#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:26:07 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181236 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/14/2231478.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2231478_Fobs loop_ _publ_author_name 'Udachin, Konstantin A.' 'Zaman, Md. Badruz' 'Ripmeester, John A.' _publ_section_title ; Bis(guanidinium) cyananilate ; _journal_coeditor_code GK2374 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2279 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.887 _cell_angle_gamma 90.000 _cell_length_a 19.4873 _cell_length_b 3.6611 _cell_length_c 20.2452 _exptl_crystal_F_000 640.00 _reflns_d_resolution_high 0.7391 _cod_data_source_file gk2374Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' zam94 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 237.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10626.65 10628.00 56.43 o 4 0 0 6622.60 7016.49 48.92 o 6 0 0 2455.46 2410.51 24.06 o 8 0 0 6006.65 6873.58 83.61 o 10 0 0 512.45 669.83 8.54 o 12 0 0 54.84 70.13 4.19 o 14 0 0 19.47 36.17 4.23 o 16 0 0 51.89 41.47 5.78 o 18 0 0 633.02 658.64 19.17 o 20 0 0 85.77 96.46 9.84 o 22 0 0 16.07 32.26 9.01 o 24 0 0 477.34 586.61 22.62 o 1 1 0 147.10 66.24 2.74 o 3 1 0 5139.63 5176.12 85.36 o 5 1 0 5211.85 5308.43 72.64 o 7 1 0 4022.82 4437.08 27.64 o 9 1 0 2779.02 3105.25 17.97 o 11 1 0 2.65 -0.28 2.06 o 13 1 0 1281.00 1268.76 12.50 o 15 1 0 124.65 134.05 5.10 o 17 1 0 67.14 73.97 4.69 o 19 1 0 123.28 94.35 6.16 o 21 1 0 174.73 218.89 8.73 o 23 1 0 182.91 219.87 10.92 o 0 2 0 1921.83 2085.61 33.44 o 2 2 0 2887.02 3055.32 19.86 o 4 2 0 3547.54 3727.35 48.90 o 6 2 0 1085.72 1077.79 12.57 o 8 2 0 0.60 1.34 3.21 o 10 2 0 453.39 449.22 7.47 o 12 2 0 4.70 -3.09 3.09 o 14 2 0 31.52 11.51 3.40 o 16 2 0 4.81 2.50 3.68 o 18 2 0 128.60 141.54 6.32 o 20 2 0 219.26 260.79 10.57 o 22 2 0 255.41 329.96 13.22 o 1 3 0 234.11 218.37 6.87 o 3 3 0 82.66 83.28 5.06 o 5 3 0 171.95 185.36 6.64 o 7 3 0 0.06 3.29 3.99 o 9 3 0 2032.04 1969.85 39.40 o 11 3 0 663.29 656.67 14.16 o 13 3 0 73.30 67.08 5.47 o 15 3 0 69.06 54.92 5.51 o 17 3 0 34.14 24.89 6.54 o 19 3 0 33.78 45.29 7.59 o 0 4 0 42.80 34.47 7.82 o 2 4 0 25.58 17.69 4.80 o 4 4 0 14.12 11.73 6.53 o 6 4 0 127.89 137.48 13.62 o 8 4 0 29.38 27.02 6.35 o 10 4 0 90.31 103.34 10.75 o 12 4 0 65.51 63.56 11.75 o 14 4 0 9.62 13.81 7.52 o -23 1 1 164.51 192.03 9.86 o -21 1 1 525.83 588.23 12.69 o -19 1 1 41.65 24.44 4.78 o -17 