#------------------------------------------------------------------------------ #$Date: 2011-10-07 16:37:56 +0300 (Fri, 07 Oct 2011) $ #$Revision: 27934 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/14/2231467.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231467_Fobs loop_ _publ_author_name 'Saraswathi, B. S.' 'Foro, Sabine' 'Gowda, B. Thimme' _publ_section_title ; N-(4-Chlorophenyl)-N'-(4-methylphenyl)succinamide ; _journal_coeditor_code DS2134 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2419 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.580 _cell_angle_gamma 90.000 _cell_length_a 17.3050 _cell_length_b 4.8446 _cell_length_c 9.7260 _exptl_crystal_F_000 332.00 _reflns_d_resolution_high 0.8301 _[local]_cod_data_source_file ds2134Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' DSC28 P21/C' _shelx_refln_list_code 4 _shelx_f_calc_maximum 162.65 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 218.34 234.75 0.95 o 4 0 0 517.57 523.94 1.65 o 5 0 0 45.86 43.28 0.69 o 6 0 0 850.81 934.44 2.59 o 7 0 0 76.45 78.93 0.97 o 8 0 0 175.70 169.40 1.41 o 9 0 0 578.40 609.34 2.68 o 10 0 0 15.03 15.67 0.83 o 11 0 0 180.36 193.52 1.82 o 12 0 0 21.49 26.37 1.09 o 13 0 0 338.72 327.40 2.59 o 14 0 0 542.91 553.22 3.35 o 15 0 0 5.27 7.38 1.17 o 16 0 0 236.09 236.88 2.47 o 17 0 0 110.23 126.57 2.01 o 18 0 0 9.10 10.13 1.14 o 19 0 0 1.36 -1.07 1.07 o 20 0 0 0.33 -1.05 1.05 o 1 1 0 76.50 93.07 0.84 o 2 1 0 15.85 13.24 0.35 o 3 1 0 905.78 948.82 1.54 o 4 1 0 157.92 158.19 0.50 o 5 1 0 1152.89 1112.72 3.01 o 6 1 0 49.59 51.34 0.66 o 7 1 0 334.66 351.68 3.82 o 8 1 0 318.81 338.51 2.55 o 9 1 0 1217.24 1223.79 8.96 o 10 1 0 9.42 12.57 0.56 o 11 1 0 43.45 48.45 1.36 o 12 1 0 89.86 87.86 1.11 o 13 1 0 37.00 35.33 0.88 o 14 1 0 15.00 12.24 0.78 o 15 1 0 2.00 -0.72 0.72 o 16 1 0 11.52 10.36 1.22 o 17 1 0 2.11 3.44 1.18 o 18 1 0 20.74 24.84 1.38 o 19 1 0 0.74 1.12 1.17 o 20 1 0 0.07 -1.09 1.13 o 0 2 0 555.78 546.72 1.05 o 1 2 0 16.84 9.82 0.27 o 2 2 0 86.47 97.84 0.65 o 3 2 0 1.23 0.99 0.29 o 4 2 0 0.91 1.64 0.28 o 5 2 0 368.63 395.35 1.31 o 6 2 0 242.47 240.40 1.05 o 7 2 0 380.47 415.05 1.36 o 8 2 0 22.27 