.35 o 1 10 1 80.66 91.90 7.93 o 2 10 1 208.96 206.42 11.85 o 3 10 1 336.72 320.49 14.72 o 4 10 1 6.27 7.25 3.75 o 5 10 1 229.07 253.10 12.44 o 6 10 1 11.19 12.43 4.20 o 7 10 1 3.24 -0.08 3.73 o 8 10 1 16.60 30.85 8.94 o 9 10 1 0.81 -2.82 3.86 o 10 10 1 205.55 205.45 15.63 o -9 11 1 185.77 215.91 22.30 o -8 11 1 63.85 68.59 12.78 o -7 11 1 91.44 80.11 13.00 o -6 11 1 101.44 105.67 8.68 o -5 11 1 455.54 461.38 18.33 o -4 11 1 164.18 163.95 10.98 o -3 11 1 97.98 86.91 8.18 o -2 11 1 53.05 53.47 6.53 o -1 11 1 62.75 50.68 6.50 o 0 11 1 7.03 7.37 3.21 o 1 11 1 40.32 29.51 12.28 o 2 11 1 76.56 68.22 7.37 o 3 11 1 119.98 111.00 10.40 o 4 11 1 0.27 -1.62 3.53 o 5 11 1 1.10 -0.96 2.93 o 6 11 1 41.46 72.21 12.43 o 7 11 1 16.17 15.92 6.34 o 8 11 1 95.47 84.92 14.38 o -7 12 1 29.00 35.42 9.44 o -6 12 1 3.04 -9.56 6.37 o -5 12 1 206.95 231.21 13.55 o -4 12 1 168.76 157.49 11.38 o -3 12 1 113.49 131.46 17.97 o -2 12 1 111.01 112.11 9.85 o -1 12 1 314.50 299.48 16.10 o 0 12 1 5.56 13.72 5.30 o 1 12 1 161.75 164.70 11.85 o 2 12 1 199.03 195.49 12.92 o 3 12 1 288.41 291.19 23.11 o 4 12 1 176.49 165.37 11.57 o 5 12 1 149.11 169.40 19.35 o 6 12 1 93.17 120.72 16.28 o -5 13 1 5.54 9.57 6.68 o -4 13 1 147.98 171.49 14.50 o -3 13 1 7.53 12.71 4.38 o -2 13 1 9.00 13.24 8.47 o -1 13 1 69.93 66.48 8.16 o 0 13 1 16.95 14.44 4.13 o 1 13 1 35.10 51.82 7.34 o 2 13 1 10.16 8.23 3.57 o 3 13 1 42.81 45.73 6.75 o 4 13 1 254.50 289.69 25.81 o -3 14 1 41.16 24.98 7.95 o -2 14 1 22.83 12.95 4.55 o -1 14 1 154.74 151.17 20.14 o 0 14 1 157.53 179.84 26.47 o 1 14 1 85.92 95.14 10.09 o 2 14 1 1.26 0.49 2.59 o -15 0 2 20.55 20.00 7.80 o -14 0 2 219.42 203.16 19.09 o -13 0 2 253.84 261.63 20.53 o -12 0 2 8.96 8.20 2.35 o -11 0 2 599.65 576.47 16.66 o -10 0 2 414.37 394.12 9.26 o -9 0 2 1.76 2.10 1.85 o -8 0 2 47.76 39.63 3.02 o -7 0 2 357.97 324.38 7.28 o -6 0 2 3985.98 4083.78 38.24 o -5 0 2 2580.48 2797.15 27.39 o -4 0 2 31.79 42.24 2.11 o -3 0 2 2412.12 2335.50 25.98 o -2 0 2 1181.24 1229.60 28.21 o -1 0 2 2237.41 2183.78 43.36 o 0 0 2 35545.78 34297.27 527.87 o 1 0 2 437.59 467.25 15.29 o 2 0 2 48.09 99.48 4.69 o 3 0 2 1740.04 1665.74 36.64 o 4 0 2 2053.37 2114.76 33.05 o 5 0 2 9.33 30.35 3.53 o 6 0 2 140.03 124.36 9.21 o 7 0 2 578.56 572.86 28.46 o 8 0 2 163.70 156.29 8.18 o 9 0 2 148.87 165.97 9.70 o 10 0 2 49.50 44.20 3.67 o 11 0 2 796.54 777.70 52.42 o 12 0 2 198.63 227.78 20.91 o 13 0 2 498.87 510.01 32.94 o 14 0 2 157.52 169.47 19.78 o -15 1 2 2.37 6.41 3.70 o -14 1 2 58.57 61.69 7.67 o -13 1 2 11.83 11.47 2.63 o -12 1 2 1.18 0.45 1.07 o -11 1 2 54.45 50.78 3.57 o -10 1 2 1380.43 1361.78 16.22 o -9 1 2 0.79 0.10 0.63 o -8 1 2 261.90 279.36 6.33 o -7 1 2 240.72 245.15 4.46 o -6 1 2 164.85 175.72 3.49 o -5 1 2 1438.62 1434.28 11.76 o -4 1 2 195.32 175.55 3.04 o -3 1 2 192.48 177.51 2.94 o -2 1 2 217.48 219.75 6.19 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