1 1 195.03 161.88 5.99 o -15 1 1 229.26 210.90 6.08 o -13 1 1 61.43 46.94 3.58 o -11 1 1 1073.29 1169.33 19.32 o -9 1 1 171.87 137.94 4.85 o -7 1 1 990.87 1086.19 13.17 o -5 1 1 8158.72 8390.35 94.28 o -3 1 1 36143.24 36299.42 102.58 o -1 1 1 3595.23 3797.71 27.19 o 1 1 1 32.28 49.72 10.08 o 3 1 1 19.10 10.94 1.79 o 5 1 1 185.89 274.05 4.83 o 7 1 1 0.33 2.97 1.75 o 9 1 1 952.46 944.55 7.16 o 11 1 1 203.72 207.10 3.97 o 13 1 1 5.86 5.85 3.03 o 15 1 1 365.39 354.69 7.49 o 17 1 1 116.66 126.00 5.58 o 19 1 1 151.09 177.49 7.54 o 21 1 1 118.14 159.28 8.07 o 23 1 1 4.86 9.02 6.83 o -22 2 1 9.52 14.70 7.02 o -20 2 1 42.45 57.34 5.50 o -18 2 1 20.22 12.19 4.22 o -16 2 1 0.16 -0.83 3.35 o -14 2 1 953.65 889.71 11.62 o -12 2 1 4089.96 3817.24 47.14 o -10 2 1 704.48 724.85 16.27 o -8 2 1 179.28 169.77 5.67 o -6 2 1 1849.83 2002.99 16.87 o -4 2 1 95.34 147.73 4.87 o -2 2 1 225.26 218.78 5.62 o 0 2 1 2156.32 2286.89 16.50 o 2 2 1 38.44 31.09 3.32 o 4 2 1 46.39 44.21 3.42 o 6 2 1 1856.76 1889.64 28.91 o 8 2 1 19.16 14.79 2.88 o 10 2 1 474.28 444.74 7.47 o 12 2 1 516.28 512.87 9.87 o 14 2 1 144.57 134.56 5.26 o 16 2 1 50.33 32.76 4.31 o 18 2 1 898.60 1036.56 16.19 o 20 2 1 94.97 111.38 8.39 o -19 3 1 5.67 9.63 6.76 o -17 3 1 47.95 45.32 5.91 o -15 3 1 49.37 54.95 5.62 o -13 3 1 123.70 137.92 5.82 o -11 3 1 214.07 201.67 6.84 o -9 3 1 164.77 156.17 6.76 o -7 3 1 686.07 689.30 11.90 o -5 3 1 427.37 463.56 12.48 o -3 3 1 592.97 563.56 10.35 o -1 3 1 2.47 -0.71 3.61 o 1 3 1 9.91 15.07 3.90 o 3 3 1 454.94 440.84 8.04 o 5 3 1 59.05 65.70 4.27 o 7 3 1 201.99 191.54 5.73 o 9 3 1 1155.89 1139.45 16.41 o 11 3 1 328.50 305.87 8.57 o 13 3 1 58.01 55.93 6.05 o 15 3 1 147.39 160.64 8.66 o 17 3 1 261.73 286.41 16.40 o -14 4 1 15.54 17.68 7.35 o -12 4 1 0.06 -1.49 6.53 o -10 4 1 8.05 3.42 6.13 o -8 4 1 94.41 95.13 9.05 o -6 4 1 278.38 260.19 10.76 o -4 4 1 0.99 1.25 4.96 o -2 4 1 1.05 -0.33 5.14 o 0 4 1 10.12 2.77 4.75 o 2 4 1 228.06 242.09 10.67 o 4 4 1 372.72 407.47 22.13 o 6 4 1 365.40 411.37 12.02 o 8 4 1 295.89 323.96 11.25 o 10 4 1 13.99 11.73 6.49 o 12 4 1 0.02 -2.60 6.88 o -24 0 2 731.75 863.52 26.25 o -22 0 2 136.12 104.15 10.87 o -20 0 2 26.60 0.16 7.43 o -18 0 2 234.72 237.20 9.51 o -16 0 2 1550.09 1557.10 26.56 o -14 0 2 407.82 461.83 8.28 o -12 0 2 702.43 706.45 9.17 o -10 0 2 11664.55 12887.85 59.81 o -8 0 2 2903.24 3437.06 154.22 o -6 0 2 66.73 63.95 3.71 o -4 0 2 3118.44 2872.67 26.19 o -2 0 2 2649.81 2965.15 62.22 o 0 0 2 136.73 177.40 