28.77 1.26 o 9 2 0 147.60 160.32 1.15 o 10 2 0 3.52 4.19 0.97 o 11 2 0 4.69 5.57 1.06 o 12 2 0 2.84 3.09 1.11 o 13 2 0 4.38 3.29 1.12 o 14 2 0 0.58 -0.96 1.20 o 15 2 0 0.89 0.07 1.17 o 16 2 0 1.54 2.22 1.11 o 17 2 0 0.69 0.28 1.19 o 18 2 0 2.95 3.42 1.17 o 19 2 0 1.07 1.18 1.26 o 1 3 0 28.92 30.64 0.40 o 2 3 0 341.59 368.22 3.12 o 3 3 0 22.92 29.48 0.46 o 4 3 0 9.98 8.77 0.47 o 5 3 0 0.04 0.25 0.44 o 6 3 0 23.18 19.44 0.91 o 7 3 0 2.11 2.57 0.82 o 8 3 0 0.43 -0.04 0.87 o 9 3 0 10.28 8.75 1.00 o 10 3 0 13.68 11.54 1.07 o 11 3 0 66.61 61.33 1.53 o 12 3 0 0.03 -0.45 1.06 o 13 3 0 4.26 3.03 1.21 o 14 3 0 6.05 3.92 1.24 o 15 3 0 5.44 3.25 1.17 o 16 3 0 1.31 1.97 1.17 o 17 3 0 0.25 0.10 1.26 o 0 4 0 28.14 30.12 1.02 o 1 4 0 4.88 5.06 0.52 o 2 4 0 5.94 5.53 0.53 o 3 4 0 6.74 7.38 0.83 o 4 4 0 7.68 6.38 0.86 o 5 4 0 155.62 173.70 2.07 o 6 4 0 114.28 116.60 1.76 o 7 4 0 27.22 24.98 1.08 o 8 4 0 0.00 0.33 0.76 o 9 4 0 6.34 5.16 0.99 o 10 4 0 32.39 32.24 1.31 o 11 4 0 77.82 87.96 1.76 o 12 4 0 29.59 29.90 1.41 o 13 4 0 3.75 3.00 1.18 o 14 4 0 13.40 13.04 1.33 o 1 5 0 10.71 9.34 0.89 o 2 5 0 37.28 35.25 1.24 o 3 5 0 90.12 92.99 1.74 o 4 5 0 39.40 38.00 1.29 o 5 5 0 24.24 27.52 1.24 o 6 5 0 27.70 23.89 1.19 o 7 5 0 7.51 7.92 1.00 o 8 5 0 2.76 3.85 0.93 o 9 5 0 3.66 2.70 0.86 o 10 5 0 1.56 0.47 0.84 o -20 1 1 4.31 6.32 1.24 o -19 1 1 17.00 17.44 1.30 o -18 1 1 14.73 10.51 1.18 o -17 1 1 8.35 7.96 1.13 o -16 1 1 66.58 66.43 1.70 o -15 1 1 3.48 3.92 0.71 o -14 1 1 96.79 95.62 2.27 o -13 1 1 55.10 52.98 1.36 o -12 1 1 5.08 5.29 0.41 o -11 1 1 70.66 70.23 0.63 o -10 1 1 17.72 19.25 0.44 o -9 1 1 115.99 146.37 1.44 o -8 1 1 0.65 0.41 0.22 o -7 1 1 176.18 165.12 1.24 o -6 1 1 49.03 49.19 0.58 o -5 1 1 522.19 562.75 1.35 o -4 1 1 312.80 295.30 0.99 o -3 1 1 121.09 137.66 0.83 o -2 1 1 6524.19 6067.66 12.57 o -1 1 1 6083.25 5855.68 12.17 o 0 1 1 1799.39 1850.93 6.33 o 1 1 1 240.68 251.56 2.25 o 2 1 1 10.62 7.81 0.36 o 3 1 1 174.93 196.08 1.16 o 4 1 1 14.24 19.18 0.28 o 5 1 1 3.36 4.78 0.31 o 6 1 1 218.42 232.27 1.67 o 7 1 1 140.01 154.63 1.14 o 8 1 1 395.26 429.27 1.57 o 9 1 1 233.82 252.28 9.93 o 10 1 1 53.07 55.86 0.80 o 11 1 1 