4.86 o 2 0 2 11701.36 10618.69 59.98 o 4 0 2 22.46 45.04 2.28 o 6 0 2 14350.45 16028.63 66.90 o 8 0 2 1817.82 2187.86 30.91 o 10 0 2 1064.96 1158.47 19.32 o 12 0 2 717.29 733.87 14.62 o 14 0 2 92.69 103.21 5.24 o 16 0 2 595.41 560.56 13.18 o 18 0 2 33.14 45.14 7.74 o 20 0 2 146.84 154.68 16.56 o 22 0 2 8.97 1.49 9.48 o -23 1 2 0.62 6.15 6.10 o -21 1 2 0.12 1.56 5.02 o -19 1 2 221.30 221.17 7.98 o -17 1 2 537.72 464.67 8.68 o -15 1 2 859.82 738.64 12.91 o -13 1 2 196.68 216.58 5.37 o -11 1 2 839.31 865.65 13.16 o -9 1 2 1801.86 1966.20 22.90 o -7 1 2 476.87 420.61 6.70 o -5 1 2 2357.96 2272.45 27.23 o -3 1 2 56206.47 54694.18 131.59 o -1 1 2 3784.80 3959.95 39.48 o 1 1 2 8907.86 8875.78 65.81 o 3 1 2 2182.93 2015.12 18.13 o 5 1 2 431.66 528.55 7.90 o 7 1 2 183.92 238.73 3.55 o 9 1 2 274.13 314.23 4.43 o 11 1 2 446.28 533.84 6.00 o 13 1 2 7.58 7.25 2.84 o 15 1 2 1134.61 1166.91 13.25 o 17 1 2 23.68 15.44 4.01 o 19 1 2 246.91 217.25 8.16 o 21 1 2 284.92 364.34 10.82 o -22 2 2 16.08 8.27 6.03 o -20 2 2 17.42 17.94 4.66 o -18 2 2 2.61 -0.29 3.80 o -16 2 2 876.70 893.78 18.15 o -14 2 2 127.85 116.86 4.97 o -12 2 2 1772.92 1575.59 17.76 o -10 2 2 3.62 1.01 3.32 o -8 2 2 2068.79 2174.75 18.40 o -6 2 2 4914.17 5381.66 87.93 o -4 2 2 189.40 153.09 4.60 o -2 2 2 290.52 307.24 6.08 o 0 2 2 251.86 250.05 8.19 o 2 2 2 988.13 1013.90 16.18 o 4 2 2 205.57 179.42 5.53 o 6 2 2 301.66 310.97 5.66 o 8 2 2 0.32 2.33 2.64 o 10 2 2 7.00 9.36 3.08 o 12 2 2 459.61 449.00 8.12 o 14 2 2 281.61 308.57 7.38 o 16 2 2 2.18 8.14 4.48 o 18 2 2 12.10 23.20 5.48 o 20 2 2 22.41 20.76 6.65 o -19 3 2 149.90 163.54 8.36 o -17 3 2 28.51 28.53 5.40 o -15 3 2 213.33 209.82 10.58 o -13 3 2 2.38 2.73 3.95 o -11 3 2 0.01 -0.87 4.17 o -9 3 2 104.34 97.64 5.82 o -7 3 2 89.59 83.81 5.28 o -5 3 2 332.96 311.32 8.07 o -3 3 2 56.17 40.71 3.62 o -1 3 2 349.34 355.71 7.34 o 1 3 2 1259.92 1313.11 21.14 o 3 3 2 43.16 47.88 3.68 o 5 3 2 0.72 -0.05 2.96 o 7 3 2 974.60 965.99 13.09 o 9 3 2 52.99 43.90 4.99 o 11 3 2 55.33 58.40 5.91 o 13 3 2 4.20 2.23 5.12 o 15 3 2 91.23 108.97 8.01 o 17 3 2 120.74 133.41 9.06 o -14 4 2 7.60 7.24 7.14 o -12 4 2 417.63 446.51 13.70 o -10 4 2 322.60 317.95 16.51 o -8 4 2 243.96 238.98 11.01 o -6 4 2 87.58 87.71 6.72 o -4 4 2 15.45 21.28 5.54 o -2 4 2 67.25 65.32 5.26 o 0 4 2 119.66 123.72 7.95 o 2 4 2 19.28 12.41 5.61 o 4 4 2 66.49 72.14 6.75 o 6 4 2 1248.22 1369.05 23.04 o 8 4 2 112.05 110.30 8.41 o 10 4 2 212.97 225.79 10.65 o 12 4 2 45.82 