129.19 123.89 1.10 o 12 1 1 25.66 27.22 1.74 o 13 1 1 154.79 151.12 1.36 o 14 1 1 83.16 83.99 2.10 o 15 1 1 86.85 88.00 1.83 o 16 1 1 20.94 21.19 1.34 o 18 1 1 3.86 0.58 1.15 o 19 1 1 5.21 7.06 1.18 o -19 2 1 1.88 -1.14 1.14 o -18 2 1 1.31 0.09 1.16 o -17 2 1 9.62 9.78 1.30 o -16 2 1 8.97 9.93 1.28 o -15 2 1 3.46 4.65 1.24 o -14 2 1 56.98 53.64 1.59 o -13 2 1 13.89 13.08 1.21 o -12 2 1 34.91 30.65 1.28 o -11 2 1 34.68 33.47 1.22 o -10 2 1 181.13 171.35 4.37 o -9 2 1 48.51 43.82 2.45 o -8 2 1 83.25 84.79 2.76 o -7 2 1 62.47 78.54 0.50 o -6 2 1 6.88 6.21 0.25 o -5 2 1 132.18 131.73 1.12 o -4 2 1 31.68 37.05 0.41 o -3 2 1 232.17 257.04 1.12 o -2 2 1 0.47 1.10 0.18 o -1 2 1 234.83 255.27 0.86 o 0 2 1 2030.61 2179.75 2.06 o 1 2 1 211.56 243.45 1.73 o 2 2 1 9.53 6.59 0.49 o 3 2 1 3.87 5.14 0.52 o 4 2 1 309.00 330.95 2.75 o 5 2 1 311.43 313.15 2.48 o 6 2 1 0.02 4.23 2.70 o 7 2 1 401.56 398.93 2.50 o 8 2 1 54.84 53.17 1.28 o 9 2 1 26.09 25.55 1.19 o 10 2 1 14.95 12.64 1.17 o 11 2 1 6.05 6.44 1.17 o 12 2 1 30.96 32.16 1.39 o 13 2 1 21.22 19.72 1.30 o 14 2 1 73.69 73.44 1.75 o 15 2 1 5.02 5.08 1.25 o 16 2 1 0.00 -1.13 1.13 o 17 2 1 0.66 -0.73 1.13 o 18 2 1 10.78 10.63 1.37 o -17 3 1 0.24 -0.85 1.16 o -16 3 1 15.89 14.20 1.29 o -15 3 1 0.20 0.64 1.13 o -14 3 1 44.73 45.59 1.56 o -13 3 1 19.63 23.48 1.34 o -12 3 1 48.81 52.25 1.47 o -11 3 1 8.42 8.66 1.04 o -10 3 1 3.15 3.61 0.56 o -9 3 1 121.57 122.81 2.38 o -8 3 1 151.35 144.87 2.80 o -7 3 1 49.36 44.16 0.89 o -6 3 1 45.27 41.89 1.04 o -5 3 1 40.57 39.66 0.54 o -4 3 1 9.04 14.36 0.38 o -3 3 1 137.53 170.73 0.99 o -2 3 1 24.74 21.58 0.32 o -1 3 1 23.18 19.43 0.98 o 0 3 1 263.23 323.84 2.86 o 1 3 1 3.10 4.96 0.47 o 2 3 1 38.11 38.57 0.91 o 3 3 1 162.44 149.94 1.64 o 4 3 1 30.93 23.42 0.60 o 5 3 1 289.18 289.02 2.11 o 6 3 1 131.74 130.60 1.63 o 7 3 1 34.63 40.74 1.18 o 8 3 1 21.12 21.24 1.21 o 9 3 1 218.29 220.13 2.31 o 10 3 1 50.73 53.80 1.47 o 11 3 1 33.44 30.36 1.35 o 12 3 1 4.15 3.68 1.19 o 13 3 1 60.77 60.03 1.68 o 14 3 1 0.03 3.05 1.26 o 15 3 1 0.00 0.05 1.13 o 17 3 1 3.99 0.92 1.23 o -15 4 1 2.23 0.98 1.20 o -14 4 1 0.01 -0.10 1.10 o -13 4 1 8.23 7.22 1.16 o -12 4 1 35.64 34.45 1.38 o -11 4 1 6.19 3.62 1.02 o -10 4 1 12.53 11.17 1.06 o -9 4 1 10.69 12.43 0.94 o -8 4 1 10.28 9.68 0.88 o -7 4 1 69.13 73.16 1.47 o -6 4 1 19.55 16.59 0.96 o -5 4 1 228.71 219.54 2.23 o -4 4 1 33.37 30.99 1.07 o -3 4 1 0.05 -0.72 0.72 o -2 4 1 10.03 10.04 0.57 o -1 4 1 5.48 3.57 0.52 o 0 4 1 70.72 65.58 0.92 o 1 4 1 73.78 60.92 0.90 o 2 4 1 99.39 92.43 1.57 o 3 4 1 1.49 2.05 0.83 o 4 4 1 88.54 97.21 1.66 o 5 4 1 60.73 60.46 1.40 o 6 4 1 62.85 72.73 1.50 o 7 4 1 7.79 8.80 0.93 o 8 4 1 2.08 2.06 0.98 o 9 4 1 76.24 84.15 1.65 o 10 4 1 8.37 11.41 1.18 o 11 4 1 15.02 19.56 1.31 o 12 4 1 8.87 13.32 1.26 o 13 4 1 0.21 -0.15 1.14 o 14 4 1 1.96 0.77 1.22 o -10 5 1 1.09 0.54 0.77 o -9 5 1 7.83 8.41 0.98 o -8 5 1 0.84 1.87 0.87 o -7 5 1 9.66 10.32 0.97 o -6 5 1 6.81 6.07 0.89 o -5 5 1 0.88 0.80 0.80 o -4 5 1 2.06 2.30 0.80 o -3 5 1 31.17 29.99 1.17 o -2 5 1 46.09 49.29 2.00 o -1 5 1 28.62 29.51 0.82 o 0 5 1 9.47 10.06 0.67 o 1 5 1 0.40 -0.15 0.83 o 2 5 1 1.63 1.10 0.85 o 3 5 1 3.13 3.78 0.89 o 4 5 1 5.61 6.80 0.96 o 5 5 1 3.48 5.43 1.00 o 6 5 1 7.93 9.72 1.01 o 7 5 1 12.28 4.47 0.93 o 8 5 1 16.30 15.85 1.16 o 9 5 1 1.26 -0.18 0.90 o 10 5 1 2.84 3.15 0.89 o -20 0 2 13.93 14.01 1.12 o -19 0 2 7.19 5.00 0.95 o -18 0 2 1.56 1.36 0.87 o -17 0 2 95.50 85.41 1.56 o -16 0 2 46.11 37.32 0.89 o -15 0 2 8.97 7.56 0.68 o -14 0 2 71.14 78.46 1.69 o -13 0 2 0.27 0.44 0.54 o -12 0 2 52.73 57.18 1.87 o -11 0 2 129.88 125.33 1.90 o -10 0 2 28.06 29.56 1.84 o -9 0 2 103.03 79.62 1.04 o -8 0 2 41.16 48.44 0.82 o -7 0 2 1308.56 1165.27 3.02 o -6 0 2 21.88 18.43 0.55 o -5 0 2 2720.86 2636.23 15.68 o -4 0 2 1853.38 1691.52 2.95 o -3 0 2 26454.90 22965.62 39.92 o -2 0 2 8.89 6.14 0.39 o -1 0 2 990.22 1030.17 1.98 o 0 0 2 38.89 31.07 0.46 o 1 0 2 541.47 524.29 0.75 o 2 0 2 360.00 348.96 0.87 o 3 0 2 1044.06 1044.71 2.54 o 4 0 2 437.52 443.06 1.81 o 5 0 2 37.16 40.56 0.72 o 6 0 2 3729.87 3829.89 5.94 o 7 0 2 1.94 2.10 0.68 o 8 0 2 47.40 62.18 1.11 o 9 0 2 226.20 235.13 1.94 o 10 0 2 268.05 282.91 2.20 o 11 0 2 439.34 454.14 2.84 o 12 0 2 100.32 111.27 1.77 o 13 0 2 480.27 497.56 3.23 o 14 0 2 230.42 260.12 2.51 o 15 0 2 0.46 0.58 