55.67 8.48 o -23 1 3 11.31 18.64 6.27 o -21 1 3 26.70 17.38 5.14 o -19 1 3 2.24 1.17 4.42 o -17 1 3 321.49 318.37 7.34 o -15 1 3 3752.26 3628.65 31.65 o -13 1 3 2494.19 2636.69 22.04 o -11 1 3 741.13 754.51 7.49 o -9 1 3 299.76 285.43 6.17 o -7 1 3 486.66 583.77 7.74 o -5 1 3 159.92 246.37 2.71 o -3 1 3 221.03 202.29 2.97 o -1 1 3 1449.48 1417.41 17.44 o 1 1 3 479.57 440.10 7.34 o 3 1 3 3820.65 4112.47 25.72 o 5 1 3 631.47 748.10 6.09 o 7 1 3 1814.63 1953.70 16.46 o 9 1 3 1739.89 1803.30 18.62 o 11 1 3 382.80 426.00 5.76 o 13 1 3 155.45 158.43 4.78 o 15 1 3 587.62 647.07 10.05 o 17 1 3 126.12 131.70 5.76 o 19 1 3 114.79 103.00 6.55 o 21 1 3 4.14 8.61 6.14 o -22 2 3 0.00 -1.31 5.42 o -20 2 3 6.60 5.17 4.40 o -18 2 3 3.01 0.59 3.80 o -16 2 3 15.44 25.99 3.83 o -14 2 3 644.41 651.41 12.06 o -12 2 3 145.23 120.73 5.55 o -10 2 3 110.29 96.64 5.02 o -8 2 3 162.00 158.64 4.32 o -6 2 3 12667.67 12735.03 156.61 o -4 2 3 2657.16 2823.81 28.00 o -2 2 3 47.31 35.92 2.75 o 0 2 3 207.64 173.69 4.00 o 2 2 3 57.59 55.10 3.29 o 4 2 3 211.64 185.23 4.29 o 6 2 3 389.56 375.18 5.60 o 8 2 3 336.10 315.88 5.49 o 10 2 3 8.66 9.29 3.04 o 12 2 3 174.45 163.48 5.52 o 14 2 3 6.13 6.88 4.11 o 16 2 3 0.30 1.67 4.54 o 18 2 3 137.89 168.29 9.00 o 20 2 3 29.48 48.44 7.52 o -19 3 3 0.17 3.41 5.39 o -17 3 3 12.01 9.38 4.45 o -15 3 3 261.05 255.68 7.62 o -13 3 3 5.48 0.07 4.30 o -11 3 3 701.95 680.04 12.66 o -9 3 3 1301.69 1295.98 23.82 o -7 3 3 19.05 17.87 4.16 o -5 3 3 410.44 379.90 8.66 o -3 3 3 0.09 -1.38 2.77 o -1 3 3 165.72 167.26 4.99 o 1 3 3 7.45 6.51 3.01 o 3 3 3 810.65 835.11 18.46 o 5 3 3 48.28 38.48 4.12 o 7 3 3 131.30 122.08 6.87 o 9 3 3 70.05 68.66 6.10 o 11 3 3 4.19 2.54 4.65 o 13 3 3 102.57 92.09 7.27 o 15 3 3 270.49 299.69 11.25 o 17 3 3 41.67 54.67 7.47 o -14 4 3 33.75 22.87 7.41 o -12 4 3 132.91 139.29 10.31 o -10 4 3 102.42 90.12 8.73 o -8 4 3 50.76 52.35 6.47 o -6 4 3 43.60 49.34 6.05 o -4 4 3 6.27 1.43 5.64 o -2 4 3 286.96 308.64 10.89 o 0 4 3 48.85 45.68 6.39 o 2 4 3 41.25 38.28 6.11 o 4 4 3 102.96 96.84 7.44 o 6 4 3 29.89 18.25 6.26 o 8 4 3 47.94 34.24 6.84 o 10 4 3 11.70 3.84 6.48 o 12 4 3 19.80 25.72 7.47 o -24 0 4 5.19 5.16 9.00 o -22 0 4 444.59 453.67 17.99 o -20 0 4 1291.20 1317.71 27.66 o -18 0 4 6965.05 7239.43 142.71 o -16 0 4 1542.50 1731.08 20.88 o -14 0 4 790.60 865.69 10.64 o -12 0 4 1589.61 1717.92 62.76 o -10 0 4 1234.10 1417.79 18.65 o -8 0 4 1215.02 1303.59 22.15 o -6 0 4 15535.89 16672.09 72.59 o -4 0 4 163.83 181.45 3.25 o -2 0 4 8962.24 8798.50 152.62 o 0 0 4 4206.10 4416.88 49.20 o 2 0 4 99.61 122.67 2.97 o 4 0 4 5895.34 6785.36 27.04 o 6 0 4 4239.81 4670.39 75.37 o 8 0 4 1480.82 1766.09 27.66 o 10 0 4 253.74 282.49 6.63 o 12 0 4 6337.61 6448.28 58.56 o 14 0 4 144.41 215.08 7.23 o 16 0 4 2216.85 1999.80 25.02 o 18 0 4 62.46 106.81 10.43 o 20 0 4 9.61 24.10 8.69 o 22 0 4 16.76 9.68 10.14 o -25 1 4 1.31 7.72 13.76 o -23 1 4 56.10 50.38 7.10 o -21 1 4 82.07 88.48 7.39 o -19 1 4 681.83 759.19 14.01 o -17 1 4 236.83 225.59 6.30 o -15 1 4 970.91 886.69 13.43 o -13 1 4 177.18 201.94 7.03 o -11 1 4 473.71 417.52 8.52 o -9 1 4 60.97 33.74 3.32 o -7 1 4 1022.60 1097.31 15.70 o -5 1 4 5015.87 5347.47 79.85 o -3 1 4 148.43 153.45 3.48 o -1 1 4 209.34 201.94 4.71 o 1 1 4 1026.08 1003.28 12.74 o 3 1 4 3899.15 4286.18 17.07 o 5 1 4 5260.58 5581.42 30.73 o 7 1 4 20.84 12.64 2.07 o 9 1 4 516.23 530.34 6.40 o 11 1 4 12.45 4.32 2.47 o 13 1 4 413.51 329.28 6.21 o 15 1 4 33.93 32.78 3.96 o 17 1 4 0.60 5.37 3.90 o 19 1 4 17.36 10.56 5.72 o 21 1 4 267.02 261.40 11.11 o -22 2 4 331.82 360.42 11.26 o -20 2 4 7.48 5.38 4.40 o -18 2 4 0.02 4.09 3.77 o -16 2 4 333.31 281.04 8.80 o -14 2 4 126.03 104.06 5.71 o -12 2 4 107.63 101.85 6.84 o -10 2 4 19.20 12.15 3.58 o -8 2 4 321.65 259.20 8.46 o -6 2 4 783.43 885.61 7.62 o -4 2 4 402.43 391.74 6.53 o -2 2 4 181.44 198.08 4.20 o 0 2 4 59.56 71.51 3.17 o 2 2 4 1289.14 1294.64 10.21 o 4 2 4 2113.54 2243.04 14.00 o 6 2 4 570.62 578.63 7.36 o 8 2 4 191.50 192.25 4.65 o 10 2 4 290.74 288.44 8.32 o 12 2 4 132.17 108.94 5.44 o 14 2 4 13.48 6.89 4.28 o 16 2 4 126.05 118.32 7.57 o 18 2 4 443.41 458.62 13.27 o 20 2 4 215.29 260.90 11.61 o -19 3 4 85.76 77.99 6.67 o -17 3 4 27.38 35.26 5.05 o -15 3 4 567.96 539.19 12.50 o -13 3 4 18.07 16.13 4.59 o -11 3 4 15.57 23.06 4.75 o -9 3 4 2041.08 1959.81 51.26 o -7 3 4 265.14 274.50 9.14 o -5 3 4 45.60 39.14 3.75 o -3 3 4 123.96 109.67 4.35 o -1 3 4 32.94 32.28 3.15 o 1 3 4 35.79 32.91 3.38 o 3 3 4 784.73 732.34 12.66 o 5 3 4 55.33 53.11 6.21 o 7 3 4 166.74 163.16 7.40 o 9 3 4 147.13 157.55 7.83 o 11 3 4 5.88 4.90 4.84 o 13 3 4 42.96 42.91 6.15 o 15 3 4 208.14 259.87 10.63 o 17 3 4 11.10 23.89 7.39 o -14 4 4 8.60 0.78 6.72 o -12 4 4 64.93 56.84 8.68 o -10 4 4 0.43 1.33 5.76 o -8 4 4 53.95 66.00 7.65 o -6 4 4 102.03 108.42 9.61 o -4 4 4 79.96 91.83 13.70 o -2 4 4 24.62 22.64 5.88 o 0 4 4 10.19 10.25 5.37 o 2 4 4 50.88 48.55 6.09 o 4 4 4 35.66 36.51 8.89 o 6 4 4 2.61 1.56 5.82 