1.02 o 16 0 2 0.03 1.74 1.02 o 17 0 2 5.88 2.50 1.04 o 18 0 2 38.03 37.78 1.45 o 19 0 2 5.87 4.05 1.13 o -20 1 2 1.29 1.28 1.38 o -19 1 2 1.39 1.33 0.74 o -18 1 2 3.68 4.47 0.91 o -17 1 2 1.99 3.19 0.75 o -16 1 2 71.37 74.62 1.71 o -15 1 2 23.70 22.74 0.75 o -14 1 2 139.97 143.11 4.80 o -13 1 2 13.17 14.73 1.55 o -12 1 2 160.72 155.88 1.80 o -11 1 2 58.85 67.19 1.97 o -10 1 2 41.85 44.50 0.64 o -9 1 2 25.04 21.05 0.50 o -8 1 2 672.35 622.95 2.73 o -7 1 2 19.57 20.67 0.44 o -6 1 2 204.89 200.13 1.44 o -5 1 2 153.36 160.82 2.44 o -4 1 2 0.18 0.28 0.60 o -3 1 2 3368.93 3231.88 11.46 o -2 1 2 40.56 28.95 0.49 o -1 1 2 3570.43 3340.45 9.35 o 0 1 2 3507.19 3465.37 10.34 o 1 1 2 86.00 85.89 0.96 o 2 1 2 12.55 13.23 0.19 o 3 1 2 725.81 736.09 1.10 o 4 1 2 717.67 730.87 1.16 o 5 1 2 737.54 717.90 1.12 o 6 1 2 2498.52 2673.81 4.26 o 7 1 2 16.24 12.48 0.71 o 8 1 2 9.15 9.68 0.65 o 9 1 2 160.72 164.23 1.16 o 10 1 2 0.00 0.57 0.56 o 11 1 2 161.43 165.23 2.06 o 12 1 2 36.59 38.50 1.42 o 13 1 2 384.96 408.58 20.41 o 14 1 2 0.05 0.98 1.21 o 15 1 2 0.96 1.41 1.12 o 16 1 2 1.28 1.17 1.06 o 17 1 2 3.52 6.73 1.19 o 18 1 2 0.03 -1.09 1.09 o 19 1 2 1.65 0.30 1.09 o -19 2 2 0.16 0.83 0.79 o -18 2 2 0.16 0.87 1.08 o -17 2 2 0.05 0.22 1.07 o -16 2 2 0.01 0.04 1.12 o -15 2 2 0.00 -0.36 1.18 o -14 2 2 3.63 3.40 1.07 o -13 2 2 0.02 -0.40 1.08 o -12 2 2 23.21 16.82 1.11 o -11 2 2 1.80 3.62 0.44 o -10 2 2 36.99 45.65 1.05 o -9 2 2 84.00 66.60 0.81 o -8 2 2 60.12 50.69 0.70 o -7 2 2 15.05 9.86 0.32 o -6 2 2 0.14 -0.03 0.25 o -5 2 2 33.27 32.01 0.49 o -4 2 2 5.01 7.14 0.29 o -3 2 2 1.08 1.13 0.16 o -2 2 2 7.91 7.84 0.18 o -1 2 2 30.76 33.75 0.28 o 0 2 2 89.26 103.44 0.90 o 1 2 2 25.39 29.45 0.69 o 2 2 2 216.59 234.78 1.48 o 3 2 2 58.90 69.85 0.56 o 4 2 2 386.30 414.24 1.25 o 5 2 2 32.64 31.54 1.34 o 6 2 2 33.62 39.15 1.13 o 7 2 2 24.68 24.72 1.09 o 8 2 2 0.03 0.04 0.93 o 9 2 2 6.77 5.40 1.08 o 10 2 2 3.05 3.02 1.07 o 11 2 2 7.59 7.98 1.29 o 12 2 2 0.25 -1.19 1.33 o 13 2 2 0.71 1.01 1.24 o 14 2 2 1.05 0.06 1.11 o 15 2 2 1.15 0.91 1.11 o 16 2 2 7.52 7.99 1.19 o 17 2 2 5.05 9.93 1.33 o 18 2 2 9.01 9.63 1.39 o -17 3 2 0.92 0.36 1.16 o -16 3 2 0.04 0.11 1.19 o -15 3 2 0.54 0.34 1.11 o -14 3 2 29.54 23.21 1.35 o -13 3 2 8.07 5.33 1.09 o -12 3 2 10.14 8.09 1.11 o -11 3 2 0.93 1.00 0.58 o -10 3 2 22.70 23.57 0.73 o -9 3 2 89.97 80.58 0.99 o -8 3 2 42.51 41.61 0.79 o -7 3 2 9.23 7.28 0.56 o -6 3 2 0.04 0.35 0.36 o -5 3 2 218.71 229.34 1.65 o -4 3 2 8.69 8.40 0.46 o -3 3 2 34.63 28.41 0.50 o -2 3 2 78.06 83.75 0.55 o -1 3 2 285.50 320.92 0.87 o 0 3 2 7.55 8.28 0.27 o 1 3 2 2.67 1.72 0.26 o 2 3 2 23.05 24.24 0.50 o 3 3 2 1.48 2.64 0.55 o 4 3 2 31.94 39.23 1.11 o 5 3 2 2.97 3.61 0.87 o 6 3 2 12.61 15.84 1.05 o 7 3 2 43.23 47.36 1.42 o 8 3 2 282.75 296.89 2.66 o 9 3 2 0.00 0.13 1.12 o 10 3 2 2.07 2.40 1.14 o 11 3 2 4.05 4.47 1.23 o 12 3 2 11.98 8.70 1.27 o 13 3 2 4.60 2.82 1.20 o 14 3 2 1.03 0.86 1.19 o 15 3 2 0.58 1.16 1.22 o 16 3 2 6.31 9.64 1.42 o -15 4 2 10.65 11.55 1.19 o -14 4 2 13.69 16.46 1.24 o -13 4 2 8.34 7.74 1.11 o -12 4 2 0.64 0.17 0.98 o -11 4 2 5.38 5.09 0.71 o -10 4 2 37.56 35.50 0.84 o -9 4 2 58.32 58.61 0.98 o -8 4 2 68.47 71.94 1.05 o -7 4 2 3.91 4.54 0.62 o -6 4 2 34.04 32.73 1.31 o -5 4 2 0.31 0.10 0.53 o -4 4 2 0.15 -0.21 0.92 o -3 4 2 7.13 6.44 0.49 o -2 4 2 8.84 10.78 0.69 o -1 4 2 0.05 0.98 0.46 o 0 4 2 9.64 10.19 0.79 o 1 4 2 47.02 47.64 1.26 o 2 4 2 95.91 94.51 1.64 o 3 4 2 68.41 73.43 1.52 o 4 4 2 45.07 42.32 1.28 o 5 4 2 3.37 3.15 0.86 o 6 4 2 0.09 1.36 0.82 o 7 4 2 96.67 102.71 3.63 o 8 4 2 170.72 178.49 2.22 o 9 4 2 12.98 17.14 1.30 o 10 4 2 2.80 3.18 1.19 o 11 4 2 30.85 29.05 1.46 o 12 4 2 2.98 1.46 1.17 o 13 4 2 0.01 2.85 1.21 o -10 5 2 8.03 6.23 0.87 o -9 5 2 3.47 4.16 0.82 o -8 5 2 0.27 0.49 0.76 o -7 5 2 37.20 32.77 1.20 o -6 5 2 53.35 50.39 1.37 o -5 5 2 10.94 12.51 0.93 o -4 5 2 1.79 0.56 0.74 o -3 5 2 0.11 -0.26 0.74 o -2 5 2 28.04 25.83 0.79 o -1 5 2 61.99 57.62 1.00 o 0 5 2 51.00 49.80 1.46 o 1 5 2 7.30 6.88 0.99 o 2 5 2 57.14 66.30 1.58 o 3 5 2 51.12 52.25 1.50 o 4 5 2 4.12 3.79 0.93 o 5 5 2 0.35 1.23 0.90 o 6 5 2 0.89 1.19 0.86 o 7 5 2 2.53 1.93 0.92 o 8 5 2 4.58 0.89 0.89 o 9 5 2 0.76 -0.12 0.92 o -20 1 3 0.05 -0.43 1.04 o -19 1 3 4.35 2.68 1.00 o -18 1 3 0.84 0.07 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