o 8 4 4 36.14 42.23 7.02 o 10 4 4 0.01 -3.16 6.61 o 12 4 4 104.16 122.91 9.40 o -25 1 5 6.39 1.78 6.67 o -23 1 5 198.41 223.08 10.32 o -21 1 5 695.36 711.12 13.30 o -19 1 5 344.31 314.28 8.74 o -17 1 5 398.68 394.08 8.74 o -15 1 5 17.59 12.23 3.82 o -13 1 5 52.70 46.50 4.36 o -11 1 5 0.81 -0.10 2.44 o -9 1 5 3390.57 3716.00 67.93 o -7 1 5 277.85 273.33 3.86 o -5 1 5 192.86 242.83 5.62 o -3 1 5 782.90 756.98 10.45 o -1 1 5 1180.91 1201.13 13.52 o 1 1 5 7014.23 7285.99 34.05 o 3 1 5 1157.90 1249.61 6.97 o 5 1 5 350.15 309.97 8.21 o 7 1 5 311.65 306.06 6.20 o 9 1 5 1282.58 1148.04 13.07 o 11 1 5 0.34 0.18 2.48 o 13 1 5 479.68 375.61 6.82 o 15 1 5 65.08 37.23 4.07 o 17 1 5 7.87 -0.07 4.52 o 19 1 5 36.06 50.92 6.70 o 21 1 5 0.59 8.00 6.96 o -22 2 5 32.11 16.29 5.56 o -20 2 5 1.09 1.03 4.18 o -18 2 5 581.26 567.24 12.94 o -16 2 5 162.44 175.78 7.49 o -14 2 5 0.39 0.50 3.49 o -12 2 5 31.35 31.78 4.13 o -10 2 5 34.24 38.69 4.09 o -8 2 5 1737.80 1801.31 15.69 o -6 2 5 137.19 157.46 4.96 o -4 2 5 639.66 689.02 15.85 o -2 2 5 0.41 -0.01 2.25 o 0 2 5 6484.77 6342.75 39.10 o 2 2 5 319.55 361.93 6.92 o 4 2 5 43.93 42.34 2.63 o 6 2 5 13.45 11.72 2.82 o 8 2 5 31.66 26.79 3.26 o 10 2 5 1064.43 1003.38 18.93 o 12 2 5 100.03 112.80 6.91 o 14 2 5 73.79 71.73 6.19 o 16 2 5 24.59 18.43 5.58 o 18 2 5 280.43 282.24 11.06 o -19 3 5 10.40 9.09 4.73 o -17 3 5 76.05 67.40 6.24 o -15 3 5 44.62 45.92 5.49 o -13 3 5 77.84 74.30 6.31 o -11 3 5 23.42 18.88 4.68 o -9 3 5 2047.97 2124.47 42.86 o -7 3 5 922.80 955.57 22.50 o -5 3 5 67.43 72.30 4.34 o -3 3 5 205.15 208.69 5.34 o -1 3 5 770.51 772.79 14.09 o 1 3 5 81.92 99.23 5.53 o 3 3 5 9.01 10.08 4.07 o 5 3 5 18.25 19.54 4.52 o 7 3 5 4.56 5.69 4.53 o 9 3 5 143.87 124.10 7.21 o 11 3 5 24.57 20.94 5.53 o 13 3 5 8.77 7.62 5.36 o 15 3 5 35.63 38.06 6.92 o -14 4 5 170.38 166.93 12.86 o -12 4 5 494.99 519.41 30.69 o -10 4 5 121.14 117.29 8.88 o -8 4 5 81.70 87.84 9.04 o -6 4 5 38.77 41.20 7.81 o -4 4 5 172.68 194.17 11.11 o -2 4 5 84.10 86.65 7.35 o 0 4 5 26.66 23.26 5.25 o 2 4 5 7.53 8.45 5.45 o 4 4 5 0.00 -0.67 5.66 o 6 4 5 5.10 14.44 6.10 o 8 4 5 31.56 18.01 6.56 o 10 4 5 26.54 17.19 6.76 o -24 0 6 0.71 0.12 8.04 o -22 0 6 6.77 3.56 7.77 o -20 0 6 581.41 560.70 37.85 o -18 0 6 313.84 292.46 9.86 o -16 0 6 0.66 7.75 10.64 o -14 0 6 78.75 61.10 6.76 o -12 0 6 2341.97 2237.77 52.63 o -10 0 6 625.89 681.72 12.67 o -8 0 6 1790.76 1744.56 14.34 o -6 0 6 2913.88 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